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Arke SO3 System - User Manual

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3. AC Mains Assembly Pneumatic Assembly Figure 5 2 Component Location Pneumatic Assembly The Pneumatic Assembly is attached to the bottom of the instrument chassis below the User Interface Assembly When removing it is suggested Replacement that the cables should be labeled in order to ensure proper reinstall Use the following procedure to replace the Pneumatic Assembly Figure 5 3 WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Perform shut down of the system Refer to Shutdown Instructions in this chapter 2 Turn off air supply to the instrument 3 On the System Control board located closest to the Optical Bench Assembly disconnect the two 2 transducer cables from connectors J23 Eductor and J7 Dilution Thermo Fisher Scientific Arke S0 System Instruction Manual 5 7 Preventive Maintenance and Servicing Pneumatic Assembly Replacement 5 8 Arke SO System Instruction Manual On the System Control Board disconnect the two 2 regulator valve cables from connectors J39 Eductor and J31 Dilution On the System Control board disconnect the two 2 mass flow control cables from connectors J33 Air and J32 SO2 Locate the Pneumatic Assembly It is bolted to the bottom of the instrument chassis directly to the left of the main power switch The
4. ae d d ee WKY GF ww we Gg q 2 Qq p Qq p q J o x ME S 3 i ie G ZN TITER e ZN S S uZ W2 NI uA d TT RT J E Lo o IITA Ni Oh l R Loue VUE qf SCENES PS d C L lj JF 2 j J 1 A VI AN STK Jg VER 7 L 5 f wee Na POL SKL ZA LE SS DIFFERENTIAL PRESSURE tH tit i RANSDUCER VALVES CABLE ASSEMBLY Figure 6 12 Probe Terminations and Pneumatics Overhead Arke SO System Instruction Manual 6 23 Troubleshooting Probe Pneumatic Cable and Wiring Connections AL B VA TERMINATIONS RAN TB TERMINAL BLOCK di es 1 sn d INSERT LEAD AND SE E WITH RE Figure 6 13 Terminal Block Table 6 2 Heater Cable Assembly Terminations From Wire Color TO TB Function A Green Yellow PET L Farth Ground B Red 1 L H1 amp H2 Probe C Red A L H1 amp H2 Probe D Blk 3 L H3 Orifice E Blk 4 L H3 Orifice F Brn 5 L H4 Generator G Brn 6 L H4 Generator H Blu AL H5 Stinger J Blu 8 L H5 Stinger K Vio 9 L H6 Spike p Vio 10 L H6 Spike 6 24 Arke S0 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Troubleshooting Probe Pneumatic Cable and Wiring Connections Table 6 3 Valve Cable Assembly Terminations
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6. 3 17 Mannar Calibration S soar DE be m vno i tdt bts EE 3 19 Calibration Coefficients cessere nennen 3 20 System OHC TID oszsceduseat dte mua Petits at dpes tute fbdte EO ote 3 21 View Calibration Spectr nis us etel p EH eet tite fe bab 3 22 Arke 03 System Instruction Manual ix Contents Current Calibration S pee i Wit s a ovens tUa oo E een to FEE PR E SERE 3 23 Calibration Write oue oni tubos uates m cie M er Du Ee iE 3 24 Instrument Controls Menu eeeeseeeeeeeeeeeee ener 3 25 GSV Ode ea tisse ane MEER IET CU EO A D IUE 3 26 Component l OWeE sustenta Ne gei e Duo b O IUIS 3 28 Instrument Component POWEls sento aiuti repa eset getan esie 3 29 Probe Component LOW dc On Mt ee 3 31 DO AVELI3gIHe E odo mt Uode tokio ORT dor terse eT ere 3 33 Blowbackschedulesssos a i ERES E MUS 3 34 Communication Settifips nies vosctemna eos irte nd hui R iei 3 35 Seral OC CNN OS S 3 36 CP WE Se PUN GS occ nane ete a ti Fere eoo duni tdi tau nadiaeaaaosags 3 37 Bir M 3 38 Set Litae D Ateste ee ae PSE aM EUM ME i S LA CO EUMD Co 3 39 Systemi Stratus and Alarms Ment eese eter gaits ee t o vet 3 40 nstr rnent 2S AUS Gene edet EIE C dieta chi aate SoPunu N 3 41 Probe SACS seco cece TERN e 3 43 Change Setpoints and Alarm Limits esses 3 45 BodPic COLS eonim Mut IMS CE x LL MR M E EIE 3 46 MOIS S ond DNUS EMI IE MEE 3 47 Data Analysis M
7. enjeleduie aqold snyejs eqoid yead 10 09 9q enjeJeduie J0 99 0q oDeyoA Jose duie Bulsnoy Jase eJnjeleduia Jose Bulpeay ueds M0J4 Ji uogniq ueds N0l4 IED ZOS eunjeleduie sisseu eJnsseld uoueg eunjeJeduje youeg uonenue2uo LOS snyejs jueunasu c eDeg nueJ A ulen Ssulle v 8 snigls uejs S Figure 3 3 Main Menu page 2 Thermo Fisher Scientific 3 4 Arke SO3 System Instruction Manual User Interface Instrument Display The Instrument Display contains the following information e SOs Screen button Displays the title SO CEMS when in the SO screen and the current SO concentration reading when in all other screens When pressed it brings you back to the SO screen e Thermo Scientific Information button Shows the contact information product information serial numbers board firmware versions and software build numbers e Main Menu buttons Includes Calibration Instrument Controls System Status and Alarms Data Analysis and Service buttons e Calibration Allows the user to calibrate the system setup automatic calibrations and view calibration data e Instrument Controls Contains controls for operating the system e System Status and Alarms Shows real time temperature pressure f
8. Baseline Service September 2011 14 08 23 System Span Back Figure 3 46 Raw Spectrum Screen Note The intensity of the blue signal curve should be greater than 0 30 If not the laser voltage may need to be increased but should not exceed 9 volts Also detector and or laser alignment may be needed A Arke SO System Instruction Manual 3 59 User Interface Data Analysis Menu Transmission Spectrum 3 60 Arke SO System Instruction Manual The Transmission Spectrum screen Figure 3 47 shows the SO transmission spectrum blue curve The red curve is the voight fit which is used to measure the strength of the SO signal resulting in a concentration ipi xi Calibration S0 1 95 ppm SCIENTIFIC Data Analysis gt Real Time Spectrum Transmission Spectrum a Instrument Controls System Status and Alarms 0 9998 Data Analysis 0 356 NN EE EN A E 15 44 73 102 131 150 50 Voigt Peak Channel 0 Service June 3 2011 14 02 05 Back Alarms Figure 3 47 Transmission Spectrum Screen The peak channel number correlates to where the SO signal is located within the chart The SO signal peak should fall within channels 5 to 5 If it falls outside that range especially during calibration the laser temperature should be adjusted see Laser Controls in the Service section If the peak channel displays 20 then the lowest peak within channels 10 to 10 is ab
9. m P B TT ma a Hotline Umbilical Dens HHO i ee epa Taj OQ i a DHL pom SD ER Ex a a Bos IL TI I I IL Ii Umbilical Strain ir Gd SS Elbow with Port Connectors Atmospheric Dump Union Figure 2 14 Hot Line Hook Up Underside Procedure Start UP Use the following procedure to start the instrument Figure 2 15 2 Turn OFF AC MAIN Switch on the right exterior of the cabinet Thermo Fisher Scientific Figure 2 15 AC Main Power Switch Arke S0 System Instruction Manual 2 13 Installation Start up Procedure 3 Turn 3 breakers inside the instrument box to the OFF position Figure 2 16 HVAC Power AC Power Pe t i Figure 2 16 Circuit Breaker Diagram for Startup 4 Locate 30 amp electrical service drop and verify supply voltage 200 to 250 VAC 5 Plug in main power cord 6 Turn ON AC MAIN Switch on the right exterior of the cabinet Figure 2 15 7 Turn ON center breaker CB2 ATX Power Supply 8 Ensure that the power switch on the ATX power supply in the ON position 2 14 Arke SO System Instruction Manual Thermo Fisher Scientific HVAC Temperature Control Board Verification Thermo Fisher Scientific Installation HVAC 9 The touch screen will start up and it may take a minute before the run screen is available 10 Check to see that both Laser and Laser Housing temperature control boards have LEDs illuminated 11 Check to see that the syst
10. After mounting probe and securing umbilical cord hot line in probe with 3 inch strain relief make the connections described in Table 2 2 Refer to Figure 2 12 Figure 2 7 and Table 2 2 for umbilical wiring hookup Thermo Fisher Scientific Arke S0 System Instruction Manual 2 11 Installation Probe Installation 2 12 Arke S03 System Instruction Manual fa ON a VY WS C X ey DILUTION EDUCTOR LS J J a u 8 O AA O NI N NS S 2 ow N Figure 2 13 Hot Line Hook Up Straight Thermo Fisher Scientific Installation otart up Procedure iw A A A A A a Ya 3 7 a
11. CI bETY INI AZI Figure 6 4 Laser and Laser Housing Temp Control Boards Bottom of board Laser Connector Board e If the Laser is not firing check all connections to this board This includes the coax cable going to CLK the TEC connector PWR connector and the two RS 485 connections e The cable that connects to J4 on this board should connect to the Laser Temperature control board which has the DIP switch in the Up position closest to the Thermo on the silkscreen It is important that these cables are not switched between the Laser Control board and the Laser Housing Small Connector Board e If it is determined that this board is faulty replace with Part Number 110819 00 e The 4 pin dc power connector J5 is located at the bottom of this board Check voltages if a board problem is suspected e The two RS 485 connectors J7 and J8 are located on the left side of this board They are interchangeable and are used to daisy chain all the boards together however this board usually is where the RS 485 terminates only one cable Thermo Fisher Scientific Arke S0 System Instruction Manual 6 15 Troubleshooting Instrument Board and Cable Assembly Connections PCE 110818 00 ASSY 1 0813 00 a Se E NE NI NE M mE m E uM M ae a amp CONNECTOR BD REU 02 RITFERMO FISHER SCIENTIFIC Figure 6 5 Laser Connector Board Laser Housing Small Connector Board e The cable that connects to J3 on t
12. Troubleshooting Instrument Devices and Alarms Instrument Devices The following outline addresses possible instrument and alarm problems and Alarms and proposes checks and possible troubleshooting solutions S0 Concentration Low Concentration e Leaks e Check Probe tubing for melted and cut sections e Check for loose fittings e Cold Spots e Ensure proper insulation at both ends of the hotline e SO Generator needs Conditioning e The SO Generator should be conditioned at least once a week An automatic schedule can be created at the screen Service SO Generator Conditioning e Detector not seeing enough light e Goto the screen Data Analysis gt Real Time Spectrums gt Raw Spectrum If the y axis maximum number is 0 20 or less then the detector is not getting enough light Laser and or detector placement may need to be adjusted Before doing that shut down and reboot the system and see if the problem gets fixed Allow 6 to 7 minutes for the laser power to turn ON High Concentration e Goto the screen Data Analysis gt Real Time Spectrums gt Raw Spectrum Ensure that the y axis maximum number is between than 0 3 and 1 0 If it is not go to the screen Service gt Laser Controls gt Laser Voltage If the maximum y axis number is below 0 3 increase the laser voltage in 1 increments Do not exceed 9 0 volts Concentration Not Updating e Laser and Detector Power e Ensure that the Laser and Detector Power found at Ins
13. Air Quality Instruments wa thermo comfaqi oO Call Center 508 520 0430 System Information Model Number 9800 Model Name SO Analyzer Instrument Serial Number SOS Beta new April 30 2012 Filter Blowback Alarms 5 14 41 23 Figure 3 7 Information Screen The Information screen contains the following information e Contact Information Customer service information e System Information Lists model number name and instrument serial number information e Firmware Information Lists board firmware information and software build information Thermo Fisher Scientific Arke S0 System Instruction Manual 3 9 User Interface Thermo Scientific Information Screen Firmware The Firmware Information screen Figure 3 8 lists board firmware Information X information and software build information Note Customer version numbers may differ A S0 1 95 ppm Information Firmware Information Instrument Firmware version 0 00 System Control Board Firmware version 0 00 Mother Board Firmware version 0 00 CPU Board Firmware version 0 00 Laser Timing Board Firmware version 0 00 Laser Temp Board Firmware version 0 00 Laser Housing Temp Board Firmware version 0 00 Detector Board Firmware version 0 00 Software Build Beta 14 minus net Software Date Beta 05 31 2011 June 2 2011 Sample 11 32 48 Figure 3 8 Firmware Information Screen 3 10 Arke SO System Instruction Manual Thermo Fisher Scientific The
14. Digital inputs serial Ports Fthernet connection 1 8 Arke S0 System Instruction Manual 200 ppm 0 2 ppm 300 second average 0 4 ppm 300 second average 0 5 ppm 2 full scale 1 full scale 1x10 5 1x10 4 0 25 L min 10 to 45 C 208 250 VAC 25 amps 30 W X 30 H X 12 D 145 Ibs 6 voltage outputs 0 100 mV 1V 10 V user selectable 5 of full scale over under range user selectable 12 bit resolution measurement output user selectable per channel 4 analog inputs user customizable 4 digital outputs 1 power fail relay Form C 10 digital relays Form A user selectable alarm output relay logic 100 mA 200 VDC 8 digital inputs user select programmable TTL level pulled high 1 RS 232 or RS 485 with two connectors baud rate 1200 115200 data bits parity and stop bits protocols C Link MODBUS Gesytec Bayern Hessen and streaming data all user selectable RJ45 connector for 10Mbs Ethernet connection static or dynamic TCP IP addressing Thermo Fisher Scientific Thermo Fisher Scientific AN Instrument Installation Chapter 2 Installation The following installation procedure for the Arke SO System describes setup and installation including turning on the instrument enabling heaters coolers and the QC laser The installation should always be followed by instrument calibration as described in the Calibration chapter of this manual For details see the following topi
15. Shutdown Instructions on page 5 5 e AC Mains Assembly Replacement on page 5 6 e Pneumatic Assembly Replacement on page 5 7 e Optical System Assembly on page 5 9 e System Electronics Assembly on page 5 11 e User Interface Assembly on page 5 12 e Air Conditioner Replacement on page 5 14 e PRO9805 Probe Replacement Parts List on page 5 15 e Factory Plumbing on page 5 16 e Replacement Tubing List on page 5 16 e Factory Wiring on page 5 19 e Dilution Eductor Replacement on page 5 22 e Inertial Filter Replacement on page 5 23 e Dilution Assembly Critical Orifice Replacement on page 5 24 e 15 Micron Filter Replacement on page 5 25 Arke SO System Instruction Manual 5 1 Preventive Maintenance and Servicing oafety Precautions e Valve Cover Gasket Replacement on page 5 25 e Valve Assembly Replacement on page 5 27 e Venturi Pressure Differential Transducer Assembly Replacement on page 5 28 e Stinger Heater Replacement on page 5 28 e Stinger Clamp Replacement on page 5 29 e Eductor Replacement on page 5 29 e Venturi Tube Replacement on page 5 29 e SO3 Generator Replacement on page 5 29 e Service Locations on page 5 30 Safet Precautions Read the safety precautions before beginning any procedures in this yp g g any p chapter WARNING The service procedures in this manual are restricted to qualified service technicians A manufacturer t
16. 352 353 Description UmbilicallempDataLog UmbilicalStitchTempDataTemp UmbilicalStitch TempDataNumber UmbilicalStitch TempDataLog EductorPresDatal emp EductorPresDataNumber EductorPresDataLog sampleDilutionAirPresDatal emp sampleDilutionAirPresDataNumber sampleDilutionAirPresDataLog VenturiPresDatal emp VenturiPresDataNumber VenturiPresDataLog sampleDilutionVacuumDatal emp sampleDilutionVacuumDataNumber sampleDilutionVacuumDataLog SO3ConcentrationRawDatalemp SO3ConcentrationRawDataNumber SO3ConcentrationRawDataLog DetectorPeakSignalMinimaYDatalemp DetectorPeakSignalMinimaY DataNumber DetectorPeakSignalMinimaYDataLog AutoCalibrationState AutoCalibrationPeriod AutoCalibrationStart AutoCalibrationZeroDuration AutoCalibrationSpanDuration AutoCalibrationTotalDuration AutoCalibrationAverage AutoCalibrationInhibited AutoCalibrationCheckState AutoCalibrationCheckPeriod AutoCalibrationCheckStart AutoCalibrationCheckZeroDuration Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 354 355 356 397 358 399 360 361 362 363 364 365 366 367 368 369 370 3 1 3 2 373 374 375 376 377 378 379 380 381 302 383 304 385 386 387 Serial Communication AK Protocol Description AutoCalibrationCheckSpanDuration AutoCalibrationCheckTotalDuration AutoCalibrationCheckAverage BlowbackscheduleState BlowbackPeriod Blowbackstart BlowbackDuration BlowbackPrevious BakeSchedulePeriod BakeScheduleStart BakeSche
17. C iii Go back to the Raw spectrum and see if the water peak is present iv If not then continue to repeat steps i iii until you reach 16 C The water peak should be seen between 10 16 C If not then troubleshooting may be required For instance be sure to check Bench Vacuum d See Raw Spectrum below The water peak blue curve should look something like this 6 28 Arke SO3 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Troubleshooting Finding and Optimizing the Correct 503 Peak Eek Wa x ra eGgh 10 175 240 99 ao Calibration S0 TES ppm ditas Data Analysis gt Real Time Spectrum gt Raw Spectrum Instrument Controls System Status and Alarms Data Analysis 0 43 85 129 172 215 Raw Spectrum Baseline n May 29 2012 Sample Alarms 2 16 00 13 Back Service e Next fine tune the water peak at the Transmission Sceen Position the water peak around channel 0 x axis i If the peak is to the left of channel 0 then increase the temperature of the laser slightly try going in small 0 05 C increments ii If the peak is to the right of channel 0 then decrease the temperature of the laser slightly f When you locate and position the Water peak record laser temperature g See lransmission Spectrum below The water peak blue curve should look something like this Arke SO System Instruction Manual 6 29 Troubleshooting Finding and Opt
18. Enables disables the auto calibration schedule state The screen responds with Are you Sure and requires a Yes or No action e Peak Adjust Enabled Disabled Enables disables the automatic peak adjust feature If enabled during an automatic calibration the laser cooler temperature will be adjusted to center the SO peak at channel 0 e Next Time Sets the date and time for the next scheduled calibration Once an automatic calibration has started the Next Time button will be updated based on the Period Arke S0 System Instruction Manual 3 15 User Interface Calibration Menu 3 16 Arke SO System Instruction Manual Period Sets the length of time between calibrations Duration Sets the length of time for zero air and span gas SO Averaging Time for Auto Cal Sets the Averaging time during auto calibration During an Automatic Calibration this averaging time will override the Sample averaging time set in the Instrument Controls menu Current Calibration Displays the date time of the most recently completed automatic calibration If an automatic calibration fails an error message will appear in red located below the Peak Adjust button When there is a calibration failure the Calibration Schedule will be aborted and the Current Background Coefficient and the Current Span Coefficient will be reset to the values prior to the automatic calibration attempt Possible automatic calibration errors Zero Bkg out of ra
19. It extracts dilutes and transports the sample y at an elevated temperature in order to keep the SO from reacting with Operation water as well as convert any extracted H2501 into SO The measurement of SO is done by molecular absorbance A Quantum Cascade QC laser emits pulses of mid infrared light through a heated optical cell The light emitted by the QC laser is at a frequency at which SO molecules absorb light Like most gases SO absorbs light to various degrees at multiple wavelengths The QC laser is tuned to an area of the spectrum where SO strongly absorbs while other gases which are common in combustion process such as SO water and CO do not This greatly minimizes any measurement interferences from these other gases The optical cell has a special coating and is heated to 220 C in order to minimize reaction of SO with the walls and other gases The cell measures 0 4 meters long but has an effective pathlength of 12 8 meters due to high temperature mirrors within The light exiting the cell excites a thermo electrically cooled MCT detector The absorption of light at certain wavelengths is proportional to the concentration of SO within the optical cell Figure 1 2 shows an absorption spectrum of SO compared to the reference spectrum 01 9556 7 rl un 15 44 73 102 121 150 50 Yoigt Peak Channel 0 June 3 2011 Sample Alarms Q 14 02 05 Figure 1 2 S0 Transmission Spectrum and Incomi
20. LUN SI E i TE AES inn Su 2 2 Arke S0 System Instruction Manual Jl F2Hi18 TTEH ETT E 1 0 Cli Pene JE pud du ael J F JC ho a 4 HE H E ii vb tn 1 TES mra E 4i QN ej PARUT Eiren Lis PA pS PARS a ee Pine mo gc e c 2 ggg i mF 1 nF I ur It i E E Ee TIT EL Jan ERIT E ET E Lo Nd aT LF ER EI P L y ri a et BE m ru Li zn T Ze bs bus ene 4 mpi CLAP dam Rete mr er is Bah P ind ret E Su ERIT seeds LALA cena dis J I Ya THERMO T ESIHZR AEN TT T n IC TES t DE EE PEN tie eee Manet PS aL Zee meet a E L gets c rara RL lx gu um eman g 4 pira m TL c aLL gt Lu A m Vett m et nd E JS ti EI 1 ri s a T SCIENTIFIC j e SOS MIB BOFRI REV A Figure 2 1 Thermocouple Connections Connect the support umbilical from the probe to the instrument noting all labels to ensure proper installation Terminate thermocouple ground lug to the nearest ground stud For details see Figure 2 2 Ensure that compressed air is supplied to the Air handling box and that the Air handling box is powered up Table 2 1 Heater Location on Power Distribution Board and Temperature oetpoints Thermocouple Location from the Front 1 cO CO wN _ oy o1F y amp S wy BR Co Heater Description opare Generator Stitch opare Umbilical Stitch Generator Orifice Stitch Prob
21. Pneumatic Assembly consists of 2 transducers 2 valves and 2 mass flow controllers and a fixed pressure regulator The cables are attached to the chassis with tie straps Cut the tie straps in order to free the 6 cables Free cables from chassis and any entanglements Disconnect the two 2 tees connected to the transducers the two 2 tees connected to the valves and the four 4 tubes connected to the mass flow controllers Label each disconnected part to ensure proper reinstallation Remove the four 4 nuts that secure the Pneumatic Assembly to the chassis 10 Remove the Pneumatic Assembly 11 To reinstall follow the above instructions in reverse Thermo Fisher Scientific Preventive Maintenance and Servicing Optical System Assembly Eductor Air Pressure Transducer Eductor Air Pressure p a Reaulator Eductor Air Pressure Transducer Dilution Air Pressure Reaulator 4 S0 Mass Flow Eductor Air Valve gt Controller Dilution Air Valve Cal Dilution Air Mass Flow Controller Fixed Pressure Regulator for Cal Dilution Air Pneumatic Assembly Plate Figure 5 3 Pneumatic Assembly Optical System The Optical System Assembly consists of the Bench Assembly Laser Ass embly Assembly Detector Assembly and Mounting Bracket The Mounting Bracket will be removed from the Instrument Chassis and the Bench Laser and Detector will remain attached to the moun
22. This value is the real time span reading based on the SO MFC and Span Dilution Air MFC A This section describes how to setup and run an automatic calibration Perform the following pre calibration procedure before calibrating the instrument For detailed information about the menu parameters and the icons used in these procedures see Chapter 3 User Interface Note The calibration and calibration check duration times should be long enough to account for the transition purge process when switching from sample to zero and from zero to span A Note Depending on the umbilical length and sample location data from the first several minutes of a zero calibration or check should be disregarded because of residual sample air Also data from the first several minutes of a span calibration or check should be disregarded because the span is mixing with the residual zero air A 1 If recently powered on allow the instrument to warm up and stabilize overnight Thermo Fisher Scientific Thermo Fisher Scientific Calibration Calibration 2 Check to see that there are no alarms 3 Go to the screen Calibration gt Auto Calibration Schedule a b Ensure that the Enabled Disabled button says Enabled If the Next Time is not set for the next desired Calibration time click on the button and set the date time you wish for the next calibration Based on the Period this date time will automatically update after the c
23. a ae PE E E E AE 6 6 SO MPC a TON eter he ee eae 6 6 Span MEC Dilution Ar PION docnit aab tenens eoa eU n o ot rtv ue 6 7 Span RETAIN Saree en te mere Re mc aei be api e UN E etae ae 6 7 MAS SE Oe A S elie etse san oes ius xcs ene eee tes 6 7 Laser T enipetat lG acbesicassed pO cient tasted no I eia ded 6 7 Laser Housing l emper atute osiusi i eiete eet re eura espe DEN HESSE 6 8 Laser dir e anette 6 8 Epalon E IreGbo sec anu I MM M EE M dL M 6 8 Detector LOWE scs tetti Gad uaa t cA Er RU 6 8 Detector le mip erature sim a ie ROC E Drop eS 6 8 B Yes reco oe Dale io aorta cem enn E ee ene 6 9 PIC euasit a E a et cad BRE Dd EE UE 6 9 INetwor cC oOBDHeoLbVTb osos a tv dod Edd eli ule Ite dod ebo ES 6 10 IM rio m H 6 10 Instrument Board and Cable Assembly Connections 6 10 Instrument Pneumatic Assembly Cables oss osse uo RU R 6 21 Detector Laser and Pneumatic Assembly Cables 6 21 Probe Pneumatic Cable and Wiring Connections 6 22 Cable Assembly Connections Heaters Valves and Optical Bench 6 26 Finding and Optimizing the Correct SO Peak 6 27 Service Locat losses beige Mero ea Eaa 6 33 System Component Description erre 1 1 IUD PM E 7 3 Computer ASSO ini Ol ia Sp DEN eodem do mte e 7 3 Touch Chooses e m u
24. 0 125 Amp See Table 3 6 for the default minimum and maximum detector values Table 3 6 Detector Values default Detection Control Default Minimum Maximum Detector Interval second 10 5 30 Detector Offset Maximum TEC Current Negative amps 0 5 0 1 25 Maximum TEC Voltages 3 5 0 10 Maximum TEC Current Positive amps N A 0 0 3125 Thermo Fisher Scientific Arke S03 System Instruction Manual 3 79 User Interface service Menu Manual SO Spike The Manual SO Spike screen Figure 3 62 is used for diagnosing problems and locating the correct SO peak area The Manual SO spike feature does not need to be routinely performed When enabled SO gas will bypass the SO generator and enter into the probe as SO gas This will be performed at the factory prior to shipment for two reasons 1 Frequency Validation A large amount of SO gas will be sent through the system bypassing the SO generator creating large SO peaks on the spectrum We use these SO peaks to locate the correct area of the spectrum to measure SO We will then turn off the Manual SO spike and use normal amounts of SO to fine tune the frequency used for SO3 2 SO Generator Efficiency During an SO calibration the SO peak area can be monitored to ensure that the SO generator is efficiently converting SO to SOs 0 1 95ppm RR Service gt Manual SO Spike aee s June 6 2011 Sample 15 35 45 Figure 3 62 Manual S0 Spike Screen The Manu
25. 3 56 is used to calibrate probe pressure regulators and the bench vacuum gauge SO 38 7 ppm EE Service gt Pressure Calibration September 7 2011 14 11 07 System Span Figure 3 56 Pressure Calibration Screen The Pressure Calibration screen allows the user to calibrate the following pressure readings Thermo Fisher Scientific Dilution Pressure Calibration Calibrate the probe dilution pressure Eductor Pressure Calibration Calibrate the eductor pressure Venturi Pressure Calibration Calibrate the Venturi pressure Bench Vacuum Calibration Calibrate the optical bench vacuum pressure Arke S0 System Instruction Manual 3 71 User Interface Service Menu Pressure Calibration Example 3 72 Arke S0 System Instruction Manual The Pressure Calibration screens Figure 3 57 are used to calibrate pressure devices Most likely no calibration will be needed and the coefficient can be left at 1 000 All pressure calibration screens function the same way This would include Dilution Pressure Calibration Eductor Pressure Calibration Venturi Pressure Calibration and Bench Vacuum Calibration screens S0 1 95 ppm Service gt Pressure Calibration Dilution Pressure Calibration Current Dilution Pressure 1 811 PSI Set to correct value of Dilution Pressure Coefficient April 30 2012 Filter Blowback Alarms 5 14 56 34 Figure 3 57 Dilution Pressure Calibration Screen The Diluti
26. A Use the following procedure to download data using the USB connection 1 Plug a flash drive into the USB connection on the front of the instrument The Download Data to USB Flash Drive screen will display Figure B 19 Arke 03 System Instruction Manual B 15 ePort PC Software Downloading Data to a Flash Drive B 16 Arke S0 System Instruction Manual 0 CEMS SCIENTIFIC Download Data to USB Flash Drive A USB flash drive is detected Are you sure you want to download the data Figure B 19 Download Data to USB Flash Drive Screen 2 To continue with the download select the Yes button To cancel select the No button then remove the USB drive 3 The Select Data screen will display Figure B 20 Select the From the beginning button to download all the data on the instrument Select the From last download button to download only the data stored since the last data download Select the OK button TEOM 1405 DF Shea PET VEL ECe Select Data r Downloads can contain all the data from instrument s database or only the data collected since the last download Download data OK Cancel Figure B 20 Select Data Screen Thermo Fisher Scientific Viewing Downloaded Thermo Fisher Scientific Data ePort PC Software Viewing Downloaded Data 4 The instrument will display a downloading data message and begin transferring data to the USB drive Note Do not remove the USB drive from t
27. Are you sure you want to download the data Figure 3 66 Export to USB Flash Drive Screen For more information on Downloading Data to a Flash Drive see page B 15 Thermo Fisher Scientific Equipment Required Pre Calibration Calibration Setting Thermo Fisher Scientific Chapter 4 Calibration This chapter describes procedures for performing an SO calibration of the Model 9800 SO Instrument The following sections discuss the required apparatus and procedures for calibrating the instrument e Equipment Required on page 4 1 e Pre Calibration on page 4 1 e Calibration on page 4 2 The following equipment is required to calibrate the instrument e 800 to 1200 ppm of SO in Air cylinder This section describes how the user should set the SO calibration span concentration The Calibration Settings screen located at Calibration Calibration Settings should be configured to reflect the desired SO calibration concentration Proper cylinder concentrations and flow rates will also need to be set The following are the parameters that need to be set in the Calibration Calibration Settings screen 1 SO Span Concentration The SO Span Concentration setpoint value is the span concentration setpoint used during System Span and Automatic System Span modes The value chosen should be the highest concentration the user expects to measure during normal operation Sample mode 2 Cylinder Concentratio
28. Arke 03 System Instruction Manual 3 1 User Interface Instrument Display Instrument To access instrument display touch screen push in on small door near latch Displ ay and pull plug The Instrument Display Figure 3 1 consists of various Main Menu buttons located on the left side as illustrated by the flowchart in Figure 3 XX and Figure 3 0XX These include Calibration Instrument Controls System Status and Alarms Data Analysis and Service The SO Screen button and Contact Information button are located at the top of the display and the Back button at the lower right The Status Bar at the bottom center displays the system gas mode active alarms status and date and time Thermo Scientific S05 Screen Button Information Button S0 1 95 ppm k SQ 1 95ppm June 2 2011 Alarms 11 08 50 Back Button Status Bar Figure 3 1 Instrument Display 3 2 Arke S0 System Instruction Manual Thermo Fisher Scientific User Interface Instrument Display Sul eyed 19S Ae dsiq sBunjes uoneoiunuJuo
29. Arke SO System Instruction Manual 2 15 Installation Power Distribution Power Distribution 2 16 Arke SO System Instruction Manual 3 After 6 or 7 minutes of turning the system ON ensure that the Laser Temperature at the screen System Status and Alarms Instrument Status is within 0 5 C of the set temperature and is able to maintain constant temperature for 10 minutes Use the following procedure to power Probe and Instrument heaters and devices 1 Ensure the left most circuit breaker is set to the OFF position 2 Go to Instrument Controls Component Power and ensure all heaters are set to OFF 3 Under System Status and Alarms ensure the following setpoints are set according to Table 2 3 Table 2 3 Heater Default Setpoints Heater Description Setpoint Degrees C Generator Stitch 300 Umbilical Stitch 220 Generator 425 Orifice Stitch 300 Probe 215 Umbilical 215 Bench 220 Stinger 350 4 Switch the left most circuit breaker to the ON position 5 Check to see that the Power Distribution Board has 10 red LEDs illuminated If any of the LEDs are not illuminated turn OFF AC Power Distribution breaker and change out the fuses for the corresponding LED Thermo Fisher Scientific Thermo Fisher Scientific Installation Power Distribution Equipment Damage If the bench heater is ON ensure that the instrument door is either open or that the Air Conditioning unit is ON If the bench heater is ON wit
30. Coefficients Screen ccecce 3 20 Figure 3 15 System Coefficient Screen 3 21 Figure 3 16 View Calibration Spectrum Screen cecer 3 22 Arke SO System Instruction Manual xv Figures xvi Arke S0 System Instruction Manual Figure 3 17 Current Calibration Spectrum Screen 3 23 Figure 3 18 Calibration Drift Screen 3 24 Figure 3 19 Instrument Controls Screen scere 3 25 Figure 3 20 Gas Mode Screen oseere 3 26 Figure 3 21 Component Power Screen ccecce 3 28 Figure 3 22 Component Power Instrument Screen 3 29 Figure 3 23 Component Power Probe Screen 3 31 Figure 3 24 S0 Averaging Time Screen 3 33 Figure 3 25 Blowback Schedule Screen seese 3 34 Figure 3 26 Communication Settings Screen 3 35 Figure 3 27 Serial Settings Screen 3 36 Figure 3 28 TCP IP Settings SChE CN tet eta ete i eb baud dads 3 37 Figure 3 29 Display SCRE C Maes adnot acide detent ietedottrti cete t Ct 3 38 Figure 3 30 Set Date Time Screen oo cee ccececcccseeeseeseeesereteteseaseteneeteeeneass 3 39 Figure 3 31 System Status and Alarms Screen 3 40 Figure 3 32 Instrument Status Screen 3 41 Figure 3 33 Probe Status Screen cecer 3 43 Figure 3 34 Set Alarm Limits Screen 3 45 Figure 3 35 Board Status Screen eerren 3 46 Figure 3 36 Voltages Screen 3 47 Figure 3 37 Data Analysis Screen 3 48 Figure 3 38 Data Logging Screen 3 49 Figure 3 39 View Logged Data Screen scce 3 51
31. Figure 3 40 Retrieve Data Screen 3 52 Figure 3 41 Streaming Data Settings Screen 3 53 Figure 3 42 Variable sss nes 3 54 Figure 3 43 Graphing Data Screen 3 56 Figure 3 44 View Graph Screen 3 57 Figure 3 45 Real Time Spectrum Screen ccce 3 58 Figure 3 46 Raw Spectrum Screen ssssssssssssme 3 59 Figure 3 47 Transmission Spectrum Screen 3 60 Figure 3 48 Erase Spectrum Log Screen 3 61 Figure 3 49 Statistical Analysis Screen 3 62 Figure 3 50 Service Screen 3 63 Figure 3 51 SO Generator Conditioning Screen s 3 64 Figure 3 52 Temperature Calibration Screen sss 3 65 Figure 3 53 Instrument Temp Calibrations Screen 3 66 Figure 3 54 Probe Temp Calibrations Screen sss 3 67 Figure 3 55 Bench Temp Calibrations Screen ssssssssss 3 69 Figure 3 56 Pressure Calibration Screen 3 71 Thermo Fisher Scientific Thermo Fisher Scientific Figures Figure 3 57 Dilution Pressure Calibration Screen ssessssss 3 72 Figure 3 58 Flow Calibration Screen 3 74 Figure 3 59 SO Flow Calibration Screen 3 75 Figure 3 60 Laser Controls Screen secere 3 76 Figure 3 61 Detector Controls Screen 3 78 Figure 3 62 Manual S0 Spike Screen ar 3 80 Figure 3 63 502 Calibration Setting Screen scce 3 02 Figure 3 64 Restore Factory Defaults Screen 3 04 Figure 3 65 Reboot SCLOBU o
32. Instrument Controls Menu S0 Averaging Time The SO Averaging Time screen Figure 3 24 allows the user to set the averaging time for SO concentration values during sample mode and the following manual modes system zero system span stinger blowback and filter blowback October 13 2011 03 21 13 System Zero Alarms 3 Figure 3 24 SO Averaging Time Screen Note The auto calibration schedule and auto calibration check schedule have their own settable averaging time A Thermo Fisher Scientific Arke S0 System Instruction Manual 3 33 User Interface Instrument Controls Menu Blowback Schedule The Blowback Schedule screen Figure 3 25 sets the schedule for automated and periodic blowback events Instrument Controls gt Blowback Schedule Period Last Blowback Duration 01 01 1970 00 00 00 Mote Half of the duration will be a Filter Blowback and the other half will be a Stinger Blowback June 2 20141 Filter Blowback 14 43 52 Figure 3 25 Blowback Schedule Screen The Blowback Schedule screen contains the following information e Enable Disable Enables disables the blowback schedule state The screen responds with Are you Sure and requires a Yes or No action e Next Time Sets the date and time for the next scheduled blowback event This can be set by the user It will also automatically be reset for the next run when a blowback cycle begins e Period Sets the length of time between blowb
33. Instrument Screen 7 The ePort Main screen will display with the selected instrument displayed in the top window Figure B 11 Repeat the process to add additional instruments to the list 8 To save this as a configuration select File then Save from the menu bar at the top of the Main screen The Save As screen will display Type in the desired name for the configuration and select Save B 8 Arke SO System Instruction Manual Thermo Fisher Scientific Finding Instruments on a Thermo Fisher Scientific Network ePort PC Software Finding Instruments on a Network Note Once you have connected to an instrument or instruments and saved a configuration file select Open Saved Configuration in the ePort Open screen to open that configuration and automatically connect to all the instruments that were saved in that configuration A eret 0000000 000 0 000 alti xj Fe Seer m SO3 beta A 9800 4 ber EI Sera uade v tt IP Ad revs otium rioei Dosi oben 5 Cmm anf Foddiey dorm af m Mogn Ple T me f D ate Voas Doomerdes ul gi Dombai ione Maemated Doveniseds ho Cyndi adi Frome d J Reet deren ed wi slant ath Ate Prr J Figure B 11 ePort Main Screen with Instrument Information Displayed You may use the ePort software to search for all instruments connected to the local network Note This function will only locate instruments on a local network To connect to instruments on o
34. K p j il Bi mi c 2j i Hi 2 m B i E pue y Figure 5 1 Pneumatic Tubing Detail Shutdown Refer to the following steps when a procedure requires shut down of the Instructions 1 At the User Interface screen choose Service gt Shutdown to shut down the system 2 Locate the power switch on the right side of the instrument chassis Turn switch to the OFF position 3 Unplug 220V power cord from power source 4 Unplug the pump cable from power source Thermo Fisher Scientific Arke SO System Instruction Manual 5 5 Preventive Maintenance and Servicing AC Mains Assembly Replacement AC Mains Assembly The AC Mains Assembly is attached to the back of the Instrument Chassis below the User Interface Assembly Use the following procedure to replace Replacement the AC Mains Assembly Figure 5 2 service representatives A N WARNING The service procedures in this manual are restricted to qualified 1 Perform shut down of the system Refer to Shutdown Instructions in this chapter 2 Locate the AC Mains Assembly Figure 5 2 There are two 2 wires that lead from the black fused terminal blocks to the AC Mains power switch Disconnect these wires from the terminal blocks 3 There are three 3 green yellow ground wires that need to be disconnected from the instrument chassis One is connected from the line filter to the chassis Remove the nut that attaches the gro
35. LaserTempVoltage3p3 LaserTempVoltage pb LaserlempVoltage12VD LaserlempVoltageCTLl LaserlempVoltagel TEC Laser empPower LaserTempThermistorReferenceCoefA LaserTempThermistorReferenceCoefB LaserTempThermistorReferenceCoefC LaserTempThermistorControlCoefA LaserTempThermistorControlCoefB LaserTempThermistorControlCoefC LaserHousing Temp LaserHousingT empRaw LaserHousingPowerControl LaserHousingPowerstatus LaserHousingl empsetpoint LaserHousingl empAlarmHigh LaserHousingl empAlarmLow LaserHousingT empCalCoef LaserHousingTempCalValue LaserHousing T empVoltage3p3 LaserHousing T empVoltage pb LaserHousingTempVoltage12VD LaserHousingTempVoltageCTLl LaserHousingTempVoltagelTEC Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 218 219 220 221 222 223 224 229 226 22 228 229 230 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 246 247 248 249 250 251 Serial Communication AK Protocol Description LaserHousing l empPower LaserHousing I hermistorReferenceCoefA LaserHousing I hermistorReferenceCoefB LaserHousingThermistorReferenceCoefC LaserHousingThermistorControlCoefA LaserHousingThermistorControlCoefB LaserHousingThermistorControlCoefC DetectorAGCState DetectorFrequency DetectorDelay Detectorlnterval DetectorOffset DetectorMaxTecCurrentN DetectorMaxTecCurrentP DetectorMaxTecVoltage DetectorTemp Detector empRaw Detector empPowerControl Detector empsetpoint Detec
36. System Instruction Manual Use the following procedure to replace the venture pressure differential transducer assembly Figure 5 17 Equipment Required Venturi pressure differential transducer assembly Extra long nut driver 5 16 inch Nut drive 1 4 inch WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Using a 5 16 inch extra long nut driver remove six 6 acorn nuts The cover is a convenient place to keep parts while working on the probe 2 Disconnect tubing and wiring Refer to Factory Plumbing on page 5 16 and Factory Wiring on page 5 19 3 Using a 1 4 inch nut driver remove the two 2 mounting screws holding the transducer to it bracket 4 Replace transducer assembly and reassemble in reverse order Use the following procedure to replace the stinger heater Equipment Required Stinger heater WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Turn off stinger probe generator and orifice heaters Let the probe cool to a safe handling temperature 2 After probe has cooled turn off air supply 3 Snip any wire clamps holding heater cables in place Disconnect wiring from position 7 and 8 heater wires and 23 and 24 thermocouple Thermo Fisher Scientific Stinger Clamp Replacement Eductor Replacement Venturi Tube Replacement S0 Generator Replacement AN Thermo Fisher Scientif
37. TimingControlBoardVoltageDataTemp Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 286 287 288 289 290 291 292 293 294 295 296 297 298 299 300 301 302 303 304 305 306 307 308 309 310 311 312 313 314 315 316 317 318 319 Serial Communication AK Protocol Description TimingControlBoardVoltageDataNumber TimingControlBoardVoltageDataLog LaserlempDatal emp LaserTempDataNumber LaserTempDatalog LaserHousingTempData Temp LaserHousing l empDataNumber LaserHousinglempDataLog DetectorTempDatalemp Detector empDataNumber Detector empDataLog Chassis TempDatal emp Chassis lempDataNumber Chassis TempDataLog ProbelempDatalemp Probe l empDataNumber ProbelempDataLog ProbeAmbientlempDatal emp ProbeAmbientl empDataNumber ProbeAmbientl empDataLog stingerlempDatal emp stinger empDataNumber stinger empDataLog SO3Generator empDatalemp SO3Generator empDataNumber SO3Generator empDataLog SO3Generatorstitch TempDatalemp o 03GeneratorStitchTempDataNumber SO3GeneratorstitchTempDataLog OrificeStitchTempDataTemp OrificeStitchT empDataNumber OrificeStitchT empDataLog UmbilicallempDatal emp UmbilicallempDataNumber Arke 03 System Instruction Manual C 11 Serial Communication AK Protocol C 12 Arke S0 System Instruction Manual PRC Code 320 321 322 323 324 325 326 327 328 329 330 331 332 333 334 335 336 33 7 338 Jag 340 341 342 343 344 345 346 347 348 349 350 351
38. Tl e 3 NVJ DI ZI Z T Re ms EE Gs Ce ojojoj oS Wire Color Yel 18 Grn Yel 18 Vio 18 Blu 18 Gry 18 Org 18 BIk 20 Wht 20 Red 20 Grn 20 Not Used BIk 18 Wht 18 Red 18 Brwn 18 Not Used To All Valves All Valves V1 2 V2 2 V3 2 V4 2 TB 27 L TB 28 L TB 15 L TB 16 L TB 11 L TB 12 L TB 13 L TB 14 L Function Line V Common V1 Return V2 Return V3 Return V4 Return DPX DPX Spare Spare Spare Spare Spare Spare Table 6 4 Differential Pressure Transducer Terminations From COMM EXC Color Black White To TB 27 U TB 28 U Arke SO System Instruction Manual 6 25 Troubleshooting Cable Assembly Connections Heaters Valves and Optical Bench Cable Assembly See Table 6 5 lists the cable connections for Heater Valves and Optical Connections Bench at the System Control board Table 6 5 Cable Assembly Connections Heaters Valves and Optical Bench Heaters Valves and i From Description To Optical Bench 2 Pin Blue 109496 00 J3 Generator Stitch 109496 00 J4 Orifice Stitch a 109496 00 J8 Stinger 109496 00 J9 Generator 109496 00 J11 Probe Chassis Ground 1 109930 00 J37 Press Xder 110966 00 Valves 109930 00 J7 Probe Solenoid Chassis Ground 2 Assembly Heaters 109496 00 J10 Route thru bottom Optical Bench Bench square of bracket Assembly IC Optical 109930 00 J28 Bench Thermo Bench Couple CB
39. ZOS exids ZOS enuen eDeyoA 23 unuixely Juano eaneben 23 1 wnwixey Jesyo 1039A jenia J0 09 9q SJoJ1u02 10 29 2q c 9 qeueA eIqeueA OvG jeu dwey es ng Jase oDue awl sisjeuy eonsneis OVC Jeu PSHO Aejaq esind uojeing dwey KouenbeJJ es ng Jese 129 yS JojeJeuec julod jag abeyo Jase OJUOD Jose 607 winyoeds eseij3 unoedg uoissiusueJ ungoeds Mes unjjoeds aul jeay 120 MOJ4 Jy UORNIIG uede Ie Mold ZOS uoneJqie2 MO 4 SIX amp A jepuooes SIXE A ABW eje Bulydeig Je2 ensseJgd uoueg Jed eJnsseJg UNUA Je duje JojeJeuec Je2 duie eoiiquim Jed eunsseJg Jojonp3 IED uoins e yuo Je2 eunssejg uonniig uoneJqije eynsseJd quajUog jnejeq oi Jesey poy d sBumes Jeo duie uoi eoiiquum Se qeueA Buiueeus sies eyeq Buiueeds uoneaqi et eunjeJeduue yoeg spJooes jo JequinN
40. a status code of 800000 is displayed which matches H 800000 Sensor Comm Problem In the 1 000 000 s place of the status code there are no 0 status codes displayed Therefore the downloaded status code 8433666 H 80B002 breaks down into the following status codes according to the example status code table H 2 Power Switch TPIC H 1000 Serial Port Problem H 2000 Line Printer Problem H 8000 Leak on Loop B H 800000 Sensor Comm Problem Arke 03 System Instruction Manual D 9
41. all data on the instrument or the data since the last download Select the Next button 5 The Select Location screen will display Use the Browse button to select a location for the data file downloaded by the software Select the Next button 6 The Download Type screen will display Select manual downloads Select the Next button 7 The Completing the Download Setup Wizard screen will display Select the Finish button Users can set up automatic downloads for the SO instrument monitor using the ePort software Use the following procedure to set up the software to automatically download data 1 Ensure that the PC and the instrument are connected to the same network using the Ethernet connection on the back of the instrument Thermo Fisher Scientific Thermo Fisher Scientific ePort PC Software setting Up for Automatic Data Downloads Refer to the previous section for information on connecting the instrument to a network 2 Use the ePort PC software to connect to the instrument and display the ePort Main screen Figure B 15 Refer to the previous sections for information on connecting to the instrument or instruments 3 Select Download Setup in the Commands window of the ePort Main screen The Download Setup Wizard will display Figure B 16 Select the Next button 4 The Select Data screen will display Select the data to download either all data on the instrument or the data since the last
42. and text color Instrument Controls Display select a display by choosing the option below that most closely represents your lighting conditions Dark lighting Black background and white text June 2 20141 Filter Blowback 14 52 41 Figure 3 29 Display Screen The Display screen contains the following information e Dark Lighting Black background and white text e Bright Sunshine White background and black text Default 3 38 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Set Time Date User Interface Instrument Controls Menu The Set Time Date screen Figure 3 30 allows the user to set the system date time Month Day Year f 02 f 2011 LE Hour Minute Second Figure 3 30 Set Date Time Screen Arke S0 System Instruction Manual 3 39 User Interface oystem Status and Alarms Menu System Status and Alarms Menu 3 40 Arke SO System Instruction Manual The System Status and Alarms menu Figure 3 31 allows the user to change device setpoints view the component status values alarm limits and current alarms of instrument and probe devices Also board status and voltage readings are accessible through this menu SO 0 00 ppm 2 system Status and Alarms June 2 2011 Filter Blowback Alarms 1 14 55 24 Figure 3 31 System Status and Alarms Screen The System Status and Alarms menu contains the f
43. as possible by adjusting a Offset Ref DAC i Decrease value Raw Spectrum mid right section goes UP ii Increase value Raw Spectrum mid right section goes DOWN iii An increase of 0 1 is a 0 2 C change in Laser temperature N WARNING Do not exceed 0 3V A b Ramp Ref DAC i Decrease value More curved on the left side Left side goes DOWN Thermo Fisher Scientific Arke S0 System Instruction Manual 6 27 Troubleshooting Finding and Optimizing the Correct 503 Peak ii Increase value Less curved on the left side Left side goes UP iii An increase of 0 1 is a 0 1 C change in Laser temperature WARNING Do not exceed 2 5V A 5 Y axis a Using the Laser Voltage control adjust the Raw spectrum y axis maximum to about 0 70 to 1 0 b Ifthere is an etalon effect repeating sine wave decrease the Laser voltage percentage in increments of 1 c Ifthe y axis maximum gets below 0 5 and the etalon is still present then increase the laser percentage in increments of 196 without exceeding 1 2 on the y axis 6 Locate Water a Put the System in Sample mode b Set the Laser Setpoint temperature to 10 C c The user will be going back and forth from System Status and Alarms screen amp Raw Spectrum screen for this step i Go to the Raw Spectrum and see if you notice a very large broad dip in signal blue curve ii If you do not see the large water peak then increase the laser temperature setpoint by 0 4
44. m e 4 THERMO FISHER SCIENTIFIC e 6 RU e e S03 PHOTO DETECTOR REV A o 9 C101 e 33 PCB 109511 00 ASSY 109512 00 22 zi is JUNE OR23 c2314 o 9 u29 n62 oa co e 24 IT EST aR WWW G ia ta Uu R 3 i ia o e m C53 C43 Ces H Me C102 BUE HERE RETE IER cC z 2 k L AE I 12 DS nv Zsa Figure 6 7 Detector Board s of board Detector Board Bottom e Detector Temperature Status LED e Located at the left of the board the LED D32 will be lit blue if the detector temperature is over the Setpoint value The LED D33 below D32 will be lit blue if the detector temperature is under the Setpoint temperature e Detector Cooler drive e There are two LEDs at the bottom left of the board When the Detector cooler is on the right LED will be lit If the Detector needs to be heated the right LED will be lit e The cable that is connected to J11 should be connected to the Detector Thermo Fisher Scientific Arke 03 System Instruction Manual 6 17 Troubleshooting Instrument Board and Cable Assembly Connections e Light Intensity LEDs The detector board s row of LEDs located on the bottom right corner of the board show the intensity of the light hitting the detector At least 3 of the 10 LEDs should be lit when the Laser and Detector are ON e If none of the LEDs are lit Ensure Laser Detector component power is ON Ensure Detector Cooler component power is ON En
45. on which device is selected the Setpoint button allows the user to change the setpoint within a pre determined range The Low and High buttons allow the user to change the alarm limits within a pre determined range When the Setpoint Low or High button is pushed the numeric keypad comes up S0 1 95 ppm system Status and Alarms gt Probe gt Set Alarm Limits Probe Temp Setpoint Alarm Limits Low Diagnostic l April 30 2012 Filter Blowback Alarms 5 14 52 25 Figure 3 34 Set Alarm Limits Screen Note Some instrument and probe devices do not have settable setpoints When this is the case the setpoint button will read No Setpoint A Thermo Fisher Scientific Arke S0 System Instruction Manual 3 45 User Interface oystem Status and Alarms Menu Board Status 3 46 Arke SO System Instruction Manual The Board Status screen Figure 3 35 provides computer board information If the board is functioning correctly the status will say OK If not it will say Fail Use the T and 4 buttons to move the page up and down SO 0 00 ppm system Status and Alarms gt Board Status Board Description Status Motherboard OK System Control Board OK Laser Timing Board OK Laser Temp Control Board OK June 2 2011 Filter Blowback Alarms 1 15 37 15 Figure 3 35 Board Status Screen The Board Status screen contains the following information Table 3 3 System Status Boar
46. pulse voltage e Laser Pulse Freq Laser pulse repetition rate e Pulse Delay Delay between series of pulses e Laser Pulse Width of the laser pulse e Ramp Duration Pulse duration used to calculate Ramp Ref DAC e Offset Ref DAC This voltage is proportional to DC offset for the laser e Ramp Ref DAC This voltage is proportional to ramp amplitude See Table 3 5 for the default minimum and maximum laser values Table 3 5 Laser Values Default Laser Control Default Minimum Maximum Laser Voltage Setpoint 50 0 100 Laser Pulse Clock Frequency kHz 500 400 500 Delay ns 60 60 241 Laser Pulse ns 7 3 75 50 Laser Ramp ramp duration us 0 925 0 1 275 Offset Reference DAC V 0 2 0 2 5 Ramp Reference DAC V i Be 0 2 9 Centering the SO peak on channel 0 During a calibration it is imperative that the SO peak is between 10 to 10 as seen at the transmission spectrum screen This is the calibration window If during system span the SO peak is outside this window the laser setpoint temperature will need to be changed in order to center the SO peak near channel 0 Laser temperature can be changed in the menu System Status and Alarms While in System Span mode increasing laser temperature will move the SO peak to the right as seen in the transmission spectrum screen Decreasing the laser temperature will move the SO peak to the left in the transmission spectrum screen The goal is to center the SO peak so that the
47. the new value or press the Cancel button to exit the keypad screen and return to the previous screen without saving the value 503 Span Setting 10 00 ppm Figure 3 5 Numeric Keypad Screen Arke S0 System Instruction Manual 3 7 User Interface S03 Screen and Keypads Alpha Numeric Keypad Screen 3 8 Arke S0 System Instruction Manual User enters a value into the box using the keypad Figure 3 6 When the user needs to change an alpha numeric value this keypad will automatically display Initially the box above the keypad will display the current value Enter a new value using the keypad and then select the Enter button to set the new value or press the Cancel button to exit the keypad screen and return to the previous screen without saving the value The alpha numeric keypad is only available when the user needs to enter alphabet characters Host Mame p g 3 K i d Figure 3 6 Alpha Numeric Keypad Screen Thermo Fisher Scientific User Interface Thermo Scientific Information Screen Thermo Scientific The Thermo Scientific Information screen Figure 3 7 lists Thermo Inf ti Scientific s Air Quality Instruments Division contact information Also it niormauon the system information Screen S0 1 95 ppm Information Contact Information Thermo Scientific
48. to Buyer for equipment and ninety 90 days for all other products the Warranty Period Seller agrees during the Warranty Period to repair or replace at Seller s option defective Products so as to cause the same to operate in substantial conformance with said published specifications provided that a Buyer shall promptly notify Seller in writing upon the discovery of any defect which notice shall include the product model and serial number if applicable and details of the warranty claim b after Seller s review Seller will provide Buyer with service data and or a Return Material Authorization RMA which may include biohazard decontamination procedures and other product specific handling instructions and c then if applicable Buyer may return the defective Products to Seller with all costs prepaid by Buyer Replacement parts may be new or refurbished at the election of Seller All replaced parts shall become the property of Seller Shipment to Buyer of repaired or replacement Products shall be made in accordance with the Delivery provisions of the Seller s Terms and Conditions of Sale Consumables including but not limited to lamps fuses batteries bulbs and other such expendable items are expressly excluded from the warranty under this warranty Notwithstanding the foregoing Products supplied by Seller that are obtained by Seller from an original manufacturer or third party supplier are not warranted by Seller but Se
49. user can send commands using the RUN key and the DATA STOP gt key to the instrument Each command is designated by a two digit code xx e ASTO Ask Storage Command The user can download a specified number of records from the internal data logger from the current position of the data storage pointer The location of this storage pointer may be defined by the SSTO command The values on each line of output are delimited by commas e SSTO Set Storage Command The user can change the location of the data storage pointer in the internal data logger and is used in conjunction with the ASTO command described above The data storage pointer is always located immediately after the last record transmitted through the RS232 port via the AK Protocol If the circular buffer overwrites this location or if the ASTO or SSTO commands have not been used the data storage pointer is positioned at the oldest record in the internal data logger Arke SO System Instruction Manual C 1 Serial Communication AK Protocol For AK communication the COM port settings are COM1 Properties Port Settings Bits per second Data bits Parity Stop bits Flow control Restore Defaults Figure C 1 AK COM Port Settings The following pages list the common PRC codes and show how RS Para 1 through RS Para 4 are defined in the AK Protocol and also detail the format of the transmission and response messages of the commands listed on the p
50. 0 60 minutes of Zero Air at the screen Calibration Manual Calibration press the Set Bkg button This will set the new Zero background based on the displayed SO concentration reading 6 Setthe instrument Gas mode to Span mode 7 After approximately 40 60 minutes of Span gas at the screen Calibration Manual Calibration press the Set Span button This will set the new Span coefficient based on the displayed SO concentration and the SO Span reading as calculated from the MFC slows located at the screen System Status and Alarms Instrument 8 Go to the screen Instrument Controls Averaging Time Set the Averaging time to the original setting 9 Putthe System in Sample mode Thermo Fisher Scientific Arke SO System Instruction Manual 4 5 Thermo Fisher Scientific Chapter 5 Preventive Maintenance and Servicing This chapter includes the following maintenance information and replacement procedures that should be performed on the 9800 SO3 Analyzer and PRO9805 Probe to ensure proper operation or is an expendable item not covered under warranty Expendable items are indicated by an asterisk in the table All plumbing type replacements should be followed up with a leak test For details see the following e Safety Precautions on page 5 2 e 9800 SO3 Analyzer Replacement Parts List on page 5 3 e Factory Plumbing on page 5 4 e 9800 SO3 Analyzer Replacement Tubing List on page 5 4 e
51. 005 abn i EGONILS ee E i raf Tt oa TIE ef ara pm EIE PETITES E MEMS MIES a 2 Tie oar drm ee ee ee C ie A DIALA Pages PAPPAL asa CAPE DRESS E 5 edozperromp eee su a Eel we Ao eS Gites ae Rte wep dee Wipe ee a M n ML RES Alz RIRH la AHA nE AH rea W AN a E niti sc e pid E L T LE ne Ten ricos inn Bie 3n ATTE CAEG E s ited TA PrE E Cl LE TIT NEL EE 3 4 Zu n umg E irn ies MD E E E E pla sg i ras 1 L1 eme LE PE Gid m a a Tit p 1 l seat a i SET wal 9 B E 5I zZ a a Ic 1 08 l one cr m m THERMO FISIIZR SCIENTIFIC S03 MIB BOFRD REV A PCE 1089828 n ASSY 109930 dO z P e MELIA S 1 C xus CLEE 0G BET Draw dn iiim g m Mgr lE E z TE Em Hi A 1E i hang d P EO d th Sa 3PhR OCR SOG Re DIL sa xCCF OG pu as ih LI LI wk Eur Ta CoE nal ie nino JE pis MS T NT owe aoe B a n DL eld Figure 6 1 System Control Board Top of board System Control Board Bottom of board e There are 8 fuses on this board that correspond to the valves in both the instrument and probe They are from top to bottom SO3 SO Blowback Filter Blowback Stinger Eductor Dilution Air Spare 1 not used Spare 2 not used If any of the corresponding valves are not functioning it is either that the valve is miss wired broken or the corresponding fuse is blown e There are green LEDS below each f
52. 1 Go ad a 1 emm c Alla ur no b qa T 1S ATH j E Liua EU Ll E ffi ia Lik UJI Figure 6 2 System Control Board Bottom of board 6 12 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Troubleshooting Instrument Board and Cable Assembly Connections Laser and Laser Housing Temp Control Boards Top of board There are 2 temperature control boards used in the Arke System and they are identical One controls the Laser Housing Temperature and the other controls the Laser Temperature Both of these boards are mounted on left side of the User Interface Assembly Each board has a dip switch which determines if it is the Laser or the Laser Housing control board If the switch is pointing up closest to the Thermo silkscreen it is configured for the Laser Temperature control If the switch is down closest to the Scientific silkscreen the board is configured for the Laser Housing temperature control It is critical that this be configured correctly if the board is replaced J6 is the 6 pin Jack that connects the board to either the laser or laser housing The 2 pin connector in the upper right powers the fans for the laser housing and detector If it is determined that this board is faulty replace with Part Number 109918 00 D4 on the right middle is a Red LED that is lit when the cooler is set to Off D2 on the upper right of the board is a Yellow LED that ligh
53. 1 2 TB1 AC CB1 4 TB1 AC2 109930 00 J1 AC IN 109946 00 J1 6 26 Arke SO3 System Instruction Manual Thermo Fisher Scientific Troubleshooting Finding and Optimizing the Correct S03 Peak Finding and If during system span or auto calibration the SO peak is not visible then Optimizing the the following procedure may be required This section of the manual Correct S0 Peak N WARNING Adjusting the detector controls and laser controls by a non instructs the user on how to locate and optimize the correct SO peak qualified individual can result in damages to the detector and laser A 1 Gas Mode Put the System in System Zero mode 2 Alignment It is assumed that the laser and detector have already been aligned and that there are at least 3 LEDs lit at the detectors LED strip a If there are less than 3 LEDs lit then increase the laser voltage percentage in increments of 1 until you see 3 LEDs lit b If there are more than 3 LEDs lit then decrease the laser voltage percentage in increments of 1 until you see 3 LEDs lit 3 Horizontal Make the blue curve at the Raw spectrum as horizontal as possible by applying the following detector adjustments a Adjust the detectors vertical angle up and down until you see a horizontal blue curve Allow 10 seconds for scrren to update b You will need to adjust the vertical position of the detector as you do part a above 4 Flat Make the blue curve at the Raw spectrum as flat
54. 10 L Table 5 6 Valves Cable Assembly Terminations Tl e 3 co zc uwu zi izir ime LHI oO TDM ojojoj S Wire Color Yel Grn Yel 18 Vio 18 Blu 18 Gry 18 Org 18 BIk 20 Wht 20 Red 20 Grn 20 Not Used BIK 18 Wht 18 Red 18 Brn 18 Not Used To All Valves All Valves V1 2 V2 2 V3 2 V4 2 TB 27 L TB 28 L TB 15 L TB 16 L TB 11 L TB 12 L TB 13 L TB 14 L Factory Wiring Function Farth Ground H1 amp H2 Probe H1 amp H2 Probe H3 Orifice H3 Orifice H4 Generator H4 Generator H5 Stinger H5 Stinger H6 Spike H6 Spike Function Line V Farth Ground V1 Return V2 Return V3 Return V4 Return DPX DPX Spare Spare Spare Spare Spare Spare Arke 05 System Instruction Manual 5 21 Preventive Maintenance and Servicing Dilution Eductor Replacement Dilution Eductor Replacement A 5 22 Arke S0 System Instruction Manual Table 5 7 Differential Pressure Transducer Terminations From Color To Comm Black TB 27 U Exc White TB 28 U Use the following procedure to replace the dilution eductor Figure 5 15 Equipment Required Dilution eductor Open end wrenches 1 2 inch and 9 16 inch Allen wrench 5 32 inch WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Disconnect associated plumbing 2 Remove five 5 sets of 10 32 cap screws thumbnuts 3 Remove fast loop top block
55. 13 614 615 616 617 618 619 620 621 622 623 624 625 Description DigitallnReg DigitallnAction DigitallnAction DigitallnAction DigitallnAction DigitallnAction DigitallnAction DigitallnAction DigitallnAction DigitallnLogicState DigitallnLogicState DigitallnLogicState DigitallnLogicState DigitallnLogicState DigitallnLogicState DigitallnLogicState DigitallnLogicState GraphingDataXMin GraphingDataXMax GraphingDataVariable1 GraphingDataVariable2 GraphingDataVariable3 YAxis1 YAxis2 YAxis3 GraphingDataPrimaryYMax GraphingDataPrimaryYMin GraphingDataSecondaryYMax GraphingDataSecondaryYMin RawspectrumYAxisMin RawSpectrumYAxisMax TransmissionSpectrumY AxisMin TransmissionSpectrumY AxisMax SO2ModeOn Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 626 627 628 629 630 631 632 633 634 635 636 637 638 639 640 641 642 643 644 645 646 647 648 649 650 651 652 653 654 655 656 657 658 659 Serial Communication AK Protocol Description SO2Spansetting SO2SpikeCylinderConcentration SO2SpikeMassFlowsetpoint LaserVoltageSaved SO2SpikeCalDilMassFlowsetpoint ProbeSerialNumber ProbeControllerFirmware ProbeControllerFirmwareLoadstatus ProbeControllerBlFirmware ProbeControllerBlFirmwareLoadStatus Probelemp ProbelempRaw ProbeHeaterPowerControl Probelempsetpoint ProbeTempAlarmHigh ProbeTempAlarmLow ProbeTempCalCoef ProbeTempCalValue ProbeHysterisis ProbeAmbientl emp ProbeAmbi
56. 1CalValuelnput AnaloglnPoint1CalValuelnput AnaloglnPoint1CalValuelnput AnaloglnPoint1CalValuelnput AnaloglnPoint2CalValuelnput AnaloglnPoint2CalValuelnput AnaloglnPoint2CalValuelnput AnaloglnPoint2CalValuelnput AnaloglnPoint3CalValuelnput AnaloglnPoint3CalValuelnput AnaloglnPoint3CalValuelnput AnaloglnPoint3CalValuelnput AnaloglnPoint4CalValuelnput AnaloglnPoint4CalValuelnput AnaloglnPoint4CalValuelnput AnaloglnPoint4CalValuelnput AnalogInPoint1UserValuelnput AnalogInPoint1UserValuelnput AnalogInPoint1UserValuelnput AnaloglInPoint1UserValuelnput AnalogInPoint2UserValuelnput Serial Communication AK Protocol Arke 03 System Instruction Manual C 17 Serial Communication AK Protocol C 18 Arke S0 System Instruction Manual PRC Code 524 525 526 527 528 529 530 531 532 533 534 535 536 537 538 539 540 541 542 543 544 545 546 547 548 549 550 551 552 553 554 355 556 557 Description AnalogInPoint2UserValuelnput AnalogInPoint2UserValuelnput AnalogInPoint2UserValuelnput AnalogInPoint3UserValuelnput AnalogInPoint3UserValuelnput AnalogInPoint3UserValuelnput AnalogInPoint3UserValuelnput AnalogInPoint4UserValuelnput AnalogInPoint4UserValuelnput AnalogInPoint4UserValuelnput AnalogInPoint4UserValuelnput AnalogInVoltagePoints AnalogInVoltagePoints AnalogInVoltagePoints AnalogInVoltagePoints AnaloglInZerolnitiate AnaloglInZerolnitiate AnaloglInZerolnitiate AnaloglInZerolnitiate AnaloglnSpaninitiate
57. 2 5 Figure 2 5 Stinger Spike and Return Tube Adjustment 2 6 Figure 2 6 Sample Tubing Connections ssssssssse 2 7 Figure 2 7 Probe Terminal Block sse 2 1 Figure 2 8 Stinger Clamp 2 9 Figure 2 9 Ash Deflector sssssssssssees 2 9 Figure 2 10 Mantle with Universal Mounting Flange 2 10 Figure 2 11 Mantle Mount sss 2 11 Figure 2 12 Umbilical Plumbing Hookup n se 2 12 Figure 2 13 Hot Line Hook Up Straight ssssssssssssssse 2 12 Figure 2 14 Hot Line Hook Up Underside o r 2 13 Figure 2 15 AC Main Power Switch scce 2 13 Figure 2 16 Circuit Breaker Diagram for Startup oo eee 2 14 Figure 3 1 Instrument Display 3 2 Figure 3 2 Main Menu page 1 3 3 Figure 3 3 Main Menu page Zsa mete tec ie Dem b to ob tutes 3 4 Figure 3 505 SECC sueta ented tna RR RUN SE EN wee 3 6 Figure 3 5 Numeric Keypad Screen 3 7 Figure 3 6 Alpha Numeric Keypad Screen sssssssssssse 3 8 Figure 3 7 Information Screen 3 9 Figure 3 8 Firmware Information Screen 3 10 Figure 3 9 Calibration Screen 3 11 Figure 3 10 Concentration Setting Screen 3 13 Figure 3 11 Auto Calibration Schedule Screen 3 15 Figure 3 12 Auto Calibration Check Schedule cece eee eee 3 17 Figure 3 13 Manual Calibration Screen ccinn 3 19 Figure 3 14 Calibration
58. 20 will turn off all heaters if the the chassis temperature reaches 120 F The snap switch labeled 140 will turn off the HVAC if the chassis temperature reaches 140 F Electronic filter that attenuates radio frequency interference RFI Figure 7 3 AC Mains Arke SO System Instruction Manual 7 5 System Component Description Analyzer HVAC Optical Assembly Heated White Cell Detector Assembly Laser assembly 1 6 Arke S03 System Instruction Manual Air conditioning unit to maintain chassis temperature Instrument chassis temperature is maintianed by the HVAC unit mounted on the right side of the chassis The Optical Assembly includes the light source laser pathway cell and laser light detection detector The heated white cell optical bench is where the SO is measured Laser light is bounced inside the bench until it reaches the detector assembly The cell has an effective pathlength of 12 meters Part of the bandwidth is absorbed by SO inside the cell This attenuation of signal is detected at the detector as the SO peak Detects the laser light after it has passed through the optical bench SO molecules will absorb part of the spectrum creating a feature peak in the spectrum which is detected at the detector This spectrum is then measured by the Process Control Program algorithm which calculates the SO3 concentration The Laser Assembly contains a thermal electrically cooled quantum cascade la
59. 28 3 TEMA di Bb E D J 18 Eb A 114158 111 15 27 4 n 15 2H 4 253 104158 102442011 15 28 3 i 2 20 41965 4 253 1 08158 I Ei air 1 16 E 1 17 4 A ok F T n Di ey besten 2013 10 23 1 Saath 2 eia jal 16s US k I Cows jj aco SS OOS ad cr d P u A mckag Ready NUM Figure B 21 Data csv File Opened in Excel Arke SOs System Instruction Manual B 17 AK Protocol Thermo Fisher Scientific Appendix C Serial Communication The Arke SO System supports AK Protocol This protocol permits a locally or remotely located computer to obtain information electronically from the unit These protocols are described in this appendix The AK Protocol allows the user to query the present value of any system variable remotely and allows the user to change those system variable values The user can also download information from the internal data logger The RPComm software program uses this protocol for two way communication directly to a personal computer or through a modem The following AK Protocol commands are presented in detail on the following pages e AREG Ask Register Command The use can query the analyzer for the current value of any system variable e EREG Enter Register Command The user can assign a new value to any system variable Great care must be taken when using this command as the value of variables should only be changed when the monitor is in the appropriate operating mode e SFxx Set Function xx Command The
60. 59 35 123 150 S03 Voigt Service October 12 2011 System fero Alarms 3 9 19 00 Back Figure 3 17 Current Calibration Spectrum Screen The Current Calibration Spectrum screen contains the following information e Blue Curve SO transmission spectrum at the end of the last auto calibration e Red Curve Voigt fit at the end of the last auto calibration Thermo Fisher Scientific Arke S03 System Instruction Manual 3 23 User Interface Calibration Menu Calibration Drift 3 24 Arke S0 System Instruction Manual The Calibration Drift screen Figure 3 18 provides information from the last two successful automatic calibrations S0 1 95 ppm Calibration Calibration Drift Values apply only to Auto Calibrations Last Two Completed Auto Calibrations Previous Cal Current Cal Calibration Drift Values Zero Drift Span Coefficient Drift Filter Blowback Alarms b Figure 3 18 Calibration Drift Screen 04 11 12 15 18 04 11 12 15 33 13 420 ppm 0 213 April 30 2012 14 51 25 The Calibration Drift screen contains the following information e Previous Cal Date and time of the previous successful automatic calibration e Current Cal Date and time of the most recent automatic calibration e Zero Drift The difference between the last two zero backgrounds e Span Coefficient Drift The difference in span coefficients between the last two automatic calibrations Thermo Fisher Sc
61. 7 4 2593 1 04158 T 10242011 15 50 d 21 1963 4 253 104128 AAT 15 51 4 D 215474 i 53 10415 102442011 15 52 4 215135 4 253 1 04158 10 24 2011 15 53 4 FREIE 25i 104128 UW es 15 54 a 1371 i 53 10415 102442011 15 55 4 22 0558 4 23 1 04158 10 24 2011 15 56 3 Z3 4215 2m 104128 ATT 1 4 561568 i 53 104152 102442011 15 58 4 23 go 4 2593 1 04158 B 1054 2011 15 55 3 43 5812 AL um3 104128 ATT cL 3 zn i 53 10415 1242011 18 1 4 I 23 47 4 253 104158 2 1024 2011 16 02 4 12554 AL umi 104128 E TDA 1 165 3 4 E FEF id a3 104158 12011 16 04 3 D 22 2815 4 253 1 04158 102011 16 05 E 41 3415 A23 1 04128 n O11 T5 E d D 1375 id 3 10415 1242011 1 07 4 i 215735 4 253 1041258 25 10 24 2011 16 08 4 4113 53 E 104128 em WaT T8TpE d i rf OF as id 53 10415 102442011 18 10 3 D EE E 4 253 1041258 E 10724 2011 16 11 4 oe Sae AL 23 1 04128 Z9 1xouxn 18 12 a D na 51 id 3 10415 T02442011 15 13 4 p 22 5275 4 253 104128 10024 2011 16 14 E r aut s A23 1 04128 Ae 2455011 16 15 3 D Ty fea 4 53 10415 102442011 18 18 4 D 22 7283 4 253 104155 24 10 24 2011 16 17 4 eS A 1 04128 328 1240011 18 18 3 D M Sel 4 753 10415 102442011 18 18 4 D 22 57458 4 253 1 08158 100245011 16 20 4 41 5347 Ee 104128 am waka 18 21 4 n A 053 4 253 104158 L 302442011 16 22 4 D 1a 7108 4 253 1 08158 TEMA 1656 73 3 D 18 b p ym 114158 TD24 2011 15 24 4 n 17 S18 4 253 104158 102442011 18 28 3 D 17 505 4 253 1041
62. AnaloglnSpaninitiate AnaloglnSpaninitiate AnaloglnSpaninitiate AnalogInVoltageSlope AnalogInVoltageSlope AnalogInVoltageSlope AnalogInVoltageSlope AnaloginVoltageYIntercept AnaloginVoltageYIntercept AnaloginVoltageYIntercept AnaloginVoltageYIntercept AnaloglInUserlnitiate AnaloglInUserlnitiate AnaloglInUserlnitiate Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 558 99g 560 561 562 563 564 565 566 567 568 569 5 0 571 572 9 3 5 4 575 576 577 578 579 580 581 582 583 584 585 586 587 588 589 590 591 Description AnaloglInUserlnitiate AnaloginUserCoef1 AnaloginUserCoef1 AnaloginUserCoef1 AnaloginUserCoef1 AnaloglnUserCoef2 AnaloglnUserCoef2 AnaloginUserCoef2 AnaloginUserCoef2 AnaloglnUserCoef3 AnaloginUserCoef3 AnaloginUserCoef3 AnaloginUserCoef3 DigitalScalarsOutCal DigitalScalarsOutCalDate DigitalOutReg DigitalOutReg DigitalOutReg DigitalOutReg DigitalOutVariable DigitalOutVariable DigitalOutVariable DigitalOutVariable DigitalOutRelaySetting DigitalOutRelaySetting DigitalOutRelaySetting DigitalOutRelaySetting DigitallnReg DigitallnReg DigitallnReg DigitallnReg DigitallnReg DigitallnReg DigitallnReg Serial Communication AK Protocol Arke 03 System Instruction Manual C 19 Serial Communication AK Protocol C 20 Arke S0 System Instruction Manual PRC Code 592 593 594 395 596 597 598 599 600 601 602 603 604 605 606 607 608 609 610 611 612 6
63. Arke S0 System Instruction Manual Part Number 111752 00 12Apr2013 2012 Thermo Fisher Scientific Inc All rights reserved Specifications terms and pricing are subject to change Not all products are available in all countries Please consult your local sales representative for details Thermo Fisher Scientific Air Quality Instruments 27 Forge Parkway Franklin MA 02038 1 508 520 0430 www thermoscientific com aqi Thermo Fisher Scientific WEEE Compliance This product is required to comply with the European Union s Waste Electrical amp Electronic Equipment WEEE Directive 2002 96 EC It is marked with the following symbol Thermo Fisher Scientific has contracted with one or more recycling disposal companies in each EU Member State and this product should be disposed of or recycled through them Further information on Thermo Fisher Scientific s compliance with these Directives the recyclers in your country and information on Thermo Fisher Scientific products which may assist the detection of substances subject to the RoHS Directive are available at www thermoscientific com WEEERoHS WEEE Compliance Thermo Fisher Scientific WEEE Compliance Thermo Fisher Scientific About This Manual This manual provides information about installing operating maintaining and servicing the Arke SO System It also contains important alerts to ensure safe operation and prevent equipment damage The manual is organized into
64. B uie cits rex erret ir a Y Pel tuendi VR CREE I SERM Rd UE 3 48 Daa boerna SOR p como IR Eat M 3 49 PA Nou os rr MEM T 3 51 Data Losesise Retrieve lata uus cras utei ue uite 3 52 Streantinp Data Serine Sereen e ua De bartstuae e molas 3 53 Data Logging and Streaming Variable Selection 3 54 Gara in a c 3 56 View Grap espina Aven DDR T Ed MU EvasbeE S eo 3 57 Real Dine Spectra sensed tanita dupla fab eo Att aane 3 58 Raw SC DUEL la bears a E M cad anrace nena oe io raid 3 59 Transimission Spectr unc i is MR tees Un IUS eae 3 60 Prase Spec E09 eod ottico ennt DUM n uae eor Te 3 61 SEALISEIC ALANNA 916 0355 et Sem Sa A Ea 3 62 Senice MeNi e ee tons tese ueste E E E HEMT GRY EE E Pr PACT Pr 3 63 50 Generator CODdIOoDI Bg accedens a detecte ta oues 3 64 Jemperature C aliDEACOR cue asec Rn eli us rice ERR SUE 3 65 Instrument Temp Calibrations eere 3 66 Probe Temp Calibration deseo bed er tete toro N 3 67 Temp CalibrauonjExample osos ANER 3 69 Presse CA DE HOT ooo tet a NES o a a Ite Dr f us 3 71 Pressure Calibration Example in HU ES ete EE ens 9272 Flow CaliBESEHOD eseria a oo sdves ced s EEE S 3 74 How Calibradom Examples o eoeesb bones at i EE EE UNUS 3 75 Erer Cono Seo eset ce bas Actor caste ne treet ien E ates iota co due NA REOR cud 3 76 Detector Contool dps cei ta asec sua usd Uere vios e dut es Ebo tur 3 78 Mangal SOAS pike a veni tidem Bua d dtd eld ERES 3 80 X Arke S03
65. B 9 A e From Main menu press Instrument Controls gt Communication Settings TCP IP Settings B 6 Arke SO3 System Instruction Manual Thermo Fisher Scientific ePort PC Software Connecting to the S03 Instrument Instrument Controls gt gt TCP IP Settings f June 2 2011 14 51 02 Filter Blowback Alarms 1 Figure B 7 System Status Screen 3 Start the ePort PC software using the icon on the PC desktop or the Start menu of the PC The ePort Main screen with the Open screen will display Figure B 8 Figure B 8 ePort Main Screen with Open Screen 4 In the ePort Open screen Figure B 8 select create new configuration A blank ePort Main screen will display Thermo Fisher Scientific Arke S0 System Instruction Manual B 7 ePort PC Software Connecting to the 503 Instrument 5 Select Instrument then New Instrument from the menu bar at the top of the ePort Main screen Figure B 9 F ePort Instrument j Mew Instrument Edit Instrument Delete Instrument Mew Group Refresh All Instruments Figure B 9 Selecting new Instrument from the Menu Bar 6 The Add New Instrument screen will display Figure B 10 Enter the IP address the name assigned to the instrument and the group if any assigned to the instrument and select the OK button ee Add New Instrument X Instrument Name s03 Instrument IP Address fi 1 1 75 240 238 Group Engineering Figure B 10 Add New
66. BSpaceCheck USBDownloadDone USBDownloadType CPUBoardSerialNumber CPUBoardStatus CPUBoardFirmware CPUBoardLoadStatus CPUBoardSoftwareBuildNumber CPUBoardSoftwareBuildDate Time MotherBoardSerialNumber MotherBoardstatus MotherBoardFirmware MotherBoardLoadStatus MotherBoardVoltage3p3 MotherBoardVoltaged MotherBoardVoltagebVSB MotherBoardVoltage12V1 MotherBoardVoltage12V2 MotherBoardVoltage3p3Negative MotherBoardVoltage12Negative TimingControlBoardSerialNumber TimingControlBoardStatus TimingControlBoardFirmware TimingControlBoardLoadStatus TimingControlBoardVoltage3p3 TimingControlBoardVoltageb TimingControlBoardVoltage12 TimingControlBoardVoltage DetectorBoardSerialNumber DetectorBoardstatus DetectorBoardFirmware DetectorBoardloadStatus DetectorVoltage3p3 Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 082 083 084 085 086 087 088 089 090 091 092 093 094 095 096 097 098 099 100 101 102 103 104 105 106 107 108 109 110 111 112 113 114 Mss Serial Communication AK Protocol Description DetectorVoltaged DetectorVoltageAnalogPlus DetectorVoltageAnalogNegative DetectorVoltage2p5 DetectorTempVoltageCTLl DetectorTempVoltagel TEC Detector empPower oystemControlBoardSerialNumber oystemControlBoardStatus oystemControlBoardFirmware systemControlBoardLoadStatus systemControlVoltage3p3 systemControlVoltaged systemControlVoltage15 oystemControlVoltage15Negative oystemControlVoltage12
67. Cables 6 21 Table 6 2 Heater Cable Assembly Terminations ssssss 6 24 Table 6 3 Valve Cable Assembly Terminations sssssss 6 25 Table 6 4 Differential Pressure Transducer Terminations 6 25 Table 6 5 Cable Assembly Connections Heaters Valves and Optical Bench 6 26 Table 6 T Mait FRG COGS ee t oa aed uon oe be ew imb nad C 2 Table D 1 Board Summary Status huie t teo ctp oe E hie te Ds D 1 Table D 2 Instr mpnt9otatls cce ic tette ete iet teda el tea tet D 2 Table D 3 Laser Temperature Control Board D 2 Table D 4 Laser Housing Temperature Control Board D 3 Table D 5 Laser Timing Control Board ssssssssssssssess D 3 Table D 6 Detector BOAT eee each ode Due Potente D 4 Table D 7 System Control Board D 4 Table D 8 Motherboard Status D 5 Table D 9 Hex Digits and Status Codes aue reteset ccc a poat Det ined ir D 6 Arke SOs System Instruction Manual xix Tables Table D 10 Example Status Code Table D 7 xx Arke S0s System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Chapter 1 Introduction The Arke SO System is designed to measure SO from combustion gas streams The measurement location can be anywhere from the air heater inlet through to the stack The system is comprised of three major components 9800 QC Laser Based SO Ana
68. Calibration Setting A S0 1 95 ppm Service gt Manual SO Spike SO Calibration Setting Please adjust settings so that span Dilution Air Flow falls within the MFC spec of 0 2 to 9 8 Limin SO Dilution Air Flow Setpoint 0 00 Limin June 6 2011 Sample Alarms 14 15 27 08 Figure 3 63 502 Calibration Setting Screen The SO Calibration Setting screen contains the following information SO Span Setting Sets the span concentration for SO mode Cylinder Concentration The cylinder concentration value should be set to the concentration of the SO cylinder SO Flow Setpoint The SO Flow value sets the SO MFC flow during a manual SO spike Allowable setpoints are from 0 020 to 0 480 L min Calibration Dilution Air Flow The calibration dilution air flow is calculated from the three variables above The calibration dilution air Thermo Fisher Scientific User Interface Service Menu flow MFC will be set to this value during a manual SO spike Allowable setpoints are from 0 20 to 9 80 L min Note Setting the 3 variables will calculate the Cal Dilution Air Flow If the variables entered make the Cal Dil Air Flow value out of range the value will show in RED A Thermo Fisher Scientific Arke S03 System Instruction Manual 3 83 User Interface service Menu Restore Factory The Restore Factory Defaults screen Figure 3 64 is used to restore system Defaults settings to original values set at th
69. Dilution Extractive Probe System Description The fast loop assembly draws sample flow from the process and returns it back to the stack The sample is pulled in by means of an eductor The orifice block which is heated contains an orifice and filter which connects the diluted sample to the heated sample line It keeps the components at or near 300 C The dilution module dilutes the sample with zero air and delivers it to the analyzer via the heated umbilical cord The outlet of the dilution module requires an atmospheric dump This dump should be plumbed to vent The venturi tube assembly provides a pressure differential that is measured by a pressure transducer to determine fast loop flow rate Thermo Fisher Scientific Critical Orifice Pre Filter Differential Pressure Transducer Inertial Filter Accumulator Tank Valves Critical Orifice Post Dilution Module Stinger Heater Assembly Thermo Fisher Scientific System Component Description Probe The critical orifice provides a constant flow pulled by the dilution module The pre filter limits particulate from getting into the sample system This transducer measures the differential pressure across the venturi This differential pressure is used to determine fast loop flow The inertial filter is a filter assembly with a porous filter element that can be cleaned in situ by simple blow back This filter element is a coated 316L stainless steel 10 inch long dif
70. I water Before replacing hold up the new or cleaned orifice to the light and ensure that a pinhole is visible before replacing Reassemble the clam shell and insulation turn the Probe Heater back on Turn the probe back on only once the probe temperature returns to Setpoint Place system in SO span mode and look for spectral features Thermo Fisher Scientific Troubleshooting Instrument Devices and Alarms Temperature Cold spot e Cold spots will allow for SO adsorption resulting in low concentrations in the optical bench Possible cold spots include all areas where SO travels but in particular at either end of the heated umbilical tubing Ensure that each end of the hotline umbilical is heated and insulated sufficiently to maintain temperatures greater than 180 C Generator Bakeout e If at the end of the span duration the span concentrations readings are low the SO3 Generator may need to be conditioned This cleaning can be automatically performed using the SO3 Generator Schedule The temperature of the Generator will be increased to 580 for at least a half hour At the end of the schedule the generator temperature will be set back to the setpoint temperature It is recommended to run Generator Conditionings every other day or at least once a week Plugged Stinger e fall other troubleshooting attempts do not correct the problem of low or no SO response it may be that either the inlet or outlet stinger is plugged Thi
71. Instruction Manual Thermo Fisher Scientific Installation Probe Installation C hole Plug Atmospheric Dump Union 9 9 5 SS Elbow w Port Connector Figure 2 3 Umbilical Strain Relief and Atmospheric Dump Parts Stinger Return This procedure sets the sample and return tube in their optimum position Tube and Stinger Heater Installation 1 Using a clockwise twisting motion screw stinger heater onto tube until bottoming out in mantle Figure 2 4 S0 Generator Stitch Heater otinger Heater Figure 2 4 Stinger and S0 Generator Stitch Heater Installation 2 Loosen but do not remove the three nylon insert nuts that secure the fast loop assembly table to the enclosure and slide table all the way towards the front 3 Asin step 2 loosen but do not remove nylon insert nuts that secure the SO generator assembly and slide the SO generator assembly towards front Thermo Fisher Scientific Arke S03 System Instruction Manual 2 5 Installation Probe Installation 4 Slide stinger and return tube through mantle from the mounting flange side approximately as shown Just beyond the edge of the flange snug fit tubing mantle fittings for later adjusting 5 Ona bench or floor taking care not to damage the atmospheric dump port remove if necessary line the mantle up with probe enclosure Figure 2 5 with 3 4 inch fitting in 12 o clock p
72. InterceptOto1V 457 AnalogOutVoltageYInterceptOto1V 458 AnalogOutVoltageYInterceptOto1V 459 AnalogOutVoltageYInterceptOto10V 460 AnalogOutVoltageYInterceptOto10V 461 AnalogOutVoltageYInterceptOto10V 462 AnalogOutVoltageYInterceptOto10V 463 AnalogOutVoltageYInterceptOto10V 464 AnalogOutVoltageYInterceptOto10V 465 AnalogOutCalibratelnitiate 466 AnalogOutCalibratelnitiate 467 AnalogOutCalibratelnitiate 468 AnalogOutCalibratelnitiate 469 AnalogOutCalibratelnitiate 470 AnalogOutCalibratelnitiate 471 AnaloglnReg 472 AnalogInReg 473 AnalogInReg 474 AnaloglnReg 475 AnaloginVoltage 476 AnaloginVoltage 47 AnaloginVoltage 478 AnaloglnVoltage 479 AnaloglnZeroCounts 480 AnaloglnZeroCounts 481 AnaloglnZeroCounts 482 AnaloglInZeroCounts 483 AnaloglIninputVoltage 484 AnaloglIninput Voltage 485 AnaloglIninputVoltage 486 AnaloglIninputVoltage 487 AnaloglninputSpanCounts 488 AnalogIninputSpanCounts 489 AnaloglninputSpanCounts C 16 Arke S0 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 490 491 492 493 494 495 496 497 498 499 500 501 502 503 504 505 506 507 508 509 510 511 912 513 514 519 516 517 518 519 520 521 522 523 Description AnaloglnInputSpanCounts AnalogInDescription AnalogInDescription AnalogInDescription AnalogInDescription AnaloglInReading AnaloglInReading AnaloglInReading AnaloginReading AnaloglnUnit AnaloglnUnit AnaloglnUnit AnaloglnUnit AnaloglnPoint
73. Jn uoneulJoju uoneulojul BEML ulojs S puy oynueros ouueu uoyng uny JeMog JuUsUOdWOD apo sec S oJ1u02 jueuunasu yug uogeJqiet unj edg uorneiqijez oiny jueunz suingoeds uoneJqiet M9SlA juemieo uleis S juemieo ueds ua ung punosbyoeg Juang Sjueioyieo UOHEIQIED uoneiqyeo jenueyy BINDEYIS YOSYD UOHEIGIED oin ueds jeS punobyoeg 18S uoneing pei qeu3 yoo eo ony ponad eui Buibeje y EOS eun IXON pejgeu3 1snfpy xeed uoneinq pejqeua e2 oiny poueq eui BuiBeje y EOS Sw IXON einpeuos uoneJqiet oin juiod jaS olJ4 ZOS UOHeUSDUOD JepulJAd Bunjes ueds Dunes uoyesqieg ed nus uen UOHEIGIED Figure 3 2 Main Menu page 1 3 3 Arke 03 System Instruction Manual ientific Thermo Fisher Sc User Interface Instrument Display umopinyg jooqes juiod jaS 0 J4 ZOS joogeay synejeq Ajoyoe J eJojsas uonequeouo Jepul o Dunes uoneJqie cos Bumes ueds ZOS Spo
74. LaserTempControlBoardSerialNumber LaserTempControlBoardStatus LaserTempControlBoardFirmware LaserTempControlBoardLoadStatus LaserHousingTempBoardSerialNumber LaserHousingl empBoardstatus LaserHousing I empBoardFirmware LaserHousingTempBoardLoadStatus otatusMotherboard otatusProbeController otatusInstrumentBoard StatusLaserBoard StatusDetectorBoard oystemGasMode SO3Concentration SO3ConcentrationRaw SO3ConcentrationRawAveraged SO3ConcentrationAlarmHigh Arke SO System Instruction Manual 5 Serial Communication AK Protocol C 6 Arke S0 System Instruction Manual PRC Code 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 148 149 Description S03ConcentrationAlarmLow SO3SpanConcentration DilutionRatio PreviousDilutionRatio SO3SpanConcentrationRead SO3SpanConcentrationReadRaw SO3SpanConcentrationReadAlarmHigh SO3SpanConcentrationReadAlarmLow LastCalibrationTime CurrentZeroBackground CurrentSpanCoefficient PreviousCalibrationTime PreviousZeroBackground PreviousspanCoefficient ZeroDrift spanDrift CalibrationError CylinderConcentration BenchPressure BenchPressureRaw BenchPressureAlarmHigh BenchPressureAlarmLow BenchPressureCalCoef BenchPressureCalValue BenchTemp BenchTempRaw BenchHeaterPowerControl BenchTempSetpoint BenchTempAlarmHigh BenchTempAlarmLow BenchTempCalCoef BenchTempCalValue ChassisTemp Ch
75. Make sure cable is free and untangled At the top of the User Interface box there is an opening The cable coming out of this square opening is the power supply cable This cable is daisy chained in series and supplies power to all the boards and instrument components This cable needs to be unplugged at all che connections When fully disconnected untangle cable from other cables so that it is free Remove the four 4 nuts holding the User Interface Assembly to the chassis Two people may be needed for the next step When removing the User Interface Assembly from the chassis the power supply cable will need to be snaked through the square hole at the top of the User Interface The cable cannot be disconnected at the power supply Carefully pull the User Interface Assembly from the chassis while pushing the power supply cable through the square hole To reinstall follow the above instructions in reverse Arke SO System Instruction Manual 5 13 Preventive Maintenance and Servicing Air Conditioner Replacement Figure 5 6 User Interface Assembly Replacement Air Conditioner Use the following procedure to replace the air conditioner Replacement 1 Perform shut down of the system Refer to Shutdown Instructions in this chapter 2 Remove 3 wires from the bottom of the right most breaker located at the AC Mains Assembly Write down which color wire goes to each terminal 3 Loosen 3 nuts located at the bott
76. NG WITH THE PRODUCTS PERFORMED BY ANY PERSON OR ENTITY OTHER THAN SELLER WITHOUT SELLER S PRIOR WRITTEN APPROVAL OR ANY USE OF REPLACEMENT PARTS NOT SUPPLIED BY SELLER SHALL IMMEDIATELY VOID AND CANCEL ALL WARRANTIES WITH RESPECT TO THE AFFECTED PRODUCTS THE OBLIGATIONS CREATED BY THIS WARRANTY STATEMENT TO REPAIR OR REPLACE A DEFECITVE PRODUCT SHALL BE THE SOLE REMEDY OF BUYER IN THE EVENT OF A DEFECTIVE PRODUCT EXCEPT AS EXPRESSLY PROVIDED IN THIS WARRANTY STATEMENT SELLER DISCLAIMS ALL OTHER WARRANTIES WHETHER EXPRESS OR IMPLIED ORAL OR WRITTEN WITH RESPECT TO THE PRODUCTS INCLUDING WITHOUT LIMITATION ALL IMPLIED WARRANTIES OF MERCHANTABILITY OR FITNESS FOR ANY PARTICULAR PURPOSE SELLER DOES NOT WARRANT THAT THE PRODUCTS ARE ERROR FREE OR WILL ACCOMPLISH ANY PARTICULAR RESULT A 2 Arke S03 System Instruction Manual Thermo Fisher Scientific Appendix B ePort PC Software For users that wish to utilize the SO instrument s Ethernet port to download instrument data users must first install che ePort software on a personal computer PC connected to the same network as the SO instrument that data will be downloaded from At the same time the ePort software is installed the installer will install Microsoft NET Framework software if the PC does not already have an up to date version of NET Framework See the following topics e Installing ePort on page B 1 e Connecting to the SO3 Instrument on page B 6 e Fin
77. Orifice TC 19 TC2 YEL Factory Orifice TC 20 TC3 RED Factory Generator TC 21 TC3 YEL Factory Generator TC 22 TC4 RED Installation Termination otinger TC 23 TC4 YEL Installation Termination otinger TC 24 TC5 RED Installation Termination opike TC 25 TC5 YEL Installation Termination opike TC 26 2 8 Arke S05 System Instruction Manual Thermo Fisher Scientific Installation Probe Installation Stinger Clamps Every 18 inches add a stinger clamp Figure 2 8 Installation otinger Clamp Figure 2 8 Stinger Clamp Ash Deflector Use the following procedure to install the deflector into the inlet stinger Installation igure 2 9 1 Slide ash deflector over tip of Sample tube Position Sample tube tip in center of deflector 2 Use a 5 32 inch Allen head wrench to tighten the two of the rings to the sample tube with the round side facing stack flow 3 Using 9 64 inch Allen head wrench lock in place Ash Deflector Adjust for Flow Direction Figure 2 9 Ash Deflector Thermo Fisher Scientific Arke S03 System Instruction Manual 2 9 Installation Probe Installation Mounting the Depending on work area manpower and other site specific criteria you Mantle to Stack may opt to install the mantle and probe at once or the mantle first and then the probe Use the following procedure to mount the mantle
78. Probe Temp Calibrations Menu for calibrating probe temperature readings Thermo Fisher Scientific Arke S05 System Instruction Manual 3 65 User Interface Service Menu Instrument Temp The Instrument Temp Calibrations screen Figure 3 53 is used to Calibrations calibrate instrument thermocouples and thermistors June 3 2011 14 28 04 Sample Figure 3 53 Instrument Temp Calibrations Screen The Instrument Temp Calibrations screen allows the user to calibrate the following temperature readings e Bench Temp Calibration Calibrates the optical bench temperature e Laser Temp Calibration Calibrates the laser temperature e Laser Housing Temp Calibration Calibrates the laser housing temperature e Detector Temp Calibration Calibrates the detector temperature e Chassis Temp Calibration Calibrates the instrument chassis temperature See Figure 3 55 for Temp Calibration example 3 66 Arke SO System Instruction Manual Thermo Fisher Scientific User Interface Service Menu Probe Temp Calibration The Probe Temp Calibration screen Figure 3 54 is used to calibrate probe thermocouples 50 1 95 ppm MERE Service gt Temperature Calibration Probe June 5 2011 Sample Alarms 14 35 15 Figure 3 54 Probe Temp Calibrations Screen The Probe Temp Calibrations allows the user to calibrate the following temperature readings e Probe Temp Calibration Calibrates the probe clam shell block temperat
79. Raw Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 694 695 696 697 698 699 700 701 702 703 704 705 706 707 708 709 710 711 712 713 714 15 716 717 718 719 720 721 722 723 724 725 726 727 Serial Communication AK Protocol Description SO3GeneratorStitchHeaterPowerControl SO3GeneratorStitchT empsetpoint SO3GeneratorStitchTempAlarmHigh SO3Generatorstitch TempAlarmLow SO3GeneratorstitchT empCalCoef SO3GeneratorstitchT empCalValue BlowbackPresPowerControl sampleDilutionAirPres sampleDilutionAirPresRaw sampleDilutionAirPresPowerControl sampleDilutionAirPresSetpoint sampleDilutionAirPresAlarmHigh sampleDilutionAirPresAlarmLow sampleDilutionAirCalCoef sampleDilutionAirCalValue sampleDilutionVacuum sampleDilutionVacuumRaw sampleDilutionVacuumAlarmHigh sampleDilutionVacuumAlarmLow sampleDilutionVacuumCalCoef EductorPres EductorPresRaw EductorPresPowerControl EductorPresSetpoint EductorPresCalSetpoint EductorPresAlarmHigh EductorPresAlarmLow EductorCalCoef FductorCalValue VenturiPres VenturiPresRaw VenturiPresAlarmHigh VenturiPresAlarmLow VenturiCalCoef Arke 03 System Instruction Manual C 23 Serial Communication AK Protocol C 24 Arke S03 System Instruction Manual PRC Code 728 729 730 731 132 133 734 720 721 722 723 724 125 726 727 728 729 730 731 732 738 734 Description VenturiCalValue AnalysisStartTime AnalysisEndTime AnalysisVariable1 Analysis
80. Screen with Searching for Instrument Message 3 All instruments located on the local network will be displayed in the Instrument frame on the left side of the Main screen To edit a displayed instrument or delete an instrument from the list right click on the instrument and select Edit Instrument or Delete Instrument Figure B 13 File Instrument Help Edit Instrument Delete Instrument Mew Instrument Delete Group Rename araup Figure B 13 Adding or Deleting an Instrument from the List Note To add an instrument from another network connected to the local network select Instrument then New Instrument from the menu bar Refer to the previous section for more information on manually adding an instrument to the configuration A Thermo Fisher Scientific ePort PC Software oetting Up for Manual Data Downloads 4 To save this list as a configuration select File then Save from the menu bar at the top of the Main screen The Save As screen will display Type in the desired name for the configuration and select Save Note Once you have connected to an instrument or instruments and saved a configuration file select Open Saved Configuration in the ePort Open screen to open that configuration and automatically connect to all the instruments that were saved in that configuration A Setti ng Up fOr Data can be remotely downloaded manually from the SO instrument Manual Data through the built in Ethernet c
81. System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Contents SOs Calibration Sete c e ooosedesd boob Een eue UMP nent ON EVE dS DE 3 82 Restore Factory Dela 0G ed ausos a e a Wat nc codi mca oda ual 3 84 loro eM ER 3 85 Export to USB Flash Drive pea e n o T nnie Sei IS cp YutaR ped 3 86 Cal DFatlOTi oic audien aU RS ra EOD oa Deaf tiom t teda 4 1 Eguipmebt Requibed seus ep ay pee RU RR POR rn qut a parete epus 4 Pie BID PAO 2x42 ot Df DE em tU 4 BPEL op 0010 S TNE ui op P DIU oaa a oM 4 dr lreyeiste e ne etre ae enn rer re ne ee eee 4 2 Avitomatic Calibration Schedule eus ties Sedi AREE oue tan Pn PRU pn US 4 2 Automatic Calibration Check and Automatic Calibration Schedule 4 4 Manual CalibE3tlon uuu tetro ted tee tente dar enl rn tias 4 4 Preventive Maintenance and Servicing 5 1 ACD tec MUONS outta su NO 5 2 9800 SO Analyzer Replacement Parts List esses 5 3 I 3ctor Plumbing oues eti rn patum o NU 5 4 9800 SO Analyzer Replacement Tubing List 5 4 Sh tdown Inste ctlols ouo n esq A eh 5 5 AC Mains Assembly Replacement eese 5 6 Pneumatic Assembly Replacement 3e Eo era teo vb Ue ass 5 7 Optical System a ASSEMIDIY rreraren E S E E 5 9 System Electronics Assembly sis esccvxed ensiateeencdvenvsesactbestconntennciatnecaltis 5 11 Wiser Interdico Asse MDI iene dice
82. System span then the MFC s may not be functioning correctly See SO MFC Cal flow and Span MFC Dilution air Flow above Laser Power Laser Power not turning on e The Laser Detector power can be turned on at the screen Instrument Controls Component Power Instrument Before the Laser Detector power can be turned on both the Laser housing cooler and Laser cooler must be ON and their temperatures within their respective alarm limits e Ensure that all connections especially coaxial cables to the laser detector and detector board are tight Laser Temperatu re Laser Temperature not reaching Setpoint Temperature e When the Laser Cooler is turned on the Laser Cooler temperature will automatically step down in temperature until reaching the setpoint temperature This should take 5 7 minutes This also will happen automatically when the user boots up the instrument The Laser temperature should not be set to a temperature greater than 25 e Ifthe Laser Temperature takes a long time to reach the setpoint temperature then ensure that the laser housing temperature is maintaining its setpoint temperature e Ifthe Laser Cooler does not cool the laser to its setpoint temperature then the peltier cooler may need to be replaced Thermo Fisher Scientific Arke S03 System Instruction Manual 6 7 Troubleshooting Instrument Devices and Alarms Laser Housing Temperature Laser Voltage Etalon Effect Detector Power Detector Tempe
83. Thermo Fisher Scientific Arke S0 System Instruction Manual 6 21 Troubleshooting Probe Pneumatic Cable and Wiring Connections Probe Pneumatic In this section Figure 6 10 through Figure 6 13 and Table 6 2 through C able and Wiri ng Table oi display the Pneumatic Cable and Wiring Connections that are on top of the Probe Connections DILUTION EDUCTOR Figure 6 10 Probe bulkheads heater and Valve Connections Front 6 22 Arke SO3 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Troubleshooting Probe Pneumatic Cable and Wiring Connections Figure 6 11 Probe Terminations and Pneumatics Side y HEATERS CABLE ASSEMBLY ERMINAL BLOCK TB TERMINATION SEE DETAIL A SEE DETAIL A FOR TERMINAL DESIGNATION PE2 ele le lelelelelelelelelel ele 12 13 1 4j Sit 6 2728 IPE ae f T e e 5 e eL o 6 8 el i i i i i
84. User Interface Assembly Figure 5 6 Note The Power Supply is connected to the Chassis not the User Interface Assembly A WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Perform shut down of the system Refer to Shutdown Instructions in this chapter 2 Ifthere is a USB cable or Ethernet cable connected to the front of the User Interface disconnect them Thermo Fisher Scientific Thermo Fisher Scientific 10 11 12 Preventive Maintenance and Servicing User Interface Assembly Disconnect the Laser TEC connector from the Laser board Disconnect the power cable labeled PWR on board Also disconnect the RS 485 cable position J6 that leads to the System Control board Disconnect the Laser Housing fan connector from the Laser board and TEC connector from the Laser Housing board Disconnect the Detector fan connector from the Laser board and the Detector TEC connector from the Detector board Disconnect the power cable labeled PWR on board At the Detector Board unplug the detector communication cable that leads to the detector Disconnect the coaxial cables J7 and J3 Be sure to label cables Disconnect the power cable labeled PWR on board Also disconnect the RS 485 cable position J6 that leads to the System Control board At the System Control board disconnect the power cable which is daisy chained to the Power Supply on the Detector board
85. Variable2 ProbeAnalogOutSolenoidDriver ProbeAnalogOutSwitch EductorPresAlarmLow EductorCalCoef FductorCalValue VenturiPres VenturiPresRaw VenturiPresAlarmHigh VenturiPresAlarmLow VenturiCalCoet VenturiCalValue AnalysisStartTime AnalysisEndTime AnalysisVariable1 AnalysisVariable2 ProbeAnalogOutSolenoidDriver ProbeAnalogOutSwitch Thermo Fisher Scientific Appendix D Error Code Troubleshooting The SO Instrument maintains the status of the circuit boards in the system In the event that one or more of the boards report a status of FAIL on the System Status and Alarms Board Status screen the following tables can be used to decode the details of the error This requires viewing the data logging table from the touch screen or offloading a data file from the instrument in order to obtain the error codes see Export to USB Flash Drive and Downloading Data to a Flash Drive for details about offloading a data file from the instrument Also the corresponding Data Logging Variable must be selected see Data Analysis Data Logging Settings Select Data Logging Variables Use Table D 1 to configure the variable identify the corresponding data file column name and identify the board specific table below Use the Alarms Flag under Data Logging Variable Selection as a top level status indication A non zero valve indicates one or more of the boards contain an error status Table D 1 Board Summary Status Boar
86. a new background value based on the current SO reading The current background is displayed to the left of the button Pressing Set Bkg responds with Are you sure you want to set the current SO reading to Zero and requires a Yes or No action e Set Span Sets new span coefficient based on the current SO reading and the actual span reading found at System Status and Alarms Instrument Span Reading The current coefficient and span value setpoint are displayed to the left of the button Pressing Set Span responds with Are you sure you want to set the current SO concentration reading to the Span value of ppm and requires a Yes or No action Thermo Fisher Scientific Arke S05 System Instruction Manual 3 19 User Interface Calibration Menu Calibration The Calibration Coefficients screen Figure 3 14 manually sets the Coefficients background or span coefficient using the keypad S0 1 95 ppm Calibration Calibration Coefficients Current Background Current Span Coef June 2 2011 sample 13 36 52 Figure 3 14 Calibration Coefficients Screen The Calibration Coefficients screen contains the following information e Current Background Displays the current background When pressed the numeric keypad will be displayed and a new background may be entered and saved e Current Span Coefficient Displays the current coefficient When pressed the numeric keypad will be displayed and a new span coefficient
87. acks e Duration Sets the total time of blowback filter and system e Last Blowback Displays date and time of last automatic blowback Note Half of the duration will be a filter blowback and the other half will be a stinger blowback A Note A 2 hour blowback schedule period is recommended A 3 34 Arke S03 System Instruction Manual Thermo Fisher Scientific User Interface Instrument Controls Menu Communication The Communication Settings screen Figure 3 26 allows the user to select Settings and configure Serial Settings and TCP IP Settings SO 0 00 ppm Instrument Controls gt Communication Settings am June 2 2011 Filter Blowback 14 49 40 Figure 3 26 Communication Settings Screen The Communication Settings screen contains the following information e Serial Settings Configures serial cable communication e TCP IP Settings Configures network cable communication Thermo Fisher Scientific Arke S05 System Instruction Manual 3 35 User Interface Instrument Controls Menu Serial Settings The Serial Settings screen Figure 3 27 allows the user to communicate with the instrument via a serial cable 0 10 8ppm Instrument Controls gt gt Serial Settings System Zero Alarms 3 October 13 2011 Qg 22 2z7 Figure 3 27 Serial Settings Screen The Serial Settings screen contains the following information e Serial Type Toggles between RS 232 and RS 485 e Baud kate Toggles baud
88. age up and down e Change Setpoints and Alarm Limits To change the alarm limits or setpoint values touch the row to highlight it Next press the Change Setpoints and Alarm Limits button This allows the user to change a temperature or pressure setpoint and or change that specific alarm limit See Change Setpoints and Alarm Limits on page 3 45 Thermo Fisher Scientific Arke S05 System Instruction Manual 3 43 User Interface oystem Status and Alarms Menu 3 44 Arke SOs System Instruction Manual Description Probe Temp Probe Ambient Temp otinger Temp Umbilical Temp Umbilical Stitch Temp Orifice Stitch Temp Generator Temp Generator Stitch Temp Eductor Pres Dilution Air Pres Dilution Vacuum Venturi Pressure Setpoint 215 390 2 5 250 300 425 300 15 45 Low 250 150 325 250 225 275 400 200 20 18 0 High 300 300 375 300 275 325 590 325 50 80 25 0 10 The Probe Status screen contains the following information Table 3 2 System Status Probe shown with default setpoints and alarm limits Units ie b pe eC eC eC G js psi psi in H20 in H20 Thermo Fisher Scientific User Interface oystem Status and Alarms Menu Change Setpoints and The Change Setpoints and Alarm Limits screen Figure 3 34 is used to Alarm Limits change temperature and pressure setpoints and set the low and high alarm limits for instrument and probe devices found in System Status and Alarms Based
89. al SO Spike screen contains the following information 3 80 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific User Interface Service Menu e SO Mode Toggles ON or OFF When ON this allows the SO to bypass the SO generator sending SO gas through the system to the bench e SO Calibration Setting Sets the SO concentration during SO mode Note Variables within the SO Calibration Setting menu are separate from the Calibration Span Settings in the Calibration menu A Actions that take place when SO mode is enabled Gas mode goes to SO mode The top banner will say SO instead of SO The top banner is in Green instead of Blue SO spike valve turns on MFC s turn on System remains in SO mode until disabled or until another gas mode is selected LaserVoltageSaved When turned ON the current SO laser voltage is saved and restored once SO2 mode is aborted Arke SO System Instruction Manual 3 81 User Interface Service Menu SO Calibration Setting 3 82 Arke S05 System Instruction Manual The SO Calibration Setting screen Figure 3 63 is used to set the SO span flow and calibration dilution air flow used during SO mode Note Variables within this menu are separate from the Calibration Span Settings in the Calibration menu When the Manual SO Spike is disabled or another gas mode is selected the flow setting will return to the settings in the menu Calibration
90. al v About This Manual oafety Safety Review the following information carefully before using the system This manual provides specific information on how to operate the system however if the system is used in a manner not specified by the manufacturer the protection provided by the equipment may be impaired Safety and Equipment This manual contains important information to alert you to potential safety Damage Alerts hazards and risks of equipment damage Refer to the following types of alerts you may see in this manual Safety and Equipment Damage Alert Descriptions PPP Equipment Damage Description A hazard is present that will result in death or serious personal injury if the warning is ignored A A hazard is present or an unsafe practice can result in serious personal injury if the warning is ignored A The hazard or unsafe practice could result in minor to moderate personal injury if the warning is ignored A The hazard or unsafe practice could result in property damage if the warning is ignored A Safety and Equipment Damage Alerts in this Manual Alert vi Arke S0 System Instruction Manual Description Use caution when removing a panel especially if it has the potential to free fall or be blown by the wind A Adjusting the detector controls by a non qualified individual can result in damages to the detector A he service procedures in this manual are restricted to qualified service perso
91. alibration starts The Period is the amount of time in between scheduled calibrations Set this to 24 hours if you wish to do a daily calibration at the same time each day The Duration values determine the amount of time the system will be in Auto System Zero mode and Auto System Span mode The user will want to set the duration times to a high enough value so that residual air is purged out of the system at the point of calibration A duration of 60 minutes for zero air and 60 minutes for span is suggested The user has the option of setting the Auto Calibration averaging time to a different value than the averaging time used during normal operation Some users set the Auto Calibration SO Averaging Time to a greater value than the Sample SO Averaging Time found in the menu Instrument Controls Averaging Time It is recommended that during calibration a higher averaging time should be used for best results For instance if the Auto Calibration SO Averaging Time for Auto Cal is set to 180 seconds then the last 180 seconds worth of concentration data during the zero duration will be used to set the Zero background and the last 180 seconds of concentration data during the span duration will be used to set the span coefficient The Current Cal date reflects the date and time of the last completed Auto Calibration Schedule The Peak Adjust button when enabled centers the SO peak over channel 0 To view the SO peak go to th
92. ansducer monitoring the dilution module vacuum in the PRO9805 Probe The PRO9805 Probe includes an inertial filter with a built in dilution module which prepares the sample for subsequent analysis by che 9800 SO Analyzer The 9800 SO Analyzer provides 220 AC voltage to the PRO9805 Probe which powers the probe block heaters SO3 generator heater stinger heater four probe solenoid valves for cal zero gas stinger blow back and filter blow back The 9800 SO Analyzer also receives a 4 20 ma signal from the fast loop venturi pressure transducer 1 4 Arke S0 System Instruction Manual Thermo Fisher Scientific Introduction PROS805 Dilution Extractive Probe ffs IT PES vata aa val f 4 Z Q9 IN FON 7ER ce Na INE Z MS A VA 4 U re S03 GENERATOR UTUBE 3 DIFFERENTIAL PRESSURE TRANSDUCER it s P rm SS os m 7 _ oq Y M gon y RETURN TO STACK Zar Mods f gu s A YR See ee ara 7 EM f f
93. are actively troubleshooting some inside the instrument The SO instrument has an over temperature snap switch manually resettable located on the AC Mains bracket If the chassis temperature exceeds 120 F the snap switch will open and cut the a c power to the heater until the switch is manually reset There is a second snap switch associated with the Air Conditioner When the chassis temperature reaches 140 C power to the Air Conditioner is shut off until the switch is manually reset S0 MFC Cal Flow No SO Flow 6 6 Arke S0 System Instruction Manual If there is no SO flow during System Span Auto System Span or SO mode then check that both the SO span cylinder and regulator are open Check that the SO valve atop the probe is activated during the above stated gas modes Thermo Fisher Scientific Troubleshooting Instrument Devices and Alarms Span MFC Dilution No Span Dilution Air Flow Air Flow e If there is no air flow for the span gas dilution air during the gas modes System Zero Auto System Zero System Span Auto System Span and SO mode ensure that the air handling system is functioning correctly See Air Handling Manual P N 110329 00 e Check that the dilution air valve atop the probe is activated during the above stated gas modes Span Reading Not getting to Span Setting Concentration e Ifthe Span Reading found at Systems Status and Alarms gt Instrument is alarming during System Span or Auto
94. assembly and other system settings View Calibration Spectrums The transmission spectrum that the current automatic calibration is based on will be saved Allows the user to view the calibration spectrum from the end of the last automatic calibration Calibration Drift Provides information for the last two automatic calibrations Thermo Fisher Scientific User Interface Calibration Menu Calibration Setting The Calibration Setting screen Figure 3 10 sets the variables needed to Thermo Fisher Scientific get a desired SO span concentration S0 1 95 ppm Calibration Calibration Setting span Dilution Air Flow setpoint 3 80 L min Filter Blowback Alarms b April 30 2012 14 50 23 Figure 3 10 Concentration Setting Screen The Calibration Setting screen contains the following information e Span Setting Sets the SO span concentration for calibrations e Cylinder Concentration The Cylinder Concentration value should be set to the concentration of the SO cylinder e SO Flow Setpoint The SO Flow setpoint value sets the SO MFC flow during calibrations The SO flow can be set between 0 02 and 0 480 cc min e Calibration Dilution Air Flow Setpoint The Calibration Dilution Air Flow setpoint is automatically calculated from the three variables above The Calibration Dilution Air Flow MFC will be set to this value during calibrations Note The Calibration Dilution Air Flow will be displayed as red
95. assisTempRaw Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 150 151 152 153 154 155 156 157 158 159 160 161 162 163 164 165 166 167 168 169 170 171 172 173 174 175 176 177 178 179 180 181 182 183 Serial Communication AK Protocol Description ChassisTempAlarmHigh ChassisTempAlarmLow ChassisTempCalCoef ChassisTempCalValue o02MassFlowPowerControl o02MassFlow o02MassFlowRaw SO2MassFlowSetpoint SO2MassFlowAlarmHigh o02MassFlowAlarmLow o02MassFlowCalCoef o02MassFlowCalValue spanDilAirMassFlowPowerControl opanDilAirMassFlow spanDilAirMassFlowRaw spanDilAirMassFlowSetpoint opanDilAirMassFlowAlarmHigh spanDilAirMassFlowAlarmLow spanDilAirMassFlowCalCoef spanDilAirMassFlowCalValue LaserPowerControl LaserPowerstatus LaserRamp LaserPulse LaserPulseClockFrequency LaserDelay LaserOffsetReferenceDAC LaserRampReferenceDAC LaserSpectFreq LaserFrequencyLock LaserVoltageSetpoint LaserVoltageAlarmHigh LaserVoltageAlarmLow LaserTemp Arke SO System Instruction Manual C 7 Serial Communication AK Protocol C 8 Arke S0 System Instruction Manual PRC Code 184 185 186 187 188 189 190 191 192 193 194 195 196 197 198 199 200 201 202 203 204 205 206 207 208 209 210 211 212 213 214 215 216 217 Description LaserTempRaw LaserTempPowerControl LaserlempPowerstatus Laserlempsetpoint LaserlempAlarmHigh LaserlempAlarmLow LaserlempCalCoef LaserlempCalValue
96. ature not reaching Setpoint Temperature Ensure that all connections especially coaxial cables to the detector and detector board are tight If communication is lost at the detector the transmissions spectrum and raw spectrum screens will not update Also the SO concentrations will not update A shutdown and reboot may be needed Thermo Fisher Scientific Detector Peak Thermo Fisher Scientific Troubleshooting Instrument Devices and Alarms SO Peak at the Transmission Spectrum Screen is outside the 5 to 5 Detector Peak Channel Range The detector peak during system span should be a large enough peak to be noticeable against the background noise It should be centered around channel 0 at the screen Transmission Spectrum If it is outside the detector channel range of 5 to 5 then the laser cooler setpoint temperature will need to be changed Note this is automatically done during an Automatic Calibration Schedule if the Peak Adjust option is selected The SO peak can be manually shifted towards channel 0 by manually changing the Laser Cooler setpoint temperature found in the menu System Status and Alarms At the Transmission Spectrum screen if during system span the SO peak is located to the right of channel 0 a positive Peak Channel number located at the bottom right of the screen then the Laser Cooler Temperature should be decreased in temperature by 0 01 C steps until the SO peak is between Peak Channel number
97. background and span coefficient will be restored Failure 3 Span Coefficient Out Of Range The allowable Span Coefficient range is 0 5 to 2 If during a calibration the Span Coefficient is set to outside this range then the auto calibration sequence will stop and both the original background and span coefficient will be restored Failure 4 Prev Span Coef Denominator 0 This failure will be displayed if the Previous Span Coefficient equals zero The Error should not happen during normal operation Both the original background and span coefficient will be restored Failure 5 Zero Bkg Out Of Range during SS The allowable Zero Background range is 100 to 100 ppm If during the span duration of an automatic calibration the Zero Background is set outside this range then the auto calibration sequence will stop and both the original background and span coefficient will be restored Arke SO System Instruction Manual 6 3 Troubleshooting Instrument Devices and Alarms 6 4 Arke S0 System Instruction Manual e Failure 6 Span Peak Too Weak During SS e If during an automatic calibration the SO peak is considered too weak then the calibration will stop and the original zero background and span coefficient will be restored SO Cylinder e Check to see that the secondary stage of the tank regulator is opened and reading at least 40 psig and that the tank is not near empty e The balance gas of the SO cylinder mus
98. been found 8 Optimize the Zero noise and Set Zero Background a Put the system in Zero mode Wait for 30 minutes b Record initial laser voltage percentage c What is the minimum y axis value It should be about 0 9990 0 002 i If it is above 0 9992 then decrease the laser voltage percentage by increments of 1 until the y axis minimum is 0 9990 ii If it is below 0 9988 then increase the laser voltage percentage by increments of 1 until the y axis minimum is 0 9990 d Record new laser voltage percentage Subtract new laser voltage percentage initial laser voltage percentage Then multiply that number by 0 02 The resulting number may be positive or negative ii Add this value to the laser temperature and save new setpoint e Here is what the zero noise should look like Thermo Fisher Scientific Arke S03 System Instruction Manual 6 31 Troubleshooting Finding and Optimizing the Correct 503 Peak 6 32 Arke SO System Instruction Manual 7x11 Sel wi a ER 10 175 240 99 ag Calibration S0 1 72 ppm SCIENTIFIC Data Analysis gt Real Time Spectrum gt Transmission Spectrum a Instrument Controls System Status and Alarms Data Analysis a as a a a a SUUS ONNEAUA Ge es DD 40 28 16 4 8 20 32 44 56 68 80 92 104 S 0O Voigt Peak Channel 1 System Span Alarms 2 foe ere Back 9 Set SO span coefficient Service a Goto the Calibration Settings screen Ente
99. clean the SOs generator catalyst It is recommended to condition the SO generator at 580 C for 60 minutes at least once a week Service SO Generator Conditioning Mext Time Period Duration Conditioning Previous Conditioning Temperature 01 01 1970 00 00 00 T June 3 2011 Figure 3 51 50 Generator Conditioning Screen The SO Generator Conditioning screen contains the following information 3 64 Arke SO System Instruction Manual Enable Disable Turns the generator conditioning schedule ON OFF Next Time Sets the next scheduled event for generator conditioning Period The time in between conditioning events Duration Sets how long the conditioning event will run Conditioning Temp The temperature of the generator during a conditioning event Previous Displays the last time the generator conditioning was run Thermo Fisher Scientific User Interface service Menu Temperatu le The Temperature Calibration menu Figure 3 52 is used to calibrate Calibration instrument and probe thermocouple and thermistors Most likely no calibration will be needed and the coefficient can be left at 1 000 S0 1 95 ppm Service gt Temperature Calibration June 3 2011 Alarms 0 14 24 55 Figure 3 52 Temperature Calibration Screen The Temperature Calibration screen contains the following information e Instrument Temp Calibrations Menu for calibrating instrument temperature readings e
100. cs e Instrument Installation on page 2 1 e Probe Installation on page 2 4 e Start up Procedure on page 2 13 e HVAC on page 2 15 e Temperature Control Board Verification on page 2 15 e Power Distribution on page 2 16 Equipment Damage Do not attempt to lift the instrument by the cover air conditioner or other external fittings A Ensure that the instrument is connected to the zero air box using the support umbilical noting all labels to ensure proper connection Connect the heated umbilical to both the probe and the instrument connector side goes toward the instrument chassis Feed the electrical connectors through the black strain relief before inserting the heated line It may be necessary to swage on the 1 4 inch ferrule to the end of the umbilical before feeding it through the strain relief Once the umbilical is fed through the strain relief connect the 1 4 inch nut to the bench assembly fitting Ensure that the heated umbilical is properly strain relieved on the outside of the instrument to prevent excessive strain on the bench assembly Once the tube is seated and tightened connect the umbilical thermocouple connectors into the proper plug per the thermocouple connections diagram Table 2 1 Plug the umbilical power into the bulk head military connector Arke SO System Instruction Manual 2 1 Installation Instrument Installation IL 14001 sur JL ESONILS i dre Troad 4 G qe AE H
101. ctrum The Real Time Spectrum screen Figure 3 45 allows the user to look at current spectrum S0 1 95 ppm Data Analysis gt Real Time Spectrum Filter Blowback Alarms b April 40 2012 14 55 07 Figure 3 45 Real Time Spectrum Screen The Real Time Spectrum screen contains the following information e Raw Spectrum Displays the latest spectrum from the detector e Transmission Spectrum Displays the latest SO transmission spectrum taken from the raw spectrum and also the voigt fit e Frase Spectrum Log Shows the number of backlogged spectrums When the user presses the Erase Spectrum Log button the backlogged spectrums will be erased Responds with Are you sure and requires a Yes or No action 3 58 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Raw Spectrum User Interface Data Analysis Menu The Raw Spectrum screen Figure 3 46 allows the user to view the raw spectrum from the detector board The y axis is intensity of signal and the x axis is channel numbers The blue curve is the signal received from the detector and the red curve is the polynomial fit baseline associated with a portion of the blue curve IDEE e Bl x Calibration S0 34 e ppm SCIENTIFIC Data Analysis gt Real Time Spectrum gt Raw Spectrum Instrument Controls system Status and Alarms Data Analysis g 43 Bb 123 172 215 HRaw Spectrum
102. ctrums Current Auto Calibration 08 31 11 11 16 Peak Detection Channel 6 October 13 2011 System Zero Alarms 3 09 18 29 Figure 3 16 View Calibration Spectrum Screen The Vew Calibration Spectrum screen contains the following information e Current Auto Calibration Spectrum Pressing this button will display the transmission spectrum screenshot at the time of the last successfully completed automatic span calibration e Peak Detection Channel The channel number where the SO signal peak is located during the last successful automatic calibration is also written The peak detection channel should be located between 5 and 5 If it is from 10 to 6 or 6 to 10 then a laser temperature adjustment should be performed in order to center the SO peak near channel number 0 see the laser controls information in the Service menu section If the SO signal peak is weak such as when in system zero the peak detection channel number will display 20 During system span if the peak detection channel equals 20 then the SO peak is most likely too weak to calibrate to 3 22 Arke S03 System Instruction Manual Thermo Fisher Scientific User Interface Calibration Menu Current Calibration The Current Calibration Spectrum screen Figure 3 17 displays the Spectrum transmission spectrum during the end of the last auto calibration Calibration Instrument Controls System Status and Alarms Data Analysis 15 42
103. d Description Status Motherboard OK oystem Control Board OK Laser Timing Board OK Laser Temp Control Board OK Laser Housing Temp Control Board OK Detector OK CPU Board OK Thermo Fisher Scientific User Interface oystem Status and Alarms Menu Voltages The Voltage screen Figure 3 36 displays board voltages This can be useful when diagnosing computer board problems June 2 2011 15 47 08 Filter Blowback Figure 3 36 Voltages Screen The Voltage screen contains the following information e Laser Timing Board Voltages Displays voltages related to laser timing control e Laser Temp Voltages Displays voltages related to laser and laser housing temp control e Detector Control Voltages Displays voltages related to detector control e System Control Board Voltages Displays voltages related to the system control board e Motherboard Voltages Displays voltages related to supply voltages Thermo Fisher Scientific Arke 03 System Instruction Manual 3 47 User Interface Data Analysis Menu Data Analysis Menu 3 48 Arke SO System Instruction Manual The Data Analysis menu Figure 3 37 is used to view and record SO concentrations and system data Various ways of analyzing data are offered including graphing data data logged lists real time spectrum and more September 7 2011 14 05 35 System Spar Alarms 4 Figure 3 37 Data Analysis Screen The Data Analysis screen contains the followi
104. d Data Logging Variable Selection Table Instrument Status Alarms Flags Table D 2 Laser Temperature Control Laser Temp Board Status Table D 3 Board Laser Housing Temperature Laser Housing Temp Board Status Table D 4 Control Board Laser Timing Control Board Laser Board Status Table D 5 Laser Detector Board Detector Board Status Table D 6 oystem Control Board oystem Control Board Status Table D 7 Motherboard Status Motherboard Status Table D 8 Thermo Fisher Scientific Arke S0 System Instruction Manual D 1 Error Code Troubleshooting AK Protocol Table D 2 Instrument Status Status Code in Description hexadecimal 0x00000000 no error 0x00000001 The CPU Board module has one or more error conditions 0x00000002 The CPU Mother Board baseboard has one or error conditions 0x00000004 The Laser Temperature Control Board has one or more error conditions 0x00000008 The Laser Housing Temperature Control Board has one or more error conditions 0x00000010 The Laser Timing Control Board has one or more error conditions 0x00000020 The Laser Detector Board MSP 0 has one or more error conditions 0x00000040 The Laser Detector Board MSP 1 has one or more error conditions 0x00000080 The System Control Board has one or more error conditions Table D 3 Laser Temperature Control Board D 2 Arke S0 System Instruction Manual Status Code in Description hexadecimal 0x00000000 no error 0x00000000 There is a communications e
105. d will post messages showing the progress of the installation When the process is complete the Finish screen will display Figure B 4 Select the Finish button i ePort 0 12 8 InstallShield Wizard InstallShield Wizard Completed The InstallShield Wizard has successfully installed ePort 0 12 8 Click Finish ba exit the wizard Cancel Figure B 4 InstallShield Wizard Completed Screen 8 Ifthe PC does not have an up to date version of Microsoft NET Framework software the system will automatically begin installing that software The Microsoft NET Framework Welcome screen will display Figure B 5 Select the Next gt button B 4 Arke SO3 System Instruction Manual Thermo Fisher Scientific ePort PC Software Installing ePort 15 Microsoft HET Framework 2 0 Setup L Welcome to Microsoft NET Framework 2 0 Setup This wizard will quide you through the installation process Cancel Figure B 5 Microsoft NET Framework Welcome Screen 9 Select Install The system will begin installing the Microsoft NET Framework software The wizard will post progress messages during the installation Note If the Microsoft NET Framework software is already installed on the PC the wizard will ask you to Repair or Remove the software Select Repair to ensure the latest version is installed on the PC or select Cancel to skip the Microsoft NEW Framework installation A 10 When the installation is complete the Setu
106. ding Instruments on a Network on page B 9 e Setting Up for Manual Data Downloads on page B 11 e Setting Up for Automatic Data Downloads on page B 12 e Performing a Data Download on page B 14 e Downloading Data to a Flash Drive on page B 15 e Viewing Downloaded Data on page B 17 Installin eP Ort Use the following procedure to install the ePort software g P 1 Locate and double click on the setup ePort _XX exe file where XX is the version number on the software CD that came with the SO instrument The Welcome to InstallShield Wizard screen will display Figure B 1 Thermo Fisher Scientific Arke S0 System Instruction Manual B 1 ePort PC Software Installing ePort ig ePort 0 12 8 InstallShield Wizard Welcome to the InstallShield Wizard for ePort 0 17 8 The Installshield R Wizard will install ePort 0 12 8 on your computer To continue click Nest WARMING This program is protected by copyright law and international treaties Cancel Figure B 1 ePort Welcome to InstallShield Wizard Screen 2 Select the Install button 3 The wizard will display the software license agreement Select Yes then select the Next gt button 4 The Windows update screen will display Figure B 2 If you have recently updated your Windows XP software select the Next gt button Note The ePort software MUST be installed on a PC with the latest Windows XP updates If you have not
107. download Select the Next button 5 The Select Location screen will display Use the Browse button to select a location for the data file downloaded by the software Select the Next button 6 The Download Type screen will display Select automatic downloads Select the Next button 7 The Download Schedule screen will display Figure 3 27 Select a starting date and time and a download frequency daily weekly hourly Select the Next button F Download Setup Wizard Download Schedule Setup Schedule For Automated Downloads Frequency Starting 11 16 2006 10 49 AM we Once a day 3 Once a week 9 Every H2 haur s Figure B 16 Download Setup Wizard Arke 03 System Instruction Manual B 13 ePort PC Software Performing a Data Download 8 The Completing the Download Setup Wizard screen will display Select the Finish button Perfo rming d Use the following procedure to download data Data Download 1 Ensure that the PC and the instrument are connected to the same network using the Ethernet connection on the back of the instrument Refer to the Connecting to the SO instrument section for information on connecting the instrument to a network 2 Use the ePort PC software to connect to the instrument and display the ePort Main screen Figure B 14 Refer to the Connecting to the SO instrument section for information on connecting to the instrument amp SO3 bet
108. ds f f i 1 OATE JR 4 fos 290 cc min j FRIT 4 f f 4 SR INDICATES HEATED BI OC AK EN sss INDICATES HEATED BLOCK CAL GAS DILUTION AIR z LINE 4 7 Figure 1 3 PR09805 Dilution Extractive Probe Plumbing The SO generator serves to calibrate the system with a known amount of SO3 The generator is located in the probe and the SO calibration gas follows the same path as the sample gas The calibration gas will pass through the probe assemblies and hotline before reaching the measurement bench Since the calibration gas passes along the same path as sample gas it will yield a reliable calibration relative to sample readings Thermo Fisher Scientific Arke S03 System Instruction Manual 1 5 Introduction PR09805 Dilution Extractive Probe Construction of the Inertial Filter Operating Principle of the Inertial Filter Tube Operating Principle of the SO Generator 1 6 Arke S0 System Instruction Manual The inertial filter is a filter assembly with a porous filter element that can be cleaned in situ by simple high pressure blow back This filter element is a silica coated 316L stainless steel 10 inch long diffusion bonded sintered seamless porous tube with a 0 5 micron grade A filter housing tube surrounds the tubular element creating a minimum volume annular plenum for sample collection A high efficiency gas eductor induces axial flow through th
109. duleDuration BakeScheduleTemp BakeSchedulePrevious AnalogscalarsQutCal AnalogScalarsOutCalDate AnalogOutReg AnalogOutReg AnalogOutReg AnalogOutReg AnalogOutReg AnalogOutReg AnalogOutVoltage AnalogOutVoltage AnalogOutVoltage AnalogOutVoltage AnalogOutVoltage AnalogOutVoltage AnalogOutLowVoltageCalValue AnalogOutLowVoltageCalValue AnalogOutLowVoltageCalValue AnalogOutLowVoltageCalValue AnalogOutLowVoltageCalValue AnalogOutLowVoltageCalValue AnalogOutLowVoltageCalCounts Arke 03 System Instruction Manual C 13 Serial Communication AK Protocol C 14 Arke S03 System Instruction Manual PRC Code 388 389 390 391 397 393 394 395 396 397 398 399 400 401 402 403 404 405 406 407 408 409 410 411 412 413 414 415 416 417 418 419 420 421 Description AnalogOutLowVoltageCalCounts AnalogOutLowVoltageCalCounts AnalogOutLowVoltageCalCounts AnalogOutLowVoltageCalCounts AnalogOutLowVoltageCalCounts AnalogOutHighVoltageCalValue AnalogOutHighVoltageCalValue AnalogOutHighVoltageCalValue AnalogOutHighVoltageCalValue AnalogOutHighVoltageCalValue AnalogOutHighVoltageCalValue AnalogOutHighVoltageCalCounts AnalogOutHighVoltageCalCounts AnalogOutHighVoltageCalCounts AnalogOutHighVoltageCalCounts AnalogOutHighVoltageCalCounts AnalogOutHighVoltageCalCounts AnalogOutVariable AnalogOutVariable AnalogOutVariable AnalogOutVariable AnalogOutVariable AnalogOutVariable AnalogOutRange AnalogOutRange AnalogOutRange A
110. e Umbilical Bench otinger Reading Degrees C Not Used 300 Not Used Not Used 425 300 275 275 230 350 Thermo Fisher Scientific Installation Instrument Installation Touch Screen Ethernet Ground Studs USB Port Bulkhead Military Connection i p ae aa Electrical Feed Through Heated Sample Line Ea dH Strain Relief r P 4 k dH Figure 2 2 Component Layout Arke SO System Instruction Manual 2 3 Thermo Fisher Scientific Installation Probe Installation Probe T
111. e 3 4 inch When replacing return tube or as needed 103709 00 otinger Clamp Assembly As needed 103657 00 otinger Heater up to 3 feet As needed 103658 XX otinger Heater 3 6 feet As needed 110093 00 Heater Cartridge Fast Loop BLock As needed 102989 00 Critical Orifice Stainless Coated As needed 110229 00 Gasket Cover As needed 110230 00 Gasket Face Plate As needed Expendable item not covered by warranty Arke SO System Instruction Manual 5 15 Preventive Maintenance and Servicing Factory Plumbing Facto ry Plumbing Table 5 4 lists the replacement tubing parts for the 9805 Dilution Extractive Probe Refer to Figure 5 7 through Figure 5 11 to identify the component location These figure illustrations and table allow for easy tube reattachment or replacement Replacement Tubing 5 16 Arke S0 System Instruction Manual List Table 5 4 lists the replacement tubing parts for the 9805 Dilution Extractive Probe Refer to Figure 5 7 through Figure 5 11 to identify the component location Depending on the conditions of the stack or duct annual or more less frequent replacement of factory tubing should be performed An ideal time would be shut down Table 5 4 9805 Dilution Extractive Probe Replacement Tubing Number cO co n7 i oOo ony C2 Description stinger BB Valve in to Acc Tank Bottom Tee Filter BB Valve in to Acc Tank Bottom Tee BB in port to Acc Tank Stinger BB Valve out to BB Fitt
112. e 6 3 Laser and Laser Housing Temp Control Boards Top of board 6 14 Figure 6 4 Laser and Laser Housing Temp Control Boards Bottom of board 6 15 Figure 6 5 aser Connector Board ssssssssssssssn 6 16 Figure 6 6 Laser Housing Small Connector Board ss 6 16 Figure 6 7 Detector Board Top of board 6 17 Figure 6 8 Detector Board Bottom 6 19 Foure 5 9 WONG 00 al Gi usce oio bts Oud dioe ode eae 6 20 Figure 6 10 Probe bulkheads heater and Valve Connections Front 6 22 Figure 6 11 Probe Terminations and Pneumatics Side 6 23 Figure 6 12 Probe Terminations and Pneumatics Overhead 6 23 Figure 6 13 erminal Block unies to petes Potete tein patte teens 6 24 Arke 03 System Instruction Manual xvii Figures xviii Arke S03 System Instruction Manual Figure 7 1 SO AnalyZe sese doti eti atttem Coe Diete ert vits 7 2 Figure 7 2 Pneumatic Assembly ssssssssssssses 7 4 Figure 7 3 AC IEEE 1 5 Figure AA LNE T EO ee Nee ee ctm cr bcn D MA M EE Figure 7 5 System Electronics Assembly 7 8 Figure 7 6 PFA Tubing Connections o n 1 9 Figure 7 1 PR09805 Dilution Extractive Probe System Description 7 10 Figure 7 2 SO Generator Components 7 12 Figure B 1 ePort Welcome to InstallShield Wizard Screen B 2 Figure B 2 Windo
113. e factory prior to shipment The screen responds with Are you Sure and requires a Yes or No action Gu lnmj x S0 1 95 ppm aeee ie June 6 2011 SUHU 15 40 02 Figure 3 64 Restore Factory Defaults Screen 3 84 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Reboot User Interface Service Menu The Reboot screen Figure 3 65 is used to reboot or shutdown the system The screen responds with Are you Sure and requires and Yes or No action S0 CEMS SCIENTIFIC Warning Are you sure you want to reboot or shut down the instrument Note Reboot may take up to one minute Figure 3 65 Reboot Screen The Reboot screen contains the following information e Reboot Reboots the system e Shutdown Will shutdown the system requiring a physical startup Arke S0 System Instruction Manual 3 85 User Interface Export to USB Flash Drive Export to USB Flash Drive 3 86 Arke SO System Instruction Manual Data logging data can be downloaded to a portable USB flash drive Figure 3 66 Insert flash drive into the USB slot located on the instrument console The user has the choice of downloading all records in the data logging table or downloading records since the last download When finished you can safely remove flash media from the instrument 0 CEMS SCIENTIFIC Download Data to USB Flash Drive A USB flash drive is detected
114. e filter element A high velocity gas flow 70 to 100 fps will develop axially through the porous filter tube From this mainstream flow a clean sample flow will develop radially through the porous tube wall at a very low face velocity 0 005 fps passing into the housing annulus and out the sample tube The ballistic effect of particle inertia will prevent particles entrained in the high velocity axial gas flow from depositing on or penetrating the porous filter wall The low radial velocity also inhibits particles from penetrating the porous wall Superfine particles that do enter the porous media form a permeable surface cake or dynamic membrane of approximately 0 010 inch deep This membrane then becomes the effective filter medium and it bars the passage of contaminants much smaller than the filter pore size Scouring or abrasive damage to the porous wall is prevented by the presence of a thin zero velocity Prandtl boundary layer While the filter is on stream sample flow continues without interruption so representative samples are constantly furnished The housing annulus has a very low volume to minimize sample dwell time and ensure fresh samples The SO generator uses a patented process by which SO sulfur dioxide gas is heated and reacted into SO sulfur trioxide gas Figure 1 4 This reaction is done a short distance from the probe injection point to help minimize contact of SO with cold spots SO will adsorb to a
115. e screen Data Analysis gt Real Time Spectrum Transmission Spectrum during System Span mode or Auto System Span mode During the span duration the laser temperature will be automatically adjusted in order to center the SO peak within the measurement window of channels 10 to 10 If the SO peak is located to the right of channel 0 peak channel number greater than 0 the laser cooler setpoint temperature will be automatically decreased If the SO peak is located to the left of channel 0 peak channel number less than 0 the laser cooler temperature will be automatically increased Arke 03 System Instruction Manual 4 3 Calibration Calibration Automatic Calibration Check and Automatic Calibration Schedule Manual Calibration 4 4 Arke S0 System Instruction Manual When the instrument time matches the Next Time date time in the 3 Automatic Calibration Schedule screen the automatic calibration will begin The following events will occur during an Automatic Calibration Schedule Table 4 7 Automatic Calibration Schedule of Events Mode Duration Purpose 1 Auto Filter Blowback 10 seconds Cleans probe of stack debris 2 Auto Stinger Blowback 10 seconds Cleans stinger of stack debris 3 Auto System Zero Zero Duration Floods the probe with zero air At the end of this mode the Zero background will be set 4 Auto System Span Span Duration Floods the probe with span gas At the end of this mode the Span coefficient will be
116. e tete batu ues ap miu M d LEUR E 7 8 Malyest 3b gsoos eset ettet Die E t ee nee ere 7 8 DIOS tec EL INCID MIEL ALL DOLORIS A A TA 7 9 Fast LOOP Sse ly a teta setenta desde ce fstnatataede dedisti aUs 7 10 O EDO CUNT E E 7 10 PNET Module RR TR 7 10 Venturi Tube Assem Dy s sencdvonmcsscsparcceunve suns yaavhesadeonaubeise doen nes a 7 10 COntical CFI Ce ce oreet a a E eU 7 11 Pre O a auum e nec d LM LD ME eR LL et EE DUM UE 7 11 Differential Pressure Transducer eee 7 11 n bt CE ec coco p E nitet osocs d us etutatesd iade uddxapdu d 7 11 Accumulator Late esae eaa ER Dit an e edet 7 11 BS ANN RN NR T dT 7 11 Critical Orifice Post Dilution Module eee 7 11 Sunger Heater Assembly ets ttaii HE dte vei v n Eee 7 11 SO Generator Component Description eese 7 12 SOS Generator U Tube cocer tone eee e cO E 7 12 MERC ALC AEREA SE E AAS dione D MEIN AA Ub LEES 7 12 Hearer Blocked ca RR aod E LEE 7 13 ThepmocoUpleus seeded etm Diti tenui EA Dette Rein 7 13 ERES ENTE TS ITE 7 13 Genemtor Buclosufeu eene eR ume a EM EE 7 13 Enclosure DEtaeketusooncec oet terit te i etude bxbeniciwtne roi Qua 7 13 Appendix A WY ciupi T A 1 Appendix B dud PG SONW ANC T C M B 1 TriState a aen ea RU Id eM EE er UM EU B 1 Connecting to the SO Instrument osos cg esse eee o a peat san eos bosse qup voa Us eh s B 6 Finding Instruments on a Network o
117. e the new cover gasket by following the previous steps in reverse Valve Cover Gasket Figure 5 16 Cover Removal 5 26 Arke SO System Instruction Manual Thermo Fisher Scientific Preventive Maintenance and Servicing Valve Assembly Replacement Valve Assembly Use the following procedure to replace the valve assembly Figure 5 17 Replacement Equipment Required Valve assembly Extra long nut driver 5 16 inch Medium slotted screwdriver WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Remove electrical access cover The cover is a convenient place to keep parts while working on the probe 2 Identify which valve is to be replaced labels on probe 3 Using a medium size slotted screwdriver remove four 4 M4x10 metric screws and lock washers from inside the probe Retain 4 Loosen screws and unplug electrical connector on top of valve Refer to Figure 5 12 on page 5 19 5 Install replacement valve in same orientation and reassemble in reverse order Venturi Pressure D T A Valve Assemblies Figure 5 17 Electrical Components Replacement Thermo Fisher Scientific Arke S03 System Instruction Manual 5 27 Preventive Maintenance and Servicing Venturi Pressure Differential Transducer Assembly Replacement Venturi Pressure Differential Transducer Assembly Replacement AN Stinger Heater Replacement AN 5 28 Arke S03
118. e to replace the System Electronics Assembly Figure 5 5 service representatives A WARNING The service procedures in this manual are restricted to qualified 1 Perform shut down of the system Refer to Shutdown Instructions in this chapter 2 Unplug all connectors from the System Control board and Power Distribution board a Make sure all cables are labeled to ensure proper reinstall b The colorful ribbon cables are connected to both boards Do not forget to re connect these when reinstalling Arke SO System Instruction Manual 5 11 Preventive Maintenance and Servicing User Interface Assembly User Interface Assembly 5 12 Arke S03 System Instruction Manual 3 When the two boards are free from all cables remove the three 3 nuts holding it to the chassis 4 To reinstall follow the above instructions in reverse Figure 5 5 System Electronics Assembly Replacement The User Interface Assembly is located at the top right of the instrument Chassis On the outside of the frame there are three 3 boards which include the Laser board Laser Housing board and Detector board Also on the outside of the frame is a touch screen USB and Ethernet ports Inside the box you will find the Motherboard hard drive and touch screen electronics When disconnecting cables from the boards it is suggested that the cables should be labeled in order to ensure proper reinstall Use the following procedure to replace the
119. eading goes into alarm the system will automatically default into Filter Blowback mode June 2 2011 Filter Blouback Alarms 1 14 21 35 Figure 3 20 Gas Mode Screen The Gas Mode screen selections are as follows Sample Probe pulls sample from the stack System Zero Zero air floods the probe making it possible to run and set a background measurement System Span Calibration gas floods the probe making it possible to calibrate the system Stinger Blowback Compressed air is released blowing residue out of the stinger Thermo Fisher Scientific User Interface Instrument Controls Menu e Filter Blowback Compressed air is released blowing residue out of the probe Thermo Fisher Scientific Arke S03 System Instruction Manual 3 27 User Interface Instrument Controls Menu Component Power The Component Power screen Figure 3 21 allows the user to select either Instrument or Probe component power buttons SO 0 00 ppm 2 Instrument Controls gt Component Power Exi June 2 20141 Filter Blowback 14 33 12 Figure 3 21 Component Power Screen 3 28 Arke S03 System Instruction Manual Thermo Fisher Scientific User Interface Instrument Controls Menu Instrument Component The Instrument Component Power screen Figure 3 22 allows the user to Power turn ON OFF Instrument devices Upon Instrument Startup the Laser Housing Cooler Laser Cooler and Laser and Detector Power will automatically turn ON i
120. eae ae ama eS 1 8 installati omna ES 2 1 Instrument Installato ieeriar odi ono e notte E E edu 2 1 Probe SCAU AIO 1 sens acaso tret ober a E 2 4 Preparing he BBeloSule sedie iti insani darsi e Ip ipe 2 4 Stinger Return Tube and Stinger Heater Installation 2 5 Sunger Clamps Installations en apis tru tre ROC Sepp Supp EeE EUR bx oe 2 9 Ash Deflector Iristallattongs ce ec t rrt E on ER CERE EUER Eau 2 9 Mounting the Mantle 0 S036 Econo t oia sers eiie 2 10 Umbilical Plumbing Hookup estes et pest tien irr a Une aed 2 11 SEARED PLO C CDOTS oai ese E vans sssaeve talis eos Diete dae 2 13 DEC ud uM M LER E C EE 2 15 Temperature Control Board Verification eeeesessss 2 15 Power DuisttiDUtiOEb esee oeeto ses cicots Durham Duns EOE tuts 2 16 User Interfd6 Baa ecd co fin acd idc i cv d cba dr a RR eu EE wv C ud 3 1 Pair Gee BILL T p eee ee 3 2 SOsSereen and Keypads osten aH b MM 3 6 Numere Keypad Sree iaronn etd adus aia SE up E vas Vete ve euis 3 7 Alpha Numeric Keypad S6I6611 4 5 5 m IR d re me UA 3 8 Thermo Scientific Information Screen eee 3 9 Firmware Informatio Mnre erre ren nr Ex oseac paved er ekoses pudo 3 10 Ali Dra OTe Meni soctomseteteacs Kanani sui dite tian tout butane ELI M A ELLE LUE 3 11 RAI EA SEDIS oec ode E Eo oM Ra eee 3 13 Auto Calibration Schedule eer rne eae erre 3 15 Auto Calibration Check Schedule
121. ed As needed Arke 03 System Instruction Manual Preventive Maintenance and Servicing 9800 S03 Analyzer Replacement Parts List 5 3 Preventive Maintenance and Servicing Factory Plumbing Factory Plumbing 9800 S05 Analyzer Replacement Tubing 5 4 Arke SO System Instruction Manual List Table 5 4 lists the replacement tubing parts for the 9800 SO Analyzer Refer to Figure 5 1 to identify the component location This figure illustration and table allow for easy tube reattachment or replacement Table 5 4 lists the replacement tubing parts for the 9800 SO Analyzer Refer to Figure 5 1 to identify the component location Depending on the conditions of the stack or duct annual replacement of factory tubing should be performed An ideal time would be shut down Table 5 2 9800 SO Analyzer Replacement Tubing Number Description Eductor in to A 3 8 PTFE Blow back to B 3 8 PTFE Dilution air to C 1 4 PTFE Cal dilution to D 1 4 PTFE Pump to optical bench 1 4 PTFE CDA in to E 3 8 PTFE 902 To Probe to F 1 4 PTFE Zero air to G 1 4 PTFE 902 in to H 1 4 PTFE 10 K to J 1 4 PTFE cO co 0o0o Gc1 4 Cc25 F Tubing Length Nut and Ferrule set 2 3 8 S S 2 3 8 S S 2 1 4 S S 2 1 4 S S 2 1 4 S S 2 1 4 S S 2 1 4 S S 2 1 4 S S 2 1 4 S S 2 1 4 S S Thermo Fisher Scientific Preventive Maintenance and Servicing shutdown Instructions F D
122. em control board has green LEDs illuminated Use the following procedure to start and validate the functionality of the HVAC unit 1 Turn on the right most circuit breaker which supplies 208 VAC power to the HVAC unit attached to the chassis Once the HVAC is started you should detect that the internal fan is on At this point try to keep the main door of the enclosure closed as much as possible during the rest of start up Use the following procedure to start and validate the functionality of the Laser Cooler and Laser Housing Cooler Ensure that the Laser Housing Temperature at the screen System Status and Alarms Instrument Status is maintaining the setpoint temperature This may take up to a minute Ensure that the temperature is stable for 5 minutes 2 Accurate Laser temperature as opposed to the Laser Housing temperature is more critical to the proper operation of the instrument The Laser Cooler setpoing temperature found at the screen System Status and Alarms Instrument Status is set at the factory and should not be changed unless a channel peak offset is seen during calibration See the Laser Controls section in chapter 3 for information on how to change the laser temperature Note Upon Startup the Laser Cooler will automatically be turned ON when the Laser Housing Cooler temperature is within its alarm limit The Laser Cooler cannot be turned ON unless the Laser Housing Cooler is ON and within alarm limits A
123. enance and Servicing 15 Micron Filter Replacement Use the following procedure to replace the 15 micron filter Figure 5 15 Equipment Required 15 Micron filter WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Disconnect associated plumbing 2 Remove 5 sets of 10 32 cap screws thumbnuts 3 Remove fast loop top block with or without orifice locks attached 4 Loosen three 3 fast loop table nylon insert nuts and slide table back 5 Replace the 15 micron filter seated flat with the arrow on top pointing at the cross union and assemble in reverse Use the following procedure to replace the valve cover gasket Figure 5 16 Equipment Required Valve cover gasket Extra long nut driver 5 16 inch WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Perform shut down of the system Refer to Shutdown Instructions in this chapter 2 Turn off air supply to the instrument 3 Remove acorn nuts from cover and screws to face plate Arke SO System Instruction Manual 5 25 Preventive Maintenance and Servicing Valve Cover Gasket Replacement 4 Label and disconnect all valve fittings from valves going through top of probe 5 Label and disconnect all heaters and thermocouples going through top of probe 6 Setassembly aside without removing umbilical connectors 7 Peeloff face gasket and replace 8 Replac
124. entTempRaw ProbeAmbientTempAlarmHigh ProbeAmbientTempAlarmLow ProbeAmbientTempCalCoef ProbeAmbientTempCalValue Umbilical Temp UmbilicallempRaw UmbilicalHeaterPowerControl UmbilicallempSetpoint UmbilicallempAlarmHigh UmbilicallempAlarmLow UmbilicalTempCalCoef UmbilicalTempCalValue OrificeStitch Temp Arke 03 System Instruction Manual C 21 Serial Communication AK Protocol C 22 Arke S0 System Instruction Manual PRC Code 660 661 662 663 664 665 666 667 668 669 670 671 672 673 674 675 676 677 678 679 680 681 682 683 684 685 686 687 688 689 690 691 692 693 Description OrificeStitch empRaw OrificestitchPowerControl OrificeStitchT empsetpoint OrificeStitchTempAlarmHigh OrificeStitchTempAlarmLow OrificeStitch empCalCoef OrificeStitchT empCalValue UmbilicalStitch Temp UmbilicalStitch TempRaw UmbilicalStitchHeaterPowerControl UmbilicalStitch TempSetpoint UmbilicalStitch TempAlarmHigh UmbilicalStitchTempAlarmLow UmbilicalStitchTempCalCoef UmbilicalStitch TempCalValue otingerTemp stinger empRaw otingerHeaterPowerControl Stinger TempSetpoint otingerTempAlarmHigh otingerTempAlarmLow otingerTempCalCoef otingerTempCalValue SO3Generator Temp SO3Generator TempRaw SO3GeneratorHeaterPowerControl SO3Generator empsetpoint SO3Generator empAlarmHigh SO3Generator empAlarmLow SO3Generator empCalCoet SO3Generatorl empCalValue SO3GeneratorConditioningstate SO3Generatorstitch Temp SO3Generatorstitch emp
125. er Location on Power Distribution Board and Temperature SE TOOL MES E E EE E A EE Me E EEEE MEO Me coSed eod 2 2 Table 2 2 Probe Terminal Block Heater and Thermocouple Wire Connections2 8 Table 2 3 Heater Default Setpoints ssssssssssssses 2 16 Table 3 1 System Status lInstrument shown with default setpoints and alar UTS NERO EPOR NE ERE 3 42 Table 3 2 System Status Probe shown with default setpoints and alarm MARS NE EO ESL PER ERE 3 44 Table 3 3 System Status Board sssssssssssss 3 46 Table 3 4 Variable List for Data Logging and Streaming 3 54 Table 3 5 Laser Values Default ssssss 3 77 Table 3 6 Detector Values default 3 79 Table 4 7 Automatic Calibration Schedule of Events sss 4 4 Table 5 1 9800 SO Analyzer Replacement Parts ss 5 3 Table 5 2 9800 05 Analyzer Replacement Tubing 5 4 Table 5 3 PR09805 Probe Replacement Parts sssss 5 15 Table 5 4 9805 Dilution Extractive Probe Replacement lubing 5 16 Table 5 5 Heaters Cable Assembly Terminations ssss 5 21 Table 5 6 Valves Cable Assembly Terminations sssssss 5 21 Table 5 7 Differential Pressure Transducer Terminations 5 22 Table 6 1 Detector Laser and Pneumatic Assembly
126. et to Current Time Sets the time period to the last two hours Select Variable 1 User selects variable from list that has been selected in data logging Select Variable 2 User selects variable from list that has been selected in data logging Thermo Fisher Scientific Service Menu Thermo Fisher Scientific User Interface Service Menu The Service Menu Figure 3 50 allows the user to set and control various system devices The Service menu will be locked out if password protection located in the Instrument Controls menu is enabled April 18 2012 11 43 57 Filter Blowback Alarms 5 Figure 3 50 Service Screen The Service Menu contains the following information SO Generator Conditioning User can schedule periodic maintenance for the SO generator Temperature Calibration User can calibrate temperature readings Pressure Calibration User can calibrate pressure readings Flow Calibration User can calibrate flow readings Laser Controls User can set laser control parameters Detector Controls User can set detector control parameters Manual SO Spike The SO flow will bypass the SO generator Restore Factory Defaults All system factory defaults will be restored Reboot Instrument will reboot or shutdown Arke S0 System Instruction Manual 3 63 User Interface Service Menu S0 Generator The SO Generator Conditioning screen Figure 3 51 is used to Conditioning periodically and automatically
127. fic Analyzer Computer Assembly Touch Screen Network Connector USB Port Motherboard ATX Power Supply Hard drive Thermo Fisher Scientific System Component Description Analyzer The following describes the analyzer components The computer Assembly contains the user interface computer boards and computer peripherals Allows the user to easily control and navigate the Instruments graphical user interface The network connecter is a Cat 5 8 position modular jack It allows the user to remotely connect to and control the Instrument and also download data logged information The USB 2 0 Port allows the user to download data logged information directly from the Instrument using a USB thumb drive The Motherboard connects the central processing unit CPU to other systems and devices It allows other components and peripherals of the system to be electrically connected The ATX Power Supply converts AC electrical energy to DC It supplies electricity to the system The Solid State High Density Drive stores and retrieves digital information The hard drive will store data logged information which can be retrieved using a thumb drive at the Instrument or remotely by using a program such as ePort Arke SO System Instruction Manual 7 3 System Component Description Analyzer Pneumatic Assembly Mass Flow Controllers Fixed Regulator for Span Dilution Air MFC Eductor Pressure Regulator Valve and Sens
128. follow the fan cord Unplug the fan Next remove the fan from the detector assembly and place inside the chassis so that it is out of the way of the Optical System At the Laser Assembly locate the fan on top of the heat sink follow the wires to the laser board and disconnect the connector from the Laser board Remove and place the fan inside the chassis so that it is out of the way of the Optical System At the Laser Assembly disconnect the power cable RS 485 cable clock coax cable and TEC cable Before removing cables make sure that they are labeled in order for proper re install Remove the five 5 nuts that hold the Optical Assembly to the chassis Remove Optical Assembly from the chassis To reinstall follow the above instructions in reverse Thermo Fisher Scientific Preventive Maintenance and Servicing oystem Electronics Assembly E a cu P Optical Bench LR i PR m SG chk t a Figure 5 4 Optical Assembly Replacement System Electronics The System Electronics Assembly consists of two printed circuit boards and Thermo Fisher Scientific Assembly the System Electronics Bracket When facing the instrument chassis the board on the left is called the System Control board and the board on the right is the Power Distribution board When disconnecting cables from either board it is suggested that the cables are labeled in order to ensure proper reinstall Use the following procedur
129. fusion bonded sintered seamless porous tube with a 0 5 micron grade A filter housing tube surrounds the tubular element creating a minimum volume annular plenum for sample collection A high efficiency gas eductor induces axial flow through the filter element The accumulator tank allows the blow back valves to blast the two sections of the sample inlet system with a volumetric force of air There are four valves at the probe SO3 SO filter blow back and stinger blow back This maintains pressure and flow of the diluted sample between the exit of the dilution module and the heated sample line The stinger heater is mounted around the portion of the stinger that is located in the mantle assembly The mantle assembly is mounted to the probe box and passes through the stack outer wall to the inner wall The stinger extends to at least three feet into the inner stack Arke SO System Instruction Manual 7 11 System Component Description Probe S0 Generator The SO Generator components refer to Figure 7 2 include Component e SO Generator U tube Description Heater e Heater Block e Thermocouple e Insulation e Generator Enclosure e Enclosure Bracket b vd Heater Insulation Generator Enclosure 475 K D Figure 7 2 S0 Generator Components S0 Generator U Tube The Generator u tube acts as a reaction chamber that generates SO gas when SO and Air are reacted together Heater The hea
130. h ME de M er epu EDU ud 7 3 Network Connector ouod eit ita tae tai adde Dae db Eire 7 3 US CAE EO TNR ERREUR 7 3 M OREDO 2 Gl oats issus FUP N BL UeuE 7 3 ATX Power Supply os ecu tuat o test shed eda bu etes 7 3 lie ores re HT a E E TT 7 3 Pneumatic Assembly aescxtestestdk east EE vb n Drei RE vp RES WADE Edd 7 4 Mass Flow Conttolloetss aoc dei OR Ud eU d e 7 4 Fixed Regulator for Span Dilution Air MFC 7 4 Eductor Pressure Regulator Valve and Sensor Assembly T4 Dilution Pressure Regulator Valve and Sensor Assembly 7 4 Thermo Fisher Scientific Contents P In EU EN R UU E 7 5 Circuit Dea eT Saget anni an eee ena EE M ED DEL ELM 7 5 Thermal Runaway Switches and Relay 7 5 Loe d E Ce T ONT 7 5 Inh s QR PET NEP ERES 7 6 Optical Assem DI usse eute eset apponi et ao rupe Udine cius ed da ep ei ans 7 6 Heated White ell uoa E o opo n EUM EI cuMCE SEE E 7 6 Detector ASSODIDIM cantus sro Dres lm Un Ee eH UR p cm Reo abra ak 7 6 Laserdassemblysisesuedus s ibd PIS RINDIDM DR IUE eR IE 7 6 System Electronics Assem Diy cute eet aes etae et eene ees iones 7 7 Power Distribution Board eeeceeeeeeeeeeeenneene 7 7 Dystemi Control BOAT under eaae nodi otto tdv ois ned tauk 7 7 Pneumatic and Tubing Connections eene 7 8 Felon T UbIBg 4 ose boba opi ies diio tubcd aeo iati dud 7 8 Heater CaS acetat
131. h the door closed and the Air Conditioning OFF thermal damage to the boards may occur A 7 Under Instrument Controls Component Power Instrument turn Bench heater ON Check under the System Status and Alarms menu to ensure that the temperature is climbing toward setpoint 8 Under Instrument Controls Component Power Probe turn on each of the heaters one at a time Check under the System Status and Alarms menu to ensure that the temperature of each component climbs toward the setpoint Again power up each circuit one at a time and check the corresponding termperature to ensure the thermocouple and heaters are not crossed 9 Check to see that all the temperatures control to within 5 C of their corresponding setpoints This may take up to 60 minutes Temperature setpoints and values are located in the System Status and Alarms menu Arke 03 System Instruction Manual 2 17 Thermo Fisher Scientific Chapter 3 User Interface This chapter describes the functionality of the touch screen user interface For details see the following topics e Instrument Display on page 3 2 e SO3 Screen and Keypads on page 3 6 e Thermo Scientific Information Screen on page 3 9 e Calibration Menu on page 3 11 e Instrument Controls Menu on page 3 25 e System Status and Alarms Menu on page 3 40 e Data Analysis Menu on page 3 48 e Service Menu on page 3 63 e Export to USB Flash Drive on page 3 86
132. he ribbon cable is tightly fastened to J34 which is the 31 pin connector at the top left Figure 6 9 Motherboard 6 20 Arke SO System Instruction Manual Thermo Fisher Scientific Troubleshooting Instrument Pneumatic Assembly Cables Instrument Pneumatic This section lists the Instrument s Pneumatic assemblies part numbers and Assembly Cables board connections Detector Laser and See Table 6 1 for the Detector Laser and Pneumatic Assembly cables Pneumatic Table 6 1 Detector Laser and Pneumatic Assembly Cables Assembly Cables From Description To Item 8 110977 00 Coax 109512 00 J3 Cable Detector Assembly J2 J1 110971 00 Preamp to Photo 109512 00 J11 Detector Assembly Fan Detector 109918 00 A J6 Laser Housing Assembly Item 12 6 Pin 111019 02 109918 00 A J4 Bottom Connector Bd J4 TEC Laser Housing Assembly Item 8 110977 00 Coax 109512 00 J7 Bottom Connector Bd J3 Cable CLK Laser Housing Assembly Item 13 110019 01 6 Pin 109918 00 B J4 Top Connector Bd J3 Laser Housing Assembly Item 14 51 010803 RS 485 109512 00 J9 RS 485 Bottom Connector Bd J8 Interconnect Cable RS 485 MFC 2 500 sccm S02 103284 00 J16 MFC 1 10 LPM S02 Dil 1032840 00 J19 Shutdown Valves 110973 00 J Pressure Transducer ED 110976 00 J15 Pressure Transducer DIL 110976 00 J25 Pressure Regulator ED 110789 00 J27 Pressure Regulator DIL 110789 00 J35 Vacuum XDCR 110968 00 J11
133. he installation procedure of the PRO9805 Dilution Extractive Probe Insta lati on involves several steps e Preparing the Enclosure e Stinger Return Tube and Stinger Heater Installation e Stinger Clamps Installation e Ash Deflector Installation e Mounting the Mantle to Stack e Umbilical Plumbing Hookup Preparing the The PRO9805 Probe is supplied with a 3 inch Strain Relief Assembly to Enclosure accommodate the Heated Umbilical Line Figure 2 3 Some disassembly will be required to mount the enclosure to the process port Both preparatory stages are described below The PRO9805 Probe allows for the Heated Line and associated strain relief to be mounted either out of the rear or the bottom of the enclosure This will allow each installation some flexibility in the sample line routing DANGER Use caution when removing a panel especially if it has the potential to free fall or be blown by the wind A Equipment Damage Do not attempt to lift the instrument by the cover air conditioner or other external fittings A Equipment Damage There is a bulkhead fitting used as an atmospheric dump on the bottom of the enclosure Take care not to damage A gt gt e Remove the two large side panels from the enclosure by rotating the compression latches counter clockwise Both panels are identical Maintain inward pressure on the center of the panel while unlatching to prevent panel from dropping Figure 2 3 2 4 Arke S0 System
134. he instrument while the data is downloading A 5 When the data download is complete the instrument will display a Download complete message and display the file name as it is stored on the USB flash drive The file name format is the instrument serial number followed by a date time stamp Remove the USB flash drive and select the OK button to continue Data files are downloaded and saved as csv files txt files through USB that can be opened and viewed with Microsoft Excel The file name format is the instrument serial number followed by a date time stamp The data files will be saved to the folder selected using the Download Setup Wizard Refer to the Setting Up for a Data Download section for information on setting up a data folder The default folder location is C Program Files Thermo ePort Data E3 crosolt Cece S0Ibeta C_20 I 10 Z5 15 90 35 c8 ale x JS bed CS sh a a HI GG PY EY ions a srl 215 a Z U EFT tn BR RRC E m Be Edk Yew pomt Formal Too Dua Weke Heb Adobe PDF F oi x za fg fua d amp b My ii v H E negn pf Window B Harej 8 zm f 23 n L de 1 SenalMumber warnt Safhw re wersion 2 SOA Imstrumaent STA D hb 3 3 Trne Slang Burer of Alania Apte Alan Flags and talus Syabern Gas Mode ZO Concentration Curent fem Geckground Current Span Coeficien System Caefficsent SCIL Span Concentration San 5 TZ AIT 15 4l 3 D J i 53 10415 ri B 10 24 2011 15 45 3 20 764
135. he protection provided by the equipment may be impaired A N WARNING Ifthe equipment is operated in a manner not specified by the 5 2 Arke SOs System Instruction Manual Thermo Fisher Scientific 9800 S0 Analyzer Replacement Parts Thermo Fisher Scientific List Part Number 111188 00 111110 00 1111542 00 109660 00 109918 00 109512 00 109930 00 109496 00 110656 00 102631 00 110803 00 110976 00 2136 336 103211 00 110657 00 111127 00 110137 00 109755 00 110646 00 109757 00 111048 00 Table 5 1 9800 05 Analyzer Replacement Parts Description Power Supply ATX Hard drive 80gb Touch screen assembly Com express board Temperature control board Photo detector board MIB Power distribution board Pneumatic assembly Mass flow controller 10LPM Mass flow controller 500 sccm Pressure transducer assembly oolenoid valve Pressure transducer 2 60 psig AC Mains assembly Fuse cartridge 30 Amp Optical bench assembly Optical system assembly Detector housing assembly Laser assembly AC Unit 3000 BTU HR Table 5 1 lists the replacement parts for the 9800 SO Analyzer Note The recommended replacement interval is site specific therefore these are only guidelines A Replacement Interval As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As needed As need
136. hen set to current the latest data will be recorded When set to min or max the minimum or maximum value during the period will be recorded The board status will automatically be set to current even if averaging is selected Erase Log Allows the user to erase all values in the data log Arke S0 System Instruction Manual 3 49 User Interface Data Analysis Menu e Reset to Default Content Allows the user to reset the default data logging fields 3 50 Arke SO3 System Instruction Manual Thermo Fisher Scientific View Logged Data Thermo Fisher Scientific User Interface Data Analysis Menu The View Logged Data screen Figure 3 39 allows the user to define which data records to view Two ways of selecting viewable data are offered Time Range and Number of records back S0 1 95 ppm Data Analysis gt View Logged Data Time Range OR Number of records back June 3 2011 10 05 30 Alarms Figure 3 39 View Logged Data Screen The View Logged Data screen contains the following information Time Range Selection e Start Time Start time to retrieve data e End Time End time to retrieve data e Retrieve Data first row Displays data logging values based on Time Range conditions Number of Records Back Selection e Number of Records Back Defines data logging retrieval by number of records e Retrieve Data second row Displays data logging values based on Number of records bac
137. his board should connect to the Laser Housing Temperature control board which has the DIP switch in the Down position closest to the Scientific on the silkscreen It is important that these cables are not switched between the Laser Control board and the Laser Housing Small Connector Board E J2 TEC2 i TES TEMP CTR SMALL ph La ums mm a A Eum CONN BD i M VEM S p Y IA IBBECLINLIBIS j REU A nd Figure 6 6 Laser Housing Small Connector Board Detector Board Top of board e Ifthe Laser and Detector Power is set to ON under Component Power the 2 highlighted Active LED lights should blink OFF ON alternately If the spectrum is not updating and the Laser and Detector Power is reading OFF under Component Power a power cycle may be necessary e Ensure that the Laser and Detector power located at the screen Instrument Controls Component Power Instrument Laser and Detector Power is turned ON 6 16 Arke SO System Instruction Manual Thermo Fisher Scientific Troubleshooting Instrument Board and Cable Assembly Connections e Ifthe Active LEDs are not blinking ON OFF every 10 to 30 seconds then ensure power and communication cables are connected Ensure the detector power cable and the 2 coax cables are connected tightly at both ends of the cable oon a o Qm N N TEL cu 1 aei es Xle e e eaxe Uy U m 2 De gt Cy N EP d a gt LL Q E Jes
138. iated with the right y axis e Commit amp View Graph Graph is displayed Note Graphic data is taken from the data logging records The list of available variables from the Graphing Data screen reflects the highlighted variables in the data logging variable list A Thermo Fisher Scientific User Interface Data Analysis Menu View Graph The View Graph screen Figure 3 44 shows the data selected over the selected time period The left blue y axis pertains to the blue curve while the right red y axis pertains to the red curve Ini xj 1 350 0 000 1 560 0 000 1 179 0 OU 0 rog 0 000 0 330 0 000 0 000 L BEEN ERE 000 2011 06 05 2011 06 03 2011 06 04 2011 06 04 2011 06 04 2011 05 03 03 00 15 03 23 15 03 45 15 10 03 15 10 32 15 10 53 14 S03 Conc ppm System Gas Mode Figure 3 44 View Graph Screen The Retrieve Data screen contains the following information Thermo Fisher Scientific Y axis Max Sets the maximum value for the primary y axis left or secondary y axis right Y axis Min Sets the minimum value for the primary y axis left or secondary y axis right X axis Min Sets the minimum value for the x axis X axis Max Sets the maximum value for the x axis Current Time amp Default Y axis Auto scales the primary and secondary y axis and sets the x axis to the last 2 hours Arke 03 System Instruction Manual 3 57 User Interface Data Analysis Menu Real Time Spe
139. ic Preventive Maintenance and Servicing otinger Clamp Replacement wires from probe terminal block Pull disconnected wires into probe The wires need to be free before disconnecting probe from mantle See Figure 2 7 and Table 2 2 4 Disconnect Return Tube and Sample tube Loosen the 3 nylon nuts that secure the fastloop table to the enclosure and slide it away from the Stinger 5 Remove probe assembly from mantle and set aside 6 Remove heater with a counter clockwise twist 7 Install new heater and reassemble in reverse order Refer to Figure 2 8 on page 2 9 to replace the stinger clamp This is only necessary for lengths of 2 feet or more past the mantle exit Refer to Figure 5 15 on page 5 23 to replace the eductor Refer to Figure 5 15 on page 5 23 to replace the venturi tube assembly Use the following procedure to replace the SO generator Equipment Required Nut driver 3 8 inch 9 16 inch combination wrench WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Remove probe doors 2 Turn OFF generator heater and allow to cool to ambient temperature 3 Disconnect heaters 5 and 6 and thermocouple 21 and 22 leads from top Pull wires through bottom Arke SO System Instruction Manual 5 29 Preventive Maintenance and Servicing oervice Locations 4 Remove the four nuts holding the generator bracket to the bottom of the probe case 5 Loosen and remo
140. ides an overview of the components in the 9800 SO Analyzer and PRO9805 Dilution Extractive Probe describes the function of the system components and provides a typical system plumbing hookup per the following The 9800 SO Analyzer components include e Computer Assembly on page 7 3 e Pneumatic Assembly on page 7 4 e AC Mains on page 7 5 e HVAC on page 7 6 e Optical Assembly on page 7 6 e System Electronics Assembly on page 7 7 e Pneumatic and Tubing Connections on page 7 8 The PRO9805 Dilution Extractive Probe components include e Fast Loop Assembly on page 7 10 e Orifice Block on page 7 10 e Dilution Module on page 7 10 e Venturi Tube Assembly on page 7 10 e Critical Orifice on page 7 11 e Pre Filter on page 7 11 e Differential Pressure Transducer on page 7 11 e Inertial Filter on page 7 11 e Accumulator Tank on page 7 11 e Valves on page 7 11 e Critical Orifice Post Dilution Module on page 7 11 Arke SO System Instruction Manual 7 1 System Component Description service Locations e Stnger Heater Assembly on page 7 11 e SO3 Generator Component Description on page 7 12 Computer Assembly HVAC Power Distribution Optical Assembly Pneumatic and Tubing ii EE s Connections in tt AC Mains Pneumatic Assembly Figure 7 1 SO Analyzer 7 2 Arke S03 System Instruction Manual Thermo Fisher Scienti
141. ientific Instrument Controls Menu Thermo Fisher Scientific User Interface Instrument Controls Menu The Instrument Controls Menu Figure 3 19 allows the user to select the system gas mode turn devices ON OFF and adjust instrument settings SCIENTIFIC June 2 2011 System Zera leris C 14 05 13 Figure 3 19 Instrument Controls Screen The Instrument Controls Menu contains the following buttons Gas Mode Selects the gas mode for the system Component Power Turns instrument and probe devices ON OFF SO Averaging Time Sets the averaging time for the SO sample measurement Blowback Schedule Schedules automatic blowbacks Input Outputs I O Sets relay settings and configurations Communication Settings Sets serial and TCP IP settings Display Sets display settings Set Date Time Sets system date and time Arke S0 System Instruction Manual 3 25 User Interface Instrument Controls Menu Gas Mode 3 26 Arke SO System Instruction Manual The Gas Mode screen Figure 3 20 allows the user to manually select the gas mode they want the system to be in The current active gas mode is in yellow The Gas Mode is also reflected in the Status Bar located at the bottom on the Instrument Display Upon startup the system default Gas Mode is Filter Blowback The system will not go into any other gas mode until all temperatures are within the Alarm limits Also during normal operation if any temperature r
142. imizing the Correct 503 Peak 6 30 Arke SO System Instruction Manual x11 c aae Drga 10 175 240 99 ao calibration S0 1674 ppm SCIENTIFIC Data Analysis gt Real Time Spectrum gt Transmission Spectrum Instrument Controls System Status and Alarms Data Analysis 40 28 16 4 8 20 32 44 56 68 80 92 104 SO Voigt Peak Channel 1 Service Sample Alarms 2 MM Soe Back 7 Locate SO a Change the gas mode to System Span and allow 30 minutes b Add 3 C to the laser temperature c Go to the Transmission Spectrum Does it look like this 20 86 10 175 240 99 S0 102 ppm Instrument Controls System Status and Alarms Data Analysis l E EN Ee ERE IEEE HANE ERES ERN ee ee HESSEN ERE DB 40 28 16 4 8 20 32 44 56 68 80 92 104 S 0 Voigt Peak Channel 1 Service Mau 29 2012 Sustem Span Alarms 2 16 35 00 d Ifit does not increase the laser temperature by 0 4 C until you see 2 large SO peaks as shown above e Position the left peak at channel 0 Thermo Fisher Scientific Troubleshooting Finding and Optimizing the Correct S03 Peak i If the peak is to the left of channel 0 then increase the temperature of the laser slightly try going in small 0 05 C increments ii If the peak is to the right of channel 0 then decrease the temperature of the laser slightly f When this has been accomplished the correct SO peak has
143. ing Filter BB Valve out to Filter Fitting 50 Valve out to S02 top generator 505 Valve out to bottom fitting on generator Diff Press Hi Side to tube Hi Fitting Diff Press Lo Side to tube Lo Fitting Cal Gas Dil port to Cal Fitting Pre heat Vacuum Port to Vacuum Eductor Port to Eductor Dilution Port to Dilution In Cal Gas Dil Post heat to generator Tubing Nut and Length Ferrule set 9 1 2 2 1 4 S S 12 2 1 4 S S 18 2 1 4 S S ag 2 1 4 S S 43 2 1 4 S S 46 2 1 4 S S 43 2 1 4 S S 13 2 1 4 S S 12 2 1 4 S S 297 2 1 4 S S 34 2 1 4 S S 50 2 1 4 S S 56 2 1 4 S S 7 PTFE 2 1 4 S S 8 Insulation Thermo Fisher Scientific Preventive Maintenance and Servicing Replacement Tubing List Diff Press Lo Side M 3 y J O LU W TA AN O NS ke Diff Press Stinger Filter S02 503 Hi Side BB BB Valve Valve Out Out Out Out Figure 5 7 Fitting Locations Undersides of Valves Stinger Blowback Filter Blowback a Ia zi aT T Bottom Tee Away from Tank Bottom Tee Nearest Tank Figure 5 8 Fitting Locations Blow Back Val
144. k Arke S0 System Instruction Manual 3 51 User Interface Data Analysis Menu Data Logging Retrieve Data 3 52 Arke SO System Instruction Manual The Retrieve Data screen Figure 3 40 displays data logging values based on time conditions or number of records The most recent records are located at the bottom Single column scrolling can be done Left Right Single or page scrolling can be done Up Down S0 0 00 ppm Data Analysis View Logged Data gt Retrieve Data x11 2 5 xi SCIENTIFIC Time Stamp Active Alarms Alarms Flag Boe 2 2 2012 05 01 15 22 43 2012 05 01 15 22 44 2012 05 01 15 22 45 Boe Dg 502 502 2142 05 01 16 20281 A 5d 2012 05 01 15 22 52 502 2012 06 01 15 22 53 502 2012 06 01 16 22 54 502 1 2012 05 01 15 22 55 BO jj j 1 2012 05 01 15 22 46 502 1 1 j Mau 1 2012 Sample Alarms 1 16 00 55 Figure 3 40 Retrieve Data Screen Thermo Fisher Scientific User Interface Data Analysis Menu Streaming Data The Streaming Data Settings screen Figure 3 41 allows the user to stream Settings data to a computer S0 1 95 ppm Data Analysis gt Streaming Data Settings June 3 2011 eile 10 07 17 Figure 3 41 Streaming Data Settings Screen The Streaming Data screen contains the following information e Select Streaming Variables User selects which variables to stream Table 3 4 for streaming variable list The firs
145. le and the four nylon nuts for the generator assembly 9 2190 9 2190 9 9 89 98 2 9 6 98 8 PE 2 5 4 5 6 819 mo 1201 Sy 4915916 27128 PE NS f 2 ui ts P Ps a M a So po y C E i gt CN E 3 C C is N O Taa ze C f C CN 3 9e0 0 00 0 0 00 0 00 0 0J0 0 o0loloaleleaoloeoosgoeeJeg 4181920212223242226 Figure 2 7 Probe Terminal Block Arke SO System Instruction Manual 2 7 Installation Probe Installation Table 2 2 Probe Terminal Block Heater and Thermocouple Wire Connections From Description Probe Terminal Block Position H1 Factory Probe Heater 1 1 H1 Factory Probe Heater 1 2 H2 Factory Probe Heater 2 1 H2 Factory Probe Heater 2 2 H3 Factory Orifice Heater 3 H3 Factory Orifice Heater 4 H4 Factory Generator Heater D H4 Factory Generator Heater 6 H5 Installation Termination otinger Heater T H5 Installation Termination otinger Heater 8 H6 Installation Termination Spike Heater 9 H6 Installation Termination Spike Heater 10 TC1 RED Factory Probe TC 17 TC1 YEL Factory Probe TC 18 TC2 RED Factory
146. ller agrees to assign to Buyer any warranty rights in such Product that Seller may have from the original manufacturer or third party supplier to the extent such assignment is allowed by such original manufacturer or third party supplier In no event shall Seller have any obligation to make repairs replacements or corrections required in whole or in part as the result of i normal wear and tear ii accident disaster or event of force majeure iii misuse fault or negligence of or by Buyer iv use of the Products in a manner for which Arke SO System Instruction Manual A 1 Warranty Warranty they were not designed v causes external to the Products such as but not limited to power failure or electrical power surges vi improper storage and handling of the Products or vii use of the Products in combination with equipment or software not supplied by Seller If Seller determines that Products for which Buyer has requested warranty services are not covered by the warranty hereunder Buyer shall pay or reimburse Seller for all costs of investigating and responding to such request at Seller s then prevailing time and materials rates If Seller provides repair services or replacement parts that are not covered by the warranty provided in this warranty Buyer shall pay Seller therefor at Seller s then prevailing time and materials rates ANY INSTALLATION MAINTENANCE REPAIR SERVICE RELOCATION OR ALTERATION TO OR OF OR OTHER TAMPERI
147. low values etc setpoints alarms and alarm limits e Data Analysis View graph and analyze data e Service Sets and calibrates temperatures pressures and flows Sets sensitive parameters for the Laser and Detector Also allows the user to set the SO generator conditioning schedule e Status Bar Displays the system gas mode active alarm status date and time e System Gas Mode Displays current gas mode e Alarms Displays the number of active alarms e Date Time Displays current date and time e Back Button When pressed displays the previous screen Thermo Fisher Scientific Arke SO System Instruction Manual 3 5 User Interface S03 Screen and Keypads S0 Screen and The SO Screen Figure 3 4 shows SO concentration in big bold characters T he SOs screen button located at top center brings you to the Keypads SO Screen gt lo x June 2 2011 Sample Alarms 11 22 33 Figure 3 4 S0 Screen 3 6 Arke S0 System Instruction Manual Thermo Fisher Scientific Numeric Keypad Thermo Fisher Scientific Screen User Interface 503 Screen and Keypads User enters a value into the box using the number keypad Figure 3 5 When the user needs to change a value such as for flow rates temperatures or pressures the keypad screen will automatically display Initially the box above the keypad will display the current value Enter a new value using the keypad and then select the Enter button to set
148. lyzer PRO9805 Dilution Extractive Probe and Air Handling System There are also three support lines that connect these measurement modules as shown in Figure 1 1 All the monitoring components are designed to be located outside of a shelter For details of the instrument s theory of operation and product specifications see the following topics e SO3 Analyzer Theory of Operation on page 1 3 e PRO9805 Dilution Extractive Probe on page 1 4 e Specifications on page 1 8 Thermo Fisher Scientific is pleased to supply this Arke SO System We are committed to the manufacture of instruments exhibiting high standards of quality performance and workmanship Service personnel are available for assistance with any questions or problems that may arise in the use of this system For more information on servicing see the Preventive Maintenance and Servicing chapter starting on page 5 1 Arke SO System Instruction Manual 1 1 Introduction 503 Analyzer Theory of Operation ELECTRI CAL BUNDLE PNEUMATI CS BUNDLE SO3 EXTRACTI ON PROBE HEATED SAMPLE LIN AIR HANDLING SYSTEM ZERO AIR DUMP CLEAN DRY AIR SO3 ANALYZER Figure 1 1 Arke S0 System Configuration 1 2 Arke 505 System Instruction Manual Thermo Fisher Scientific Introduction 503 Analyzer Theory of Operation S0 Analyzer The Arke SO System is designed to measure SO from a combustion Theory of SEn industrial process
149. m A SEDO eral amber tena IF Akiras 1D La at Deere acl ci nca ead Deor adn xs abies m Prae wd D imid a ML TL md hai mdh data aen Figure B 17 ePort Main Screen 3 On the left side of the screen click on the instrument you wish to download information from 4 Select Download Data in the Commands window of the ePort Main screen The Download Data screen will display Figure B 18 B 14 Arke SO3 System Instruction Manual Thermo Fisher Scientific Downloading Data to a Flash Thermo Fisher Scientific Drive ePort PC Software Downloading Data to a Flash Drive ae To download data from SO3 beta C click Begin Download Begin Download pen Folder Figure B 18 Download Data Screen 5 Select the Begin Download button The ePort software will download data based on the settings created in the Download Setup wizard Refer to the previous section for information on setting up downloads The message window will display a Downloading Data message while the software is downloading data from the instrument When the download is complete it will display a Download Complete message Select the Done button to exit the Download Data screen The SO instrument also supports data downloads using the USB connection on the front of the instrument and a USB flash drive Note Depending on the size of the storage buffer downloading all stored data could take up to 30 minutes or more
150. may be entered and saved 3 20 Arke SO System Instruction Manual Thermo Fisher Scientific User Interface Calibration Menu System Coefficient The System Coefficient screen Figure 3 15 is a multiplier for the SO concentration based on the Probe dilution assembly and other system and software factors This setting should not need to be changed often Clicking on this will bring up the keypad For instance if the user has 100 ppm span gas going through the system but the concentration reading is reading 200 ppm then the user can reduce the system coefficient by half to get a more reasonable concentration S0 6 87 ppm Calibration System Zero Alarms 3 October 13 2011 03 17 53 Figure 3 15 System Coefficient Screen Note Before changing the system coefficient span gas should be run for at least 30 minutes Also it is recommended that the Span Coefficient be set to 1 000 at the Calibration Coefficients screen before changing the System Coefficient When the System Coefficient is changed a full calibration should then be performed A Thermo Fisher Scientific Arke 03 System Instruction Manual 3 21 User Interface Calibration Menu View Calibration The View Calibration Spectrum screen Figure 3 16 displays the date of Spectrum the most recently completed automatic calibration and allows the user to access the spectrum used for the automatic span calibration SO 7 73 ppm MEM Calibration View Calibration Spe
151. n Enter the concentration of the SO cylinder that you are using Forethought should be used when determining what cylinder concentration to buy Span concentration setpoint and calibration flow rates should be considered It is suggested that a 1000 ppm SO in Air cylinder be used Arke SO System Instruction Manual 4 1 Calibration Calibration Calibration Automatic Calibration Schedule 4 2 Arke S03 System Instruction Manual 3 SO Flow Setpoint This button sets the SO gas flow rate to flow through the SO Generator assembly An SO flow of 0 2 to 0 4 L min is suggested However the operating range of this Mass Flow Controller is 0 02 to 0 48 L min 4 Span Dilution Air Flow Setpoint When the three variables above are set the instrument will automatically set the Span Dilution Air Flow Setpoint The value is located to the right of the SO Flow Setpoint button and must be within the operating range of the Span Dilution Air Flow Mass Flow Controller which is 0 2 to 9 8 L min If the calculated value falls out of this range an error message will appear and the user will need to adjust one or more of the three variables Calibrations will not take place if this screen has an error message Note The combined flow rates should be at least 3 L min A Note At the moment of span calibration the span value will be used to calibrate the system This value is found at System Status and Alarms Instrument Span Reading
152. n that order The entire sequence will take 5 7 minutes June 2 2011 14 34 02 Filter Blowback Figure 3 22 Component Power Instrument Screen The Component Power Instrument ON OFF options are as follows e Bench Heater Heaters at the optical bench assembly e Laser and Detector Power Turns the laser and detector power ON OFF This cannot be turned ON if either the laser housing cooler or laser cooler is OFF or if either is in an alarm state e Laser Cooler Peltier cooler located at the laser The laser cooler cannot be turned ON if the laser housing cooler is OFF or the temperature is in an alarm state When the laser cooler is turned ON it will automatically step down the laser cooler temperature incrementally until it reaches the setpoint temperature This will take 5 7 minutes If the laser cooler is turned OFF the laser and detector power will automatically be turned OFF also Thermo Fisher Scientific Arke S0 System Instruction Manual 3 29 User Interface Instrument Controls Menu e Laser Housing Cooler Peltier cooler located at the laser housing If the laser housing cooler is turned OFF both the laser cooler and laser and detector power will automatically be turned OFF If the laser housing temperature is ON and gets to 29 C it will automatically shutoff and so will the laser cooler and the laser and detector power e Detector Cooler Peltier cooler located at the detector Note When cycling the power fo
153. nalogOutRange AnalogOutRange AnalogOutRange AnalogOutMinValue AnalogOutMinValue AnalogOutMinValue AnalogOutMinValue AnalogOutMinValue Thermo Fisher Scientific Serial Communication AK Protocol PRC Code Description 422 AnalogOutMinValue 423 AnalogOutMaxValue 424 AnalogOutMaxValue 425 AnalogOutMaxValue 426 AnalogOutMaxValue 42 AnalogOutMaxValue 428 AnalogOutMaxValue 429 AnalogOutVoltageSlopeOto100mV 430 AnalogOutVoltageSlope0to1 00mV 431 AnalogOutVoltageSlope0to1 00mV 432 AnalogOutVoltageSlope0to1 00mV 433 AnalogOutVoltageSlope0to1 00mV 434 AnalogOutVoltageSlope0to1 00mV 435 AnalogOutVoltageSlopeOto1V 436 AnalogOutVoltageSlopeOto1V 437 AnalogOutVoltageSlopeOto1V 438 AnalogOutVoltageSlopeOto1V 439 AnalogOutVoltageSlopeOto1V 440 AnalogOutVoltageSlopeOto1V 441 AnalogOutVoltageSlope0to10V 442 AnalogOutVoltageSlope0to10V 443 AnalogOutVoltageSlope0to10V 444 AnalogOutVoltageSlope0to10V 445 AnalogOutVoltageSlope0to10V 446 AnalogOutVoltageSlope0to10V 447 AnalogOutVoltageYInterceptOto100mV 448 AnalogOutVoltageYInterceptOto100mV 449 AnalogOutVoltageYInterceptOto100mV 450 AnalogOutVoltageYInterceptOto100mV 45 AnalogOutVoltageYInterceptOto100mV 452 AnalogOutVoltageYInterceptOto100mV 453 AnalogOutVoltageYInterceptOto1V 454 AnalogOutVoltageYInterceptOto1V 455 AnalogOutVoltageYInterceptOto1V Thermo Fisher Scientific Arke SO System Instruction Manual C 15 Serial Communication AK Protocol PRC Code Description 456 AnalogOutVoltageY
154. nd Cable Assembly Connections Figure 6 8 Detector Board Bottom Motherboard e RS 485 communication connectors J8 amp J9 are located on the right side directly below the white 3 pin connector These two jacks are interchangeable and are daisy chained with the other boards e SATA Connections There are 4 SATA Connections that may be used to connect to the hard drive The default is J30 which is the top most left SATA connector e Ifthe touch screen display does not have a backlight ensure connection at J35 4 pin connector at the upper left corner of the board e There are two power connections The main ATX power connection connects to the 24 pin connector at the upper right J25 The second is the four pin connector located at J33 e The Network jack on the front panel of the instrument should connect to the network jack closest to the blue VGA connector J3 e The USB port J16 is used to connect the touch screen to the motherboard It is the top 10 pin connector located on the right side Thermo Fisher Scientific Arke S0 System Instruction Manual 6 19 Troubleshooting Instrument Board and Cable Assembly Connections e The USB port J15 is used to connect the front panel USB drive to the motherboard When a thumb drive is inserted and the system doesn t recognize it ensure that it is connected properly Some thumbdrives may not be compatible e If the display is lit and there is no communication ensure that t
155. ng Spectrum Thermo Fisher Scientific Arke SO System Instruction Manual 1 3 Introduction PR09805 Dilution Extractive Probe PR09805 Dilution The PRO9805 Dilution Extractive Probe is configured as one component of Thermo Scientific s Arke SO System The probe with its built in Extra ctive Probe diluting assembly has been designed specifically to monitor SO at various locations within a coal fired power plant The PRO9800 Probe is constructed of a 316 stainless steel enclosure To prevent sample condensation all key elements Inertial Filter Diluting Probe and Sample Eductor have been mounted between heated aluminum blocks that can be maintained at temperatures as high as 300 C The enclosure also houses an accumulator tank for back purging of the inertial filter tube blow back External to the enclosure is a section with the electrical connections solenoids for filter and stinger blow back cal gas zero gas and a differential pressure transducer A special 4 inch adapted mounting flange has been supplied for installation onto the port of the stack or duct Clean dry pressurized 80 psig air feeds two electronic pressure regulators within the 9800 SO Analyzer which adjust and maintain output pressure to the PRO9805 Probe eductor and dilution module Figure 1 3 Also contained within the 9800 SO Analyzer are three electronic pressure transducers associated with the individual regulators as well as an electronic vacuum tr
156. ng buttons Data logging Settings User selects the parameters for collecting data View Logged Data User views historical data Streaming Data Settings User can stream data to a computer real time Graphing Data User can graph two sets of data from the information stored in view logged data Real Time Spectrum Allows the user to view the current raw spectrum and the transmission spectrum Statistical Analysis The user can view the minimum maximum and standard deviation of two items over a specified period of time Thermo Fisher Scientific Thermo Fisher Scientific User Interface Data Analysis Menu Data Logging The Data Logging Settings screen Figure 3 38 allows the user to select Settings data to be stored and how it is stored June 2 2011 15 48 40 Filter Blowback Figure 3 38 Data Logging Screen The Data Logging screen contains the following information Select Data Logging Variables User selects system variables to log The following variables are always selected and cannot be disabled Date Time Number of Active Alarms Alarms Flag System Gas Mode and SO Concentration See Table 3 4 for data logging variable list As a default all variables are selected Period User selects how often data is collected by setting the duration between logged data Data Treatment Toggles between Average Current Min and Max When set to average the average value during the period will be recorded W
157. nge during System Zero The new background calculated at the end of system zero is outside the acceptable range Current Span Coefficient Denominator 0 The new span coefficient is equal to zero which is not acceptable Span Coefficient out of range The new span coefficient falls outside the range of 0 500 to 2 000 Zero Bkg out of range during System Span When a new span coefficient is calculated a new zero background is also calculated If this new zero background falls outside the acceptable range this error will appear Span too weak during Syste Span The SO peak between channels 10 to 10 as seen on the Transmission Spectrum screen was too weak for it to be considered an SO feature Thermo Fisher Scientific Auto Calibration Check Schedule Thermo Fisher Scientific User Interface Calibration Menu The Automatic Calibration Check Schedule screen Figure 3 12 automatically runs a background and span at designated times This schedule does not change background or coefficient variables See Chapter 4 Calibration for more information on the Automatic Calibration Check Schedule SO 1 95 ppm fern Calibration 50 Auto Calibration Check Schedule Mext Time Period Duration 30 Total Minutes S0 Averaging Time For Auto Cal Check d April 18 2012 Filter Blowback Alarms 5 11 41 55 Figure 3 12 Auto Calibration Check Schedule The Automatic Calibration Check Schedule screen contains the foll
158. nications error with the board over the serial link 0x00000002 The 3 3V supply is high 0x00000004 The 3 3V supply is low 0x00000008 The 5V supply is high 0x00000010 The 5V supply is low Qx00000020 The 12V supply is high 0x00000040 The 12V supply is low 0x00000080 A pulse clock error has been detected Arke 03 System Instruction Manual D 3 Error Code Troubleshooting AK Protocol D 4 Arke SO3 System Instruction Manual Table D 6 Detector Board Status Code in Description hexadecimal 0x00000000 No error 0x00000001 There is a communications error with the board over the serial link 0x00000002 The 3 3V supply is high 0x00000004 The 3 3V supply is low 0x00000008 The 5V supply is high 0x00000010 The 5V supply is low Qx00000020 The 2 5V supply is high 0x00000040 The 2 5V supply is low 0x00000080 The 8V supply is high 0x00000100 The 8V supply is low Qx00000200 The 8V supply is high 0x00000400 The 8V supply is low Table D 7 System Control Board Status Code in Description hexadecimal 0x00000000 No error 0x00000001 There is a communications error with the board over the serial link 0x00000002 The 3 3V supply is high 0x00000004 The 3 3V supply is low Qx00000008 The 5V supply is high 0x00000010 The 5V supply is low Qx00000020 The 15V supply is high 0x00000040 The 15V supply is low 0x00000080 The 15V supply is high 0x00000100 The 15V supply is low Qx00000200 The 12V s
159. nnel only A If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired A Adjusting the detector controls and laser controls by a non qualified individual can result in damages to the detector and laser A Do not exceed 0 3 V A Thermo Fisher Scientific Alert 1 Equipment Damage About This Manual WEEE Symbol Description Do not exceed 2 5 V A Do not attempt to lift the instrument by the cover air conditioner or other external fittings A There is a bulkhead fitting used as an atmospheric dump on the bottom of the enclosure Take care not to damage A If the bench heater is ON ensure that the instrument door is either open or that the Air Conditioning unit is ON If the bench heater is ON with the door closed and the Air Conditioning OFF thermal damage to the boards may occur A Adjusting the laser control by a non qualified individual can result in damages to the laser and laser housing A WEEE Symbol The following symbol and description identify the WEEE marking used on the instrument and in the associated documentation Symbol A5 Marking of electrical and electronic equipment which applies to electrical and electronic equipment falling under the Directive 2002 96 EC WEEE and the equipment that has been put on the market after 13 August 2005 A Where to Get Help Service is available from exclusive distributors worldwide Con
160. ny cool surface below 220 C The SO gas is originated from a standard SO in air cylinder If operated and maintained correctly the generating efficiency of SO into SO is 59796 An SO source with a nitrogen balance will not produce SO3 Thermo Fisher Scientific Introduction PROS805 Dilution Extractive Probe A Am 905 Out Figure 1 4 U lube Flow Diagram Calibration Method The Arke SO System is calibrated by introducing the span gas at the stinger In this way both the span gas and sample gas will follow the same path through the system This will produce a more reliable calibration If there are losses in the sample gas there will be similar losses during calibration S0 Cylinder The SO cylinder should have a concentration between 1000 and 1200 ppm depending on the desired SO range and be in a balance of air The regulated output pressure should be between 30 and 40 psig If the balance gas is No it will not work Note Balance gas must be air A Thermo Fisher Scientific Arke S03 System Instruction Manual 1 7 Specifications Table 1 1 lists the specifications for the Arke SO System Table 1 1 Arke S0 System Specifications Range Zero noise Lower detectable limit Zero drift 24 hour opan drift Linearity Water Interference 50 Interference sample flow rate Operating temperature Power requirements Analyzer physical dimensions Analog outputs Analog inputs Digital outputs
161. o the raw flow value coming from the board Restore Defaults When pressed the coefficient will be set to 1 000 The displayed flow will equal the raw flow coming from the board Arke S0 System Instruction Manual 3 75 User Interface Service Menu Laser Controls The Laser Control screen Figure 3 60 is used to adjust laser setting which affects the SO spectrums and concentration The screen responds with Are you Sure and requires a Yes or No action Equipment Damage Adjusting the laser control by a non qualified individual can result in damages to the laser and laser housing A Note Fach of these buttons function the same way Each button will lead to a keypad where the user can enter new values A Note The laser power controlled in the component power screen cannot be turned on unless both the laser cooler temperature and the laser housing cooler temperature have reached within 1 C of their setpoints A Note Once the laser is started and running if the laser cooler temperature or the laser housing cooler temperature is turned off or creates an alarm then the laser power is turned OFF A June 3 2011 15 24 35 Sample Alarms Figure 3 60 Laser Controls Screen 3 76 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific User Interface service Menu The Laser Controls screen allows the user to adjust the following laser parameters e Laser Voltage Setpoint Laser
162. oftware for Eport connectivity e Ifusing DHCP the instrument must be connected to the network upon startup Pump Bench pressure is greater than 28 inches mercury e Nominally the pump should be rebuilt or replaced annually To determine if the pump needs to be replaced insert a vacuum gauge at the Pump bulkhead on the right side of the Instrument Chassis Ensure that the pump is pulling greater than 28 inches mercury vacuum Instrument Board The following section describes the functionality of each of the computer and Cable Assembly boards See Appendix D Error Code Troubleshooting for Board Status i and Error Codes Connections System Control Board Top of board e All thermocouple connections for both the instrument and the probe get plugged in at the top of this board The corresponding labels are printed to the left of the connector Ensure all connections are inserted properly It is possible to verify correct thermocouple connection by unplugging each thermocouple one at a time and use the System status and Alarms screen to see if the correspondig temperature reads 0 0 e All transducers pressure regulator and mass flow controllers MFCs plug into this board All jacks are labeled e lfitis determined that this board is faulty replace with Part Number 109930 00 6 10 Arke SO3 System Instruction Manual Thermo Fisher Scientific Troubleshooting Instrument Board and Cable Assembly Connections pt 14
163. ollowing buttons Instrument Status Displays status of instrument devices Probe Status Displays status of probe devices Board Status Displays status of each computer board Voltages Displays instrument voltages Thermo Fisher Scientific User Interface oystem Status and Alarms Menu Instrument Status The Instrument Status screen Figure 3 32 provides information with respect to instrument components devices setpoints and readings Real time values and alarm limits are shown Alarm limits can be changed Values that trigger alarms will be shown in red Temperature and Pressure Setpoints can be viewed and changed S0 11 2 ppm system Status and Alarms Instrument Description Setpoint Yalue Low oO Conc 11 2 0 000 Bench Temp 190 Bench Pressure 10 0 Chassis Temp October 13 2011 System Zero Alarms 3 09 23 29 Figure 3 32 Instrument Status Screen The Instrument Status screen contains the following buttons e Up and Down Use the T and 4 buttons to move the page up and down e Change Setpoints and Alarm Limits To change the alarm limits or setpoint values touch the row to highlight it Next press the Change Setpoints and Alarm Limits button This allows the user to change a temperature or pressure setpoint and or change that specific alarm limit See Change Setpoints and Alarm Limits on page 3 45 Thermo Fisher Scientific Arke SQ3 System Instruction Manual 3 41 User Interface
164. om of the air conditioner 4 Lift Air Conditioner up and away from the Instrument Chassis mounting bar The AC unit hangs from a mounting bar that is bolted to the Instrument Chassis 5 To reinstall follow the above instructions in reverse 5 14 Arke SO System Instruction Manual Thermo Fisher Scientific Preventive Maintenance and Servicing PRO9805 Probe Replacement Parts List PR09805 Probe Replacement Parts List Table 5 3 lists the replacement parts for the 9805 Dilution Extractive Probe Note The recommended replacement interval is site specific therefore these are only guidelines A Table 5 3 PR09805 Probe Replacement Parts Thermo Fisher Scientific Part Number Description Replacement Interval 102624 00 Dilution Eductor As needed 101074 00 Filter 15 Micron Annual 110214 00 Filter Inertial coated As needed or cleaned 103571 00 Fitting Adapter Assembly As needed 111368 00 Orifice Critical 011 ID As needed 110172 00 Ash Deflector As needed or cleaned 105479 00 Strain Relief Assembly As needed 102623 00 oulfinert Cross As needed 110833 00 Valve Assembly no offset As needed 110833 01 Valve Assembly 45 offset As needed 110833 02 Valve Assembly 90 offset As needed 103434 00 Venturi Differential Pressure As needed or cleaned Transducer Assembly 103570 00 Venturi Tube Assembly As needed 100634 00 Graphite Ferrule 1 2 inch When replacing stinger tube or as needed 100635 00 Graphite Ferrul
165. on Pressure Calibration screen contains the following information e Current Dilution Pressure Displays current dilution pressure e Set to correct value of Using a calibrated pressure gauge the user measures the pressure at the spot where the dilution pressure gauge is connected The user then enters the correct pressure value using the keypad e Calibrate Dilution Pressure Based on the current pressure and correct value entered by the user this button adjusts the pressure coefficient thus calibrating the current dilution pressure reading e Dilution Pressure Coefficient This dilution pressure coefficient value is the result of pressing the Calibrate Dilution Pressure button This Thermo Fisher Scientific User Interface Service Menu coefficient will be applied to the raw pressure value coming from the board e Restore Defaults When pressed the coefficient will be set to 1 000 The displayed pressure will equal the raw pressure coming from the board Thermo Fisher Scientific Arke S03 System Instruction Manual 3 73 User Interface service Menu Flow Calibration The Flow Calibration screen Figure 3 58 is used to calibrate the mass flow controllers MFC s The MFC s control the SO flow and span dilution air flow during calibration S0 1 95 ppm Service gt Flow Calibration E June 3 2011 Alarms 0 14 45 43 Figure 3 58 Flow Calibration Screen The Flow Calibration screen allows the user
166. on screens SO 1 95 ppm service Temperature Calibration Instrument Bench Temp Current Bench Temperature Set to correct value of Bench Temperature Coefficient June 3 2011 Alarms 9 14 37 09 Figure 3 55 Bench Temp Calibrations Screen The Bench Temp Calibrations screen contains the following information e Current Bench Temperature Displays current bench temperature e Set to correct value of Using a calibrated thermocouple reader or similar device the user measures the bench temperature coming from the thermocouple and enters the correct temperature value using the keypad Thermo Fisher Scientific Arke S0 System Instruction Manual 3 69 User Interface Service Menu e Calibrate Bench Temperature Based on the current temperature and correct value entered by the user this button adjusts the temperature coefficient thus calibrating the current bench temperature reading e Bench Temperature Coefficient This temperature coefficient value is the result of pressing the Calibrate Bench Temperature button This coefficient will be applied to the raw temperature value coming from the board e Restore Defaults When pressed the coefficient will be set to 1 000 The displayed temperature will equal the raw temperature coming from the board 3 70 Arke S0 System Instruction Manual Thermo Fisher Scientific User Interface service Menu Pressure Calibration The Pressure Calibration screen Figure
167. onc Reading opan Flow opan Dilution Air Flow Bench emp Bench Pressure Laser Voltage Laser Temp Laser Housing Temp Detector Temp Detector Peak Signal Chassis Temp Probe Probe Temp Probe Ambient Temp stinger Temp 505 Generator Temp 505 Generator Stitch Temp Orifice Stitch Temp Umbilical Temp Umbilical Stitch Temp Eductor Pressure Dilution Pressure Venturi Pressure Dilution Vacuum System Status Motherboard Status oystem Control Board Status Laser Board Status Laser Temp Board Status Laser Housing Board Status Detector Board Status CPU Board Status User Interface Data Analysis Menu Arke SO System Instruction Manual 3 55 User Interface Data Analysis Menu Graphing Data 3 56 Arke SO System Instruction Manual The Graphing Data screen Figure 3 43 allows the user to choose one or two variables to graph The data is taken from the data logging records Only the variables that are currently selected for data logging will appear Use the T and 4 buttons to select the variable Next press the Commit amp View Graph button Yellow indicates that the variable is selected Data Analysis Graphing Data Primary Y axis Secondary Y axis p June 5 2011 Sample Alarms 10 55 46 Figure 3 43 Graphing Data Screen The Graphing Data screen contains the following information e Primary Y axis Variable data will be associated with the left y axis e Secondary Y axis Variable data will be assoc
168. onnection using the ePort software Use the following procedure to set up the software to manually download data Downloads Ensure that the PC and the instrument are connected to the same network using the Ethernet connection on the front of the instrument Refer to the previous section for information on connecting the instrument to a network 2 Use the ePort PC software to connect to the instrument and display the ePort Main screen Figure B 14 Refer to the previous two sections for information on connecting to the instrument or instruments eO pueda Le tee wp inier SO3 bets A 9800 ENT oieverdiudl d lider Linc ad inu Ls bki Lia Praag a Fins Tm Pt D ge Open E Pomi ir idm wn aet beat Comrie iste des ora ed Doreen adis Has Figure B 14 ePort Main Screen Thermo Fisher Scientific Arke S03 System Instruction Manual B 11 ePort PC Software setting Up for Automatic Data Downloads Setting Up for Automatic Data Downloads B 12 Arke S0 System Instruction Manual 3 Select Download Setup in the Commands window of the ePort Main screen The Download Setup Wizard will display Figure B 15 Select the Next button BP Download Setup Wizard aa Welcome to the Download Setup Wizard This wizard helps vau setup downloads From the instrument in easy steps Figure B 15 Download Setup Wizard 4 The Select Data screen will display Select the data to download either
169. or Assembly Dilution Pressure Regulator Valve and Sensor Assembly 7 4 Arke S03 System Instruction Manual Figure 7 2 Pneumatic Assembly The Pnematic Assembly includes devices to regulate and control air and span gas going to the probe The 2 mass flow controllers regulate the SO span gas and Span Dilution Air flows during calibration Maintains precise air pressure feed to the Span Dilution Air MFC Regulates the eductor flow which pulls sample gas through the fastloop of the probe Regulates the system dilution flow to the dilution module Thermo Fisher Scientific AC Mains Circuit Breakers Thermal Runaway Switches and Relay Line Filter Thermo Fisher Scientific System Component Description Analyzer The AC Mains includes switches to turn on off instrument and probe devices and boards The 3 circuit breakers are electrical switches used to turn on off different parts of the system The left circuit breaker controls the heaters used by the Instrument and Probe The center circuit breaker provides power to the Power Supply The right circuit breaker provides power to the Air Conditioner In cases where there is a runaway in temperature inside the Chassis there are 2 thermal runaway snap switches which will power down the Instrument in order to avert thermal damage If activated the user can reset them by pressing the button They are located on the AC Mains assembly The snap switch labeled 1
170. or all tubing going to and from the Instrument and Probe Heater cable connections that go from the Instrument Chassis to the Probe Valve cable connections that go from the Instrument Chassis to the Probe Thermo Fisher Scientific Thermo Fisher Scientific Probe System Component Description Probe Figure 7 6 PFA Tubing Connections The following describes the analyzer components The probe weighs approximately ninety five pounds and consists of a 2 inch mounting flange 2 side access panels an isolated electrical compartment and the main compartment The electrical compartment houses a filter blow back valve stinger blow back valve Cal zero valve a venturi tube differential pressure transducer and a Phoenix DIN rail block for all electrical connections The main compartment consists of a fast loop assembly an SO P P y generator and a 3 inch strain relief for the umbilical cord The fast loop assembly consists of an inertial filter particulate filter critical orifice main eductor assembly dilution eductor assembly venturi tube assembly and a pressure tap all of which are entombed in a heated aluminum block Arke S0 System Instruction Manual 7 9 System Component Description Probe Fast Loop Assembly Orifice Block Dilution Module Venturi Tube Assembly 1 10 Arke S03 System Instruction Manual fe gt A wee i lt E Figure 7 1 PR09805
171. osition u Insert SO Generator Stitch and Stinger Mantle Fittings tubing in Fast Loop and generator Return Tube 3 4 OD Mantle sample Tube 1 2 OD support Block Mantle bolted in place from inside with 4 5 8 11 x 1 1 2 bolts Fast Loop Tube in forward position Figure 2 5 Stinger Spike and Return Tube Adjustment 6 Bolt mantle in place with four 5 8 inch 11 x 1 1 2 inch bolts and split lock washers 7 Fully insert stinger and SO generator stitch tubing into their unions and tighten fittings The spike tube 1 4 inch is welded to the stinger tube on one side and unites with the generator output on the other side The stinger tube unites with the fast loop sample 1 2 inch in union 2 6 Arke S0 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Installation Probe Installation Insert Tubing into Fittings sail a ad amp amp Figure 2 6 Sample Tubing Connections 8 Insert the return tube into the 3 4 inch union on return loop 9 Compress fittings at mantle end Refer to probe terminal block Figure 2 7 and Table 2 2 and terminate stinger heater SO generator stitch heater and T C leads 10 Tighten the three nylon nuts to secure the fast loop tab
172. ove 0 9995 In this case the SO signal is weak and the voigt fit red curve will be centered at channel 0 This might occur during zero and sample mode Thermo Fisher Scientific Erase Spectrum Log Thermo Fisher Scientific User Interface Data Analysis Menu The Erase Spectrum Log Figure 3 48 erases all pending spectrum logs User should not have to use this feature unless the spectrum log gets backed S0 9 66 ppm Data Analysis gt Real Time Spectrum October 13 2011 09 28 03 System Zero Alarms 3 Figure 3 48 Erase Spectrum Log Screen Arke S0 System Instruction Manual 3 61 User Interface Data Analysis Menu Statistical Analysis 3 62 Arke S0 System Instruction Manual The Statistical Analysis screen Figure 3 49 provides statistical data for SO concentration and system devices This information is pulled from the information found in data logging Therefore only the variables currently selected in the data logging menu will be available for statistical analysis The minimum maximum and standard deviation values for each variable are displayed EE Data Analysis gt Statistical Analysis Variable 1 Variable June 3 2011 14 14 33 Sample Alarms Figure 3 49 Statistical Analysis Screen The Statistical Analysis screen contains the following information Start Time The beginning of the period under analysis End Time The end of the period under analysis Res
173. owing information e Enable Disable Enables disables the auto calibration check schedule state The screen responds with Are you Sure and requires a Yes or No action e Next Time Sets the date and time for the next scheduled calibration check Once an automatic calibration check has started the Next Time button will be updated based on the Period e Period Sets the length of time between calibration checks e Duration Sets the length of time for zero air and span gas e SO Averaging Time for Auto Cal Check Sets the Averaging time during calibration check During an Automatic Calibration Check this Arke S0 System Instruction Manual 3 17 User Interface Calibration Menu averaging time will override the averaging time set in the Instrument Controls menu 3 18 Arke SO3 System Instruction Manual Thermo Fisher Scientific User Interface Calibration Menu Manual Calibration The Manual Calibration screen Figure 3 13 calibrates the background or span coefficient based on the current SO concentration reading See Chapter 4 Calibration for instructions on how to run a Manual Calibration S0 1 95 ppm Calibration Manual Calibration Current Background 1 200 ppm Current Coefficient 1 050 Current Span Value 10 000 ppm June 2 2011 Sample Alarms 13 35 96 Figure 3 13 Manual Calibration Screen The Manual Calibration screen contains the following information e Set Bkg Manually sets
174. oystem Status and Alarms Menu The Instrument Status screen contains the following information Table 3 1 System Status Instrument shown with default setpoints and alarm limits Description Setpoint Low High Units 505 Conc 0 100 ppm Bench Temp 220 200 250 WB Bench Pres 20 90 torr Chassis Temp 10 50 eG 90 Cal Flow 0 000 0 500 L min span Dil Air Flow 0 000 10 0 L min Span Reading 9 50 10 5 ppm Laser Temp 9 8 6 ae Laser Housing Temp 20 15 25 oC Laser Voltage 6 8 V Detector Temp 50 65 55 oC Detector Peak 5 D Channel Note Information on how to center the SO peak on channel 0 as seen in the Transmission Spectrum screen can be found in the Service Menu gt Laser Controls section of this manual A 3 42 Arke S0 System Instruction Manual Thermo Fisher Scientific User Interface oystem Status and Alarms Menu Probe Status The Probe Status screen Figure 3 33 provides information with respect to the probe devices setpoints and readings Real time values and alarm limits are shown Alarm limits can be changed Values that trigger alarms will be shown in red Temperature and Pressure Setpoints can be viewed and changed p EE system Status and Alarms gt Probe Description Setpoint X Value Istinger Temp 220 October 13 2011 System Zero Alarms 3 09 24 04 Figure 3 33 Probe Status Screen The Probe Status screen contains the following buttons e Up and Down Use the T and 4 buttons to move the p
175. p Complete screen will display Figure B 6 Select the Finish button to complete the ePort and Microsoft NET Framework installation Thermo Fisher Scientific Arke S03 System Instruction Manual B 5 ePort PC Software Connecting to the S03 Instrument H Microsoft HET Framework 2 0 Setup m Setup Complete Microsoft NET Framework 2 0 has been successfully installed IE is highly recommended that yeu download and install the latest service packs and security updates For this product For more information visit Ehe Following Web site Figure B 6 Microsoft NET Framework Setup Complete Screen Connecting tO When the ePort software is installed and the SO instrument and the PC th e S0 are connected to the same network the software can connect to the 3 instrument and download data Instrument Use the following procedure to connect to the instrument Ensure that the PC and the instrument are connected to the same network using the Ethernet connection on the back of the instrument Refer to the previous section for information on connecting the instrument to a network 2 In the System Status screen of the machine from which you want to download data locate and record the IP address Figure B 7 of that unit Note Instead of looking up the address on the TCP IP Settings screen users can also scan for instruments when the instruments are on the same LAN Refer to Finding Instruments on a Network on page
176. peak channel number located below the transmission spectrum reads 0 Note This procedure can be automatically done if the Peak Adjust button is enabled at the screen Calibration Auto Calibration Schedule A Arke SO System Instruction Manual 3 77 User Interface Service Menu Detector Controls 3 78 Arke SO System Instruction Manual The Detector Control screen Figure 3 61 is used to adjust the SO detector Changing these settings will affect the SO spectrum and concentration The screen responds with Are you Sure and requires a Yes or No action WARNING Adjusting the detector controls by a non qualified individual can result in damages to the detector A Note Fach of these buttons function the same way Each button will lead to a keypad where the user can enter new values A S0 1 95 ppm Service gt Detector Controls Maximum TEC Current Positive 0 00 Amps June 3 2011 sample 15 24 18 Figure 3 61 Detector Controls Screen The Detector Controls screen allows the user to adjust the following detector parameters e Detector Interval The amount of time that spectrum data is collected and averaged e Detector Offset Detector voltage baseline offset e Maximum TEC Current Negative Default is 0 5 Amp Thermo Fisher Scientific User Interface service Menu e Maximum TEC Voltage Default is 3 5 V e Maximum TEC Current Positive Maximum TEC current negative divided by 4
177. r any of the devices the user should wait at least 30 seconds before turning power back ON A 3 30 Arke SO3 System Instruction Manual Thermo Fisher Scientific Probe Component Power Thermo Fisher Scientific User Interface Instrument Controls Menu The Probe Component Power screen Figure 3 23 allows the user to turn ON OFF Probe devices System Zero Figure 3 23 Component Power Probe Screen The Component Power Probe ON OFF options are as follows Probe Heater Heaters located in the probe clam shell assembly Stinger Heater The heater at the stinger assembly which is between the stack and probe Umbilical Heater The heated line that runs from the probe to the instrument Umbilical Stitch The heated stitch of tubing going from the umbilical line to the bench This can be lelft OFF The umbilical stitch is not installed at the factory and will not be needed for most installations Orifice Stitch The heater at the sample orifice between the probe and the umbilical line SO Generator Heaters located in the SO generator assembly Generator Stitch The heater between the SO generator and stinger Arke S0 System Instruction Manual 3 31 User Interface Instrument Controls Menu e Sample Dilution Air Turns ON OFF the valve that supplies air to the dilution assembly e Fductor Valve Turns ON OFF the eductor valve 3 32 Arke S0 System Instruction Manual Thermo Fisher Scientific User Interface
178. r these settings i Span Setting 100 ppm ii Cylinder Concentration set to actual SO cylinder concentration iii SO Flow Setpoint 0 30 L min b Put the system in Span mode Wait for 30 minutes c Go to the Transmission Spectrum screen and fine tune the left SO peak so that it is at or near channel 0 d Make the SO reading as close to 100 ppm as you can by increasing or decreasing the System Coefficient e Go to Manual calibration and press on Set Span f The SO Transmission Spectrum should look like this Thermo Fisher Scientific Service Locations Troubleshooting service Locations xmumoaoOsum SQ 102 ppm Data Analysis gt Real Time Spectrum Transmission Spectrum m 10 175 240 99 Calibration SCIENTIFIC Instrument Controls System Status and Alarms Data Analysis 40 28 16 4 44 56 68 80 S 0 Voigt Peak Channel 1 May 23 2012 Alarms 2 16 36 00 20 32 Sustem Span For additional assistance Thermo Fisher Scientific has service available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at Thermo Fisher Scientific www thermoscientific com aqi 1 866 282 0430 Toll Free 1 508 520 0430 International Arke SO System Instruction Manual 6 33 Thermo Fisher Scientific Chapter 7 System Component Description The System Component Description chapter prov
179. rates from 1200 to 115200 e Data Bits Toggles between 7 and 8 e Parity Toggles between None Even and Odd e Stop Bits Toggles between 1 and 2 e Instrument ID Sets instrument ID with the keypad e Comm Protocol User selects AK Protocol MODBUS or Streaming e AK Protocol Settings User configures AK Protocol settings Station code and channel numbers can be changed Note The default settings are shown above A 3 36 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific User Interface Instrument Controls Menu TCP IP Settings The TCP IP Settings screen Figure 3 28 allows the user to communicate with the instrument via a network cable If the IP Setting is set to DHCP ON then the bottom three buttons are greyed out September 7 2011 14 04 48 System Span Alarms 4 Figure 3 28 TCP IP Settings Screen The TCP IP Settings screen contains the following information IP Setting Toggles DHCP ON OFF IP Address IP address of the instrument This is settable when DHCP is OFF Netmask Netmask of instrument This is settable when DHCP is OFF Gateway Gateway of instrument This is settable when DHCP is OFF Host Name Host name of instrument Note The default settings are shown above A Arke S0 System Instruction Manual 3 37 User Interface Instrument Controls Menu Display The Display screen Figure 3 29 sets display settings User can choose background
180. rature 6 8 Arke S0 System Instruction Manual Laser Housing Temperature not reaching Setpoint Temperature If the Laser Housing temperature cannot reach its setpoint temperature ensure that the Air Conditioner is working properly If the instrument is in a warm environment and the Chassis temperature is not being cooled and maintained then the Laser Housing Cooler may not be able to reach its setpoint temperature If the Laser Housing cannot reach its setpoint temperature then the g P p peltier coolers may need to be replaced Laser Voltage reading 0 The laser voltage should generally be set between 8 9 Volts If there is a problem with the board or if the voltage goes to zero reboot the instrument Sine Waves in the Transmission Spectrum affecting SO Concentration If there are pronounced sine waves in the blue curve of the transmission spectrum then marked noise will be prevalent in the concentration readings Increasing the Laser voltage by 2 or 3 percent may get rid of this etalon effect Detector Power not turning on The Laser Detector power can be turned on at the screen Instrument Controls gt Component Power gt Instrument Before the Laser Detector power can be turned on both the Laser housing cooler and Laser cooler must be ON and their temperatures within their respective alarm limits Ensure that all connections especially coaxial cables to the laser detector and detector board are tight Detector Temper
181. revious page Table C 1 Main PRC Codes PRC Code Description 001 SerialNumber 002 FirmwareVersion 003 InstrumentName 004 Instrument ype 005 Placeholder2 006 Placeholder3 007 Placeholder4 008 Placeholderb 009 Placeholder6 010 Placeholder 011 Placeholder8 012 Placeholder9 013 Placeholder10 C 2 Arke S0 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific PRC Code 14 015 016 017 018 019 020 021 022 023 024 025 026 027 028 029 030 031 032 033 034 035 036 037 038 039 040 041 042 043 044 045 046 047 Serial Communication AK Protocol Description Placeholder1 1 Placeholder12 Placeholder13 Command DatabasePointer Placeholder OperatingMode otatusCondition AlarmsActive ProtectionLevel Password RegLoginterval DisplayColor DatabaseStatus DataLogsuspend oystemWalitTime GUlStarted Instrument Time HostName NetworkProtocolstatic otaticlPAddress StaticSubnetMask Gateway AKStationCode AKChannelNumber AKSetTime serialMode oerialCommunicationProtocol oeriallnstrumentlD oerialBaudRate oerialDataBits oerialParity oerialStopBits USBDetected Arke SO System Instruction Manual C 3 Serial Communication AK Protocol C 4 Arke S0 System Instruction Manual PRC Code 048 049 050 051 052 053 054 055 056 057 058 059 060 061 062 063 064 065 066 067 068 069 070 071 072 073 074 075 076 077 078 079 080 081 Description USBMounted US
182. rmo Fisher Scientific User Interface Calibration Menu Calibration The Calibration Menu Figure 3 9 provides several ways to calibrate the Menu system See Chapter 4 Calibration for further instructions on how to run a calibration September 7 2011 13 59 46 Alarms 4 Figure 3 9 Calibration Screen The Calibration Menu contains the following buttons Calibration Setting Sets the variables needed to get the correct SO span concentration Auto Calibration Schedule Automatically runs a background and span at designated times This will calibrate the system by setting a new background and new span coefficient This screen will also allow the user to enable an automatic Peak Adjust whereby the SO peak will be centered at channel 0 by adjusting the laser temperature Auto Calibration Check Schedule Automatically runs a background and span at designated times This schedule does not change background or span coefficient variables and does not calibrate the system Manual Calibration The user manually calibrates the background or span coefficient based on the current SO concentration value Calibration Coefficients Manually sets the background or span coefficient using the keypad Arke S0 System Instruction Manual 3 11 User Interface Calibration Menu 3 12 Arke SO System Instruction Manual System Coefficient This value is a multiplier for the SO concentration based on the probe dilution
183. rror with the board over the serial link 0x00000000 The 3 3V supply is high 0x00000000 The 3 3V supply is low 0x00000000 The 1 5V supply is high 0x00000000 The 1 5V supply is low Qx00000000 The 12V supply is high 0x00000000 The 12V supply is low 0x00000000 The power draw on the 12V supply is too high 0x00000000 The reference thermistor is disconnected 0x00000000 The control thermistor is disconnected 0x00000000 The board has shut off the TEC because the temperature is outside the safety shutdown bounds Thermo Fisher Scientific Error Code Troubleshooting AK Protocol Table D 4 Laser Housing Temperature Control Board Status Code in hexadecimal 0x00000000 0x00000001 0x00000002 0x00000004 0x00000008 0x00000010 0x00000020 0x00000040 0x00000080 0x00000100 0x00000200 0x00000400 Description no error There is a communications error with the board over the serial link The 3 3V supply is high The 3 3V supply is low The 1 5V supply is high The 1 5V supply is low The 12V supply is high The 12V supply is low The power draw on the 12V supply is too high The reference thermistor is disconnected The control thermistor is disconnected The board has shut off the TEC because the temperature is outside the safety shutdown bounds Table D 5 Laser Timing Control Board Thermo Fisher Scientific Status Code in Description hexadecimal 0x00000000 No error 0x00000001 There is a commu
184. s amp H800000 oensor Comm Problem amp H10000000 Pinch Valve In the one s place of the status code a status code of 2 is displayed In the one s place of the status code table the 2 status code matches the H 2 Power Switch TPIC status code This is one of the status codes that the unit is displaying in its status code In the ten s place of the status code there are no 0 status codes displayed In the 100 s place of the status code there are no 0 status codes displayed In the 1 000 s place of the status code a status code of B is displayed Because there are no status codes in the status code table that match this number the numbers needs to be broken down further Convert B to a decimal number using Table A 2 which converts B to 11 Next look at the status code table to decipher the status code In the 1 000 s place of the table there are three status codes that when added together will total 11 H 1000 Serial Port Problem H 2000 Line Printer Problem and H 8000 Leak on Loop B These are three more of the status codes that the unit is displaying in its status code Thermo Fisher Scientific Thermo Fisher Scientific Error Code Troubleshooting Deciphering Status Codes In the 10 000 s place of the status code there are no 0 status codes displayed In the 100 000 s place of the status code 800000
185. s 2 and 2 If the SO3 peak is located to the left of channel 0 a negative Peak Channel number located at the bottom right of the screen then the Laser Cooler Temperature should be increased in temperature by 0 01 C steps until the SO peak is between Peak Channel numbers 2 and 2 You will need to wait 30 to 60 seconds each time after changing the Laser Cooler setpoint temperature to see where the SO peak settles before making another Laser Cooler setpoint temperature change If the SO peak is weak just beyond the noise then the SO Generator Conditioning Schedule should be performed more often Perhaps once every two days or even once a day If during an automatic calibration schedule the SO peak isn t greater than the noise the schedule may be cancelled and the system will not be calibrated HVAC Chassis Temperature is not maintaining temperature It is critical that the Air Conditioning unit is working especially in warm environments Open up the Instrument Chassis door and feel the coolness coming out of the air conditioner unit In warm environments the air should be cool to the touch If this is not the case or if the chassis temperature is below 15 C and above 32 C then the HVAC unit may need to be serviced or replaced Arke SO System Instruction Manual 6 9 Troubleshooting Instrument Board and Cable Assembly Connections Network Cannot remotely connect to the Instrument Connectivity e See Appendix B ePort PC S
186. s aaaeetatgenteee sata eee 5 12 Air Conditioner Replacement iu vester ertet eter oe eto Rein be bI Re hien 5 14 PRO9805 Probe Replacement Parts List eeeeseseess 5 15 Jee fo Pm o obit bd cM en rU 5 16 Replacement Tubing E Isbo socios pet a GR NRI DX UE US 5 16 Pacton WinDS secpsssrra raia A 5 19 Dilution Eductor Replacement 12 ae tite eto S RE Uo nue baba e 5 22 Ferial Fiter Rema cent emt rerien desi ER Dem e ud 5 23 Dilution Assembly Critical Orifice Replacement 5 24 L Microw Filer Replacements eor lomo re died ipod aunts 5 25 Valve Cover Gasket Beplacenietitasose so detur tno ise Red 5 25 Valve Assembly Replacenentisssss ip RON a Ne anu eI Ut PIU 5 27 Venturi Pressure Differential Transducer Assembly Replacement 5 28 Stinger Heater Replacement assassanin e oaia ein 5 28 Stinger C lamp Replacement lel stb I net 5 29 Educ tore Dae nae see cia di tp e A beta dU Rt 5 29 Ventari Dube Rep acembelitsadbosqeic unte Irun Reate 5 29 SO Gelerator Replacement rosea rh t US de e NES 5 29 DEFVICe WO CATIONS a e E 5 30 Arke 03 System Instruction Manual xi Contents xii Chapter 6 Chapter 7 Arke S0 System Instruction Manual Troublesnootlng unico crinis inn necne nr n i pner SY a c 6 1 lHistriment Devices and APIS ouai even itane det a dee va vA pU d Dunne 6 2 SO Concentr itO RR M 6 2 E E A E A E E A AET 6 3 Bench Temperat Cerios ia e o E OT 6 5 Doc Pres Ure ar o a 6 6
187. s may be a stronger possibility if the probe was left in the duct or stack while cold See Stinger Heater Replacement on page 5 28 System Coefficient e Ifthe system coefficient continually increases it is possible that less and less SO3 is making it to the optical bench Generator bakeouts may need to be performed more readily e If during a calibration the span coefficient is attempting to set a value outside of the 0 5 2 0 range the System Coefficient may need to be adjusted Bench Temperature No Reading e Check thermocouple and heater wire connections Thermo Fisher Scientific Arke S03 System Instruction Manual 6 5 Troubleshooting Instrument Devices and Alarms Bench Pressure No Reading e Check hotline umbilical tubing connections at both ends the bench connection and the probe connection High Reading e The Pump may need to be replaced if it has been in use for over 1 year Chassis Air Conditioner Temperature If the chassis temperature exceeds the maximum alarm setting the system may not be able to keep the laser housing temperature low enough for proper operation Check to see if the Air Conditioner discharge air is cold to the touch in the case of an excessively high chassis temperature If the discharge air is not cold lt 20c after 25 minutes the air conditioner may need to be serviced or replaced It is imperative that the chassis door stay closed while the air conditioner is on unless you
188. ser A specific wavelength of light is generated whereby a portion of it is absorbed by SO molecules This light or lack of light passes through the optical bench and is detected by the detector Thermo Fisher Scientific System Component Description Analyzer Figure 7 4 Line Filter System Electronics The System Electronics Assembly consists of two boards attached to the Assembly center panel in the Instrument Chassis and provides power to Instrument and Probe components Power Distribution Board The Power Distribution Board located on the right side of the center panel in the Instrument Chassis contains relays and fuses for heater control System Control Board System Control Board located on the left side of the center panel located in the Instrument Chassis supplies power to components such as valves and regulators It also connects the thermocouples inputs for heater control It also contains eight fuses six for the gas mode solenoids and two spares Thermo Fisher Scientific Arke S03 System Instruction Manual 7 7 System Component Description Analyzer Pneumatic and Tubing Connections Teflon Tubing Heater Cables Valve Cables 1 8 Arke S03 System Instruction Manual Figure 7 5 System Electronics Assembly The Pneumatic and Tubing Connections includes all lines going from the Instrument to the Probe On the left side of the outside of the Instrument Chassis there are bulkhead connector fittings f
189. set and the Zero background will be adjusted accordingly If Peak Adjust is enabled the S0 peak will be centered towards 0 at the end of the span duration At the end of the Automatic Calibration Schedule the system will go to Sample mode The Automatic Calibration Check Schedule has the same operating parameters as the Auto Calibration Schedule However there are some ifferences in function The Check Schedule does not set a new Zero background or Span coefficient and does not offer automatic Peak Adjust The function of this schedule is not to calibrate the instrument Rather it will go through all the gas mode events of a calibration without actually changing the Zero background and Span coefficient The Manual Calibration located at the screen Calibration Manual Calibration allows the user to calibrate the system without using the Automatic Calibration Schedule The following are steps that can be taken to calibrate the system using the Manual Calibration feature 1 Go to the screen Instrument Controls gt Averaging Time Record what the averaging time is set to Change the averaging time to a value greater than or equal to 180 seconds 2 Set the instrument Gas mode to Filter blowback for approximately 10 seconds Thermo Fisher Scientific Calibration Calibration 3 Set the instrument Gas mode to Stinger blowback for approximately 10 seconds 4 Setthe instrument Gas mode to Zero mode 5 After approximately 4
190. so Ite do Eat B 9 Setting Up for Manual Data Downloads sess B 11 Thermo Fisher Scientific Arke S05 System Instruction Manual xiii Contents Setting Up for Automatic Data Downloadis B 12 Pertormitiea Data Download si dest UR pecie antico iab i B 14 Downloading Data to a Flash DEVE i esie rto rte tem B 15 Viewing Downloaded Data iier te tr teh on rope B 17 Appendix C Serial Communication eere ee eee ene renean aar tntnanananss C 1 ani HQ C 1 Appendix D Error Code Troubleshooting eres D 1 Converting Decimal Hexadecimal Numbers D 6 Deciphering Status Codes nmn Lo rM ORE ident D 7 EX3Imple enses pau RSS ana a eRe D 7 xiv Arke S0 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Figures Figure 1 1 Arke S0 System Configuration 1 2 Figure 1 2 505 Transmission Spectrum and Incoming Spectrum 1 3 Figure 1 3 PR09805 Dilution Extractive Probe Plumbing 1 5 Figure 1 4 U Tube Flow Diagram 1 7 Figure 2 1 Thermocouple Connections 2 2 Figure 2 2 Component Layout 2 3 Figure 2 3 Umbilical Strain Relief and Atmospheric Dump Parts 2 5 Figure 2 4 Stinger and SO Generator Stitch Heater Installation
191. sure Detector Fan is plugged into either the laser board or laser housing board and is functioning properly Check to see if the two coax cables are tight at the board and at the detector and laser assemblies Ensure that the mini coax that is connected to the CLK connector is connected the connector labeled CLK on the Laser Board Ensure that the mini coax that is connected to the Preamp connector is connected to the Detector Increase Laser Power at the screen Service gt Laser Controls gt Laser Voltage Setpoint Increase the percentage Caution should be exhibited when exceeding a Laser Voltage of 9V At a last resort loosen the hex screw that secures the detector mount and re position the detector in front of the bench exit window e Ifall the LEDs are lit determine if it is due to light saturation or Detector Dark current by blocking by inserting a piece of paper between the laser housing and the bench input window 6 18 Arke SO System Instruction Manual If the LEDS remain lit when the light is blocked ensure tat the Detector Cooler power is ON Component Power If the LEDs go out decrease Laser Power at the screen Service gt Laser Controls Laser Voltage Setpoint Decrease the percentage If decreasing the percentage by 2 or 496 doesn t change the number of LEDs lit then set the percentage back to its original value as this is not the problem Thermo Fisher Scientific Troubleshooting Instrument Board a
192. t 5 variables are always selected and cannot be disabled e Period Sets the time between streamed data e Reset to Default Content Resets default streaming conditions Note When streaming over RS 232 or RS 485 the setting at menu Instrument Controls Communication Settings Serial Setting Comm Protocol needs to be set to Streaming A Thermo Fisher Scientific Arke S05 System Instruction Manual 3 53 User Interface Data Analysis Menu Data Logging and The Select Data Logging Variables screen and the Select Streaming Streaming Variable Variables screen Figure 3 42 allows the user to select which variables to Selection track The Data logging and Streaming variable lists are exclusive from each other but contain the same variable selections Use the T and 4 buttons to select the variable Next press the Commit Changes button Yellow buttons indicate that the variable is selected September 7 2011 System Span Alarms 5 14 06 54 Figure 3 42 Variable Table 3 4 contains the variables that can be selected for Data logging Table 3 4 Variable List for Data Logging and Streaming Instrument Date Time fixed Number of Action Alarms fixed Alarms flag fixed oystem Gas Mode fixed 503 Conc ppm fixed Zero Background opan Coefficient 3 54 Arke S03 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Instrument oystem Coefficient 505 Span Conc Setting 505 Span C
193. t be air The SO generator will not work properly if any other balance gas is used Eductor Air Flow In order for the system to be calibrated properly the flowrate of the calibration gas must exceed the flowrate of the sample gas being pulled into the probe via the eductor If the span is unstable or does not appear consistent from one calibration cycle to the next adjust the eductor pressure either up or down until the span response is highest and stable The default Eductor Pressure is 2 psig and the flowrate of the calibration gas should be at least 3 LPM Plugged Orifice If the system does not respond to SO and there are no spectral features on the Transmission Spectrum Screen at 100 ppm switch to SO Mode under the Service screen and look for any SO spectral features If no peaks are observed then the critical orifice may be plugged See Dilution Assembly Critical Orifice Replacement on page 5 24 Assuming the rest of the system is working properly and there are no leaks put the system in Blowback mode and turn the Dilution Pressure off turn the Pump off switch is located on the pump and turn the Probe Heater off Let he probe cool down remove the clamshell insulation and remove the 5 thumbscrews that clamp the top half of the clam shell to the bottom half Remove the orifice which is 1 5 inch long located between the inertial filter Tee fitting and the Dilution module Replace or sonically clean the orifice with D
194. tact one of the phone numbers below for product support and technical information or visit us on the web at www thermoscientific com agi 1 866 282 0430 Toll Free 1 508 520 0430 International We continue to support our customers with advanced online resources Our Air Quality Instruments Online Library allows our customer s access to product documents and information on a constant basis Available 24 hours a day and seven days a week the online library provides quick access to information regardless of time zone or office hours To register for an account or log in please visit www thermoscientific com agilibrary Thermo Fisher Scientific Arke SO System Instruction Manual vii About This Manual Where to Get Help viii Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Chapter 1 Chapter 2 Chapter 3 Contents Introduction uo n e Cb ecc c Crede a AS 1 1 SO Analyzer Theory ot Operation goiari te teta e Ead R s 1 3 PRO9805 Dilution Extractive Probe eee 1 4 Construction of the Inertial Filter eere 1 6 Operating Principle of the Inertial Filter Tube 1 6 Operating Principle of the SO Generator esse 1 6 Calibration Methodiose asa tan ope eu te EE Nee san 1 7 56015 unde Bseasendss sante cetus E a UP pura E tutup tud 1 7 DDScIBICAEIOIIS diua a ua ag ef E
195. ter is a 240 V 450 W firerod style heater that heats the heater block and generator weldment to approximately 425 C to facilitate the oxidation reaction 1 12 Arke S03 System Instruction Manual Thermo Fisher Scientific Heater Block Thermocouple Insulation Generator Enclosure Enclosure Bracket Thermo Fisher Scientific System Component Description Probe The heater block encloses the SO Generator U tube ensuring even heating Type K thermocouple used to measure the Generator temperature The insulation surrounding the heater block helps maintain a uniform and constant temperature The SO Generator enclosure is an aluminum box that contains the oxidizer components The SO Generator Enclosure is screwed into the Enclosure Bracket The Enclosure Bracket is secured to the probe case Arke SO System Instruction Manual 7 13 Thermo Fisher Scientific Appendix A Warranty Seller warrants that the Products will operate or perform substantially in conformance with Seller s published specifications and be free from defects in material and workmanship when subjected to normal proper and intended usage by properly trained personnel for the period of time set forth in the product documentation published specifications or package inserts If a period of time is not specified in Seller s product documentation published specifications or package inserts the warranty period shall be one 1 year from the date of shipment
196. the following chapters and appendixes to provide direct access to specific operation and service information Chapter 1 Introduction provides an overview of the product describes the system configuration and the operating principle of the system Chapter 2 Installation describes how to install and start up the system This will include how to install the probe and umbilical plumbing hookup Chapter 3 User Interface provides information on how to use the touch screen display Each menu and submenu is explained Chapter 4 Calibration provides an overview on the equipment needed for calibrations and a description on how to calibrate the system Chapter 5 Preventive Maintenance and Servicing describes the periodic maintenance procedures that should be performed on the system instruments and components to ensure proper operation Chapter 6 Troubleshooting provides details and guidance on how to determine and solve common problems Chapter 7 System Component Description provides an overview and describes the function of the system components M Appendix A Warranty is a copy of the warranty statement Appendix B ePort PC Software provides a description on how to install and use the ePort PC software Appendix C Serial Communication provides information on the AK protocol procedure Appendix D Error Code Troubleshooting provides a list of error codes for the instrument Arke SO System Instruction Manu
197. ther connected networks you must know the IP address of the instruments and the gateway address if necessary and connect to the unit manually using the New Instrument function of the software Figure B 9 Refer to the previous section for information on connecting to an instrument off the local network Instruments on a network must have a unique IP address or be connected through a router A Use the following procedure to locate all instruments on the network 1 Open the ePort software program and select Find Samplers in the Open screen Figure B 8 2 The ePort Main screen will display with a Searching for Instruments message As instruments are located by the software Arke SO System Instruction Manual B 9 ePort PC Software Finding Instruments on a Network B 10 Arke S0 System Instruction Manual they will be added to the list in the Instrument frame on the left side of the screen Figure B 12 F e instrunmet Heb SO3 beta A 9800 Serial Number 503 beta amp EP Address 10 175 240 25 Status Active Lommand Download Detads m Downicad ss Download older Locations C Program Fieri Thermore PotD ata Open r Remote Inrerd sce Last Download m Dorio Soke Mitomated Downloads Dusbled Notes Dowrdead From Lit Domendeud ot Selected Date mt Tere Nmd do edomd wil start with data alter oa Nov 2011 1040 52 Ede a arate rumen TTT Figure B 12 ePort Main
198. ting bracket Use the following procedure to replace the Optical System Assembly Figure 5 4 WARNING The service procedures in this manual are restricted to qualified service representatives A 1 At the User Interface screen choose Instrument Controls gt Component Power gt Instrument Turn off the Laser amp Detector Power Laser Cooler Laser Housing Cooler and Detector Cooler 2 Turn off the Sample Pump Then wait 2 minutes for the bench pressure to reach atmospheric pressure Thermo Fisher Scientific Arke SO System Instruction Manual 5 9 Preventive Maintenance and Servicing Optical System Assembly 5 10 Arke SO3 System Instruction Manual 10 11 12 13 At the top of the bench disconnect the umbilical line At the bottom of the bench locate the 1 4 inch stainless steel bench exhaust tubing that runs behind the laser assembly To the right of the laser assembly is an elbow disconnect the PFA tubing from the elbow Disconnect the bench thermocouple from the System Control board Follow the bench thermocouple wire to the System Control board It is the 9 one from the front Untangle the wire so that it is free from other wires Disconnect the Bench heater wires from the Power Distribution board It is located at position J6 Untangle the wire so that it is free from other wires At the Detector Assembly remove the communication cable and the coax cable At the Detector Assembly locate the fan and
199. to calibrate the following flows e SO Flow Calibration Calibrate the SO flow going to the SO generator e Span Dilution Air Flow Calibration Calibrate the span dilution air flow 3 74 Arke S03 System Instruction Manual Thermo Fisher Scientific Flow Calibration Example Thermo Fisher Scientific User Interface Service Menu The Flow Calibration screens Figure 3 59 are used to calibrate MFC s used during calibrations Most likely no calibration will be needed and the coefficient can be left at 1 000 The SO Flow Calibration and the Span Dilution Air Flow Calibration screens function the same way S0 1 95 ppm Service gt Pressure Calibration gt 30 Flow Calibration Current 50 Flow 0 000 Limin Set to correct value of SO Flow Coefficient June 3 2011 Sample Alarms 14 47 13 Figure 3 59 SO Flow Calibration Screen The SO Flow Calibration screen contains the following information Current Flow Displays current SO flow Set to correct value of Using a calibrated flow meter the user measures the flow of SO The user enters the correct flow using the keypad Calibrate SO Flow Based on the current flow and correct value entered by the user this button adjusts the SO flow coefficient thus calibrating the current SO flow reading SO Flow Coefficient This flow coefficient value is the result of pressing the Calibrate Flow button This coefficient will be applied t
200. to hexadecimal in this case also 5 to match the status code table Only two status codes would add up to a value of 5 Table D 9 By looking at instrument s specific table and breaking down the downloaded status codes you will be able to decipher which status codes the unit has displayed Repeat the operation for each place in the hexadecimal code 10 s 100 s etc For example decipher the following decimal status code 8433666 for an instrument with the given example status code table Table D 10 First convert the decimal status code downloaded from the monitor to a hexadecimal number using the Windows or another scientific calculator 8433666 H 80B002 Table D 10 Example Status Code Table Code amp H1 amp H2 amp H4 amp H8 amp H10 Warning Flash Memory Power Switch TPIC Valve A Valve B Filter A Temperature Arke SO System Instruction Manual D 7 Error Code Troubleshooting Deciphering Status Codes D 8 Arke S0 System Instruction Manual Code Warning amp H20 Filter B Temperature amp H40 Heater A Temperature amp H80 Heater B Temperature amp H800 External Sample Tube Temperature amp H1000 Serial Port Problem amp H2000 Line Printer Problem amp H4000 Leak on Loop A amp H8000 Leak on Loop B amp H10000 Audit Failure amp H20000 oystem Reset amp H40000 Power Failure amp H80000 sample Volume Low amp H100000 Meter Out of Range gt 09 amp H400000 AC Voltage Out of Bound
201. to stack m Align mantle thru holes Figure 2 10 to stack sample port thru holes so probe is in desired position Refer to Figure 2 11 and install hardware in four places PORT MOUNTING THRU HOLES Figure 2 10 Mantle with Universal Mounting Flange 2 10 Arke SO System Instruction Manual Thermo Fisher Scientific Installation Probe Installation N O eo N N E D C Z E N I I Co C ns r N x pa m C 50 ES ae ul c S 5 x us c Q co C e c um c LO Sa C LO LO I e A ES A S N Gasket Thermo Supplied Figure 2 11 Mantle Mount Umbilical Plumbing Figure 2 12 shows the umbilical plumbing hookup Hookup There are two umbilical lines that connect the probe to the SO instrument One is a single heated line sample The other contains cold tubes to supply compressed air and signal to the probe Attach hotline umbilical cord to probe as shown in Figure 2 14 Attach 1 4 inch stainless steel tubing to the atmospheric dump union and bend tubing so that air flow is directed out of probe
202. tor empAlarmHigh Detector empAlarmLow Detector empCalCoef Detector empCalValue DetectorPeakSignal DetectorPeakSignalMinimaY DetectorPeakSignalCal DetectorPeakSignalAlarmHigh DetectorPeakSignalAlarmLow DataLoggingPeriod DataLogging Treatment DataLoggingstart DataloggingEndDatelime DataloggingRecordsBack otreamingPeriod Arke SO System Instruction Manual C 9 Serial Communication AK Protocol C 10 Arke S0 System Instruction Manual PRC Code 292 253 254 255 256 25 7 258 259 260 261 262 263 264 265 266 267 268 269 270 271 272 273 274 275 27b 277 278 279 280 281 282 283 284 285 Description streaming reatment OtherPulserPulsesPerSec OtherAveragingTime OtherStartTime OtherEndTime RegLoglIntervalDivisor opectrumBacklog opectrumSpikesLaserDataLenath spectrumSpikesLaserData20Percent opectrumSpikesLaserVoltageRange opectrumSpikesTotal TempAlarmsActive o03ConcentrationDataTemp SO3ConcentrationDataNumber SO3ConcentrationDataLog SO3SpanConcentrationDatal emp SO3SpanConcentrationDataNumber SO3SpanConcentrationDataLog SO3SpanConcentrationReadDatal emp SO3SpanConcentrationReadDataNumber SO3SpanConcentrationReadDataLog SO2MassFlowDatalemp o02MassFlowDataNumber 502MassFlowDataLog spanDilAirMassFlowDatalemp spanDilAirMassFlowDataNumber spanDilAirMassFlowDataLog BenchTempDatalemp BenchTempDataNumber Bench TempDataLog BenchPressureData lemp BenchPressureDataNumber BenchPressureDataLog
203. trument Controls gt Component Power gt Instrument Laser and Detector Power is ON The Laser Housing Cooler and Laser Cooler will need to be ON before the Laser and Detector Power can be turned ON 6 2 Arke S0 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Troubleshooting Instrument Devices and Alarms Laser Housing Cooler and Laser Cooler are not on or have temperature alarms Check for loose cables at the Laser Detector and Detector board If communication is lost at the detector the transmissions spectrum and raw spectrum screens will not update Also the SO concentrations will not update A shutdown and reboot may be needed Calibration Automatic Calibration Schedule Failure Modes If a failure occurs a failure message will appear at the screen Calibration Auto Calibration Schedule under the Peak Adjust button Failure 1 Zero Bkg Out Of Range During SZ The allowable Zero Background range is 100 to 100 ppm If during the zero duration of an automatic calibration the Zero Background is set to outside this range then the auto calibration sequence will stop and both the original background and span coefficient will be restored Failure 2 Current Span Coef Denominator 0 This failure will be displayed if any of the variables in the Span coefficient equation creates a 0 in the denominator The Error should not happen during normal operation Both the original
204. ts when the actual temperature of the cooler is too far above the Setpoint When the cooler circuit is driving above 50 power usually this only happens when the cooler initially tries to reach it s setpoint the blue LED D9 located at the top of the board turns ON Under normal circumstances this LED will tapper off as the setpoint is reached Arke SO System Instruction Manual 6 13 Troubleshooting Instrument Board and Cable Assembly Connections ju 012 LE 013 GLA 927 m C o h o QE bN SH E Lr 9 IE IIa E RITE Figure 6 3 Laser and Laser Housing inm Control Boards Top of board Laser and Laser Housing Temp Control Boards Bottom e D10 isa green LED that blinks when the board is communicating e The 4 pin dc power connector J7 is located at the bottom of this board Check voltages if a board problem is suspected e The two RS 485 connectors J3 and J4 are located on the left side of this board They are interchangeable and are used to daisy chain all the boards together 6 14 Arke SO System Instruction Manual Thermo Fisher Scientific Troubleshooting Instrument Board and Cable Assembly Connections neg e 9 fd SOW na ma 0i 0 COO Linv48ea IO TH JIJILNdIOS H3HSI3 ONU o en nci 6Tdl ESIM mG m I JOMINO2 dWAl OS QN9O One e E cdl UJ e gt 7 U m lt D D uU inom a X O wo Co CD Dr Ns Mm dem O O eO
205. ttached 5 Loosen three 3 fast loop table nylon insert nuts and slide table back 6 Usinga 1 1 16 inch 7 8 inch and 9 16 inch open end wrench replace the inertial filter and reassemble in reverse order Dilution Assembly Use the following procedure to replace the critical orifice Figure 5 15 Critical Orifice Equipment Required Replacement Critical orifice Open end wrenches 1 1 8 inch 1 1 16 inch 7 8 inch and 9 16 inch Allen wrench 5 32 inch N WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Using a 1 1 8 inch and 1 1 16 inch open end wrench disconnect Return Tube 2 Using a 1 1 16 inch and 7 8 inch open end wrench disconnect stinger tube from the inertial filter 3 Remove 5 sets of 10 32 cap screws thumbnuts 4 Remove fast loop top block with or without orifice blocks attached 5 Loosen three 3 fast loop table nylon insert nuts and slide table back 6 Using a 1 2 inch and 9 16 inch wrench remove critical orifice Note Contaminated orifices that are removed can be ultrasonically cleaned using a non base solution PH must not be greater than 8 A 7 Replace with new or cleaned orifice Ensure that these are no leaks as this will cause measurement errors 5 24 Arke SO System Instruction Manual Thermo Fisher Scientific 15 Micron Filter Replacement AN Valve Cover Gasket Replacement Thermo Fisher Scientific A Preventive Maint
206. umber and the status codes on the table into place holders the one s ten s 100 s 1 000 s 10 000 s and 100 000 s and the 1 000 000 s place Each place in the converted code will have a hexadecimal digit Each hexadecimal digit 0 F in each place will have a unique status code or set of status codes that go with it Table D 9 Hex Digits and Status Codes Decimal Number Hex Number Code sum of Codes 0 0 0 1 1 H 1 2 2 H 2 3 3 H 1 H 2 4 4 H 4 5 5 H 1 H 4 6 6 H 2 H 4 Thermo Fisher Scientific Deciphering Status Codes Thermo Fisher Scientific Example Decimal Number Error Code Troubleshooting Deciphering Status Codes Hex Number Code sum of Codes H 1 H 2 H 4 H 8 H 1 H 8 H 2 H 8 H 1 H 2 H 8 H 4 H 8 H 1 H4 H 8 H 2 H 4 H 8 H 1 H 2 H 4 H 8 n1 ri Cc c u 0 co o005 When the unit shows more than one status code it adds the codes together and displays them as a decimal sum For example if the unit displays a Memory status code listed as hexadecimal number H 1 on the instrument s specific status code table and a Valve A status code listed as hexadecimal number H 4 on the instrument s specific status code table at the same time the two status codes when downloaded would be displayed as the decimal number 5 The decimal number 5 must then be converted back
207. und wire to the instrument chassis The other two are connected from the green yellow terminal blocks to the chassis Remove the nuts that attach these two ground wires to the chassis 4 There are three 3 AC breakers with two 2 wires connected to each The left AC breaker powers the heaters connected to the Power Distribution board The middle AC breaker connects to the Power Supply The right AC breaker connects to the AC unit Remove all six 6 wires from the bottom of the three breakers Label each wire when disconnecting to ensure proper reinstallation 5 Remove the four 4 nuts that secure the AC Mains bracket to the chassis 6 Remove AC Mains Assembly 7 To reinstall follow the above instructions in reverse 5 6 Arke SO System Instruction Manual Thermo Fisher Scientific Preventive Maintenance and Servicing Pneumatic Assembly Replacement User Interface Assembly SN i 5 DER 4 p Optical System Assembly oystem Electronics Assembly
208. updated your Windows XP system select the Cancel button and use the Windows Update function of the PC to update the operating system before attempting to install the ePort software A B 2 Arke S03 System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific ePort PC Software Installing ePort i ePort 0 12 8 InstallShield Wizard Readme Information Please read the Following readme information carefully Important Note Supported Operating Systems o Windows XP sp2 o Windows 2000 sp3 and sp4 o Windows 2003 Server BEFORE installing rp Communicator EXIT this installation and install the Critical Windows Updates http windowsupdate microsoft com 7 Figure B 2 Windows Update Notice 5 The Customer Information screen will display Type in the information and select the Next button 6 The Ready to Install Program screen will display Figure B 3 Select the Install button i ePort 0 12 8 InstallShield Wizard Ready to Install the Program The wizard is ready to begin installation IF vau want to review or change any oF your installation settings click Back Click Cancel to exit the wizard Current Settings Setup Type Destination Falder Program FilesiThermo User Information Mame Company Cancel Figure B 3 Ready to Install the Program Screen Arke S0 System Instruction Manual B 3 ePort PC Software Installing ePort 7 The wizar
209. upply is high Qx00000400 The 12V supply is low 0x00000800 he stinger thermocouple is disconnected 0x00001 000 The probe thermocouple is disconnected Thermo Fisher Scientific Status Code in hexadecimal 0x00002000 0x00004000 0x00008000 0x00010000 0x00020000 0x00040000 0x00080000 0x00100000 0x00200000 0x00400000 0x00800000 0x01000000 0x02000000 0x04000000 0x08000000 0x10000000 Error Code Troubleshooting AK Protocol Description The SO generator thermocouple is disconnected The umbilical thermocouple is disconnected The bench thermocouple is disconnected The S0 generator stitch thermocouple is disconnected The chassis temp thermistor is disconnected The probe ambient thermocouple is disconnected The 100ft umbilical thermocouple is disconnected The umbilical temperature control shutdown automatically due to limits being reached The bench temperature control shutdown automatically due to limits being reached he stinger temperature control shutdown automatically due to limits being reached The probe temperature control shutdown automatically due to limits being reached he generator temperature control shutdown automatically due to limits being reached The SO generator stitch temperature control shutdown automatically due to limits being reached The 100ft umbilical temperature control shutdown automatically due to limits being reached The orifice stitch temperat
210. ure e Probe Ambient Temp Calibration Calibrates the probe ambient temperature e Stinger Temp Calibration Calibrates the stinger temperature e Umbilical Temp Calibration Calibrates the umbilical line temperature e Umbilical Stitch Temp Calibration Calibrates the umbilical stitch temperature e Orifice Stitch Temp Calibration Calibrates the probe orifice stitch temperature e SO Generator Temp Calibration Calibrates the SO generator temperature Thermo Fisher Scientific Arke S03 System Instruction Manual 3 67 User Interface Service Menu e SO Generator Stitch Temp Calibration Calibrates the SO generator stitch temperature See Figure 3 55 for Temp Calibration example 3 68 Arke SO3 System Instruction Manual Thermo Fisher Scientific User Interface Service Menu Temp Calibration The Temp Calibration screens Figure 3 55 are used to calibrate Example temperature devices Most likely no calibration will be needed and the coefficient can be left at 1 000 All temperature calibration screens function the same way This would include Bench Temp Calibration Laser Temp Calibration Laser Housing Temp Calibration Detector Temp Calibration Chassis Temp Calibration Probe Temp Calibration Probe Ambient Temp Calibration Stinger Temp Calibration Umbilical Temp Calibration Umbilical Stitch Temp Calibration Orifice Stitch Temp Calibration SO Generator Temp Calibration and SO Generator Stitch Temp Calibrati
211. ure control shutdown automatically due to limits being reached The orifice stitch thermocouple is disconnected Table D 8 Motherboard Status Status Code in Description hexadecimal 0x00000000 no error TBD TBD Thermo Fisher Scientific Arke S03 System Instruction Manual D 5 Error Code Troubleshooting Converting Decimal Hexadecimal Numbers Converting Decimal Hexadecimal Numbers D 6 Arke SO3 System Instruction Manual Error codes in the data logging table are decimal base 10 based numbers which need to be converted to hexadecimal base 16 numbers in order to defifer the board error The easiest way to convert the decimal numbers reported by the unit is to use the calculator on a Windows based PC To convert a decimal status code to a hexadecimal number 1 Open the Windows calculator From the Start menu choose All Programs Accessories 2 Select View Scientific to open the scientific style calculator 3 Select Dec to choose the decimal calculator option and then enter the decimal status number into the calculator 4 Select Hex to choose the hexadecimal calculator option The new number displayed in the calculator is the hexadecimal number you will use to decipher the status code list Note To convert a hexadecimal to a decimal number select Hex type in the hexadecimal number then select Dec A To properly use the hexadecimal numbers converted from the decimal data download separate the converted n
212. use holder that light when that valve is supposed to be open You can use these LEDS to ensure that Thermo Fisher Scientific Arke S0 System Instruction Manual 6 11 Troubleshooting Instrument Board and Cable Assembly Connections this board is receiving the correct Gas Mode valve selection assigned through the GUI e The 4 pin dc power connector J14 is located at the bottom of this board Check voltages if a board problem is suspected e The two RS 485 connectors J29 and J34 are located on the left side of this board They are interchangeable and are used to daisy chain all the boards together If you suspect a communication problem with this board check these connections and associated cables then verify under System Status and Alarms Board Status that the communication is OK TY Ti ad Ys LL zu ls i eine ase SE Dr RI iil X c Ba HIFI zd cu d Oy Eg aor E LJ Li PLI I l 4 TED Mew S41 E amp LE ae L JT rae L mhi 1 EE mr 4 g l ET LI Es 5 pe LET E da a loa Tr P Ur t cen d5 D adJ L LI ne ani TERN TES ae be len Hm Ju m ie dL aE2 tn nne Pec TH eI Bi LI 2 lute pauni imm MIT REST T AUT Lus LEAN CE FETI of FETI e enim ung i con mmi Lp DIE i waa e Ban ai TT TA oo 00 oo 0548 DC OP PET ti lt i TE _all l a
213. ve both the inlet and outlet tubing from the generator 6 Remove generator assembly 7 Replace the generator and reassemble in reverse order Service Locations For additional assistance Thermo Fisher Scientific has service available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermoscientific com agi 1 866 282 0430 Toll Free 1 508 520 0430 International 5 30 Arke SO System Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Chapter 6 Troubleshooting This chapter provides the following troubleshooting and service support information for the Model 9800 e Instrument Devices and Alarms on page 6 2 e Instrument Board and Cable Assembly Connections on page 6 10 e Instrument Pneumatic Assembly Cables on page 6 21 e Probe Pneumatic Cable and Wiring Connections on page 6 22 e Cable Assembly Connections Heaters Valves and Optical Bench on page 6 26 e Finding and Optimizing the Correct SO3 Peak on page 6 27 e Service Locations on page 6 33 The Technical Support Department at Thermo Fisher Scientific can also be consulted in the event of problems See Service Locations at the end of this chapter for contact information In any correspondence with the factory please note both the serial number and program number of the instrument Arke SO System Instruction Manual 6 1
214. ves and Accumulator Tank Arke 03 System Instruction Manual 5 17 Thermo Fisher Scientific Preventive Maintenance and Servicing Replacement Tubing List A Vacuum eo c Dilution Eductor Cal Gas Dil Figure 5 9 Fitting Locations Umbilical Connections Eductor In ERN fo f D Sy Dilution In 9 gt S Net NN Pa a Filter Blowback In ll 3 x EE Cal Gas Dilution In gt X P ER Figure 5 10 Fitting Locations Fast Loop Assembly Flange End 5 18 Arke SO System Instruction Manual Thermo Fisher Scientific Preventive Maintenance and Servicing Factory Wiring SO In Cal Gas Dilution In Fy PA a A in E po OA m To Stinger iN EN i Ssi po Ira X p L1 O Apm c SO In Figure 5 11 Fitting Locations Generator Facto ry Wiring Figure 5 12 and Table 5 5 through Table 5 7 shows the factory wiring and wiring terminations for the Model 9805 Probe TERMINAL BLOCK TB TERMINATIONS SEE DETAIL A
215. when out of the specified range of 0 20 to 9 8 L min An error box will pop up asking you to change the Calibration settings Calibrations will not take place if this screen displays flow setpoint errors A Arke S0 System Instruction Manual 3 13 User Interface Calibration Menu Note A minimum of 3 L min is recommended for the Span Dilution Air Flow Setpoint A Note A cylinder concentration of 1000 ppm SO in Air is recommended A 3 14 Arke SO3 System Instruction Manual Thermo Fisher Scientific Auto Calibration Thermo Fisher Scientific Schedule User Interface Calibration Menu The Automatic Calibration Schedule screen Figure 3 11 sets periodic automatic calibrations It will automatically run a background and span at designated times When run this schedule calibrates the system by setting a new background and new span coefficient See Chapter 4 Calibration for further instructions on how to run an Automatic Calibration Schedule If Peak Adjust is enabled the laser temperature will be adjusted to center the SO peak on channel 0 S0 195 ppm 2 Calibration Auto Calibration Schedule an Mext Time Period Duration Current Cal 04 11 2012 15 39 00 SQ Averaging Time For Auto Cal April 18 2012 Filter Blowback Alarms 5 11 27 22 Figure 3 11 Auto Calibration Schedule Screen The Automatic Calibration Schedule screen contains the following information e Auto Cal Enabled Disabled
216. with or without orifice locks attached 4 Loosen three 3 fast loop table nylon insert nuts and slide table back 5 Using a 1 2 inch and 9 16 inch open end wrench disconnect the dilution eductor 6 Replace the dilution eductor and reassemble in reverse order Thermo Fisher Scientific Preventive Maintenance and Servicing Inertial Filter Replacement Venturi Return Tube Inertial Filter N NE Silcolloy Tee 4 15 micron Filter Figure 5 15 Fast Loop Replacements Note When replacing parts use appropriate open end wrenches and make orientation of part A Inertial Filter Use the following procedure to replace the inertial filter Figure 5 15 Repl acement Replace only after the probe has cooled or use heat resistant gloves Equipment Required Inertial filter Open end wrenches 1 1 8 inch 1 1 16 inch 7 8 inch and 9 16 inch Allen wrench 5 32 inch WARNING The service procedures in this manual are restricted to qualified service representatives A 1 Using a 1 1 8 inch and 1 1 16 inch open end wrench disconnect Return Tube 2 Using a 1 1 16 inch and 7 8 inch open end wrench disconnect stinger tube from the inertial filter Thermo Fisher Scientific Arke S03 System Instruction Manual 5 23 Preventive Maintenance and Servicing Dilution Assembly Critical Orifice Replacement 3 Remove 5 sets of 10 32 cap screws thumbnuts 4 Remove fast loop top block with or without orifice blocks a
217. ws Update Notice B 3 Figure B 3 Ready to Install the Program Screen B 3 Figure B 4 InstallShield Wizard Completed Screen B 4 Figure B 5 Microsoft NET Framework Welcome Screen B 5 Figure B 6 Microsoft NET Framework Setup Complete Screen B 6 Figure B Z System Status SEFGell ue n Dd etu Nu SUR NUN MS B 7 Figure B 8 ePort Main Screen with Open Screen B 7 Figure B 9 Selecting new Instrument from the Menu Bar B 8 Figure B 10 Add New Instrument Screen B 8 Figure B 11 ePort Main Screen with Instrument Information Displayed B 9 Figure B 12 ePort Main Screen with Searching for Instrument Message B 10 Figure B 13 Adding or Deleting an Instrument from the List B 10 Figure B 14 ePort Main Screen ccce B 11 Figure B 15 Download Setup Wizard B 12 Figure B 16 Download Setup Wizard sssssssssssse B 13 Figure B 17 ePort Main Screen ccce B 14 Figure B 18 Download Data Screen B 15 Figure B 19 Download Data to USB Flash Drive Screen B 16 Figure B 20 Select Data Screen ccecce B 16 Figure B 21 Data csv File Opened in Excel B 17 Figure C 1 AK COM Port Settings C 2 Thermo Fisher Scientific Thermo Fisher Scientific Tables Table 1 1 Arke S0 System Specifications ssssssssssssssss 1 8 Table 2 1 Heat
218. x o Uu S en Uu Pu UN UN ees 3 85 Figure 3 66 Export to USB Flash Drive Screen 3 00 Figure 5 1 Pneumatic Tubing Detail 5 5 Figure 5 2 Component OCHO eue Do caedis epe deli tone odes 5 Figure 5 3 Pneumatic Assembly sssssssssne 5 9 Figure 5 4 Optical Assembly Replacement sssssssssssss 5 11 Figure 5 5 System Electronics Assembly Replacement 5 12 Figure 5 6 User Interface Assembly Replacement 5 14 Figure 5 7 Fitting Locations Undersides of Valves sss 5 17 Figure 5 8 Fitting Locations Blow Back Valves and Accumulator Tank 5 17 Figure 5 9 Fitting Locations Umbilical Connections 5 18 Figure 5 10 Fitting Locations Fast Loop Assembly Flange End 5 18 Figure 5 11 Fitting Locations Generator 5 19 Figure 5 12 Factory Wiring Terminal Block Terminations 5 19 Figure 5 13 Terminal Block Terminations 5 20 Figure 5 14 Valve lerminations sssssssem 5 20 Figure 5 15 Fast Loop Replacements sssssssssssee 5 23 Figure 5 16 Cover Removal 5 26 Figure 5 17 Electrical Components Replacement ssssss 5 2 Figure 6 1 System Control Board Top of board eee 6 11 Figure 6 2 System Control Board Bottom of board oo eee eee 6 12 Figur

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