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        Nitrogen Generator LCMS User`s Manual
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1.   MATHESON  TRI GAS    ask     The Gas Professionals        Nitrogen Generator  LCMS    User   s Manual    Supplied by     Matheson Tri Gas  Inc    166 Keystone Drive  Montgomeryville  PA 18936 USA  Telephone  1 215 641 2700  Fax  1 215 641 2714  E mail  info matheson trigas  Web site  www matheson trigas com    Nitrogen Generator N2 Misral LCMS User s Manual Index    Index  INDEX titi caia 1  INTRODUCTION  id  2  SEOPE DE THE VON NU A a andes 2  SPECIAICA TIONS di e EA TEE Cee A id ETE DEE N 2  NOTES ON  FCC COMPEIANCE ai a N A ede nace et gadme en oaeee 2  CORRECTUS E oE E at lie is de Mod do de o de e E N lena 3  HEAT ANDES ARES Co ias 4  PACKIN OE A A O a O O E Se 5  DESCRIPTION a e EN eN e soc E E E E AE E EEE E E E 5  INSTALACION  a a a casdeasnosecececeseenccuateccucee 6  RECEIVING THE GENERATOR Morr a ne ore A 6  PLACING THE GENERATOR nds 6  SYMBOLS USED ON THE GENERATOR e dele 6  SCO NINE CTO ING cee cee ee ado e ee bd dd ds e NO 6  TNTTTA E STAR A O A ese ceases ae 7  STARTN2  ROC CO heehee e a a e e Vann ata 7  OPERATION Sotelo gst tte dec iets Sate eh tees ear le cso Siku a mse Se sist dave ead Naku a ese a atacara tae 7  MENGUSIR TURE a e a a MAR e a e ld ia e 8  PRE ALARMSANDALAR MS nr r aai 9  MAT TEN A D een ee ne een ta meno aera E EE nc Rear ARREST REST PER On E wea RR a 10  ROUTINE MANA O E e dc as does ds 10  RETURNING THB UNE lant wandealiabenatansedosaiiersalalieasaabarueks 15  SPARE PAR Tels E ose 16    Nitrogen Generator N2 Misral LCMS User s Manual   
2.   Returning the unit    In the event of any faults or damage  first notify the agent or distributor who supplied the unit   Please also provide full details of the problem  including the model and serial number  In   structions will then be provided for the service or the return of the unit  If the warranty has  expired  or the fault is due to misuse of the unit  all repair and shipping costs are to be paid  by the customer  All other costs are borne by the customer  except as otherwise expressly  agreed upon     WARNING   If the unit has to be transported  make sure to use suitable packaging     The unit should be transported in an upright position  this warning should be reported on  the outside of the packaging        16    Nitrogen Generator N2 Misral LCMS User s Manual Spare parts list    Spare parts list    The table below provides a list and description of the spare parts of the nitrogen generator     List of spare parts     N2 MISTRAL LCMS    p n DESCRIPTION  NS 404 4 000 hours maintenance kit  NS 401 8 000 hours maintenance kit    NS 406 Air compressor 230V   50Hz  NS 407 Air compressor 110V   60Hz          IMPORTANT   The manufacturer reserves the right to change or modify its products without prior notice     17    
3.  Introduction    Scope of the manual    Introduction    This manual provides operation and maintenance instructions for model N2 Mistral LCMS ni     trogen generator     Specifications    Specifications of the nitrogen generator    Nitrogen flow rate    STP  Standard temperature and  pressure  20 C  1 bar     Max outlet pressure  Purity   Weight   Power consumption    Input voltage  Fuse    Pressure accuracy  Microprocessor controlled display    Index of protection    Operating conditions     Temperature    Relative humidit    Over voltage category  Pollution degree  Sound pressure level    Case dimensions    Notes on FCC compliance    Model Mistral LCMS 0 35 L min at STP    8 bar  116 psi  35L min  98    O2 lt 2   at STP  170 kg   1300 W    110 or 230V   50 or 60Hz    Circuit breaker 110 V   16A and 230V   10A    0 1 bar    0 5     Graphic display  128 x 64 pixels  IP2x    15  C to  35  0 80   non condensino    II   2    lt  60 dB A    482 x 835 x 641 mm  WxDxH     This equipment has been tested and found to comply with the limits for a Class B digital de   vice  pursuant to part 15 of the FCC Rules  These limits are designed to provide reasonable  protection against harmful interference in a residential installation  This equipment generates   uses and can radiate radio frequency energy and  if not installed and used in accordance  with the instructions  may cause harmful interference to radio communications  However   there is no guarantee that interference will not occur 
4.  s Manual Introduction    Health and safety    Correct use of the N2 MISTRAL LCMS nitrogen generator is important for your personal  safety and for trouble free functioning of the N2 MISTRAL LCMS  Incorrect use can cause  damage to the N2 MISTRAL LCMS or can lead to incorrect gas supply     Warning    A N      Read this manual before you start the installation and putting into operation of  the N2 MISTRAL LCMS  Prevent accidents and damage to the N2 MISTRAL   LCMS    Contact your supplier if you detect a problem that you cannot solve with this  manual    Only service engineers  that are qualified to work on electric and pneumatic  equipment  are allowed to do the installation  maintenance and repairs  Un   qualified people are not allowed to repair the equipment  Lift the N2   MISTRAL LCMS with a forklift  Follow the legislation and instructions for op   erating the forklift    Do not tamper or experiment with the equipment  Do not exceed the technical  specifications for the N2 MISTRAL LCMS     Warning  nitrogen and oxygen    The N2 MISTRAL LCMS generates nitrogen as a product  Oxygen enriched air is  released as waste     A  AS    Nitrogen can cause suffocation     Oxygen enriched air leads to increased risk of fire in the event of contact with  inflammable products  Make sure that there is adequate ventilation at all  times    The N2 MISTRAL LCMS is not designed for installation in an Exx classified  area    Do not install the N2 MISTRAL LCMS in an area where explosive mix
5.  section 2  the temperature inside the section 2 is over the  maximum limit  Check if the room temperature respects the specifications and if there  is enough space in the rear side of the unit for the ventilation  Otherwise  remove the  right panel of the machine and the cabinet panel and check if all the fans are working   If it is all right  call the service  Press the reset button     e Min pre alarm press  Section1  the pressure in the output reservoir is less than the  lower limit  Call the service  Press the reset button    e Max pre alarm oxygen  only if the optional oxygen analyzer is installed   the Ne pu   rity is decreasing  Call the service  Press the reset button    e Work time pre alarm compressor 1  the compressor 1  must be changed  Call the  service  Press the reset button    e Work time pre alarm compressor 2  the compressor 2  must be changed  Call the  service  Press the reset button    e Pre alarm service 4000 h  the filters must be changed  See the maintenance section  of this manual relatively to the 4000 h service kit  Call the service to order the new kit   Press the reset button    e Pre alarm service 8000 h  the filter and the silencer must be changed  See the main   tenance section of this manual relatively to the 8000 h service kit  Call the service to  order the new kit  Press the reset button    e Pre alarm clock failure  the clock is broken  Call the service  Press the reset button     Alarms     Max alarm section 1  the temperature inside sec
6.  unit  Enter the menu  go to the special func   tlons and insert the number     26103    This procedure reset the 4000 h work time counter     NOTE  If the cover of the filter is difficult to remove  probably there is still pressure inside it  To    solve the problem  unscrew partially the bottom cap of the cover until the internal pressure  reach the ambient pressure        13    Nitrogen Generator N2 Misral LCMS User s Manual Maintenance    8000 hours service kit   Every 8000 hours the user must replace the filter and the silencer of the unit    A specific maintenance kit is available as spare part  This kit includes all required parts   Specifically  each kit includes     1  New filter element  2  New silencers    Exchange the filter element    See the 4000 h service kit without inserting the reset code     Exchange the silencer    e unscrew partially the three bottom screws of the side panel with the wrench     ee       Screws    e unscrew the three rear screws of the side panel     Screws       e remove the panel     14    Nitrogen Generator N2 Misral LCMS User s Manual Maintenance       Silencers    e unscrew the silencer and replace it  Be careful and avoid to screw strongly the silencer     Silencer       e reassemble   e reconnect the power line and switch on the unit  Enter the menu  go to the special func   tlons and insert the number   26104    This procedure reset the 8000 h work time counter     15    Nitrogen Generator N2 Misral LCMS User s Manual Maintenance  
7. e generator and theirs purpose is  to compress air up to 5 bar and force it into the tubes containing the carbon molecular sieve     The generated nitrogen gas is accumulated in a specific reservoir and then compressed by a  compressor to give the requested 8 bar      lt  10  10 10    T1  VA DA Y H  vs Y HY ve X HY PL2  AnS S    Es      10  4 10 4  RR    ti    10    ZEX  V OF332 HP Head  m Cooler Coalescing   gt  OF312  Coil  filter V1 X y X  1 1  BP  q      6 E D  verseur  Alim    me  P Flexible HP i A E 4   E  de   Purge Sy   10 V  OF332 Low ik a    Pressure Head  OUTLET Pout  8 to 8 5 bar          10                              Inlet Filter    Nitrogen Generator N2 Misral LCMS User s Manual Initial start up    Installation    Receiving the generator    All units have been carefully inspected before transport  Visual checks for damage and func   tional tests should be performed upon receipt  Any damage must be immediately noted and  reported  The generator must only be returned according to the shipping instructions pro   vided     Placing the generator    The nitrogen generator must be placed on a flat  level  vibration free  shock free surface  Do  not place the generator over a source of heat  as this may cause the device to overheat  The  unit should not be in contact with any other objects on any side  and the air inlet must not be  blocked  Leave at least 30 cm of free space at rear for ventilation  Do not operate the  generator in a sealed or unventilated room  Do n
8. e internal components of the nitrogen generator do not need to be cleaned and should not  be accessed by the user for cleaning  To clean the outside of the unit  only use a damp cloth   no detergents  acids or aggressive or abrasive substances      Service kits    e Every 4000 hours the user must replace the filters of the unit   e Every 8000 hours the user must replace the filters and the silencer of the unit     WARNING     Only qualified personnel should perform service on this product  Any damage done to this  product as a result of improper maintenance procedure will void the warranty        11    Nitrogen Generator N2 Misral LCMS User s Manual Maintenance    4000 hours service kit   Every 4000 hours the user must replace the filters of the unit    A specific maintenance kit is available as spare part  This kit includes all required parts   Specifically  each kit includes     1  New filter elements    Exchange the filter element    e switch off the instrument and disconnect it from the power line   e unscrew partially the two bottom screws of the front panel with the wrench             e remove the front panel        Filter    12    Nitrogen Generator N2 Misral LCMS User s Manual Maintenance    e click the button  rotate the cover of 1 8 turn in a left hand direction and then push it in the  bottom direction     B  utton Gaver    e unscrew the filter element and replace it with the new one     Filter element       reassemble   e reconnect the power line and switch on the
9. hows the work time for the 4000 h service   SRV 8000 Shows the work time for the 8000 h service       Alarm history  Shows the history of the alarms of the unit   Set clock    Allow the regulation of the clock of the unit  The central button of the display increases the  values and the left button passes to the next number     Special function  Allow the activation of some special function  i e  the reset of the working time counter of the    filter  with the digitations of a code  The central button of the display increases the values  and the left button passes to the next number     Nitrogen Generator N2 Misral LCMS User s Manual Initial start up    Codes     e Reset of the 4000 h work time counter  26103   e Reset of the 8000 h work time counter  26104     Pre alarms and alarms    There are a series of pre alarms and alarms on the unit  When a pre alarm starts  a sound  advertise about a problem and the type of problem is displayed on the main screen  When an  alarm starts  the unit also stops     What do they mean and how to proceed   Pre alarms     e Max pre alarm Temp section 1  the temperature inside section 1 is over the maxi   mum limit  Check if the room temperature respects the specifications and if there is  enough space in the rear side of the unit for the ventilation  Otherwise  remove the  right panel of the machine and the cabinet panel and check if all the fans are working   If it is all right  call the service  Press the reset button    e Max pre alarm Temp
10. ics of the unit           Output Date hour  pressure   Oxygen Flow rate  content       Messages row    In the main screen  the three buttons have the following function     Left button  start stop   Central button  reset the alarms   Right button  enter menu     In the menu  the three buttons change their function   Left button  scroll     Central button  select   Right button  exit the selected menu voice     Nitrogen Generator N2 Misral LCMS User s Manual Initial start up    Menu structure    Parameters    Item   Description Options   Range    Pressure units Sets the desired unit of measure for bar   kPa  psi ba  the pressure  Temperature Sets the desired unit of measure for   C   F   C  units the temperature  O  5    i r  the flow rate   Sets whether the unit automatically N  starts production when power is  switched on   play    Sets the possibility to see the pre   list alarms in the alarm history list  Stand by mode   Put the device in stand by mode if NO  the tank is full          Diagnostic  C1 temp Shows the instant temperature in the section 1 of the cabinet    C2 temp Shows the instant temperature in the section 2 of the cabinet  S 1 press Shows the pressure in the section 1 before the second compressor  Shows the instant pressure in the output reservoir    Shows the instant output pressure  Shows the output flow    Oxygen Shows the instant oxygen content  only if the optional O   analyzer is in   stalled    WT CMP Shows the work time of the compressor   SRV 4000 S
11. in a particular installation     If this equipment does cause harmful interference to radio or television reception  which can  be determined by turning the equipment off and on  the user is encouraged to try to correct  the interference by one or more of the following measures    e Reorient or relocate the receiving antenna    e Increase the separation between the equipment and receiver     Nitrogen Generator N2 Misral LCMS User s Manual Introduction    e Connect the equipment into an outlet on a circuit different from that to which the re   ceiver is connected   e Consult the dealer or an experienced radio TV technician for help        WARNING   Any changes or modifications to this equipment not expressly approved by the manufac   turer may void the user s authority to operate the equipment     Correct use    Nitrogen generator is designed to produce nitrogen for laboratory use  The unit must only be  operated for this purpose  according to the specifications and instructions provided in this  manual  In particular  the following warnings must be observed at all times    e Indoor use only   e Never operate the unit in below zero temperatures    e Only operate the unit in a room with sufficient ventilation  see    Placing the unit        e Always unplug the unit from the mains power supply before accessing the internal   components for replacement   e Only the parts described in the    Spare parts list    can be replaced by the user     Nitrogen Generator N2 Misral LCMS User
12. ot operate the generator at below freezing  temperatures  Operation is guaranteed at operating temperatures between  15 and  35  C     WARNING     Normal precautions for any nitrogen supply should be taken when using the generator   DO NOT use in sealed or unventilated rooms  Nitrogen can cause suffocation        Symbols used on the generator         Earth symbol   This symbol marks the earth connections to the chassis of the nitro     gen generator     Gas connections    Pure nitrogen at regulated pressure is available at the nitrogen outlet port at the rear of the  generator  This port must be connected to Y    ubing using a stainless steel Swagelok con   nector  Teflon connectors are not suitable  The pressure at this port is shown on the display     WARNING     The line from the relief port should never connected in such a way that back pressure can  develop        Nitrogen Generator N2 Misral LCMS User s Manual Initial start up    Initial start up  Start N2 Mistral LCMS      Switch on the unit      Connect the N2 Mistral LCMS to your application     Press start      lt will at least 60 minutes before the nitrogen produced will reach the stated purity     The system is ready for use now     Operation    The operating status of the unit is shown on the main screen on the graphic display    The main screen has three options at the bottom  corresponding to the three buttons on the  unit  which are used to run the various functions and access the configuration and diagnos   t
13. tion 1 is too high    Max alarm section 2  the temperature inside section 1 is too high    Min alarm press  section 1  the pressure in the section 1 is too low    Max alarm press  outlet  the outlet pressure is too high  Check if the output fitting is   free  If it is all right  call the service    e Max alarm oxygen  only if the optional oxygen analyzer is installed   the N   purity is  over the maximum limit    e Work time alarm compressor 1  the compressor 1 must be changed    e Work time alarm compressor 2  the compressor 2 must be changed     Nitrogen Generator N2 Misral LCMS User s Manual Initial start up    e Alarm service 4000 h  the filter must be changed  See the maintenance section of  this manual    e Alarm service 8000 h  the filter and the silencer must be changed  See the mainte   nance section of this manual    e Alarm EEP failure  failure of the static memory  Call the service     10    Nitrogen Generator N2 Misral LCMS User s Manual Maintenance    Maintenance    With proper care and maintenance  your nitrogen generator should provide you with years of  trouble free operation  There are no adjustments to be made to the generator  The only rou   tine service operations are those described below     Nonetheless  the generator should be inspected approximately every 2 years  Contact your  supplier     Routine maintenance    The following section describes the maintenance operations required for the correct opera   tion of the nitrogen generator     Cleaning   Th
14. tures  may occur     Warning  electricity    A     Only service engineers  that are qualified to work on electric equipment  are  allowed to do the installation  maintenance and reparations    Disconnect the main power supply before you do the maintenance or repair    If a service engineer has to work on the N2 MISTRAL LCMS while the elec   tric power it is connected  the service engineer must be very careful with re   spect to the electric hazards     Warning  safety precautions    A     Make sure that the ventilation rate is sufficient in the room where the enriched  oxygen is ventilated  or lead the enriched air outside    Keep the ambient temperature between 10 and 35   C    Install the peripheral equipment  piping and nitrogen storage vessels accord   ing to standard procedures    Do regular maintenance to the N2 MISTRAL LCMS     Nitrogen Generator N2 Misral LCMS User s Manual Installation    Packing list    List of items included in the shipment    Nitrogen generator  Instruction manual    ON OFF manual valve  if not installed     Description       The nitrogen generator produces pure nitrogen through the filtration of compressed air  The  key element of the generator is a carbon molecular sieve that is able to separate the nitrogen  molecules from the oxygen ones present in the compressed air stream  The carbon molecu   lar sieve tubes are self regenerating cyclic  PSA   pressure swing adsorption method   The  compressor  two compressors on Sirocco 5  is integral in th
    
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