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User`s Manual - Cole

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4. 4 5 Men asa M 4 5 Mema TICE T 4 6 MI A M 4 7 High Temperature Catolica oa 4 15 Stopping the CANA DONE aia 4 16 Contents Power DO noia 4 16 e e E e oO at a 4 16 RESTA o m 4 16 Section 5 Preventive Maintenance eeeeeeeeennnnennnnn nnn 5 1 5 1 Condenet Plis mini 5 1 Testing the Safety Pool aa diia 5 2 Section 6 Troubleshooting U a u aa 6 1 Eitrot Displays 6 1 Check Eist 6 3 Appendix Serial Communications Protoceol s 1 Declaration of Conformity RoHS Declaration of Conformity Cole Parmer pm 99 JURVA JOADUIYA 9A9 PMY m IOUO urojs s Teu1o3xo oup pue sour SUREM YY ur 249 12doad ayy uraureui o puvy uo pmp exo d y urojs s eugo1xo uv Surdumd vayy p 1e u voy puedxo spiny poseq ro pro y 8 1 7 wo c c Apoavurrxoadde ae sr ne oA9 Aor au doy n Ao q 8 5 W p Apyerurxozdde ye sr SUTUJEM MOJ u L Tenutur oos UMOP MYS TA 12391 pue dumd uonvaoSngoz ou anus qp MUN n TT AVA Y qam UNI o sonunuoo PUN IP ONINYVA P42 MO Y WM Bury 910394 unuq oy olur sr ureuo 3no oov d Surid
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6. The Setpoint is the desired fluid temperature The circulator can store up to five setpoints SP1 through SP5 The procedure for changing the stored setpoint values is discussed later in this Section Use the navigation arrows and move to the SP1 window and then press e to highlight it as shown below v 20 0 C Setpoint Value Window Use the up and down navigation arrows to bring up the desired setpoint and then press The display on the Setpoint Value Window will now indicate the corre sponding setpoint s stored value If desired you can change the displayed setpoint value by using the navigation arrows to highlight the Setpoint Value Window and then pressing The right most digit will have a cursor beneath it _ 35 0 C Use the left and right arrows to move the cursor to the desired digit and then use the up and down arrows to change the value Once all the desired changes are made press 0 to save the change Setpoint Value Window NOTE Using this procedure also changes the setpoint s stored value A 4 4 Cole Parmer Section 4 Operation Menu Displays The circulator uses menus to view change the settings NOTE The circulator does not need to be running to view change these settings A For all Menu displays once 0 is pressed to change a display you can press 23H to return to the previous screen 1 Use the right arrow button to highlight 2 Use the up and down arrow to highlight the Menu a
7. select it Cole Parmer 4 9 Section 4 Operation Set Clock is used to set the controller s time On Off Timer is used to enable and set the hr min sec and date year month day controller s timer 1 With On Off Timer highlighted press e to display the on 1 and off O time as well as the enable box I 2010 01 01 08 00 00 O 2010 01 01 08 00 00 Enable After setting the on and off times select Enable to activate the timet Auto Restart is used to enable the auto restart feature When enabled the circulator will automati cally restart after a power failure or power interruption condition 1 With Auto Restart highlighted press to toggle between enable and disable Energy Saving is used to enable the energy savings mode The Energy Saving mode is primarily designed for applications running under a stable load Enabling the mode saves energy by reducing the circulator s heater power and cooling requirements This can result in substantial energy savings over the life of the circulator The default setting is ON 1 With Energy Saving highlighted press to toggle between enable and disable The default is disable except for C15 baths which have an enable default Interfaces is used to enable configure the optional serial communications feature Available options 1 With Interfaces highlighted press e to Serial Type RS232 RS485 Off display the list of parameters Baud 19200 9600 4800 24
8. Cole Parmer Section 4 Operation 1 With PID Tuning highlighted press e to 2 Highlight the desired PID and press 0 to display display Cool PID Heat PID Factory values are P 05 0 I 0 10 D 0 00 H igh Tempe rature To protect your application the adjustable High Temperature Cutout HTC ensures the heater will not exceed temperatures that can cause o Cutout 20 120 High Temperature fault occurs when the temperature of the sensor eC exceeds the set temperature limit serious damage temperature sensor is located in the bath fluid A HTC Temperature range varies with type of immer sion circulator In the event of a fault the circulator will shut down and display a fault message see Section 6 The cause of the fault must be identified and corrected before the circulator can be restarted The cutout is not preset and must be adjusted To set the cutout with the circulator off use a flat head screwdriver to turn the red dial fully clockwise Start the circulator Adjust the setpoint for a few degrees higher than the highest desired fluid temperature and allow the bath to stabilize at the temperature setpoint Then slowly turn the dial counterclockwise until the circulator shuts down and the message appears Press the enter key to clear the message Before you can restart the circulator it has to cool down a few degrees To restart press the black ring surrounding the red dial and then press the ent
9. 3 1304 N5 150 3 230 50 1 9 3 2138 Country Specific Cole Parmer 3 3 Section 3 Installation 3 4 Remote Temperature Sensor Communications cable from bath Cable connection required for proper communication between the bath and the circulator Line cord from bath cooling heating baths only Return Flow USB Connection xal Outlet Flovv Never apply line voltage to the connection A a 3 DU dede BB 2O a 1 b TI TT TT Pla y A als vr V Im I O Circuit Protector e Outlet Flow Line cord connection Remote Temperature Sensor pe O a Qu IL TT Advanced Immersion Circulator TE TIT Return Flow The optional remote temperature sensor is enabled using the circulator see Section 4 Pin Pin 1 White 7 2 3 NA 8 4 White 9 5 6 NA Red NA Red 4th wire not connected to the control board Cole Parmer Cole Parmer External Circulation Approved Fluids A DANGER A DANGER Section 3 Installation The plumbing connections for external circulation are located on the rear of the circulator is the return flow from the external application i is the outlet flow to the external application supply side The connec
10. Fluids Type in this Section A 4 With the desired line highlighted press O The right most digit will have a cursor beneath it O Use the left and right arrows to move the cursor to the desired digit and then use the up and down m artows to change the value Once all the desired changes are made press e to save the change or to cancel it Cole Parmer 4 7 Section 4 Operation Alarms is used to view adjust the high and low temperature alarm limits to enable disable the audible alarms and to configure the low level warning reaction 1 With Alarms highlighted press to display Temperature Alarms Audible Alarms O Low Level Warning 3 Highlight the desired limit and press 2 With Temperature Alarms highlighted press to display High Fault Follow the same procedure used to change a setpoint If the Fault temperature is exceeded the circulator will shut down and if enabled the audible alarm will sound If the Warn temperature is exceeded the circulator will continue to run and if enabled the audible alarm will sound In both cases a message will be displayed High Fault cannot be set below High Warn High Warn cannot be set below Low Warn Low Fault cannot be set above High Warn 1 With Audible Alarms highlighted press to display the alarms Highlight the desired alarm and press o to toggle between enable and disable mode Faults If Faults is enabled the alarm will sound when a fa
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12. port on the front of the bath is sed and that all plumbing connections are secure Also ensure any residue is thoroughly removed before filling Before using any fluid refer to the manufacturer s MSDS and EC safety data sheets for handling precautions A To avoid spilling place your containers into the bath before filling With a low level WARNING the circulator continues to run with a FAULT the circulator will shut the refrigeration pump and heater will shut down see Section 6 The low level warning is at approximately 4 cm 1 5 8 below the top the low level fault is at approximately 5 5 cm 2 1 8 Avoid overfilling oil based fluids expand when heated A gt When pumping to an external system keep extra fluid on hand to maintain the proper level in the circulating lines and the external system Note Monitor the fluid level whenever heating the fluid A Drainin g Before draining any fluid refer to the manufacturer s MSDS and EC g any safety data sheets for handling precautions A Ensure the fluid is at a safe handling temperature 40 C Wear protective clothing and gloves A place a suitable vessel underneath the drain If desired attach an 8 mm id tube on the drain slowly turn the drain plug until low is observed 3 8 Cole Parmer Section 4 Operation Heati ng The Cole Parmer Heating Immersion Circulators have a digital display and easy to use touch pad five programmable setpoint tempera
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14. 0 to 150 C Ambient 410 to 200 C Ambient 18 to 212 F Ambient 18 to 302 F Ambient 18 to 392 F 0 05 C 0 05 C 0 025 C 1 2 1 0 1 2 1 0 2 0 1 2 320 0 x 111 8 x 205 7 320 0 x 111 8 x 205 7 340 4 x 144 8 x 218 4 12 6 x 44 x 8 1 12 6 x 44 x 8 1 13 4x 5 7 x8 6 4 1 9 0 4 1 9 0 5 0 11 0 Force only Force only Force Suction e Lower process fluid temperature ranges available with supplemental cooling e Stability is measured as follows Heated baths Fluid is water at 70 C work area cover is on Baths run in factory ambient at nominal line voltage Pump speed set to high with no external pumping Refrigerated baths Fluid specific heat of 0 55 Btu Ib F at 10 C work area cover is on Baths run in factory ambient at nominal line voltage Pump speed set to high with short insulated loop on pump lines Stability is defined as Y the total span of measured data over approximately 30 minutes Pump testing is done with water at 20 C bath at nominal line voltage on high pump speed Approximately one meter loop on pump with flow transducer and 2 pressure transducers with a ball valve to adjust the flow rate Cole Parmer reserves the right to change specifications without notice Cole Parmer Section 2 General Information Stainless Steel Cooling Heating Circulating Baths Nameplate Part Number 1 C6 1 C6F 1 C15 1 C15 Catalog Part Number 115V 60Hz 12122 02 12122 16 12122 32 12122 46 230V 50Hz 12122 04 12122
15. 00 1200 Highlight the desired parameter and press 600 300 to view the available options Parity Noas Odd Even Data Bits 8 Stop Bits 1 2 Serial Type Baud Parity Data Bits See the Appendix for additional information 4 10 Cole Parmer Section 4 Operation Settings Display Options is used to view adjust the display s Temperature Units the Temperature Resolution the displayed Language and the Display Contrast and Display Delay 1 With Temp Unit highlighted press Ol Use the up down arrows to highlight the desired temperature scale Press 3 With Language highlighted press Use the up down arrows to highlight the desired language Scroll down for additional languages Press LI Deutsch O Francais L Espanol 2 With Temp Resolution highlighted press Use the up down artows to highlight the desired resolution Press E 0 01 4 With Display Contrast highlighted press Press e again and use the up down arrows keys to change the contrast With the desired con trast showing press again Contrast 32 NOTE Holding SSH for five seconds resets the display contrast to the default level and also brings up the language menu to change if needed the displayed language A 5 With Display Delay highlighted press o to enable disable it Use the up down arrows to highlight the time and press e again Use the up down arrows to change the value Once the desired delay is display
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17. 18 12122 34 12122 48 Temperature Range 20 to 100 C 20 to 100 C 28 to 100 C 35 to 100 C 4 to 212 F 4 to 212 F 18 to 212 F 31 to 212 F Bath Volume liters 5 4 6 5 5 4 6 5 6 8 8 6 6 8 8 6 gallons 1 4 1 7 1 4 1 7 1 8 2 3 1 8 2 3 Cooling Capacity watts 20 C 250 250 500 800 Refrigerant R134a R134a R134a R404a Dimensions H x W xL mm 622 3 x 203 2 x 416 6 426 7 x 467 4 x 416 6 650 2 x 259 1 x 4902 688 3 x 370 8 x 528 3 inches 24 5 x 8 0 x 16 4 16 8 x 18 4 x 16 4 25 6 x 10 2 x 19 3 27 1 x 14 6 x 20 8 Net Weight kg 26 3 29 0 35 8 54 9 Ib 58 0 64 0 79 0 121 0 Nameplate Part Number 2 C15 2 C15 Catalog Part Number 115V 60Hz 12122 36 12122 b2 230V 50Hz 12122 38 12122 54 Temperature Range 28 to 150 C 35 to 150 C 18 to 302 F 31 to 302 F Bath Volume liters 6 8 8 6 6 8 8 6 gallons 1 8 2 3 1 8 2 3 Cooling Capacity watts 20 C 500 800 na Refrigerant R134a R404a E aa J Dimensions x WxL mm 650 2 x 259 1 x 4902 688 3 x 370 8 x 528 3 n MC e 7x inches 25 6 x 10 2 x 19 3 27 1x14 6 x 20 8 L Cue w Net Weight kg 35 4 54 9 A a Ib 78 0 121 0 i Nameplate Part Number 3 C6 3 C6F 3 C15 3 C15 Catalog Part Number 115V 60Hz 12122 12 12122 26 12122 42 12122 56 230V 50Hz 12122 14 12122 28 12122 44 12122 58 Temperature Range 20 to 100 C 20 to 100 C 28 to 200 C 35 to 200 C 4 to 212 F 4 to 212 F 18 to 392 F 31 to 392 F Bath Volume liters
18. 2 26 12122 28 B 12122 32 12122 34 12122 36 12122 38 12122 42 12122 44 100 Time to Temperature Heating 90 g0 12122 42 c 12122 4 A 10 12122 56 5 60 pa B B 12122 32 S 50 12122 34 12122 36 5 12122 38 30 12122 46 20 12122 48 12122 52 10 12122 54 0 20 40 60 Time minutes Cole Parmer Section 2 General Information Stainless Steel Heating Circulating Baths Nameplate Part Number Catalog Part Number115V 60Hz 230V 50Hz 1W7 12134 60 12134 62 1 W11 12134 64 12134 66 1 W24 12134 68 12134 70 Temperature Range Ambient 10 to 100 C Ambient 18 to 212 F Ambient 10 to 100 C Ambient 18 to 212 F Ambient 10 to 100 C Ambient 18 to 212 F Bath Volume liters 5 1 6 5 7 5 9 5 15 4 19 6 gallons 1 3 1 7 2 0 2 5 4 1 5 2 Dimensions H x W x L mm 396 2 x 215 9 x 363 2 396 2 x 302 2 x 363 2 396 2 x 363 2 x 561 3 inches 15 6 x 8 5 x 14 3 15 6 x 11 9 x 14 3 15 6 x 14 3 x 22 1 Net Weight kg 10 0 11 3 15 9 Ib 22 0 25 0 35 0 Nameplate Part Number 2W7 2W11 2 W24 115V 60Hz 12121 02 12121 22 12121 42 230V 50Hz 12121 04 12121 24 12121 44 Temperature Range Ambient 10 to 150 C Ambient 18 to 302 F Ambient 10 to 150 C Ambient 18 to 302 F Ambient 10 to 150 C Ambient 18 to 302 F Bath Volume liters gallons 5 1 6 5 1 3 1 7 75 95 2 0 2 5 15 4 19 6 4 1 52 Dimensions H x W x L mm 396 2 x 215 9 x 36
19. 3 2 396 2 x 302 2 x 363 2 396 2 x 363 2 x 561 3 inches 15 6 x 8 5 x 14 3 15 6 x 11 9x 14 3 15 6 x 14 3 x 22 1 Net Weight kg 10 0 11 3 15 9 Ib 22 0 25 0 35 0 Nameplate Part Number 3W7 3 W11 3 W24 Catalog Part Number115V 60Hz 12121 06 12121 26 12121 46 230V 50Hz 12121 08 12121 28 12121 48 Temperature Range Low pump speed Ambient 10 to 200 C Ambient 18 to 392 F Ambient 10 to 200 C Ambient 18 to 392 F Ambient 10 to 200 C Ambient 18 to 392 F Temperature Range High pump speed Ambient 25 to 200 C Ambient 45 to 392 F Ambient 20 to 200 C Ambient 36 to 392 F Ambient 10 to 200 C Ambient 18 to 392 F Bath Volume liters gallons Sil e6 1 3 1 7 179 95 2 0 2 5 15 4 19 6 4 1 5 2 Dimensions H x W x L mm 414 0 x 215 9 x 363 2 414 0 x 302 2 x 363 2 414 0 x 363 2 x 561 3 inches 16 3 x 8 5 x 14 3 16 3 x 11 9 x 14 3 16 3 x 14 3 x 22 1 Net Weight kg 10 9 12 2 16 8 lb 24 0 27 0 37 0 Refer to nameplate on the back of the bath for part number Refer to pump curves on page 2 2 Lower temperature ranges available with supplemental cooling Overall dimensions Add 15 mm to L for drain fitting e Cole Parmer reserves the right to change specifications without notice 2 5 Cole Parmer 2 6 Section 2 General Information Performance Curves for Stainless Steel Heating Circulating Baths Time to Temperature Heating St
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22. 54 65 54 65 6 8 8 6 6 8 8 6 gallons 1 4 1 7 1 4 1 7 1 8 2 3 1 8 2 3 Cooling Capacity watts 20 C 250 250 500 800 Refrigerant R134a R134a R134a R404a Dimensions H x W x L mm 640 0 x 203 2 x 416 6 444 5 x 467 4 x 416 6 655 3 x 259 1 x 490 2 706 1 x 370 8 x 528 3 inches 25 2 x 8 0 x16 4 17 5 x 18 4 x 16 4 25 8 x 10 2 x 19 3 27 8 x 14 6 x 20 8 Net Weight kg 21 2 29 9 36 3 55 8 Ib 60 0 66 0 80 0 123 0 Refer to nameplate on the back of the bath for part number Refer to pump curves on page 2 2 Overall Dimensions Add 15 mm to L for drain fitting 2 3 Cole Parmer Section 2 General Information Performance Curves for Stainless Steel Cooling Heating Circulating Baths Heat Load watts Temperature C Temperature C 2 4 1000 900 800 700 600 500 400 300 200 100 Cooling Capacity 40 20 0 20 O A 12122 12 12122 28 40 60 Temperature C 12122 14 12122 26 PA O O O B 12122 02 12122 04 12122 16 12122 18 N co c 10 Time minutes A 12122 46 C 12122 16 12122 48 12122 18 12122 52 12122 26 12122 54 12122 28 12122 56 12122 58 D 12122 02 12122 04 B 12122 32 12122 12 12122 34 12122 14 12122 36 12122 38 12122 42 12122 44 100 A 12122 02 C 12122 46 12122 04 12122 48 12122 16 12122 52 12122 18 12122 54 12122 12 12122 56 12122 14 12122 58 1212
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26. Refrigerated baths should be left in an upright position for 24 hours at room temperature before starting This will ensure the lubrication oil has drained back into the compressor A The bath can operate with 0 clearance on two exhaust sides as long as the third exhaust side has untestricted air flow Blocked ventilation will increase the bath s temperature reduce its cooling capacity and on refrigerated bath eventually lead to premature compressor failure Ventilation Options The circulator construction provides protection against the risk of electrical shock by grounding appropriate metal parts The protection will not function unless the power cord is connected to a properly grounded outlet It is the user s responsibility to assure a proper ground connection is provided A The circulator is intended for use on a dedicated outlet Note If the circuit protector activates allow the temperature to cool before resetting Restart the circulator Contact us if it activates again A The circuit protection is designed to protect the circulator and is not intended as a substitute for branch circuit protection Position the bath so it is not difficult to operate the disconnecting device The circulator s power cord is used as the disconnecting device it must be easily accessible at all times A Refer to the nameplate on the rear of the circulator for specific electrical requirements Voltage deviations of 10 are permissible The outl
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28. ajue asjejague uapand ojos soIquie3 so Jopejo1juoa Jap ejjeyued e a ninsai s A SOIQUJE2 50 ueja3uea as 0100 a sa uo pepiun ej ap esadsa opou a eAnaesep A AIE uoioq 9153 do oz 2 oo 0 08 09 P sa JeJap so ue3l dx as jenuew ja u3 epenaja emejaduie ap joydnugjui a 1e3snfe esed ajuese pe opuew ja 991 opejonuoa Jap ejjeyued ej ua soiquieo sepuenB A Jezi e9 esed ais ugiquie pepiun e auenap as A eoueJe S ugioq e1s8 uo S9J0 e so 1ejsnfe A Jope o uoo op se eued se 10d asjezejdsap esed uan 1IS ugi2eBaneu ap SEYI ono sejs3 e eueg JeulDd 9 02 c7 FIe9S JoOd ey91eu ua ejsang Cole Parmer Compliance Warranty Unpacking Preface Refer to the Declaration of Conformity in the back of this manual Cole Parmer warrants to the direct purchaser that the Cole Parmer Polystat immersion circulators distributed by Cole Parmer will be free from defects in material or workmanship for a period of two years from the date of delivery Cole Parmer will repair or replace the product or provide credit as its sole option upon prompt notification and compliance with its instructions The Distributor warrants to Customer that upon prompt notification and compliance with Distributor s instructions that the Distributor will repair or replace at Distributor s sole option any Product which is defective in material or workmanship Distributor expressly d
29. allation 3 6 Chlorine Short term usage of tap water may not cause any adverse affects on the circulator or your application but in the long term problems may arise To help alleviate these problems Fisher Scientific recommends the use of chlorine The duration of time that chlorine remains in solution depends on factors such as water temperature pH and availability of direct sunlight We recommend maintaining chlorine levels at proper levels using chlorine test strips generally 1 to 5 ppm is adequate For best results maintain the fluid pH between 6 5 and 7 5 Do not add additional chlorine s without first determining the concentration ratio that already exists in the fluid supply Corrosion and degradation of the circulation components can result from concentration ratios that are too high Contact our customer support for additional information 5 C to 95 C Distilled Water or Deionized Water up to 3 MQ cm Normal tap water leads to calcareous deposits necessitating frequent circulator decalcification see table on next page Calcium tends to deposit itself on the heating element The heating capacity is reduced and service life shortened 30 C to 80 C Water with Glycol Below 5 C water has to be mixed with a glycol The amount of glycol added should cover a temperature range 5 C lower than the operating temperature of the particular application This will prevent the water glycol from gelling freezing near the
30. andard Standard Plus Circulators 100 A 12134 60 90 12134 62 A 12121 02 c 9 4 C 12121 04 o es 70 Sm B 12134 64 w 12134 66 2 50 12121 22 12121 24 S 40 30 20 10 0 20 40 60 80 100 120 140 Time minutes Time to Temperature Heating Advanced Circulator 00 A 12121 06 12121 08 B 12121 26 12121 28 D C 12121 46 gt 12121 48 5 Time minutes C 12134 68 12134 70 12121 42 12121 44 Cole Parmer Section 2 General Information Open Heating Circulating Baths Polyphenylene oxide PPO Circulating Baths Nameplate Part Number 1 W5P Catalog Part Number 115V 60Hz 12134 30 230V 50Hz 12134 32 1 W14P 1 W21P 12134 34 12134 38 13134 36 12134 40 Temperature Range Ambient 10 to 100 C Ambient 10 to 100 C Ambient 10 to 100 C Ambient 18 to 212 F Ambient 18 to 212 F Ambient 18 to 212 F 4 3 5 3 1 1 1 4 Bath Volume liters gallons 18 0 22 5 4 8 5 9 11 3 14 1 10 9 7 Overall Dimensions H x W x L mm 348 0 x 190 5 x 388 6 348 0 x 358 1 x 452 1 348 0 x 358 1 x 642 6 inches 13 7 x7 5 x 15 3 13 7 x14 1 x 17 8 13 7 x 14 1 x 25 3 Net Weight kg 5 4 6 8 7 7 Ib 12 0 15 0 17 0 Transparent Acrylic Circulating Baths Nameplate Part Number 1 W6A 1 W12A 1 W19A Catalog Part Number 115V 60Hz 12134 00 12134 04 12134 08 230V 50Hz 12134 02 12134 06 12134 10 Te
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34. bstances Directive ROHS Cole Parmer certifies that these Polystat models contain less than the following indicated amounts of the six ROHS banned substances with the exemption stated in Note 2 below containing up to 4 lead by weight Substance Threshold Level Lead Pb Less than 0 1 1 amp 2 Mercury Hg Less than 0 1 Hexavalent Chromium Cr VI Less than 0 1 Polybrominated Biphenyls PBB Less than 0 1 Polybrominated Diphenyl Ethers PBDE Less than 0 195 Cadmium Cd Less than 0 0196 Notes 1 Tolerated maximum concentration value by weight in homogeneous materials 2 Exemptions Lead as an alloying element in steel containing up to 0 3596 lead by weight aluminum containing up to 0 496 lead by weight and as a copper alloy Manufacturey s Authorized Representative r Mark Sinclair R amp D Manager D of C DWG 096221 4 Date 18 October 2011 Form 094233 REV 17 Apr 07
35. cm compensated to 25 C Unfavorably high total ionized solids TIS can accelerate the rate of galvanic corrosion These contaminants can function as electrolytes which increase the potential for galvanic cell corrosion and lead to localized corrosion such as pitting Eventually the pitting will become so extensive that refrigerant will leak into the water reservoir As an example raw water in the United States averages 171 ppm of NaCl The recommended level for use in a water system is between 0 5 to 5 0 ppm of NaCl Recommendation Initially fill the tank with distilled or deionized water Do not use untreated tap water as the total ionized solids level may be too high This will reduce the electrolytic potential of the water and prevent or reduce the galvanic corrosion observed 3 7 Section 3 Installation Additional Fluid When working with fluids other than water Do not use any fluid until you have read and understood the label and Precautions the Material Safety Data Sheet MSDS Do not blend any fluids Ensure any fluid residue or any other material is thoroughly removed before filling the bath with a different fluid Always wear protective clothing especially a face shield and gloves e Avoid spattering on any of the circulator s components always slowly add fluid When adding point the opening of a container away from yourself Use fume hoods Filli ng Requireme nts Ensure the reservoir drain
36. dling or draining A Never operate damaged or leaking equipment or with any damaged cords A Never operate the circulator or add fluid to the reservoir with panels removed A Do not clean the circulator with solvents only use a soft cloth and water A Drain the bath before it is transported and or stored in near or below freezing temperatures Always turn the circulator off and disconnect the supply voltage from its power source before moving or before performing any service or maintenance procedures A Transport the circulator with care Sudden jolts or drops can damage the its components A Refer service and repairs to a qualified technician A Performance of installation operation or maintenance procedures other than those described in this manual may result in a hazardous situation and will void the manufacturer s warranty A 1 2 Cole Parmer Description Intended Use Sample Nameplate Equipment Ratings Cole Parmer Section 2 General Information The Cole Parmer Polystat Heating Immersion Circulators are used with cooling heating and heating baths All circulators can pump to an external system All have a digital display and easy to use touch pad five programmable setpoint temperatures acoustic and optical alarms and offer adjustable high temperature protection The circulating bath is used as a temperature controlled bath or to circulate to an application fluid to an externally to an application It is designed f
37. ed press Cole Parmer Dela With Display Delay enabled and the Start Display showing if no arrows are pressed the Start Display will change to the Status Display after the delay expires 4 11 Section 4 Operation System Messages is used to view any Warning or Fault messages 1 With Messages highlighted press o to display the options VVarnings System Run Time is used to view the circulator Unit and pump operating hours 1 With Run Time highlighted press o to display the times xxx hours A xxx hours System Configuration is used to view the circulator s configuration 1 With Configuration highlighted press 0 to display the settings Head 1 NOTE Heating baths display Bath Unknown A FW XXXXXXX A Checksum XXXX Bath C6 115V FW XXXXXXX A 4 12 Cole Parmer Section 4 Operation System Password Reset is used only by a qualified technician Changing the password enables circulator reset options the temperature sensor calibration procedure and displays PID values 1 With Password Reset highlighted press 2 Press and change the number to 1 to display Level Passvvord Passvvord 3 Press 0 to display Level Operator A NOTE The circulator resets to the User mode whenever it is turned off The display also resets to Password L the User mode whenever the Start Status Dis Reset play is displayed continuously for 10 minutes A Calibration Scroll down to disp
38. ed with a value W A value that can be requested in a read command or sent as patt of a set command Winx Maximum allowed value Part of error message when set value is too high V un Minimum allowed value Part of error message when set value is too low Value Read commands return analog V or bit B values or settings while set commands send analog or bit settings Read commands return values with the same displayed precision Set command messages missing the space character between the command and the setting will be rejected as the user s intent is unclear Units A read command returning an analog V value or setting will include the units U associated with that value or setting A set command sending an analog value will not include the units The units returned by the complementary read command are assumed Termination character A carriage return CR is used to terminate command and response messages Typically the Enter key on the keyboard Note The inter character timeout time between transmitted characters is set to 30 seconds Exceeding the timeout will clear the receiver buffer and require the message to re retransmitted Note Special characters backspace delete insert etc are not recognized by the protocol and generate error responses Commands Table Commands All messages from master and slave are terminated with a carriage return CR Command Description Notes Master Sends ua S
39. er key again If Auto Restart is enabled the circulator will restart if disabled use the Start Up procedure NOTE We recommend periodically rechecking operation or if the circulator is moved A Cole Parmer 4 15 Section 4 Operation 4 16 Stopping the Circulator Power Down Shut Down Restarting Ensure the stop symbol is highlighted if not use the arrow keys to navi gate to the symbol Press The circulator will stop and the stop symbol will turn into a start symbol Stop Symbol 7 E Press O The display will go blank Place the circuit protector on the front of the circulator to the O position Using any other means to shut the circulator down can reduce the life of the compressor A Always turn the circulator off and disconnect it from its supply voltage before moving A The circuit protector located on the front of the circulator is not intended to act as a disconnecting means A NOTE When quickly restarting the compressor may take up to 10 min utes before it starts to operate A Cole Parmer Cleaning Condenser Fins Cole Parmer Hoses Section 5 Preventive Maintenance Laboratory Grade Ethylene glycol EG is poisonous and flammable Before performing any preventive maintenance refer to the manufacturer s most current MSDS for handling precautions A Disconnect the power cord prior to performing any maintenance A Handle the circulator with care sudden jolts or dro
40. et must be rated as suitable for the total power consumption of the bath see below Cole Parmer Section 3 Installation Ensure the electrical cords do not come in contact with any of the plumbing connections or tubing A Ensure all communication and electrical connections are made 44 CAUTION prior to starting the circulator and that the cords do not come in contact with any of the plumbing connections or tubing A For refrigerated baths ensure the line cord from the bath is securely connected to the rear of the circulator For all ensure the communications cable from the bath is connected to the RJ45 connectors similar to Ethernet on the rear of the circulator For all connect the supplied line cord to the circulator and to a properly grounded outlet The following power options ate available Unit Volts Hertz Phase Amps Total Wattage Plug Type C6 C6F 115 60 1 11 5 1328 N5 15 1 230 50 1 6 8 1573 Country Specific C6 C6F 115 60 1 11 5 1328 N5 15 3 230 50 1 10 3 2373 Country Specific C15 115 60 1 11 7 1345 N5 15 1 2 230 50 1 6 9 1596 Country Specific C15 115 60 1 11 7 1345 N5 15 3 230 50 1 10 4 2396 Country Specific C15 115 60 1 14 4 1662 N5 20 1 2 230 50 1 7 8 1798 Country Specific C15 115 60 1 14 4 1662 N5 20 3 230 50 1 11 3 2598 Country Specific All Heated Units 115 60 1 96 1104 N5 15 1 2 230 50 1 5 8 1338 Country Specific All Heated Units 115 60 1 11
41. evaporating coil Excess glycol deteriorates the temperature accuracy due to its high viscosity other temperatures SIL 200 5150 and 6200 only SIL 300 6200 only Silicone oil with a long life span over 1 year and negligible smell SYNTH 260 6200 only Synthetic thermal liquid with a medium life span several months and little smell annoyance Heat transfer fluids are supplied with an EC Safety Data Sheet Ensure when selecting the heat transfer fluid that no toxic gases can be generated Flammable gases can build up over the fluid during usage A Cole Parmer Cole Parmer Section 3 Installation Ensure the over temperature cut off point is set lower than the fire point for the heat transfer fluid selected A The highest working temperature as defined by the EN 61010 IEC 1010 must be limited to 25 C below the fire point of the bath fluid A Water Quality and Standards Process Fluid Permissible PPM Desirable PPM Microbiologicals algae bacteria fungi 0 0 Inorganic Chemicals Calcium lt 25 lt D 6 Chloride 25 10 Copper 13 1 0 0 020 ppm if fluid in contact with aluminum Iron 0 3 0 1 Lead 0 015 0 Magnesium 12 401 Manganese lt D 05 lt D 03 Nitrates Nitrites lt 10 as N 0 Potassium 20 0 3 Silicate 25 1 0 Sodium 20 0 3 Sulfate 25 1 Hardness 17 0 05 Total Dissolved Solids 50 10 Other Parameters pH 6 5 8 5 7 8 Resistivity 0 01 0 05 0 1 MQ
42. h temperature protection and low liquid level protection must be checked at regular intervals We recommend checking at least twice a year or if the circulator is moved High temperature protection Set a cut off temperature that is lower than the desired setpoint temperature Switch on the circulator and ensure it shuts down at the set cut off temperature If the circulator does not shut down have the it checked by a qualified technician Reset the safety to the desired temperature Acrylic units maximum high temperature setting should be limited to the temperature indicated on the label on the front of the bath 80 C A Low liquid level protection With the circulator on use a screwdriver and slowly push down on each sensor until the error message indicated below appears See Section 6 for details on error messages If either message does not appear have the circulator checked by a qualified technician FAULT LLC HTC Low Level Fault Low Level Cutout PRESS ENTER Advanced only Cole Parmer Cole Parmer Error Displays Section 6 Troubleshooting Error messages are cleared by pressing the enter key O Once the cause of the error message is identified and corrected to restart the circulator on circulators with an HTC error press the black ring surrounding the red dial and then for all circulators press the enter key again If Auto start is enabled the circulator will restart if disabled use the Start Up pr
43. he circulator using only the supplied line cord The circulator s power cord is used as the disconnecting device it must be easily accessible at all times A Section 1 Safety Never operate the bath without fluid in the reservoir A Ensure the electrical cords do not come in contact with any of the plumbing connections or tubing A Never place the circulator in a location or atmosphere where excessive heat moisture or corrosive materials are present A Ensure the tubing you select will meet your maximum temperature and pressure requirements A Ensure all communication and electrical connections are made prior to starting the circulator A Many refrigerants which may be undetectable by human senses are heavier than air and will replace the oxygen in an enclosed area causing loss of consciousness Refer to the circulator s nameplate and the manufacturer s most current MSDS for additional information A Other than water before using any fluid or when performing maintenance where contact with the fluid is likely refer to the manufacturer s MSDS and EC Safety Data sheet for handling precautions A Ensute that no toxic gases can be generated by the fluid Flammable gases can build up over the fluid during usage A When using ethylene glycol and water check the fluid concentration and pH on a regular basis Changes in concentration and pH can impact system performance A Ensure the fluid is at a safe temperature 20 C to 40 C before han
44. high temperature protection limit exceeded check limit setting check fluid selection it can take over 10 minutes for the motor temperature to get low enough before the circulator can be restarted MOL allow circulator to cool down Motor Overload Open RTD1 open internal temperature sensor Internal Open RTD2 open external temperature sensor External Shorted RTD1 shorted internal temperature sensor Internal Shorted RTD2 shorted external temperature sensor External Warning Displays The circulator will continue to run with a warning A warning also sounds the alarm if enabled Bad Calibration High Temperature adjustable high temperature protection limit exceeded check limit setting check fluid selection Low Level reservoir fluid level too low for safe operation check fluid level Low Temperature adjustable low temperature protection limit exceeded check limit setting check fluid selection Cole Parmer Cole Parmer Checklist Section 6 Troubleshooting Circulator will not start Check for error codes see Error Codes in this section Ensure the circuit protector is in the on 1 position Make sure supply voltage is connected and matches the unit s nameplate rating 10 No display Recycle the circulator s circuit protector Circulator will not circulate process fluid Check the reservoir level Fill if necessary Check the application for restrictio
45. irements for electrical equipment for measurement control and laboratory use Part 2 010 Particular requirements for laboratory equipment for the heating of materials Manufacturer s Authorized Representative Date 18 October 2011 Mark Sinclair R amp D Manager DofC 096221 1 Form 094233 DWG 096221 REV 17 Apr 07 RoHS DECLARATION OF CONFORMITY Manufacturer Cole Parmer Address 625 East Bunker Court Vernon Hills IL 60061 Products Polystat cooling heating and heating liquid baths non refrigerated heating liquid baths and immersion liquid circulators with the following bill of material numbers 212111100 212111800 212112100 212112800 212113100 212113800 212114100 212114800 212115100 212115800 212116100 212116800 212117100 212117800 212118100 212118800 212119100 212119800 212131100 212131800 212132100 212132800 212133100 212133800 212134100 212134800 212180100 212180800 212190100 212190800 212211100 212211800 212212100 212212800 212213100 212213800 212233100 212233800 212234100 212234800 212280100 212280800 212290100 212290800 212311100 212311800 212312100 212312800 212313100 212313800 212331100 212331800 212332100 212332800 212333100 212333800 212334100 212334800 212390100 212390800 All models rated 115 Volts 60 Hz or 230 Volts 50 Hz Cole Parmer certifies that the above Polystat models meet the requirements of DIRECTIVE 2002 95 EC Restriction of Hazardous Su
46. is manual please contact us DANGER indicates an imminently hazardous situation which if not avoided result in death or serious injury WARNING indicates a potentially hazardous situation which if not avoided could result in death or serious injury CAUTION indicates a potentially hazardous situation which if not avoided may result in minor or moderate injuty It is also be used to alert against unsafe practices The lightning flash with arrow symbol within an equilateral triangle is intended to alert the user to the presence of non insulated dangerous voltage within the circulator s enclosure The voltage magnitude is significant enough to constitute a risk of electrical shock This label indicates the presence of hot surfaces This label indicates read the manual Observe all warning labels A Never remove warning labels A Refrigerated circulators should be left in an upright position for 24 hours before starting This will ensure the lubrication oil has drained back into the compressor A The circulator s construction provides protection against the risk of electrical shock by grounding appropriate metal parts The protection will not function unless the power cord is connected to a properly grounded outlet It is the user s responsibility to assure a proper ground connection is provided A The circuit protector located on the rear of the circulator is not intended to act as a disconnecting means A Operate t
47. isclaims all other warranties whether expressed implied or statutory including the warranties of merchantability and fitness for a particular purpose Distributor s sole responsibility and the Customer s exclusive remedy for any claim arising out of the purchase of any Product is repair or replacement as described above In no event shall Distributor s liability exceed the purchase price pain therefor nor shall Distributor be liable for any claims losses or damage of any third party or for lost profits or any special indirect incidental consequential or exemplary damages howsoever arising even if Distributor has been advised of the possibility of such damages Retain all cartons and packing material until the circulator is operated and found to be in good condition If the circulator shows external or internal damage contact the transportation company and file a damage claim Under ICC regulations this is your responsibility Cooling heating circulators should be left in an upright position at room temperature for 24 hours before starting This will ensure the lubrication oil has drained back into the compressor A Preface ii Cole Parmer Cole Parmer Safety Warnings A DANGER PE D Section 1 Safety Make sure you read and understand all instructions and safety precautions listed in this manual before installing or operating your circulator If you have any questions concerning the operation or the information in th
48. l Communications Protocol Serial communication is accomplished through the USB port on the chiller If your operating system does not automatically recognize the optional driver log on to http www ftdichip com FTDrivers htm for instructions Note This appendix assumes you have a basic understanding of communications protocols Information on the NC STANDARD and NAMUR protocols is available upon request A Note Keypad operation is still available with serial communications enabled A All commands must be entered in the exact format shown in the tables on the following pages The tables show all commands available their format and responses Chiller responses are either the requested data or an error message The chiller response must be received before the host sends the next command The host sends a command embedded in a single communications packet then waits for the chiller s response If the command is not understood the chiller responds with an error command Otherwise the chiller responds with the requested data Commands are not case sensitive Upper or lower case letters may be used Commands are listed in the Commands Table error responses are given in the Errors Table and symbols are shown in the Key Table Symbol Meaming B A binary value 0 or 1 0 Off FALSE or Disable d 1 On TRUE or Enable d CR Carriage return used as the termination character U Text representing the units associat
49. l O3 Avorre UMOP 94 Surssoad doo QU Y 38 3x JO SOUN DAY Ae dsrp was s s um s ATUO UB z rfonuuo v IIUIS nua nuew 931 nusw Section 4 Operation Settings Application Settings is used to view adjust the five Setpoints and Real Temperature Adjustments RTA enable disable the alarms change the fluid type set the pump speed configure the interfaces optional set the clock turn the timer on or off and turn auto restart and en ergy savings on ot off 1 With Application Settings highlighted 2 Scroll down for additional options press to view Interfaces Pump Adjustment 3 With Setpoints highlighted press to display the list Use the up down artows to highlight the desired SP NOTE Use the down arrow to display SP5 A SP1 XX X If this temperature on the Start Status Display does not accurately reflect the actual temperature in the reservoir an RTA can be applied The RTA can be set 10 C 18 F As an example if the circulator s temperature is stabilized and displaying 20 C but a calibrated reference thermometer reads 20 5 C the RTA should be set to 0 5 C After you enter a RTA value allow it to stabilize before verifying the temperature in the bath NOTE If display accuracy is required we recom mend repeating this procedure at various setpoint temperatures and on a regular basis A NOTE You cannot adjust the setpoint closer than 0 1 C to either of the fluid s system limits see
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51. lave 2525 Read Temperature Internal RT VIC FR Read Temperature 2 External RT2 VC FK Read Displayed Setpoint RS VIC FR Read Setpoint X X 1 to 5 RSX VIC FK Read High Temperature Fault RHTF VIC FK Read High Temperature Warn RHTW VIC FK Read Low Temperature Fault RLTF V C FK Read Low Temperature Warn RLTW V C FK Read Proportional Heat Band Setting RPH V Read Proportional Cool Band Setting RPC V fr Read Integral Heat Band Setting RIH V Repeats per minute Read Integral Cool Band Setting RIC MV JRepeats per minute Read Derivative Heat Band Setting RDH V Minutes Read Derivative Cool Band Setting RDC U Minutes Read Temperature Precision RTP IVI Read Temperature Units RTU V3 Read Unit On RO B Read External Probe Enabled RE B Read Auto Restart Enabled RAR B Read Enetgy Saving Mode REN B Read Time RCK hh mm ss Read Date RDT mmi ddl yyyy or ddl mim yyyy Read Date Format RDF MM DD YYYY or Commands All messages from master and slave are terminated with a carriage return CR Command Description Notes Master Sends Sample Slave Response echo off Alternate units Read Firmware Version RVER V Read Firmware Checksum RSUM V Set Displayed Setpoint SS V OK Set Setpoint X X 1 to 5 SSX V OK Set High Temperature Fault SHTF T OK Set High Temperature Warning SHTW OK Set Low Temperature Fault SLTF UJ OK Set Low Temperature Warning SLTW OK Set Propo
52. lay PID Tuning see page 4 15 1 If desired highlight Reset and press o to display Reset user settings Reset PID settings Reset both Highlight the desired reset option and press 7 A confirmation message will appeat press 0 again Cole Parmer 4 13 Section 4 Operation 1 To calibrate the temperature sensor highlight Calibration and press to display NOTE Ensure the RTA is set to O before doing a calibration A Internal RTD External RTD 3 With Calibrate highlighted press to display Internal RTD Lovv 5 Press 7 and enter the desired calibration temperature nternal RTD Calibrate 2 With the desired sensor highlighted press o to display Calibrate Restore User Cal Save User Cal 4 Highlight the SP temperature box and enter either the desired high or low setpoint value Internal RTD High 6 Highlight Calibrate and the press 0 to complete the procedure Internal RTD High Low 0 11 113 SP 7 Repeat for the other calibration point Once the calibration is complete you can store it into the circulator s memory by selecting Save User Cal and pressing You can later restore the same calibration by highlighting Restore User Cal and pressing 1 Another option is to restore the factory calibration values by highlighting Restore Factory Cal and pressing 7 The Save Factory Cal option is designed to be used only by a qualified technician 4 14
53. mperature Range Ambient 10 to 80 C Ambient 18 to 176 F Ambient 18 to 176 F Ambient 18 to 176 F Ambient 10 to 80 C Ambient 10 to 80 C 5 5 7 0 1 5 1 8 Bath Volume liters gallons 10 1 12 8 2 7 3 4 15 6 19 9 4 1 5 3 Overall Dimensions H x W x L inches 13 3x 7 4x 16 7 Net Weight kg 5 9 Ib 13 0 mm 337 8x188 0 x 424 2 337 8 x 353 1 x 365 8 337 8 x 353 1 x 543 6 13 3 x 13 9 x 14 4 13 3 x 13 9 x 21 4 7 7 9 1 17 0 20 0 Refer to nameplate on the back of the bath for part number Refer to pump curves on page 2 2 Lower temperature ranges available with supplemental cooling Add 6 mm to L for drain fitting Cole Parmer reserves the right to change specifications without notice Wetted Materials Immersion Circulators Viton EPDM Ryton Ultem Vectra Stainless Steel 2 7 Stainless Steel Circulating Baths Stainless Steel 316 Stainless Steel 304 EPDM drain fitting Ryton Zotek N cover seal Transparent Acrylic Circulating Baths Poly acryl Polyphenylene oxide PPO Circulating Baths Polyphenylenoxid Cole Parmer Section 2 General Information 2 8 Cole Parmer Section 3 Installation Immersion Circulator The immersion circulator is designed for continuous operation and for indoor use Only Never place the immersion circulator in a location where excessive heat moisture inadequate ventilation or corrosive materials a
54. n of bits BO b5 unused Vi B6 rtdl shorted B7 rtdl open BO HTC fault V2 Bl high RA temperature fault B2 b7 unused BO low level warn Bl lo temperature warn B2 high temperature warn B3 low level fault ie B4 lo temperature fault B5 high temperature fault B6 low temperature fixed fault B7 high temperature fixed fault BO PWM heat duty cycle gt 0 Bl compressor On Off B2 Pump On status B3 Unit On status 2 B4 Unit Stopping B5 Unit fault status B6 unused B7 Beeper On status BO Pump speed fault Bl MOL fault B2 HPC fault B3 Cool Icon On steady unit is cooling at max capacity Vs B4 Cool Icon flashing unit is B5 Heat Icon On steady B6 Heat Icon flashing B7 External sensor controlling Refer to Key table on page 1 for explanation of symbols and their meanings Examples Set Setpoint Read Temperature Host Host ST S 2 0 cr RIT CR DENET v ICR Controller Controller CR L3 kol 101 CR Command CR V U CR Accepted Read Temperature 2 Hos RIT 2 CcR Controller 2 101 ala CR Set Setpoint to 22 C when minimum allowed is 20 C Minimum allowed is V Hes S S ffr LILI 1 Controller 2 M i fafi m ujm Jajtjifo wjefaf Fi si 2 0 CR DECLARATION OF CONFORMITY Manufacturer Cole Parmer Address 625 East Bunker Court C Vernon Hills IL 60061 Year of inception 201 1 We decla
55. nd the display brings up the Main desired setting and then press to bring up Menu Display additional submenus s i Menu Application Setinas Settings Display Options See page 4 7 Messages Run Time Configuration Password Reset See page 4 12 Menu The Menu line at the bottom of all the submenu displays is another way to return the circulator back to the Main Menu Display 1 From any submenu display use the down 2 Press 0 to return to the Main Menu arrow button to highlight Menu Display Application Settings SP1 A Men Display Options Settings Pressing from the Menu line returns you to the previous screen Cole Parmer 4 5 Section 4 Operation E 09 ejeq syne3 r suuely eiqipny S Kejeq ejdsig I sg dois 1 l 918 6120 ce lSejuoo I Aed I Lu pneg sequod edsa H i wuwoo eues O00Z inej mo7 I i I 9002 Bululemn MO o et sore 900 8 Buruuem U IH SIEDUEI i i 900 8 unea UBIH I I yojneq I 3J4O eieg swew einigJjeduiel usifBu3 Ee El wey s um s did ME qonesqileo 20585 rouen o9 185 Em josey 2 1X9 Vid jut V pe NO1 sBuliAes 61 u3 Sun dwa juauysn py dwind So J9JEM ie nO 00 9 He s M oiny ed spin 4 sjuiodjes ou uny uonnjoses dua sjne EN 4 suondo Aeldsig sBunjeg voneoddy I suondo Aue m m seGessew
56. ns in the cooling lines The pump motor overloaded The pump s internal overtemperature overcurrent device will shut off the pump causing the flow to stop This can be caused by low fluid debris in system operating circulator in a high ambient temperature condition or excessively confined space Allow time for the motor to cool down Make sure supply voltage matches the circulator s nameplate rating 10 Inadequate temperature control Verify the setpoint On refrigerated baths make sure the condenser is free of dust and debris Check the fluid concentration Ensure installation complies with the site requirements in Section 3 Make sure supply voltage matches circulator nameplate rating 210 If the temperature continues to rise make sure your application s heat load does not exceed the rated specifications Check for high thermal gradients e g the application load is being turned on and off or rapidly changing Circulator shuts down Ensure button wasn t accidently pressed Ensure the circuit protector is in the on 1 position Check for error codes Make sure supply voltage is connected and matches the circulatot s nameplate rating 110 Restart the circulator 6 3 Section 6 Troubleshooting 6 4 USB Driver Not Recognized If your operating system does not automatically recognize the optional driver log on to http www ftdichip com FTDrivers htm for instructions Cole Parmer Appendix AC Seria
57. ocedure FAULT HTC Low Level Fault PRESS ENTER Error Message Typical Fault Displays SP typical The heating element pump and if applicable refrigeration shut down with a fault A fault also sounds the alarm if enabled Message Action High Fixed Temp circulator s nonadjustable high temperature protection limit exceeded check fluid selection check environmental conditions High Temperature adjustable high temperature protection limit exceeded check limit setting check fluid selection ensute circulator has adequate ventilation High Temperature check voltage supply Refrigeration the refrigeration may need servicing HPC check for obstructions to air flow High Press Cutout the refrigeration may need servicing HTC Low Level if the fluid level is greater than approximately Fault 5 5 cm below the tank top it is a low level fault Fill fluid to proper level if not high temperature protection limit exceeded check limit setting allow circulator to cool down to at least 10 C cooler than the HTC setting reset HTC by pressing black ring set HTC to desired setting 6 1 Section 6 Troubleshooting 6 2 LLC Low Level Cutout Low Fixed Temp Low Temperature reservoir fluid level too low for safe operation check fluid level check for leaks circulator s nonadjustable low temperature protection limit exceeded check fluid selection adjustable
58. or continuous operation on a bench top and for indoor use in accordance with all the procedures and requirements stated in this manual e 32 Cole Parmer 1 800 323 4340 BOM XXXXXXXXXXXX 1 SIN POLYSTAT Y ZZZ 115V 60HZ 1 R134A XXX OZ HI XXX PSIG LOW XXX PSIG 1 1 Use the nameplate on the rear to identify your immetsion circulator circulating bath its electrical requirements and if applicable the refrigeration data Y identifies the circulator and if applicable ZZZ the bath For example 1 C6 The corresponding Cole Parmer catalog part numbers are listed in the specification tables in this section Ambient Temperature Range 10 C to 40 C 50 F to 104 F Maximum Relative Humidity 80 at 31 C 88 F Operating Altitude Sea Level to 2000 meters 6560 feet Overvoltage Category il Pollution Degree 2 Degree of Protection IP 20 Section 2 General Information Nameplate Part Number Catalog Part Number 115V 60Hz 230V 50Hz Process Fluid Temperature and Setpoint Range Temperature Stability Heater Capacity KWatts 230V 115V Overall Dimensions HxWxD mm Inches Net Weight kg lb Pump Type Pumping Capacity Pressure mbar Digital Immersion Circulator Standard 1CL 1BR Standard Plus 2CL 2BR Advanced 3CL 12120 01 or 12120 08 12120 03 or 12120 11 12120 13 12120 02 or 12120 09 12120 04 or 12120 12 Ambient 410 to 100 C Ambient 41
59. polystat cf Cole Parmer Heating Immersion Circulators Cooling Heating Circulating Baths Heating Circulating Baths Manual P N U01165 Rev 10 18 2012 CE User s Manual Cole Parmer Quick Starts Preface Section 1 Section 2 Section 3 Section 4 Table of Contents I Complicado 1 bic i Unpacking has aha 1 Safety iii iii ii 6 1 1 Safety AT alas al q d amal at at cu 1 1 General Informatiopn J J J 2 1 Descrip 2 1 intended iei cnica inicio sas 2 1 Sample Dlatmeplab aia iia aia 2 1 Equipinent Batini apasiona 2 1 DDBCHICQHONMS it odia 2 2 Wetted PATES cet o a bl ata at alai 2 7 Installation cis oa 3 1 Jinmersi n Circulator Olarra 3 1 Circulatiao Baths aaa 3 2 a A o pp dap era 3 2 Electrical Requires anita 3 2 Remote Temperature BENSON ainia papa 3 4 Juxtermal Pinal ADIO ft d at t pita m d aa ja a aaa 3 5 Approved iiny ith a a 3 5 Additional Fluid Precautions a a do R n pa 3 8 Filing Requitements coapta enuei p A 3 8 DANE oido a dada a 3 8 o nn 4 1 Controle 4 1 qo unla a da a a d 77 4 2 Start Umata tata 4 2 Stats Display naaa 4 3 ici spdhore il qasa 4 3 Chasing the Span a Hp smi i PUT pt 4 4 Mero Lip m
60. ps can damage its components A There are no user serviceable components within the equipment panels After time the circulator s stainless steel surfaces may show spots and become tarnished Normal stainless steel cleaners can be used Clean the bath vessel and built in components at least every time the bath liquid is changed Use water and a soft cloth Do not use scouring powder A The inside of the bath must be kept clean in order to ensure a long service life Substances containing acidic or alkaline substances and metal shavings should be removed quickly as they could harm the surfaces causing corrosion If corrosion e g small rust marks should occur in spite of this cleaning with stainless steel caustic agents has proved to be suitable These substances should be applied according to the manufacturer s recommendations For cleaning the baths do not use any substances which contain solvents A For refrigerated baths in order to maintain the cooling capacity of the bath clean the fins two to four times per year depending on the operating environment Switch off the circulator and unplug the power cord Clean the fins with compressed air For extreme soiling a qualified technician will need to remove the cooling compressor casing Inspect and tighten the circulatot s external hoses and clamps daily 5 1 Section 5 Preventive Maintenance Testing the Safety Features 5 2 The safety features for hig
61. re present A into the bath or that its line cord does not make contact with the bath contents A A CAUTION Carefully install the immersion circulator to ensure it does not fall Immersion Circulators come with either an adjustable clamp or are mounted on an adjustable bridge For immersion circulators equipped with a clamp Attach and secure the clamp to your bath container The maximum wall thickness is 25 mm 1 immersion depth is 75 to 145 mm 3 to 5 2 Your bath container must be sturdy enough to support the weight of the assembly approximately 3 8 kilograms 8 5 pounds For immersion circulators equipped with a bridge The bridge is designed to fit baths that are 400mm to 800 mm wide Slide the bridge support rods to the desired length and secure them in place with the supplied eight 3 mm Phillips Head screws If possible secure the bridge to your bath using the two supplied thumb screws The immersion depth is 75 to 145 mm 3 to 5 Your bath container must be sturdy enough to support the weight of the assembly approximately 3 8 kilograms 8 5 pounds Cole Parmer 3 1 Section 3 Installation 3 2 Circulating Baths Ventilation Electrical Requirements The circulator is designed for continuous operation and for indoor use Never place the bath in a location where excessive heat moisture inadequate ventilation or corrosive materials are present A
62. re that the following products conform to the Directives and Standards listed below Products Polystat cooling heating and heating liquid baths non refrigerated heating liquid baths and immersion liquid circulators with the following bill of material numbers 212111100 212111800 212112100 212112800 212113100 212113800 212114100 212114800 212115100 212115800 212116100 212116800 212117100 212117800 212118100 212118800 212119100 212119800 212131100 212131800 212132100 212132800 212133100 212133800 212134100 212134800 212180100 212180800 212190100 212190800 212211100 212211800 212212100 212212800 212213100 212213800 212233100 212233800 212234100 212234800 212280100 212280800 212290100 212290800 212311100 212311800 212312100 212312800 212313100 212313800 212331100 212331800 212332100 212332800 212333100 212333800 212334100 212334800 212390100 212390800 All models rated 115 Volts 60 Hz or 230 Volts 50 Hz Equipment Class Measurement control and laboratory Directives and Standards 2004 108 EC Electromagnetic Compatibility EMC Directive EN 61326 1 2006 Electrical equipment for measurement control and laboratory use EMC Requirements EMC Class A 2006 95 EC Low Voltage Directive LVD EN 61010 1 2001 Safety requirements for electrical equipment for measurement control and laboratory use General Requirements EN 61010 2 010 2003 Safety requ
63. ro INE NDID ur NESATU ojsm joy uio puty f q JOISIDO A PIX u1291s s UJ91XO U29 uodwod f q pnoH rq yn u212z siseq ro do usjjoisroo A JOA STU 310439823 19d NA 8 1 2 W ge rq do Sunols neoaru Ste op 3uvuoAoq op puo 8 s Dub y 32249360 liq do ypaon SUIMNYISIVEA nvoAru See aq Zurpro putu op orz am IWH ua d rod arun ap APTOS SNTWO LS u rq tuere run ap yl ONIMAHOSAV VA Veu See uao rq USULONIOOA 9 UISTOU WO JNA n JPPIOOA peq JOY l SJopnou An sed NA Jun n 3ep300A PIDP EMIDA Srpuo33 UASI 1004 sU2423 SIOZ uayo soSuve ulrz poos uogunm suveSurpro AV IEP uo SI 2 0 527 JUN DP ULA JULYIOOA DP Ut HOAIISI JOY UBA 3100d320Ajt JO 122 031u07 U23J9OUJ 293IEA UD yerd pa x 3lrq jour UIpPIOA u sun nisueeSuipr uouuny ymaq d peq 3uJ9 Uui 194 UE n J99UUtA JOU 3SEA uosunm sueeSulpro 192 e UAANOAIS UIPIOM PU u urpi JOISPO A o3xmaqo3 uva y r yucuye sr LPLIDICUISUTPIO ASIA PY e ua xppusimgsuee uope12ui rq 1990 Sou ipy 5 arp yeyar ddo urpr y do asoy 1937 101 uo1njejoduroisjfrpoq 23oq 199Z Oye nom iq xfiposour agorp oz Surssedooa op seed ua 193ourerp 2391018 use Jou FUPI uoo Jho Sow sees xmaqoc aramqus
64. rtional Heat Band Setting SPH T 7 OK Set Proportional Cool Band Setting SPC V OK Set Integral Heat Band Setting SIH T7 OK Set Integral Cool Band Setting SIC T7 OK Set Detivative Heat Band Setting SDH V OK Set Derivative Cool Band Setting SDC T OK Set Temperature Resolution STR U OK Set Temperature Units STU V OK Set Unit On Status SO B OK Set External Probe On Status SE B OK Set Auto Restart Enabled SAR B OK Set Energy Saving Mode SEN V OK Set Pump Speed SPS V L H OK Errors Table Errors Error Description Notes Slave Responds Not defined not implemented or incorrectly formatted Unsupported command Extra characters Format error Set value too high Maximum allowed is 7 Set value too low Minimum allowed is Vun Argument to binary set command not 0 or 1 Value must be 0 or 1 Set command attempted while in read only mode Mode is read only Set command failed e g SO 1 with low level Failed RUFS Read Unit Fault Status This command returns 5 values These are decimal representations of hexadecimal values Each individual bit of the value represents a different warning fault or status decimal hex B7 B6 B5 B4 B3 B2 Bl BO 1 1 0 0 0 0 0 0 0 1 2 2 0 0 0 1 4 4 0 0 0 0 0 1 0 0 8 8 0 Oo CO O tf WO O 16 10 0 0 0 1 0 0 0 0 32 20 0 01 64 40 0 1 0 0 0 0 0 0 128 80 1 0 0 0 0 0 0 0 Value Descriptio
65. s prose oT Un oq Surg 230joq paowa uSnoszou1 sr onprsox Aur 23nsuo OS V 3995 33 SUOR22UUOD Surquinjd 3841 put 2270 2 st HUN v JO JUOTF m uo qod werp JIOAJO9S2J v 3MSUH sjnu uorun pue aje d porddns y yya oq ue suono2ouuoo Surqumid oui fuo uyeq puau v Sursn VY sdumo Sursn SUOTH22UUOO qm T 3MIIS e 3u q JO oq JOU 3SNUI SIQNI pasa pmbr 194suex ye q ay uo spuadap aqui pombos oui e S IZZOU JEVU YIM BOLO SI STY o2egins qn1 JY uo sojme3oduro ur mx pea pm sonyezodura Supezado ouroxixqq v OF o qissod Sv SOT st uontvorndde oui vid put qm I pm e asn fq ssod PAY mqus oup uo 399379 9338 v dae y Qroede SUBO n qru peurquioo j uuurp sir put qm jo y Sua IYL T SS A eugo1xo DUY Jo pue W07 zis oq uo spuodop qm pIu umuurxeur U Y uoneordde peuzazxa ue o dumd oui 122uuoo o pasn Aqpeurjou sr Surqny p309 Q19 od E uu 1 1 02 ur SIUIOD Suiqm n jo uou 31nsu qT Suiqni Jo suon vuo Surquinjd ay Jo Kue qru 12 3u00 UI uo 1ou OP SPIOI ye r y q IINSUH un op pm parddns sduwp puv sqreq soq wu z JO wu g DU ffE3SUT 03 s yeyd pue sinu uorun oq MOWY TO WW 9 21v suonoouuoo ay apis 4qddns uoneordde eusayxa oui 01 MOP PPNO AP sr ES uoneomdde
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67. t refer to Section 6 Troubleshooting Place the circuit protector located on the front of the circulator to the position B Press O the Start Display will appear Ensure the start symbol has a highlight box around it if not use the arrow keys to navigate to the symbol Reservoir ighlighte Fluid Start Symbol Sa DI Temperature Start Display Press The circulator will start and the start symbol will turn into a stop symbol Mi Stop Symbol 5 GI NOTE It will take 30 seconds for the compressor to start A NOTE After start check external plumbing connections for leaks A The SP1 and Menu portions on the top of the display are used to view and or change the controller s settings They ate explained in detail later in this Section 4 2 Cole Parmer Section 4 Operation Status Display If desired press to toggle between the Start Status Displays Refrigeration Running uM Symbol Selected Reservoir Fluid Pump Running Symbol Heater Running Symbol Reservoir Fluid Temperature Status Display 1 Standby Mode Press O the display will go blank and the circulator will be in the standby mode Cole Parmer 4 3 Section 4 Operation Changing the NOTE You cannot adjust the setpoint closer than 0 1 C to either of the fluid s system limits see Fluids Type in this Section or beyond the Setpoint circulator s temperature range A The setpoint can be changed with the circulator running or not
68. tions are 16 mm O D Remove the union nuts and plates to install the supplied 8 mm or 12 mm hose barbs and clamps Ensure the electrical cords do not come in contact with any of the plumbing connections or tubing A The user is always responsible for the fluid used Never use corrosive fluids with this bath A Never use 100 glycol A Handling and disposal of liquids other than water should be done in accordance with the fluid manufacturers specification and or the MSDS for the fluid used A Adjust the circulator s software to the fluid used see Section 4 A When using water above 80 C closely monitor the fluid level frequent top offs will be required It will also create steam A Water glycol mixtures require top offs with pure water otherwise the percentage of glycol will increase resulting in high viscosity and poor performance A The fluid information is only a guide since specifications may change Fisher Scientific takes no responsibility for damages caused by the selection of an unsuitable bath fluid Unsuitable bath fluids are fluids which are very highly viscous much higher than 30 mPas at the respective working temperature have cortosive charactetistics ot tend to break down at high temperatures For fluid selection consider application requirements operating temperature range material compatibility safety concerns and environmental issues 3 5 Section 3 Inst
69. tures acoustic and mmersion optical alarms and adjustable high temperature protection Circulator polystat f Cole Parmer Hl Use this button to place the circulator in and out of standby mode Use these navigation arrows to move through the displays and to adjust values Use this button to start stop the circulator This button is also used to make and save changes on the display screen Use this button to cancel any changes and to return the circulator to its previ Esc ous display Canceling a change can only be made before the change is saved In some cases it is also used to save changes NOTE Holding this button for five seconds resets the display contrast to the default level and also brings up the language menu to change if needed the displayed language See Settings Display Options in this Section A C Use the adjacent dial for adjusting the High Temperature Cutout Details are explained in this Section Cole Parmer 4 1 Section 4 Operation Setup Cooling heating baths should be left in an upright position at room temperature 25 C for 24 hours before starting This will ensure the lubrication oil has drained back into the com pressor A 44 CAUTION Before starting the circulator double check all USB optional electrical and plumbing connections A Sta rt Up Do not run the circulator until fluid is added to the bath Have extra fluid on hand If the circulator will not star
70. ult occurs If Warnings is enabled the alarm will sound when a warning occurs Esc Press or use the Menu window to save and return to the previous display 4 8 Press or use the Menu window to save and return to the previous display 1 With Low Level highlighted press 7 to toggle the low level warning alarm on off Temperature Alarms Audible Alarms Low Level Warning Press 2 or use the Menu window to save and return to the previous display Cole Parmer Section 4 Operation Fluids Type is used to identify the type of fluid used The controller uses the fluid type to automati cally set certain operating parameters 1 With Fluid Type highlighted press o to Fluid system limits High C Low C display the list of acceptable fluids Midis Highlight the desired fluid and press to select it Distilled Water 98 2 DI Water up to 3 0 98 2 1 EG Water 103 35 O EG Water ES gt O PG Water Other For Standard Plus circulators SIL 200 153 17 For Advanced circulator 2 With the desired fluid selected press OT SIL 200 203 17 use the Menu window to save and return to the previous display SIL 300 203 77 SYNTH 260 203 42 Pump Adjustment is used to review set the NOTE The range is also limited by the bath tem desired pump speed perature range see Section 2 A 1 With Pump Adjustment highlighted press to display the speeds Highlight the desired speed and press 7 to
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User`s Manual - Cole

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