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1. 154 Loading a Rack Using the Remote Control 155 Loading a Sample Using the Display 156 Loading a Sample Using the Remote Control 157 Changing the Operation Mode eseseseeeeeee 158 Removing Measured Samples eseseeseeeee 159 Repair procedure 2 rta xa ex u Url XREE EE INA ERR FEX 161 Information regarding repairs essere 161 Safety and Repair Declaration sussusse 162 Technical Data nennen tun enata 163 Saele La MC i 163 Supply on Operation esee 163 Required Place in the Lab eeeseeeeeeeeeeee 164 DISPIaY MC 165 Cycle TIMES Acc r 165 Temperature Limitations 02242420020n00 Eon nn anna nennen 165 Sample Insertion Depth cece cece cece ee eeeeeeeeeeeeeeeees 166 LO VAL RT E 167 vcrc A 167 Weight of components cece cece cece ee ec eee eeeeeeeeaeaeeeeaees 168 Cooling Specifications 2 0 cece e cece ee eee cena eee eaeaeeeeeeeees 168 BRUKER BIOSPIN Users Manual Version 4 0 21 12 22 22 1 22 2 22 3 Users Manual Version 4 0 Contents Extension Specifications ccccc cece ece cece sees eaeeeeeeaeeeeaes 169 Bruker Biospin Cont
2. eseeseseeeene 62 Code Reading Problems cccccccecececeeeeceeeseeeaeeseaeaes 63 Carousel 99 9 urn een RETE SERE EB 65 What is the Carousel 99 5 oo ccc cece ccc ce eens ee eeeaeneneees 65 Using the Carousel 99 5 uusususesenensnnunenenenennnnnnnnennnnnn 67 The Shuttle Storage cccccccceceececeeeeceeeeceeeueeenaesneaeas 67 Correct Placing of the Tubes on the Grate 68 Working with a Waste Rack cccceccceeceaeeeee ease eeneaeenes 69 Cooling option zes t spedin vacenscteredcoreenteess 71 What is the Cooling ccccccceececeeeeceeeeeeseaeeseaeseeseaeenes 71 Important Remarks un enter 72 The carousel 30 5 cooled sees 73 Using TS COG MING suisses rennen 74 Switching on and off the cooling cece ccc ce eee een en 74 Cleaning the Heat Exchanger ccccccceeeceeeeeeeeeeeeeeeees 75 Carousel 47 5 V 77 What is the Carousel 47 5 sese 77 Using the Carousel 47 5 esses nene 78 BRUKER BIOSPIN Users Manual Version 4 0 12 12 1 12 2 12 3 13 13 1 13 2 13 3 13 4 13 5 13 6 13 7 13 8 14 14 1 14 2 14 3 15 15 1 15 2 15 3 15 4 15 5 15 6 15 7 16 16 1 16 2 16 3 16 4 16 5 16 6 16 7 16 8 Users Manual Version 4 0 Contents Using Bruker NMR Software 79 INELOQOUCUO
3. 222242020 sneenennnnennnnenen nenn 107 16 Initial Configurations 109 Figure 16 1 Hosts file Mt 111 Figure 16 2 Web server start up window eeeusesensnsnennenennnennnnnnnnnnnen nenn 111 Figure 16 3 Log in web server window c cece cece eee ceeeec eases eaeeeeeenenes 112 Figure 16 4 Installed firmware version ccccceceee eee eeeeec eases eaeeeeeeneees 112 Figure 16 5 TopSpin TTY window esses 114 Figure 16 6 TopSpin BACS window sees 114 Figure 16 7 Configuration Information after CH usueeusueuse 115 Figure 16 8 IConNMR Express Setup Window esee 117 Figure 16 9 ICONNMR start window esses 117 Figure 16 10 Selecting the automation device sueueseesss 118 Figure 16 11 The number of sample holders eessuseese 119 17 Calibration 121 Figure 17 1 The lift bypass screws sesesseemmm mH 125 18 Supplies and Accessories 129 19 Printout Section 147 Figure 19 1 A1 B1 H1 and Jump to A2 eeeseeeem 149 Figure 19 2 A1 A2 A12 and Jump to B1 esses 149 Figure 19 3 H1 G1 A1 and Jump to H2 sseseseeeee 150 Figure 19 4 H1 H2 H12 and Jump to G1 cece cece cece ee eee ee eaees 150 Figure 19 5 A12 B12 H12 and Jump to A117 cece cece ee ee eee eeenees
4. Window menu Users Manual Version 4 0 BRUKER BIOSPIN Initial Configurations 120 183 BRUKER BIOSPIN Users Manual Version 4 0 Calibration Calibrating the SampleJet 17 1 The drives and the lift have to be calibrated after the initial installation and starting up of the SAMPLEJET Every calibration is stored with its date The following calibrations have to be carried out in the given order They are de scribed on the next pages 1 Coordinate Calibration Calibrates all the hardware positions 2 Lift Calibration Calibration of the lift for each shuttle or spinner type 3 Vision Calibration If the system is equipped with a camera the camera also needs to be calibrat ed The coordinates of the system have to be recalibrated when updating to firmware version 6 Users Manual Version 4 0 BRUKER BIOSPIN 121 183 Calibration Important Knowledge about the Calibration 17 2 The SAMPLEJET will refuse any work until it is calibrated This behavior protects the device from damaging itself by moving into wrong positions If the SAMPLEJET is miscalibrated for any reason the calibration procedure has to be repeated A A If the SAMPLEJET is moved in any way from the SAMPLEJET BASE PLATE the BST coordinates have to be recalibrated 122 183 BRUKER BIOSPIN Users Manual Version 4 0 Coordinate Calibration Coordinate Calibration 17 3 One can calibrate the coordinates of the entire system or
5. 72 183 BRUKER BIOSPIN Users Manual Version 4 0 The carousel 30 5 cooled The carousel 30 5 cooled 10 3 This carousel has a insolation keeping the 5 standard racks cold The finger plate in every rack slot is a perfect heat exchanger and guaranties the same tempera ture for all of the 96 tubes in a rack For every rack the actual temperature is con trolled separately and can be read out Figure 10 2 The heat exchanger Since the heat exchanger has a much bigger mas then the rack with the tubes the temperature stays constant when inserting and removing racks The rack slots do not need to be covered when not in use Figure 10 3 Carousel cooled top view A cold rack slot A warm position on the openshop ring Every slot has its own temperature readout ns LES LES LE E a en LAE e su LE E aa a As TT eh E a Tur JE o gt oe u xu tHg t s Em E LE E LEN E E bd s Users Manual Version 4 0 BRUKER BIOSPIN 73 183 Cooling option Using the Cooling 10 4 There aren t any settings for the cooling but the system needs to have the cooled carousel in the system configuration This is because of the different geometry of the carousel Since cold tubes getting wet on ambient temperature the tubes need to be warmed and dried in the pre heating unit See Extension Option on page 83 Operating the SAMPLEJET with and without the cooling has only one difference Coo
6. Contents 4 183 5 7 5 8 5 9 5 10 6 1 6 2 6 3 6 4 6 5 6 6 7 1 7 2 8 1 8 2 8 3 8 4 9 1 9 2 9 3 10 10 1 10 2 10 3 10 4 10 5 10 6 11 11 1 11 2 EITOF RECOVERY weine rennen were 42 Hardware ONING ansehen 45 Emergency Stop iu 46 Important Things to Keep in Mind 46 Operating Modes 1 nenn 47 INLLOQUCION rr M 47 SampleJet Operating Modes eese 47 The X Xmm Shuttle Operating Mode 48 The Spinner Operating Mode seseeeeeeeee 49 The Manual Operating Mode eeeeeseeeesse 50 Changing the Mode cccccccccececeeeeseeeeeeeeaeuseeeaesseaeaes 51 USER SELUNGS nenne csc eee 53 IILLOQUCNON rannte une 53 SampleJet User Settings 2222220202000nnn non nn nenne nennen 54 VISION une en ee 59 ADOUL VISION ae nee einen 59 Using the VISION for Bar Codes eese 60 Rack IdentifiCalloOhi u ne 60 Bar Code Reading Behavior eseeeseeseesee 60 Bar Code Specifications ccccccceceececeeeeeeeeeeeseaessenes 61 Using the VISION for Matrix Codes eee 62 Tube Diameter Safety zessssusensnseneneneennnnennnnennnnn nenn 62 Requirements for matrix code reading 62 Matrix Code Definitions
7. 3 Folow the instructions on the Display 158 183 BRUKER BIOSPIN Users Manual Version 4 0 Removing Measured Samples Removing Measured Samples 19 10 1 Navigate to the main menu and press the Remove Measured Samples but ton 2 Open the front door 3 Remove the samples as displayed They will be moved to the front door Figure 19 16 Removing Measured Samples System State Remove Measured Samples sample in magnat Eosp dips EDGE Tae Measured Samples 1 2 3 Change Operating Mode 1 3 5 6 Remove Measured Samples Advanced Menu samples Removed system Idle System Idle system Idle 4 Close the front door 5 Press Samples Removed 6 If other samples needs to be removed repeat from step 2 T Press Done The SAMPLEJET may start moving after 60 seconds inactivity Users Manual Version 4 0 BRUKER BIOSPIN 159 183 Printout Section 160 183 BRUKER BIOSPIN Users Manual Version 4 0 Repair procedure Information regarding repairs 20 1 If a SAMPLEJET ever has to be sent to BRUKER BIOSPIN for repairs or a BRUK ER BIOSPIN engineer has to do any service work on the device please take note of the following The customer has to accept and sign a photocopy of the Safety and Repair Declaration form on page 162 or a newer version of the BRUKER form ZFQS0083 before any service work can be carried out on the SAMPLEJET Users Manual Version 4 0 BRUKER BIOSPIN 161 183 Repair procedure Safe
8. Be careful with the touch screen If you apply too much force to the display the glass will break If the SAMPLEJET does not respond press the emergency button and release it This will restart the application Users Manual Version 4 0 BRUKER BIOSPIN 25 183 Using the SAMPLEJET Change Remove Nvidia Operating Measured Load Sample Load Rack System State deni Mode Tubes Users Manual Version 4 0 D 5 5 z z a Shutdown Load MMI Restart Calibration Handle Error System Ba Appliction Tp gt O a m 2 X b Coordinate Vision Lift w C Calibration Calibration Calibration gt m t ca pi 17mm Storage BST Matrix Codes Bar Codes 1mm Shuttle Shuttle 3mm Shuttle 5mm Shuttle Spinner 3 D U Depending on the hardware in the Depending on the touchscreen service Depending on the enabled operating Default screen when display not system configurations password in the user settings modes in the user settings accessed for 3 minutes Y e eo q w to N Accessing the SAMPLEJET Access from the Web Interface 5 3 2 Device Information Documentation About Us Login The web interface was built for setup and service only The display on the SAM PLEJET is to be used for manual operation The SAMPLEJET is connected to an ethernet switch in the console This switch connects all the NMR system internal devices in a closed network This closed network is no
9. Rotate the carousel 1 10 of a full rotation Set the countdown to unlock the system to 60 seconds Any further press on one of the hidden buttons will Rotate the carousel 1 10 of a full rotation Reset the countdown to unlock the system to 60 seconds While Touch to get more time countdown a press on one of the hidden buttons will Reset the countdown to unlock the system to 60 seconds Closing the last open door will Unlock the system immediately Users Manual Version 4 0 BRUKER BIOSPIN 35 183 Using the SAMPLEJET Loading Samples into the Openshop Ring 5 5 3 Figure 5 12 Loading samples To access a sample in the openshop ring storage use the Load Sample function in the Main menu of the SAMPLEJET display This will rotate the chosen sample position to the front door Figure 5 13 Bring the desired tube to the door select Sample 9 i Ls Ce Je system Idle see also the detailed description in chapter Loading a Rack Using the Dis play on page 154 36 183 BRUKER BIOSPIN Users Manual Version 4 0 Loading and Unloading Probes Unloading Samples from the Openshop Ring 5 5 4 Already measured samples will be flagged in the software and can be easily re moved guided by the display Newer IconNMR software will control this status flag itself and can therefore even handle several interrupted NMR measurements on the same tube correctly Those interruptions are common if you are wo
10. eeseeeee 145 19 Printout Section 147 Table 19 1 The home positions of the shuttles 148 Table 19 2 The diameter setup of the storage 148 Table 19 3 General information cc cece eee ec eee ee eee eeeseeeeaeeaeesees 153 Table 19 4 Samples in the ACK sun a 153 20 Repair procedure 161 21 Technical Data 163 Table 21 1 STUDIS Mer 163 Table 21 2 Supply on operation eeesenmm mm 163 Table 21 3 TMC display Em 165 Table 21 4 CV CRS IMOS M 165 Table 21 5 Temperature limitations esee eene 165 Table 21 6 Insertlion Depin eu 166 Table 21 7 Moving parts on the SAMPLEJET 167 Table 21 8 Safety specifications sese 167 Table 21 9 weight of components sesessesessenneene 168 Table 21 10 Cooling specifications Lesser 168 Table 21 11 Parking specifications ccc ccc cece ec ec eee ee esses eaeeeeeeaees 169 Table 21 12 Heater specifications cccccccececeececeeesceceseeeeaeeeeaeas 169 BRUKER BIOSPIN Users Manual Version 4 0 Tables 22 Bruker Biospin Contact 171 Users Manual Version 4 0 BRUKER BIOSPIN 181 183 Tables 182 183 BRUKER BIOSPIN Users Manual Version 4 0 Notes Users Manual Version 4 0 BRUKER BIOSPIN 183 183 Bruker BioSpin your
11. One can perform an automated change of the operating mode triggered manu ally from the Basic Commands page of the web interface or on the display of the SAMPLEJET To change between the modes press Change Operating Mode on the main menu of the SAMPLEJET display The list of available modes depends on the en abled operating modes in the User Settings see chapter User Settings on page 53 Figure 6 4 Changing the operation mode on the display Change Operating Mode Load Sample Load Rack Imm Shuttle 1 mm Shuttle Smm Shuttle 5mm sShuttla Change Operating Made Advanced Menu system Idle system Idle Users Manual Version 4 0 BRUKER BIOSPIN 51 183 Operating Modes 52 183 BRUKER BIOSPIN Users Manual Version 4 0 User Settings Introduction 7 1 There are several different ways in which a SAMPLEJET may be used in the lab To adapt the SAMPLEJET to its environment a lot of settings can be set All the values are on one User Settings page of the web interface Before you can ac cess this page you have to log in as a User with the password bruker This pre vents from the unintentional changing of a value To access the page do the following 1 The system has to be in idle state 2 Open a web browser and type samplejet or http 149 236 99 55 3 Log in to the web page as a user password Bruker 4 Click on User Settings in the Basic Service menu If you change a value on the
12. nance M QM sampPuvieset i N a a BR KER PLUS O TRASHIELD 2 e SampleJet Firmware Users Manual think forward Bruker BioSpin Version 4 0 NMR Spectroscopy The information in this manual may be altered without notice BRUKER BIOSPIN accepts no responsibility for actions taken as a result of use of this manual BRUKER BIOSPIN accepts no liability for any mistakes contained in the manual leading to coincidental damage whether during installation or operation of the instrument Unauthorized reproduction of manual contents without written permission from the publishers or translation into another language either in full or in part is forbidden This manual was written by Reto Schmid January 22 2010 Bruker Biospin AG Fallanden Switzerland P N Z31749 DWG Nr Z4D9717E Contents 1 1 1 2 123 1 4 2 1 2 2 2 3 2 4 2 5 2 6 2 7 2 8 3 1 3 2 9 1 5 2 9 3 9 4 5 5 5 6 Users Manual Version 4 0 CONTENTS ccc EEEE EE 3 INTFOQUCUON san 9 What is a SampleJet uu222u222sunenennnnnnnnnnnnnnnennnen nenn 9 SampleJet Benefits Overview esses 10 SampleJet Overview nusessenenennnnennnnenennnnennnnnnnnnnnennn nennen 11 Inside the SampleJet cccccccceececeeceeeeeeeeeeseseeanaesneaeas 12 SALE 8 sieut E iR E 13 Warnings and Notes in this Manual ssse 13 Potentially Hazardous
13. 4 Phase Modulator Preemphasis Gradient Unit Lockswitch Lockswitch ino v Previous Cancel 23 Tick the box Should the sample changer control the lift 24 Enter 0 in Delay between SX and next command s Figure 16 6 TopSpin BACS window Additional configuration Security configuration Enable peak power check POWCHK I Sample changer configuration Should the sample changer control the lift Delay between SX and next command s o BACS options Fast SampleRail mode Previous Cancel 114 183 BRUKER BIOSPIN Users Manual Version 4 0 Setting up TopSpin 25 A summary of all the hardware installed called Configuration Information is supplied at the end of the cf If the SAMPLEJET has been recognized by cf it can be found in this file Figure 16 7 Configuration Information after cf BACS Sample Changer device connected to 149 236 99 243 dev ttyO4 Capacity 596 holders Firmware 970111 use BACS air yes BACS sx delay Ds Sample Hail fast changer mode no Table 16 2 Supported SX commands Command Remark sx holder number Removes the previously inserted sample automatically Inserts the chosen sample from the holder into the magnet Removes sample from the magnet and puts it back to its origin Users Manual Version 4 0 BRUKER BIOSPIN 115 183 Initial Configurations Setting up IconNMR 16 7 This chapter describes the setting
14. For operating modes 1mm Shuttle Manual 132 183 BRUKER BIOSPIN Users Manual Version 4 0 1mm Parts Table 18 2 1mm Parts for the SAMPLEJET Part Attribute Value _ ie i aa Users Manual Version 4 0 BRUKER BIOSPIN 133 183 Supplies and Accessories 1 7mm Parts 18 7 Table 18 3 1 7mm Parts for the SAMPLEJET Part Attribute Value 1 7mm Shuttle Part Number 2106558 Diameter 1 7mm Clamping the tube No Rotatable No Transportable Yes Max temperature 150 C 80 for ECL lt 01 00 For operating modes 1 7mm Shuttle Manual 134 183 BRUKER BIOSPIN Users Manual Version 4 0 1 7mm Parts Table 18 3 1 7mm Parts for the SAMPLEJET Part Attribute Value i ia ah Users Manual Version 4 0 BRUKER BIOSPIN 135 183 Supplies and Accessories 3mm Parts 18 8 Table 18 4 3mm Parts for the SAMPLEJET Part Attribute Value o mine Pme zu O ewe m For operating modes 3mm Shuttle Manual 136 183 BRUKER BIOSPIN Users Manual Version 4 0 3mm Parts Table 18 4 3mm Parts for the SAMPLEJET Part Attribute Value Snubs wih Caps PartMumber ZNZ eposon Users Manual Version 4 0 BRUKER BIOSPIN 137 183 Supplies and Accessories Table 18 4 3mm Parts for the SAMPLEJET Part Attribute Value Sm Tubes and Caps Part Number ZTGH8 10 pes ach t For operating modes 3mm Shuttle Spinner Manual 3mm Tubes and Caps Part Number 2117559 100 pcs each mm
15. on page 129 1 Below magnetic centre of system 2 If range is not smaller specified for short tubes given by the shuttle 166 183 BRUKER BIOSPIN Users Manual Version 4 0 Moving Moving The axis have the following parameters Table 21 7 Moving parts on the SAMPLEJET Data General absolute precision Max moving speed X Y and Z axes Max rotating speed rotating tray Max acceleration X Y und Z axes Max acceleration rotating tray Nominal force X axis Nominal force Y axis Nominal force Z axis Nominal force rotating tray biggest radius Force of moving part in gripper Force of sliders in BST ADAPTER UNIVERSAL Nominal power X axis Nominal power Y axis Nominal power Z axis Nominal power rotating tray Value Unit ei Safety These are the relevant safety specifications Table 21 8 Safety specifications Data Value Unit Min strain on the SampleJet before magnet tilt Er Axes behaviour on exception Axes position and current are per manently monitored oample tubes checked on inserting and removing from magnet Behaviour on broken sample tube Reaction time on emergency stop Users Manual Version 4 0 BRUKER BIOSPIN 167 183 Technical Data Weight of components 21 10 These are the weights of the SAMPLEJET components Table 21 9 weight of components Data Value Unit Premounted main part approx 40 USC CASING approx 13 Cooling Speci
16. 0 Loading and Unloading Probes Never insert a covered rack into the SAMPLEJET Figure 5 17 Remove the cover of the rack Do always insert the racks entirely that they will stand leveled Figure 5 18 How to insert a rack correctly Users Manual Version 4 0 BRUKER BIOSPIN 39 183 Using the SAMPLEJET Sample Holder Numbers 5 6 In TopSpin and IconNMR the samples are addressed by numbers Newer ver sions of IconNMR will show the rack enumeration For details see SAMPLEJET Together with IconNMR on page 80 There are gaps within the list They should not be used otherwise the SAMPLE JET will return a sample missing message The exact numbers of the holders is depending on the carousel See the holder numbers in the corresponding chapter of the carousel For carousel 99 5 read Carousel 99 5 on page 65 e For carousel 30 5 cooled read Cooling option on page 71 For carousel 47 5 read Carousel 47 5 on page 77 Table 5 3 The holder numbers Previous IconNMR Newer IconNMR sx commands eres aarti 86 fesersmen rock nz aan m orstonsompesinterack one wann feseemen gendi Number of slots Used for 401 496 4A1 4H12 096 For short samples in the rack 4 501 596 5A1 5H12 os Se For short samples in the rack 5 To set the sample position enumeration according to your needs check the User Settings on page 53 The default starts with A1 B1 H1 and jumps to A2 40 183 BRUK
17. 2007 1141 nmr X Eile Bun Holder View Find Parameters Coton Help amp p u OF Dil 184 Hvailanle CENTER ljn Biia E Solvent Experiment Par Title Orig Pr 1 Ell 18 i Fil 15 1 Gil 187 1 Hil 1 TE suit Freceding Experi 4 Date Availale Hvailabla Aa DOT MI Stale ABCDEFGH ioo 00000 nom o 60666 o0 i eoo 090000000808 0900000000090 gt eee OOo OOO 2090 606666666666 AB CDEFGH 00000000 6000000 00000000 0000000 g 00000000 d 0000 An openshop sample m Qo a 00000000 06000000 7 G00000000 0000000 5 1 99 100000000 a 00000000 z 86000000 100086000 For detailed information about the IconNMR please refer to the IconNMR docu mentation Users Manual Version 4 0 BRUKER BIOSPIN 81 183 Using Bruker NMR Software 82 183 BRUKER BIOSPIN Users Manual Version 4 0 Extension Option What is an Extension 13 1 There is some free space between the rotary tray and the BST Adapter in the SAMPLEJET Different extensions can be mounted in this gap to the existing SAMPLEJET hardware A PARKING UNIT parking only 2109175 A PRE HEATING UNIT parking with preheating Z109174 comes with an installation kit Figure 13 1 The PREHEATING UNIT Users Manual Version 4 0 BRUKER BIOSPIN 83 183 Extension Option What is the Parking Unit used for 13 2 The parking se
18. Areas sees 13 Byte IRR ERR RTI T are 14 Emetdercy VOD ui ee 15 Site Considerations ssesesssseseeen nne 15 Before Mounting the SampleJet sseesseseeesse 15 While Mounting the SampleJet eeeesess 15 DUNG ODCIALON NER ERIT Ep 15 FIFIDWaFe HINIS qoo tions aua c xau E REP ERR RENE ERE 17 What is new in Firmware sese 17 Upgrading to Firmware sees mmn 19 EIFSESIEDS user 21 Getting Familiar with the SAMPLEJET 21 Using the SAMPLEJET eene 23 INITOAUCLON ROTE 23 SampleJet states 2 0 cece ccece esse ee eeeeaeeeeeeaeeeeaeseeeeaeaes 23 Accessing the SAMPDEBEBJE T aussen 24 Access from the Display ccccccececeeeeceeeeeeeeaeseeeees 24 Access from the Web Interface uuessse 27 Cas and C AMON Ss ae 30 COIOISCCODCODE ee tc i LIPS 30 CAS TEMERE 31 er quic eu RE Se een 32 Loading and Unloading Probes 042022s20 san nennen 33 System Locked by User eeeseeeeeeeeeenene 34 Rotating the Carousel eese 35 Loading Samples into the Openshop Ring 36 Unloading Samples from the Openshop Ring 37 LE OAGING RACKS ongan S 38 Sample Holder Numbers cccccececeeeececeeeeseaeeeeeeaeees 40 BRUKER BIOSPIN 3 183
19. Do not start the SAMPLEJET with sx commands or IconNMR jobs unless the SAMPLEJET is calibrated correctly This is described in Calibrating the SampleJet on page 121 Starting the SAMPLEJET 1 Make sure the emergency button is released 2 Switch on the 24 V power supply of the SampleJet which is located in the con sole 3 Wait until the touch screen on the front of the SampleJet starts up This may take up to 30 seconds Users Manual Version 4 0 BRUKER BIOSPIN 109 183 Initial Configurations 4 Follow the startup procedure Note read the advice given on the display care fully If the starting sequence leads into the error state again and again some cabling hoses may be incorrectly installed Check the installation and try again Readjusting the BSMS Lift 16 2 The SAMPLEJET controls the BST lift itself except in the SAMPLEJET manual mode After installing a SAMPLEJET the BST lift controlled by the BSMS has to be set up again in the service mode of the BSMS This lift mode is used if the SAMPLEJET is operated in manual mode 5 Change the SAMPLEJET operation mode to manual 6 Switch on the BSMS lift 7 Insert a long sample with the heaviest carrier the customer is using 8 Adjust the BSMS lift to a value which brings the sample to the top Setting up the Service Access with a Web Browser 16 3 A web server on the SAMPLEJET provides a simple way of managing the SAM PLEJET Access is gained via a
20. data BRUKER BIOSPIN can acquire additional debugging information from these files These files do not contain any information about your company samples or spec tra BRUKER BIOSPIN will not give any information to a third party The easiest way to send all the required data is to create a pack of the latest log files on the web page All the system data will be included automatically Log Files 15 6 1 The SAMPLEJET stores a large amount of data in two different log files These textfiles may not make sense to users and service engineers They are intended to be used by the development team Table 15 1 The different types of logfiles Log file Content Description Details All data All information is stored in detail Summary Overview Contains an abstract of the information in the details file and give an overview Log file conventions The SAMPLEJET firmware handles all the files automatically If needed the per manent files are compressed and stored and a new file will be generated The file names of archived logfiles contain the date and time of the last log entry in YYYYMMDD HHMM format Users Manual Version 4 0 BRUKER BIOSPIN 105 183 Basic Service System Data 106 183 Downloading Logfiles There is a simple way to download more than one file by creating a compressed package of files This is described on the web page 1 Open a web browser and type in samplejet or http 149 236 99 55 2 L
21. of all the carousel and delivered as the standard ver sion until 2009 Figure 11 1 The CAROUSEL 47 5 47 tubes on the openshop ring On the outer openshop ring 47long 7 tubes with spinners can be placed S racks 5 racks can be placed in the middle of the storage Users Manual Version 4 0 BRUKER BIOSPIN 77 183 Carousel 47 5 Figure 11 2 The CAROUSEL 47 5 storage 5 rack slots on the inner side m Uh Wi mm M gw A i NC I E at Rd Y p EG li I F 47 holders for openshop tubes with spinners Using the Carousel 47 5 11 2 The firmware will recognize the CAROUSEL 99 5 option if it is set in the System Configuration The new storage requires a new storage calibration Depending on what tube diameter you work with the setting can be changed in the User Settings on page 53 to suit the diameter of the openshop ring The SAMPLEJET will make sure the system is in the right operating mode when using tubes from the ring Table 11 1 The holder numbers for a standard carousel Previous IconNMR Newer IconNMR sx commands 1 47 1 47 47 Long samples with a spinner in the openshop ring 101 196 1A1 1H12 98 For short samples in the rack 1 Number of slots Used for m maa 66 forsone ne O oe maa 03 forsone nea me maa 66 Forsbonsonssin wreck e ma 66 fesotsemishTendS 78 183 BRUKER BIOSPIN Users Manual Version 4 0 Using Bruker NMR Software 1 2 Introduct
22. the hole in the bottom of the frame 4 Connect the plug to the control box on top of the SAMPLEJET position RES1 and fix the cable with lacing cord gt Screw driver 2 There are several similar plugs Use the RES1 to connect the REMOTE CONTROL Figure 14 2 Where to connect the REMOTE CONTROL gt 4 et Jl TU pu it d al al A a L Connect the plug here 5 Remount the cover on the right side gt Angled allen key 2 5 96 183 BRUKER BIOSPIN Users Manual Version 4 0 How to use the Remote Control 6 If a SAMPLEJET STAIR 4 STEPS is used the REMOTE CONTROL can be mounted to the hand rail gt Angled allen key 2 5 If not attach it to a ladder with the pads or place it on a table Figure 14 3 The pads How to use the Remote Control 14 3 Just press the or button to turn the rotary tray step wise to the left or the right One step is half a rack or 5 samples If a sample is in the magnet the tray will move slower in order to not disturb a run ning measurement Figure 14 4 Using the REMOTE CONTROL Rotate Tray Turn the rotary tray left Turn the rotary tray right e aystem locked SAMPLEJET Users Manual Version 4 0 BRUKER BIOSPIN 97 183 Remote Control Option Table 14 1 The REMOTE CONTROL LEDs LED LED s System locked Rotate Tray Meaning system locked by another process The System is locked for the user of the REMOTE CONTROL comm
23. to do it on your own You may get hurt Beware of the strong magnetic field while working around the magnet Keep all metal objects such as tools screws or any metallic parts away from the mag net Remove any mechanical watches or metallic objects while working around the magnet Do not turn the SAMPLEJET on during installation 2 8 Use only new sample tubes in the specified diameter range or otherwise the caps may fall off while the system is running Avoid putting hands or objects in the path of the gripperarm or tray when the SAMPLEJET is running as this may cause personal injury or damage to the equipment Therefore it is recommended to keep the doors on the front and back side closed during normal operation Be aware that the SAMPLEJET s horizontal and vertical axes the tray or the gripper may start a movement unexpectedly Glass tubes may contain hazardous substances If a glass tube breaks refer to the corresponding precautions and cleaning disinfection instructions Only trained personnel should be allowed to operate the SAMPLEJET Staff training BRUKER BIOSPIN 15 183 Safety is the responsibility of the owner of the system BRUKER BIOSPIN will not be responsible for damage resulting from improper training The use of nitrogen as an operating resource instead of compressed air may lead to an oxygen deficiency in the laboratory e g through a technical defect burst in pneumatic hose It is highly recommended t
24. 1 10 21 11 Calibration a 121 Calibrating the SampleJet eseseeseeeeeeeee 121 Important Knowledge about the Calibration 122 Coordinate Calibration cc cece cece eee eeeeec ee eeeeeeeeeeeaeees 123 ETC Atl POO MMs HT 124 The Presetting for the Lift eessseuse 125 Running the Lift Calibration cece ece cece eae e aes 126 Vision Calibration ccc cece eee e cece eee mme 127 Supplies and Accessories eene 129 SAMPLEJET on Workload eeeeseeeeeeeeeee 129 General statements cccccccce esse eeeceeeeseeeeeeseaeseeenaeaes 129 What is to consider cece ccecc ec eceeceeeeaeeceaeeaeeseseeaneetans 130 Where to get consumables ccccccececeeseeeeseeeeeeeeeaes 130 Remarks on the Hardware List seesesuesuess 131 ATAVUS ABS eer TT 132 dis TIMMINS anstatt E FERTERnCO UDINE VUE OR CHR PIER NEIN NEED 134 Ont its 6 oou metit re nee 136 OH AIS een ee IMMUNE SEM EE 140 Minucio RR 145 PIINIOULSECHON iiie conr RR uU VERUM EMEN 147 What is this Chapter about eese 147 Diameter Setup u sen 148 Rack Enumerations ccccccceceececeeceaseceeeeaseceeseaeeseeneas 149 Content of a Rack nn ee 153 Loading a Rack Using the Display
25. 111 183 Initial Configurations The Log in Window 16 3 2 Figure 16 3 Log in web server window Bruker SampleJet Derice information Documentation About Ls Login Bruker BioSpin AG Swirnerfancd ARTUSA State Operating Mode Smm Shut Select the user Service for setting up the SAMPELET contact BRUKER BIO SPIN if you don t know the password For more information about the users please read Access from the Web Interface on page 27 Check Firmware Version 16 3 3 The functionality of the SampleJet depends on the firmware version that is in stalled The installed version can be seen on the web page 11 Open a web browser and type in samplejet or http 149 236 99 55 12 In Device Information see the System Configuration Figure 16 4 Installed firmware version Bruker SampleJet Display Syanem Configuranan Device Informalton f Documentation Ten About Ls Login 7 Hardware Componen t Production ID ECL Serial Number r Bio spin AG Swirrenand Operating Mode 112 183 BRUKER BIOSPIN Users Manual Version 4 0 Setting up the System Settings Setting up the System Settings 16 4 Currently there is only one setting that can be changed This concerns the shim system it will affect the lift air 13 Open a web browser and type in samplejet or http 149 236 99 55 14 Log in to the web page as service contact BRUKER BIOSPIN if you do not know the password The password is for BRUK
26. 13 2 Heater States ee scat eens Table 13 3 Heater settings for example 1 Users Manual Version 4 0 BRUKER BIOSPIN 13 17 21 23 iae 28 stus 30 M 40 47 T 48 m 49 53 ies 56 59 65 RN 67 71 77 DEREN 78 79 ee 79 ule teils 80 179 183 Tables 180 183 Table 13 4 Heater settings for example 2 sseesesesssse 91 14 Remote Control Option 95 Table 14 1 The REMOTE CONTROL LEDs esee 98 15 Basic Service 101 Table 15 1 The different types of logfiles sss 105 16 Initial Configurations 109 Table 16 1 Where the hosts file are located 111 Table 16 2 Supported SX commands 2022220220sensensnnennennen 115 Table 16 3 Selecting the Automation Mode 116 17 Calibration 121 Table 17 1 Basic Lift Analysis aussen ee 126 18 Supplies and Accessories 129 Table 18 1 Remarks on Hardware ccccccccccc eee eeeeaeeeeeaeeneeneeneeas 131 Table 18 2 1mm Parts for the SAMPLEJET sess 132 Table 18 3 1 7mm Parts for the SAMPLEJET 134 Table 18 4 3mm Parts for the SAMPLEJET esses 136 Table 18 5 omm Parts for the SAMPLEJET eeeeees 140 Table 18 6 Limitations on the SAMPLEJET
27. 151 Figure 19 6 A12 A11 A1 and Jump to B12 0 0 ccc cece cence eee eeeaees 151 Figure 19 7 H12 G12 A1 and Jump to H11 cece cece cece eee ee ee ees 152 Figure 19 8 H12 H11 H1 and Jump to G12 cece cece eee ee ee en ees 152 FIgure 19 9 Change rack seinen ae ee 154 Figure 19 10 Points to check 22224222020 00nennnnnnen anne nenn meme 154 Figure 19 11 The REMOTE CONTROL 0 022ssssssssenenenensnenenennen 155 Figure 19 12 Points to check 222222u2020 0nnennnnn nennen nenn emen 155 Figure 19 13 Change sample 2usessusesensneenennnnnnnnennnennennnnenen nennen 156 Figure 19 14 The REMOTE CONTROL esee 157 Figure 19 15 Change operating mode ssssesessesesee 158 Figure 19 16 Removing Measured Samples seeeseseeeese 159 Users Manual Version 4 0 BRUKER BIOSPIN 175 183 Figures 20 Repair procedure 161 21 Technical Data 163 Figure 21 1 SAMPLEJET dimensions esses 164 22 Bruker Biospin Contact 171 176 183 BRUKER BIOSPIN Users Manual Version 4 0 Index C GallDratlon ms tT 121 CIS pcm MCCC C PP PEE NT idl ieee 30 rape ecc 104 D D LAY Sostieni a Bee LIEU Nue A SMELL NU M ure Seo 24 E singers gre STOP T m 45 ipis gn e P a M EE 42 F PEMA Sad RNC C M 107 H Hardware ON Desaster 45 M Manual MOIE ei si 48 49 N
28. 5 6 The web page menu tree Webpage Device Advanced Basic Service Information Service System Configuration Software Releases System User Settings Corficinition Download Statistics Date amp Time Manual System Settings System Commands Basic Commands Date amp Time Coordinate Calibration HM Selftest System Database Error Lift Calibration Inputs amp Outputs Warnings Vision Upload System Calibration Data Upload Details Logfile Firmware Error Statistics Download Logfiles Summary Logfile Vision Statistics Reset to Default Download system Data Inputs amp Outputs Basic Commands Heater Commands Users Manual Version 4 0 BRUKER BIOSPIN Documentation Accessing the SAMPLEJET About Us Login Contact Login Bruker Biospin AG Logout Bruker Web Store Development Team Production Team Service Team Only for User login Only for Service login Depending on hardware 29 183 Using the SAMPLEJET Caps and Carriers Color Concept 30 183 9 4 The SAMPLEJET can accommodate different sample diameters The cap on top of each sample serves as an interface between the different samples and the grip per Different sample carriers and caps are used depending on the operating mode of the SAMPLEJET see Introduction on page 47 5 4 1 In future all caps and carriers of
29. 5min cet Samples in Heater 4 cet System Idle The state of the heater will be indicated in the status bar of the display Table 13 1 Heater indication Indication Meaning H blinking Heater is on temperature not stable H stable Heater is on temperature is stable 86 183 BRUKER BIOSPIN Users Manual Version 4 0 Using the Preheating If you have to stop an IconNMR run for any reason you can return all the samples in the heater to their original positions with the Return All Samples To Storage button on the Basic Commands page of the web interface Figure 13 6 The Basic Commands page Bruker SampleJet Basic Commands Device Information Transport Sample Basic Service EE User Settings To Storage System Commands Coordinate Calibration mpl To Magnet Lit Calibration Sampe Vision Calibration 101 Upload Firmware TeHeaer Download Logfiles Download Images To Parking Download System Data Inputs amp Outputs Eject Sample From Magnet Recovery from Error cias Basic Commands Heater Commands Return All Samples To Storage Advanced Service Change Operating Mode Documentation Current mode 5mm Shuttle About Us mm Login 00 o mse 3mm Shuttle 5mm Shuttle Bruker BioSpin AG Switzerland State Operating Mode Login Info Service Users Manual Version 4 0 BRUKER BIOSPIN 87 183 Extension Option Prehe
30. AMPLEJET Together with IconNMR on page 80 you can choose for each tube if it should go to the wase rack or not Read Racks on page 55 to set up a rack slot as a waste rack The waste racks will be filled in a predefined order The SAMPLEJET starts filling a rack at position 1 and remembers the last used position After reaching position 96 in a rack it goes back to position 1 If more than one waste rack is defined the SAMPLEJET will give them priorities according to their slot numbers The lowest slot number has the highest priority and therefore will be filled first The SAMPLEJET will not search for a free position in a rack Always empty a waste rack completely before inserting it If position 1 is occupied a rack will be recognized as full If there are no free positions in the waste racks the sample tubes will be returned to their original position in the openshop ring A rack defined as a waste rack can not be accessed by the user Once a sample is in the waste rack the SAMPLEJET will not bring it to the magnet again Users Manual Version 4 0 BRUKER BIOSPIN 69 183 Carousel 99 5 70 183 BRUKER BIOSPIN Users Manual Version 4 0 Cooling option What is the Cooling 10 1 The cooling option for the SAMPLEJET stores the tubes in the carousel at a re duced temperature Temperature sensitive samples will not be destroyed when waiting for the NMR measurement 5 standard racks fits into the special carousel and
31. AMPLEJET tries to read it again Stray light from outside the SAMPLEJET can disturb a reading Closing the doors prevents this problem Bar Code Specifications 8 2 3 Bruker specifies the bar codes for all automation devices in a separate manual Please refer to Barcodes for BRUKER Automation User Manual Z31588 for bar code specifications Users Manual Version 4 0 BRUKER BIOSPIN 61 183 Vision Using the VISION for Matrix Codes 8 3 Tube Diameter Safety 8 3 1 The matrix code reading can be used to verify if the diameter of the tube and the shuttle correlates with the chosen operating mode The SAMPLEJET is able to change the operating mode on its own if it is not correlating Requirements for matrix code reading 8 3 2 The SampleJet with a VISION gripper needs the following to read the codes A key is required in order to activate the code reading A calibration for the matrix codes is needed This calibration is described in Vision Calibration on page 127 Matrix Code Definitions 8 3 3 All matrix codes on caps and shuttles are labeled by BRUKER Therefore no specification is available on matrix codes Some definitions of the content of the codes are described below Caps The whole information from the code is also labeled in ten digits The first two digits define the diameter of the tube The remaining eight digits are a unique serial number of the cap Shuttles The whole information from t
32. Diameter 3 Cap label Matrix code and number For operating modes 3mm Shuttle Spinner Manual Part Number 2107474 100 pcs For operating modes 3mm Shuttle Spinner Manual 138 183 BRUKER BIOSPIN Users Manual Version 4 0 3mm Parts Table 18 4 3mm Parts for the SAMPLEJET Part Attribute Value o mmea Pannur zoren 0 For operating modes 3mm Shuttle Spinner Manual Part Number EE ELI AN aes fcr Transportable For operating modes Spinner Manual Users Manual Version 4 0 BRUKER BIOSPIN 139 183 Supplies and Accessories 5mm Parts 18 9 Table 18 5 5mm Parts for the SAMPLEJET Part Attribute Value o mms Partnumber tees 140 183 BRUKER BIOSPIN Users Manual Version 4 0 5mm Parts Table 18 5 5mm Parts for the SAMPLEJET Part Attribute Value Emm Tubes wih Caps PartMumber ZNZ Epes rack Users Manual Version 4 0 BRUKER BIOSPIN 141 183 Supplies and Accessories Table 18 5 5mm Parts for the SAMPLEJET Part Attribute Value TS Tubes and Caps Part Number EUM pes eae s For operating modes 5mm Shuttle Spinner Manual Part Number 2105683 100 pcs For operating modes 5mm Shuttle Spinner Manual 142 183 BRUKER BIOSPIN Users Manual Version 4 0 5mm Parts Table 18 5 5mm Parts for the SAMPLEJET Part Attribute Value Smaps PartNumber zweien ENLI NNI NN ee fewer For operating modes Spinner Manual Use
33. ER BIOSPIN Users Manual Version 4 0 Sample Holder Numbers Figure 5 19 The enumeration of the rack Rack index E 4 E aide d er 12 ma rm LETT AA WE I Tu e e T be me F A d i Users Manual Version 4 0 BRUKER BIOSPIN 41 183 Using the SAMPLEJET Error Recovery 9 7 The error recovery is used to set the SAMPLEJET in a well defined state There are 3 occasions when an error handling is carried out e After a power up After a restart of the application e g after an emergency stop f an error occurs during operation To handle an error just click Handle on the SAMPLEJET display and follow the instructions If the SAMPLEJET application is restarted an error recovery has to be started by pressing Start on the display Error Messages Figure 5 20 An error message ERROR sample lost The error messages do always containing 4 screens 1 A short error message 2 A detailed error message 3 The cause of the error 4 Instructions about how to get rid of this error 42 183 BRUKER BIOSPIN Users Manual Version 4 0 Error Recovery Error during error recovery If the system runs into another error while carrying out an error recovery these are two options Repeat the error recovery If you made a mistake on the error recovery or you have a different error mes sage to the first one Go to the manual mode If you get the same error mes
34. ER service engineers only 15 Choose System Settings in the Advanced Service menu 16 Select the BST type installed on your system The Z number can be looked up on the label on the top of the BST Setting up the Time and Date 16 5 The system time is important when solving logged problems The user may refer to a problem at a certain time 17 Open a web browser and type in samplejet or http 149 236 99 55 18 Log in to the web page as user with the bruker password 19 Choose Date amp Time in the Basic Service menu 20 Set the time to the local winter time Setting up TopSpin 16 6 This chapter describes the setup for TopSpin 1 3 2 1 or 3 0 carry out the setting up of where a XwinNMR 3 5 is installed analogical to the description The SampleJet must be turned on and connected to the console via tty 21 Do cf in TopSpin or XwinNMR 22 Enter the tty channel which the SampleJet is connected to Users Manual Version 4 0 BRUKER BIOSPIN 113 183 Initial Configurations Figure 16 5 TopSpin TTY window specify the channel to which external devices are connected RS 232 485 channels for external devices HPPR Preamplifier 1 BSMS Smart Magnet Control System Lock Signal LC NMR Software HyStar VTU Variable Temperature Unit Gradient Temperature Unit BCU 20 MAS Pneumatic Control Unit BACS Bruker Automatic Changer Barcode Printer Cryo Controller HPCU High Power Control Unit
35. Figure 15 4 Filename nomenclature samplejet 3r20060708 i386 deb tooo Extension Processor Date Helease Product Acquiring new firmware The current firmware can be downloaded from the BRUKER ftp server ftp ftp bruker ch pub NMR download SAMPLEJET Remove all samples from the magnet and PRE HEATING UNIT before load ing a new firmware To check the installed firmware 1 Open a web browser and type in samplejet or http 149 236 99 55 2 Log in to the web page as a user password bruker 3 Click on Firmware on the Device Information menu To load new firmware 1 The system has to be in idle state 2 Open a web browser and type in samplejet or http 149 236 99 55 3 Log in to the web page as a user password bruker 4 Click on Upload Firmware on the Basic Service menu 5 Follow the instructions shown on the webpage The web site layout depends on the installed firmware Users Manual Version 4 0 BRUKER BIOSPIN 107 183 Basic Service 108 183 BRUKER BIOSPIN Users Manual Version 4 0 Initial Configurations Introduction 16 1 This chapter will lead you through the configuration fine adjustment procedures pneumatic settings and final setup of the SAMPLEJET These adjustments should be made after the SAMPLEJET has been mounted in accordance with the mounting instructions The initial configuration should only carried out by a BRUKER service engineer
36. N MM TERN 19 SAMPLEJET Together with TOPSPIN ese 79 SAMPLEJET Together with IConNMR 80 Extension Option euere een een 83 What is an Extension uueusessnsensensnnennennnnennnnnnnennenenn 83 What is the Parking Unit used for 84 What is the Preheating Unit used for 84 Using the Parking sese 85 Using the Preheating 2z2u20 0020n0nnnnonnn nennen nenne 86 Preheating Settings u2222020s20n0nannennnnnnnnnnne nennen nennen 88 The four preheating settings eseseseeeeeses 88 Examples of Preheating Settings 90 Preheating on a Power Failure Leeeueeuueus 92 Extension Overview ssssssssssssesn nene nennen nennen 93 Remote Control Option 95 What is the Remote Control used for 95 How to Install the Remote Control sse 96 How to use the Remote Control eseueeeususs 97 Basic Service runs aqnis tex pM sere 101 Basic Service carried out by the Operator 101 Calibrating the Device cece cece cece ease ea eeeeeeaeeeenes 101 Changing the O RING sauna oum PSone ciuem neas 101 Replacing the Pincer c
37. NUMOGI sexu uode rar dd t i DD T D C DUC PME Re MU eer 40 O ONEIN OW e DEO UNIONIS ETE RE 11 P Pa OWO US deiode ida ncaa one ec efus bue deum om eat teas Die 28 R Remote CONTO xi vicies ae een uu Ld tex sina 59 65 77 83 95 Users Manual Version 4 0 BRUKER BIOSPIN 177 183 Index 178 183 S Cy BERE 13 Sales IH IOHNAUON MUERTE 171 T Technical ASSIStANOG quse eb cesetiYenitantubbt bru xad bbcada Naa Paare bi ai Ve dob add ox dn RUE 171 W VV SEIN Nl ACS RR T m 2 BRUKER BIOSPIN Users Manual Version 4 0 Tables 1 Introduction 2 Safety 3 Firmware Hints 4 First Steps 5 Using the SAMPLEJET Table 5 1 LOGIMA DIS sisi erdum eye fais guit ex oput devo Oe ds Table 5 2 The defined colors o us Table 5 3 The holder numbers crm 6 Operating Modes Table 6 1 Number of holders for tubes without spinners Table 6 2 Number of holders for spinners 7 User Settings Table 7 1 Automatically mode change restrictions 6 Vision 9 Carousel 99 5 Table 9 1 The CAROUSEL 99 5 holder numbers 10 Cooling option 11 Carousel 47 5 Table 11 1 The holder numbers for a standard carousel 12 Using Bruker NMR Software Table 12 1 TOPSPIN Commands HRRH IRR Table 12 2 IConNMR Features for SAMPLEJET 13 Extension Option Table 13 1 Heater indication sseen Table
38. Ring Occupied position Free position check default enabled disabled If a lot of different people are inserting and removing samples in the openshop mode these safety options should be switched on The SAMPLEJET will move to the openshop position and check if it is free before inserting the currently measured sample If the position is occupied an error is displayed and the SAMPLEJET stops If you do not want to stop the device choose the option of placing the sample into another storage number if one is free The SAMPLEJET will check for both tube and spinner If there are door sensors indicating the doors were not opened between the in serting and removing of a sample into and from the magnet the check will not be proceeded Check sample diameter with matrix code option default disabled If you have the VISION and the CAROUSEL 99 5 option you can choose if the diameter of the tubes in the slots 1 96 correspond with the preset diameter of the option OpenShop Ring on page 55 Shuttles e Shuttle home positions ECL s default nothing defined If you want to use the automated change of operating modes you have to tell the system where the shuttles are stored when not in use If your shuttle has no ECL on a label set this value to 0 0 For shuttles you do not have choose none in the Unit field e Sample insertion depth for samples in clampable shuttles default 20mm 54 183 BRUKER BIOSPIN Us
39. Version 4 0 Printout Section What is this Chapter about 19 1 The next pages contain drawings forms and guidance for the daily usage of a SAMPLEJET Print or copy these pages and place them in a noticeable spot in your lab if required There is a page per topic Users Manual Version 4 0 BRUKER BIOSPIN 147 183 Printout Section Diameter Setup 19 2 These are the settings from the User Settings page on the web interface for shuttle homes and diameters Shuttle homes If a shuttle is not used it will be stored in its home position Table 19 1 The home positions of the shuttles 5mm Shuttle Diameters These are the chosen diameters for each of the storages Table 19 2 The diameter setup of the storage Storage Rack 96 short 1mm to 5mm Samples mixed Rack 96 short 1mm Samples only Rack 96 short 1 7mm Samples only Rack 96 short 3mm Samples only Rack 96 short 5bmm Samples only Rack 96 waste for CAROUSEL 99 5 1mm to 5mm Samples mixed 1 mm Samples only 5mm Samples only 1mm Samples only 3mm Samples only Openshop Ring 148 183 BRUKER BIOSPIN Users Manual Version 4 0 Rack Enumerations 19 3 Rack Enumerations Figure 19 1 A1 B1 H1 and Jump to A2 COGO GO X 8 eo lo e BEER i S2 0 8 0 8 8 8 i 20 8 0 GO 23 JOQOG OVOCE M 0 O8 009 i 2 2 G0 G0Q Joto I 83008 08 mo nooiuiui ru o Figure 19 2 A1 A2 A12 and Jump to B1 BOO monooiu
40. a specific part of it The calibration routine can be started from the display or the web interface Calibrations Calibrate Entire System This routine will calibrate the sample storage the BST and Extension if present All calibrations will be saved and dated It takes about 18 minutes to calibrate everything Calibrate Storage The length of the storage calibration depends on the installed carousel Check if all the racks are inserted correctly before starting the calibration Calibrate BST The SAMPLEJET will automatically find the calibration notch on the SAMPLE JET BST ADAPTER UNIVERSAL and calibrate it in about 3 minutes Calibrate Extension SAMPLEJET will calibrate the parking and preheating positions The calibra tion is only available if the hardware is listed in the System Configuration Calibrating from the display 1 The system has to be in idle state 2 Choose the Advanced Menu in the Main Menu 3 Choose Service in the Advanced Menu 4 If there is a service code set in the System Settings of the web interface type in the number 5 Click on Calibration and then Coordinate Calibration 6 Choose a calibration routine and follow the instructions on the display Calibrating from the web interface 1 The system has to be in idle state 2 Open a web browser and type in samplejet or http 149 236 99 55 on the spectrometer control computer 3 Log in to the web p
41. act eene 171 General Questions ccsssssssee Imm 171 Contact for Sales Information s 171 Contact for Additional Technical Assistance 171 xli u cS 173 MOO a 177 TADIOS Merc 179 BRUKER BIOSPIN 7 183 Contents 8 183 BRUKER BIOSPIN Users Manual Version 4 0 Introduction What is a SampleJet 1 1 The SAMPLEJET is a high capacity high throughput sample robot system opti mized for NMR applications It is based on a modular concept The basic system takes care of common functionality of a sample handling robot and provides all parts to integrate the SAMPLEJET with standard AVANCE spec trometers Although capable of stand alone operation the SAMPLEJET is con nected to the console via a regular RS232 interface allowing standard control through IconNMR or the XwinNMR TopSpin commands B ACS interface Figure 1 1 SAMPLEJET System 1 SAMPLE PLUS a J gt I un lt q tr E DO The SAMPLEJET is a push button system which runs under complete computer control enabling modern interfaces like Ethernet and a comprehensive communi cation link for service and diagnostics with web based mechanisms It s built in electronics control and continuously monitor all operations needed for an entirely automatic sample handling The basic system provides all the necessary parts power supply cables et
42. age as a user password bruker 4 Choose Coordinate Calibration in the Basic Menu 5 Choose a calibration routine and follow the instructions Users Manual Version 4 0 BRUKER BIOSPIN 123 183 Calibration Lift Calibration 124 183 17 4 Given the fact that each type of shuttle or spinner has a different weight and a di ameter tolerance the SAMPLEJET needs to calibrate each one of them With some iterations the SAMPLEJET tries to find the fastest set up of the air flow with out hitting the sample too hard on the bottom or on the top Some carriers are cal ibrated with a sample tube others without The thicker tubes carriers need the tubes to acquire the normal amount of weight and airflow The lift calibration routine can only be started from the SAMPLEJET display Never operate a carrier that was not calibrated correctly Only the Enabled Operating Modes in the User Settings are available for cali bration except the Manual mode The calibration of the lift has two layers 1 The lift presetting 2 The lift calibration BRUKER BIOSPIN Users Manual Version 4 0 Lift Calibration The Presetting for the Lift 17 4 1 The gas used to blow out a carrier needs to exhaust at the top end of the shim system to decelerate the carrier Therefore the SAMPLEJET hardware has some bypass holes in it But if the gas supply is not strong enough those holes needs to be closed with screws to have enough g
43. al Note Indicates important information or helpful hints WARNING Indicates the possibility of severe personal injury loss of life or equipment damage if the instructions are not followed Potentially Hazardous Areas 2 2 The symbols shown below indicate a potentially hazardous area and strong LA SER ISO 3864 DIN 40008 Figure 2 1 Warning hazardous area The symbol is placed on the following areas of the SAMPLEJET 1 On the front cover just right of the door side that is away from the magnet Users Manual Version 4 0 BRUKER BIOSPIN 13 183 Safety 2 On the rear side left and right side that is over the magnet Warning Keep cover closed unless manual action has to be done Figure 2 2 Warning LASER hazard The symbol is placed on the following area of the SAMPLEJET 1 On the SAMPLEJET BST ADAPTER UNIVERSAL on top of the magnet Do not remove any parts until the SAMPLEJET is turned off If one of these symbols is missing please contact BRUKER BIOSPIN for a re placement Disclaimer 2 3 The unit should only be used for its intended purpose as described in this man ual Use of the unit for any purpose other than that for which it is intended is done so at the users own risk and invalidates any and all manufacturers warranties e Service or maintenance work on the unit must be carried out by qualified per sonnel Only those persons trained in the operation of the SAMPLEJET shoul
44. ands from the work station are buffered on Blinking The rotary tray is turning in the direction indicated by the LED Blinking On REMOTE CONTROL is loosing the locked status Blinking Blinking SAMPLEJET is in error state If the System locked LED starts blinking the SAMPLEJET will shortly ac cept commands from IconNMR and may start moving If the System locked LED is blinking you gain more time by pressing one of the buttons In this case the tray will not move if the button is only pressed shortly Pressing both buttons for more than 15 seconds will restart the application 98 183 BRUKER BIOSPIN Users Manual Version 4 0 How to use the Remote Control Figure 14 5 System locked by REMOTE CONTROL System State Press Button to get more time 10s 123 system Idle To learn more about the system locked state of the SAMPLEJET read System Locked by User on page 34 Figure 14 6 The standard sequence system is not locked by another process System is locked by the REMOTE CONTROL Rotate Tray ystem locked SAMPLEJET Button is pressed Users Manual Version 4 0 BRUKER BIOSPIN 99 183 Remote Control Option 100 183 BRUKER BIOSPIN Users Manual Version 4 0 Basic Service Basic Service carried out by the Operator 15 1 There are some simple service operations the user may perform Calibrating the device Changing the O ring Changing the pincer Cleaning
45. anual Operating Mode 6 5 If you do not use the SAMPLEJET and work manually with the BSMS lift use this mode the BSMS lift is used if the Lift button on the BSMS keyboard is pressed ej or ij is entered in Topspin All the sliders inside the SAMPLEJET BST ADAPTER UNIVERSAL are open and the gripper moves away from the BST Use the Manual mode for working with a MAS or CryoFit system Figure 6 2 The open sliders Both sliders are open Open the door on the back of the cover to insert and remove samples The door stays open if you slide it to the very top Figure 6 3 The door on the back 50 183 BRUKER BIOSPIN Users Manual Version 4 0 Changing the Mode Changing the Mode 6 6 There are 2 different possibilities to change an operating mode Depending on the setting in the User Settings a manual or an automated change of the operating mode will be performed Use the option Let system change operating mode auto matically and define the shuttle homes if you would like to change the mode auto mated Manual change of operating mode This procedure can only be triggered from the display of the SAMPLEJET In structions are shown on the display to help change the mode Automated change of operating mode The SAMPLEJET will get the right shuttle or no shuttle for the operating mode This procedure is automatically triggered depending on the User Settings or on the VISION option if available
46. art run nit user login Default Automation Mode Eject last sample in queue Process Data Sets ater Acquisition Generate Spectrum Print Out fle in data set for possible dispatch to E mail recipient later shire wh File PT ie Autom E User Settings General C ICON Nul kA ICON NER Canl iguntiinm Automatic Lock Program ker Manager Doapoes LL Exquers mont Additional Users Originator Items Run Control Default Automat lon Moda Soplo Sequence E N Tr Eject last maple in queue Buta mati n Wirk Be Leck Shin Devt bons JE NIIT Conligqueriion Tanperatig amp User Settings L HMR Dp User Manager SampleTra Compos lto Expers iani fail Seta Additional User diets Inti Originator Items General Opti E Automation Too lB Set aster Eultches ccart ing r Butamation Uindow EF Lock Shin Opt lone Sol vent Probe Dependenc Lez Tun lg Matching i Priority Tesperature Handling L HHR Gol ions r SampleTrack Ootions Fail Sete Error Handling et Irnter tace General Options Too lBe Setup Acmount ing 118 183 x Hever Rotate the Sample Start run st user login Solvent Erw beer Pars ura Default Automat lon Moda mem Eject last maple in queue X Hover Rotata the Sample Steet run ek uper login Processing Control Benarate a Spectrum Printout Process Data Sets after Acquisition Generate Spectrum Print uk flle in data set fon possible dispatch to E mail recip
47. as a waste rc 8001 596 9 For short samples in rack 5 or used as a waste rack The Shuttle Storage 9 2 1 In the User Settings on page 53 you can define the home position of each shuttle in the Shuttle Storage Whenever the SAMPLEJET will change the oper ating mode the shuttle will be picked up from one of these 6 holders Figure 9 3 A 1mm shuttle in the Shuttle Storage Users Manual Version 4 0 BRUKER BIOSPIN 67 183 Carousel 99 5 Correct Placing of the Tubes on the Grate 9 2 2 Take care to hang the tubes correctly into their holders The caps are guided by the holder and in most cases the caps will fall into the right position when inserting the tubes If a tube is not hanging correctly the gripper will try two times to grab the cap because the first attempt to grab will often push the cap down in the hold er The second attemp has then no problem to grab the cap correctly Figure 9 4 Hanging tubes on their caps into the grate 68 183 BRUKER BIOSPIN Users Manual Version 4 0 Working with a Waste Rack Working with a Waste Rack 9 3 Up to 5 racks can be defined as waste racks in the User Settings on page 53 Short sample tubes from the openshop ring will be placed there after the NMR measurement It is easier to remove a rack with many measured openshop sam ples than to pick them from the openshop one by one Long samples will always be moved back to the openshop ring With new IconNMR software S
48. as to blow the carrier up Those inserted screws in the bypass holes serves as a presetting for the lift calibration If the set ting of the screws does not match the existing gas supply the lift calibration will fail or the carrier will not be handled smoothly The lift presetting with the bypass screws is important to get a correct lift calibration Figure 17 1 The lift bypass screws If the black DISTANCE TUBE is not installed use the bypass screws on the FLANGE for the presetting If the black DISTANCE TUBE is installed use its bypass screws for the presetting In this case insert all the screws in the FLANGE Users Manual Version 4 0 BRUKER BIOSPIN 125 183 Calibration Running the Lift Calibration 17 4 2 Calibrate from display 1 The system has to be in idle state 2 Choose the Advanced Menu from Main Menu 3 Choose Service in the Advanced Menu 4 If there is a service code set in the System Settings of the web interface type in the number Click on Calibration and then Lift Calibration C1 6 Choose a calibration routine and follow the instructions on the display Calibrate from the web interface The lift calibration is currently not available in the web interface Check the quality of the lift calibration with the lift calibration feedback on the web interface Table 17 1 Basic Lift Analysis Behaviour Reason Instruction Lift failed error during calib
49. ating Settings 13 6 The PRE HEATING UNIT has four settings which are described in the next chap ter Two examples can be found in the chapter after next Always keep in mind that the Minimum conditioning time has the higher priority than the Automatic heater allocation setting The four preheating settings 13 6 1 Heater state If the preheating is not required you can switch it off These are the 4 heater states Table 13 2 Heater states If the heater is switched off the SAMPLEJET will go to ERROR state as soon as it should put a tube into the preheating To disable preheating completely switch off the heater Set the automatic alloca tion to No automatic allocation and the conditioning time to 0 88 183 BRUKER BIOSPIN Users Manual Version 4 0 Preheating Settings Target temperature You can choose a target temperature in a given range See the table in Ex tension Specifications on page 169 for the limitations The preheating will never get colder than the ambient temperature Maximum number of subsequent samples in heater You can choose the number of samples you want to have preheating at the same time This value depends on your experiment duration your target tem perature and the tube diameter Even if it is set at zero the samples will be in serted into the preheating when the Minimum conditioning time is not zero Minimum sample conditioning time You can set a minimu
50. c to integrate a SAMPLEJET into a NMR laboratory The SAMPLEJET s capacity allows it to handle 5 racks of 96 samples 1 mm 1 7mm 3mm and 5 mm diameter and 30 47 or 99 samples max 7 length on Users Manual Version 4 0 BRUKER BIOSPIN 9 183 Introduction the outer ring of the rotating tray While the 5 racks are designed to hold tubes from batch jobs the outer ring is great for open access operating type SampleJet Benefits Overview 1 2 e SAMPLEJET can be mounted on magnets from 300MHz to 7OOMHz Fast high capacity sample changer For high throughput and openshop applications 480 sample tubes arranged in 5 racks in 96 well plate format for batch oper ation 1mm 1 7mm 3mm and 5mm tubes possible 47 sample tubes in spinners for open shop sequential operation 3mm and omm tubes or 96 short or long sample tubes 1mm 1 mm 3mm and 5mm without spinners for open shop sequential operation and 3 positions for tubes with spinners In addition 6 positions will store the shuttles or Cooling for the 5 rack positions and 30 sample tubes in spinners for open shop sequential operation 8mm and 5mm tubes Easy access for manual sample handling e Simple IconNMR control Identify racks from IconNMR by reading their barcodes with a camera Read diameter of tubes and shuttles from a matrix code Remote control option for changing openshop samples during measurement Light and door switches kit for
51. calibration shuttle and the matix code library registration file to activate the matrix code reading If one of both is missing please contact BRUKER Calibrating from the display 1 O1 The system has to be in idle state Choose the Advanced Menu from Main Menu 2 3 4 Choose Service in the Advanced Menu If there is a service code set in the System Settings of the web interface type in the number Click on Calibration and then Vision Calibration Choose the required calibration Follow the instructions on the display Calibrating from the web interface 1 2 Users Manual Version 4 0 The system has to be in idle state Open a web browser and type in samplejet or http 149 236 99 55 on the spectrometer control computer Log in to the web page as a user password bruker Choose Coordinate Calibration in the Basic Menu Choose the required calibration and follow the instructions BRUKER BIOSPIN 127 183 Calibration 128 183 BRUKER BIOSPIN Users Manual Version 4 0 Supplie Accessories s and SAMPLEJET on Workload 18 1 Once a SAMPLEJET is installed high amounts of various tubes can be mea sured BRUKER provides different hardware to meet your needs General statements Users Manual Version 4 0 18 2 Short tubes are approximately 4 long and the cap long tubes are 7 long The standard package size is 96pcs
52. can be cooled beside them 30 not cooled tubes with spinner can be placed The cooling keeps the tubes in the racks at 279 K when stored in the SAMPLE JET Carousel 30 5 cooled Cooling basic set Preheating unit See Extension Option on page 83 Figure 10 1 The carousel 30 5 cooled Users Manual Version 4 0 BRUKER BIOSPIN 71 183 Cooling option Important Remarks 10 2 Connect the nitrogen separator to compressed air when ever possible This will guaranty a normal oxygen level in the lab If the separator or the cooling is con nected to nitrogen the room needs a proper ventilation and an alarm system indi cating low oxygen concentration If the separator or the cooling is connected to nitrogen the concentration of oxygen in the air may drop to a critical value Cooled tubes may get wet from the ambient humidity When ever installing a cool ing make sure the SAMPLEJET is equipped with a SAMPLEJET preheating unit Otherwise the wet tubes will bring water into your probe head and may destroy it or disturb the NMR measurement Never operate a cooled SAMPLEJET without a SAMPLEJET preheating unit The temperatures in the preheating and the cooled carousel can be read out any time In case of a system failure these temperatures can exceed the specified range and destroy sensitive liquids in the tubes Check the temperature of the rack slots periodically Tubes are submitted for cooling at owners risk
53. ccececeececeeeececeaeeseaeseeseaeeaes 102 Cleaning the SAMPLEJET esee 104 Storing the System Data and Log Files 105 LEO mil Si M 105 System Data m 106 Loading new Firmware occ cece eee ce eee ee eee e eae eseeeeaeeaeaneas 107 Initial CONTIG UI AU M 109 ID EOQUELON see c 109 Readjusting the BSMS Lift cece cece eee ee eee eens 110 Setting up the Service Access with a Web Browser 110 The Main Window cssssesem IH 111 The Log in Window ceeeeeem mmm 112 Check Firmware Version ccccececeeceeeeeeeeeeeeeeenenees 112 Setting up the System Settings cece cece eee ee nena ees 113 Setting up the Time and Date cece cece ence eee eees 113 Setting up TOPSPIN cece ce ececeececeeeeeeaeeeeeesesseaeaeeseaeas 113 Setting up IconNMR cece cece ce eee c cece eae eeeeeeeeeaeaeeneaees 116 Setting up IconNMR for First Time Use 116 Setting up the IconNMR if already in use 117 BRUKER BIOSPIN 5 183 Contents 6 183 17 17 1 17 2 17 3 17 4 18 18 1 18 2 18 3 18 4 18 5 18 6 18 7 18 8 18 9 18 10 19 19 1 19 2 19 3 19 4 19 5 19 6 19 7 19 8 19 9 19 10 20 20 1 20 2 21 21 1 21 2 21 3 21 4 21 5 21 6 21 7 21 8 21 9 2
54. ction is designed for carriers which should remain permanently in the SAMPLEJET The best way to store the SAMPLEJET shuttles is in these park ing slots They do not occupy storage slots but the SAMPLEJET can use them to perform an automated change of the operating mode What is the Preheating Unit used for 13 3 If the SAMPLEJET is equipped with a cooling system the cold tube needs to be dried and warmed before it is inserted into the magnet The temperature of the samples is controlled with a heater and a fan to a con figurable target temperature The warming up of a sample takes place just be fore the measurement If you measure more than one probe the preheating will warm the second probe while the first is in the magnet This leads to very little loss of time Cold samples would immediately fog up due to the wet ambient air To avoid the water coming into the NMR System a little gas flow streams around the sample tubes and dries them 84 183 BRUKER BIOSPIN Users Manual Version 4 0 Using the Parking Using the Parking 13 4 To use the parking as shuttle storage you have to set the shuttles in the User Set tings to the according slot Figure 13 2 Shuttles in the parking T ry Figure 13 3 Setting the shuttles in the parking 1mm shuttle in parking slot 3 Shuttles imm Shuttle 7107648 Unit Parking Slot 3 Bhuttle ECL 1 7mm Shuttle 7106558 Unit OpenShop Ring Slot o7 Shuttle ECL Automat
55. d default 8096 The lifetime of the touch screen backlight can be extended if it is dimmed when not used You can choose the degree of dimming with this setting The recom mended value is 10 BRUKER BIOSPIN Users Manual Version 4 0 SampleJet User Settings Backlight brightness when not dimmed default 1096 The touchscreen backlight can be adjusted to suit the ambient light in the lab Light amp Door Kit option Door mode default Normal You can choose between two modes The light flashes in the Normal door mode if a door is open and the device is working This is a warning to prevent the user from grabbing a sample or rack when parts are moving In the Service door mode there is no warning when parts are moving Light mode default Automatic The light blinks slowly in the case of an error and flashes in case of danger There are four different modes for the light behavior You can switch the light on and off let the doors control the light automatically like the light in a refriger ator or choose the observe mode to have light when the SAMPLEJET is working Axes Axes speed factor default 10096 If vibrations and sample losses are not a problem you can increase the speed of your SAMPLEJET If trouble arises decrease the axes speed factor for eas ier observation The axes speed is not proportional to the sample change cycle time as the lift and communication will always take the sam
56. d oper ate the unit Read this manual before operating the unit Pay particular attention to any safety related information BRUKER BIOSPIN is not responsible or liable for any injury or damage that oc curs as a consequence of non approved manipulations of the SAMPLEJET 14 183 BRUKER BIOSPIN Users Manual Version 4 0 Emergency Stop Site Considerations Emergency Stop 2 4 The red emergency button on top of the SAMPLEJET is used to disconnect the power supply to all the drives This will immediately stop any movement of the carousel and the gripper To turn off the power completely use the switch on the back side of the SAMPLEJET POWER SUPPLY 2 5 The SAMPLEJET should be setup in a standard laboratory environment Maxi mum room temperature should not exceed the range from 17 25 C For more in formation refer to the Avance spectrometer manual on site planning available from BRUKER BIOSPIN Before Mounting the SampleJet 2 6 Make sure the magnet is firmly secured to its base in order to prevent the in strumentation from tipping over e Please check if this magnet needs a sample changer foot to extend the mag net base to get the desired stability This is the case for some 300 and 400 MHz magnets Contact BRUKER BIOSPIN if in doubt While Mounting the SampleJet 2 7 During Operation Users Manual Version 4 0 Lifting the SAMPLEJET up to the magnet requires at least two people ca 40 kg Do not try
57. e 19 4 Samples in the rack SAMPLE No SAMPLE Nof SAMPLE SAMPLE Users Manual Version 4 0 BRUKER BIOSPIN 153 183 Printout Section Loading a Rack Using the Display 19 5 1 Navigate to the main menu and press the Load Rack button 2 Select the rack to be exchanged it will then move to the front Figure 19 9 Change rack System State Load Rack 1 of 3 Change Operating Made sample in magnat 1 E 3 4 5 123 3 Open the front door and remove the old rack if there is one 4 Insert the new rack and close the front door The rack will only fit in one direc tion 5 Press Done The SAMPLEJET may start moving after 60 seconds inactivity Check that the rack is not covered and that it stands flatly on the rotary tray Figure 19 10 Points to check No cover Correct inserted 154 183 BRUKER BIOSPIN Users Manual Version 4 0 Loading a Rack Using the Remote Control Loading a Rack Using the Remote Control 19 6 1 Open the front door 2 Press a button on the REMOTE CONTROL to rotate the rack to the front Figure 19 11 The REMOTE CONTROL 3 Remove the old rack if there is one 4 Insert the new rack The rack will only fit in one direction 5 Close the front door The SAMPLEJET may start moving after 60 seconds inactivity Check that the rack is not covered and that it stands flatly on the rotary tray Figure 19 12 Points to check No cover Correct i
58. e time Figure 7 1 Cycle time vs axes speed The effect of the axes speed factor E o i m E z 20 30 Moving time s for a defined distance Users Manual Version 4 0 BRUKER BIOSPIN 57 183 User Settings Move slowly when a sample is in the magnet default enabled Normally the SAMPLEJET will reduce the revolving speed of the carousel if there is a sample in the magnet Otherwise a possible ongoing NMR acquisi tion may be disturbed If you do not care about disturbances affecting the mag net you can switch off this speed reduction Idle time until axes are switched off default Never switch off gt Defines the time after the axes switch off their current if not being used in creasing their lifetime and saving energy 58 183 BRUKER BIOSPIN Users Manual Version 4 0 Vision About Vision 6 1 The VISION option is a special GRIPPER ARM with a camera and an integrated spot light VISION is standard on newer systems and an upgrading option for pre vious SAMPLEJETS The camera can read 1 Bar code labels on the racks 2 Matrix codes on sample caps and shuttles Figure 8 1 The GRIPPER ARM 2 for the VISION option The vision calibration The camera The spotlight shuttle Figure 8 2 Barcode and matrix code The codes on different hardware Users Manual Version 4 0 BRUKER BIOSPIN 59 183 Vision Using the VISION for Bar Codes 8 2 Rack Identification To enab
59. eading the advantage is even bigger Tube diameter check and tube identification is performed by the SAMPLEJET firm ware Where to get consumables 18 4 Please contact your local BRUKER representative to get consumables or check the BRUKER web store Check the BRUKER store for shuttles tubes and caps www store bruker biospin com 130 183 BRUKER BIOSPIN Users Manual Version 4 0 Remarks on the Hardware List Remarks on the Hardware List 18 5 Table 18 1 Remarks on Hardware Pictures The pictures shows the hardware at the date of release of this manual Older or newer Hardware may look different Everything labelled with this sign has a matrix code on it and can be read with the camera of the SAMPLEJET Tubes labelled with a rack are delivered in these racks This indicates operating modes that can only be used with the CAROU SEL 99 5 This is the guaranteed insertion depth Depending on tolerances the range could be wider Try to exceed the range and check for warnings on the web interface The ECL engineering change level indicates the version of a hardware Users Manual Version 4 0 BRUKER BIOSPIN 131 183 Supplies and Accessories 1mm Parts 18 6 Table 18 2 1mm Parts for the SAMPLEJET Part Attribute Value ENKCUCCNENLI ANN CI NN 150 C 80 for ECL 01 00 Insertion depth short tubes Defined by the probehead 1mm Tubes with Caps Part Number 107503 96 pcs in a rack v Cap label
60. ers Manual Version 4 0 SampleJet User Settings You can set the insertion depth for every clampable shuttle See Supplies and Accessories on page 129 for the specifications of the shuttles Vision calibration shuttle home position ECL option The SAMPLEJET needs to know were the vision calibration shuttle is located to perform the calibration Racks e Rack Types default Rack 96 short 1mm to 5mm Samples mixed Preselect the allowed tube diameters in the rack This will have an influence on the automated change of operating modes and of the sample security if you have the vision option If you choose the Rack 96 short 1mm to 5mm Samples mixed option without having the VISION option the customer is responsible for selecting the right operating mode for the tubes being used In this case there are no safety checks for the right diameter The Rack 96 short 1mm to 5mm Samples waste for CAROUSEL 99 5 is for removing short sample tubes originally stored in the openshop ring after the NMR measurement e Sample order in the rack default Start with A1 B1 H1 and jump to A2 Some laboratories may have a certain way of addressing a rack 8 different possibilities can be chosen See also Sample Holder Numbers on page 40 If you use an IconNMR version supporting the SAMPLEJET IconNMR 4 2 and up this value will be overwritten with the settings from IconNMR nsertion test default enabled If an untrained pers
61. fications 21 11 This are the specifications for the cooling with the carousel 30 5 cooled Table 21 10 Cooling specifications Value Unit Nominal temperature Maximum temperature tolerance Temperature control Each rack separately f 0 Temperature read out Each rack separately f Maximum power consumption carousel Maximum power consumption cooler Compressed air consumption Minimum compressed air pressure EET Bar Maximum temperature of compressed air dew point 1 Standard conditions for gas 20 C 101 3kPa 65 rH ANR norm liters after ISO R558 2 3 and ISO R554 2 2 2 Work pressure supply pressure 1bar Gas flow at work pressure after ISO 1217 168 183 BRUKER BIOSPIN Users Manual Version 4 0 Extension Specifications Extension Specifications 21 12 This are the specifications for the parking section of the extension unit Table 21 11 Parking specifications Description Value Unit Parking slots for long tubes with spinners or empty Slots shuttles This are the specifications for the heating section of the extension unit Table 21 12 Heater specifications Description Value Unit Heating slots for short sample tubes with a diameter Slots of 1 to 5 mm Configurable target temperature Effective temperature Absolute temperature tolerance Relative temperature tolerance Automatic overheating protection 343 3 Temperature indicated as stable Temp offset lt 0 5 K H on display no
62. for short tubes with caps in a rack and 100 pcs for tubes with loose caps or loose caps without glass BRUKER sells also caps without glass Customers may buy their own glass that mandatory needs to fulfill the diameter specification of the caps Mounting caps on small glass diameter 1mm and 1 7mm is delicate and will be done and testes by BRUKER only Therefore we do not sell loose caps of this diameter The premounted caps on the tubes in a rack do always have a hole to allow fill ing them without removing the cap Not premounted caps do never have a hole because the tubes are filled before the cap are mounted The SAMPLEJET will never work with long tubes together with the racks be cause tubes are centered in the racks on the caps Besides the market prices short tubes are easier to produce and therefore cheaper than long tubes in the same quality BRUKER gives a progressive quantity discount on consumables BRUKER BIOSPIN 129 183 Supplies and Accessories What is to consider 18 3 Short tubes Short tubes are cheaper do not need a separate spinner for each tube and can be transported and stored in the racks When using the CAROUSEL 99 5 you can even use them for open shop applications with single tube submis sion Caps with codes Labeled caps are a gain in convenience even for systems without a code read er Since the caps have an unique number you will never mix them up For systems with a camera for code r
63. front of the SAMPLEJET Table 21 3 The display Data Value colors white on blue E Cycle Times 21 5 The time needed to exchange a Sample in the magnet depends on the operating mode the magnet and the selected safety checks These are the minimum cycle times at 10096 axes speed Table 21 4 Cycle times Operating Mode Value 1mm and 1 7mm Rack Mode approx 30 S 3mm and 5mm Rack Mode approx 35 EN Openshop Mode approx 40 EE Temperature Limitations 21 6 Do not exceed these temperature limits Table 21 5 Temperature limitations Ambient temperature Read the limitations in Site Planning for AVANCE Sys tems 300 700 MHz Z31276 Max temperature for shuttles See Supplies and Accessories on page 129 Max temperature for standard spinners Read the limitations in OpenShop and Manual Mode Probes User Manual Z31339 Max temperature of sample tubes Limitations given by the shuttles spinners Users Manual Version 4 0 BRUKER BIOSPIN 165 183 Technical Data Sample Insertion Depth 21 7 Table 21 6 Insertion Depth Data Value Unit Insertion depth for tubes in unclamped shuttles Defined by probehead Min insertion depth for tubes in clamped shuttles Default from Probehead 15 Max insertion depth for tubes in clamped shuttles Default from Probehead 2 Additional insertion depth limits for short tubes in See shuttle specification in chapter clamped shuttles Supplies and Accessories
64. ges in the Basic Service menu 4 Unreadable codes will be shown as images and can be downloaded Users Manual Version 4 0 BRUKER BIOSPIN 63 183 Vision 64 183 BRUKER BIOSPIN Users Manual Version 4 0 Carousel 99 5 What is the Carousel 99 5 9 1 This option can be mounted instead of the standard storage The CAROUSEL 99 5 storage leads to new possibilities when working without the racks This option requires at least firmware 6 Figure 9 1 The CAROUSEL 99 5 Users Manual Version 4 0 High capacity on openshop ring This storage has 96 slots for short or long sample tubes in the openshop ring and 3 additional slots for tubes with spinners No spinners needed on openshop ring The 96 tubes on the openshop ring will use one single SAMPLEJET shuttle for each diameter There is no need to store the tubes with a spinner anymore Capable of handling different tubes The 96 tubes in the openshop ring can accommodate the following diameters 1mm 1 7mm 3mm and 5mm Defined insertion depth The SAMPLEJET is responsible for adjusting the tubes in clampable shuttles BRUKER BIOSPIN 65 183 Carousel 99 5 to the right insertion depth This value can be set in the User Settings within a certain range bracks 5 racks can be placed in the middle of the storage The inserting and removing of racks is very soft preventing the magnet from shaking Separate storage for 6 shuttles Special holders on the trays will ho
65. hat oxygen warning de vice s be installed in the laboratory Always have the covers closed while working with the system 16 183 BRUKER BIOSPIN Users Manual Version 4 0 Firmware Hints What is new in Firmware 7 3 1 Support for new clampable shuttles with metal inset The clampable shuttles got a new design higher temperature limit and need ed some adjustment in shuttle handling for the lift the automated change of operating modes and in the error recovery Error recovery redesigned fast recovery possible now In some cases the error recovery does not need to operate the lift Therefore the SampleJet knows now a fast error recovery for actions which does not touch the shim system Remote control functionality added to touchscreen In the default screen on the display the System State we built in two big invis ible buttons Just press on the left or the right half of the display to rotate the carousel The system will be locked for the user with a countdown of 60s New commands for communication with IconNMR added IconNMR and SampleJet are now closer working together Current IconNMR version 4 3 will now tell the SampleJet if all measurements of a tube are fin ished and if a tube should be put in the waste rack While the first one is impor tant when working with day and night experiments the second one can separate tubes to trow away from tubes that needs to be kept Guided clearing out of measured tubes from
66. he code is also labeled in characters This in cludes the diameter x xmm the part number Zxxxxxx and the version ECLxx xx Figure 8 3 A picture captured by the VISION 62 183 BRUKER BIOSPIN Users Manual Version 4 0 Code Reading Problems Code Reading Problems 8 4 Known reasons for unreadable codes If the SAMPLEJET is not able to read a code there could be various reasons why The bar code does not match the specifications The bar code label was not stuck on the right place or is aslope he matrix code may be destroyed covered or overwritten The camera is not properly calibrated for bar codes or matrix codes Light sources from outside the SAMPLEJET disturb the reading Assure the cover is complete and the doors are closed Check what the camera reads All the codes the SAMPLEJET reads will be shown on the System Database web page For matrix codes feedback information about the readability will be shown there 1 Open a web browser and type in samplejet or http 149 236 99 55 2 Choose System Database in the Device Information menu Downloading unreadable code pictures The last 10 unreadable codes are stored as a picture and can be downloaded to give an idea of the problem The pictures get lost if the SAMPLEJET is switched off 1 Open a web browser and type in samplejet or http 149 236 99 55 2 Log in to the web page as a user password bruker 3 Choose Download Ima
67. he insertion depth is defined by the probehead Table 6 1 Number of holders for tubes without spinners Carousel Part number Holders CAROUSEL TYPE PMMA 5 Racks Z105513 5x96 5 racks CAROUSEL 30 5 COOLING Z112451 5x96 5 racks CAROUSEL 99 5 Z110929 5x96 96 5 racks openshop ring 48 183 BRUKER BIOSPIN Users Manual Version 4 0 The Spinner Operating Mode The Spinner Operating Mode 6 4 In the spinner mode the long sample tubes will be stored with their spinner in the openshop ring The user is responsible for adjusting the tube to the right insertion depth The number of spinner slots available for storage differs depending on the hard ware Table 6 2 Number of holders for spinners Carousel Part number Holders CAROUSEL TYPE PMMA 5 Racks Z105513 CAROUSEL 30 5 COOLING Z112451 CAROUSEL 99 5 Z110929 Check the height of the tube in the spinner If it is too high the SAMPLEJET could break the sample tube while moving above it The black reference caps and non BRUKER tubes are especially critical If the SAMPLEJET detects a tube beyond limitation the system stops with an error For the spinner mode the maximum allowed height of the upper tube and cap length is 60mm Figure 6 1 Limitation in the spinner mode 5 2 MEIN HI i The SAMPLEJET will break longer tubes I pil I AT Users Manual Version 4 0 BRUKER BIOSPIN 49 183 Operating Modes The M
68. ic operating mode a oe mW G change only works for shuttles 3mmc Shuttle 7105909 Unit none Slot 3 Shuttle ECL with defined home position p 5mm Shuttle 7105515 Unit OpenShop Ring Slot 99 Shuttle ECL 0 Shuttle Home Positions Shuttle ECL s Users Manual Version 4 0 BRUKER BIOSPIN 85 183 Extension Option Using the Preheating 13 5 As soon as the preheating station is set in the System Configuration list you can configure and switch on the heater to a target temperature on the Heater Com mands page or on the display in the Advanced menu in the Heater window Figure 13 4 The Heater Commands Bruker SampleJet Heater Commands Heater state off n of Current temperature 15 42K 257 73 C Target temperature 793K 324K Biz Maximum number of subsequent samples in heater P No automate altacaton Number of subsequent samples in same rack which are filled into Sel heater automatically Device Information Minimum sample conditioning time Documentation Minimum time each sample stays omn S In heater te get dry and hot About Us Login Retesh Bruker BioSpin AG Switzerland GEN Operating Mode Figure 13 5 Heater window on the display state aff Temp 30b 9K On Heater indication Target Temperature 310 5K visible on all windows Conditioning Time 1
69. ient Perform Structure Consistencuy Check DataSet M rcspement Ignore the Tanin Prorol Parameters Delebe bosponarss datasets after emnimnt ond x Allou Overurite of existing Requisition Data BEST Mode Settings Enable BEST A Alege ort Standard Ho Barcodes e BRUKER BIOSPIN Lemon Tuning M Filo bein i Priority Users Manual Version 4 0 Figure 16 11 The number of sample holders 34 poON Hidi Config in El User Settings ser Manager enge Experiments Additional Users Agence feres Automation window TaosB Setup E Automation Configuration kaser Switches i Shimming shimming Cantal Autistic Shim Fie Loading Autematie uning timeri riprity Temperature Handing Chin Opens Sample Track Options WEB ICON Interace General Options ICON NMR Account 32 Change the Default Number of Sample Holders to 596 in the Automation Setting up the IconNMR if already in use Holder Status Display Style Gyal Viewer ight Click an History of set up window Taueh Screen Large leons Hode Default Number of Sample Holders Automatic Experiment acquisition time calculation Logout ide Users Automatically Logout Delay minutes Enable Auinmaton Controls Window Autpmatic Setup File Save Approx Overhead Gime tor sample change secs External Setup Direciory Default Solvents and Experiments Deliut Sovent Default Experiment HTML Setup File HTML History File
70. if ferent colors 4 2 2 1 Supporting Vision The expanded protocol for the communication between SAMPLEJET and IconNMR enables faster work and support for the SAMPLEJET VISION option Rack Identification 4 2 2 1 One can choose between working with tube positions or working with rack identifications when using Bruker SampleTrack software Sample Order in Rack 2 2 1 IconNMR can change the sample order in the racks that was made in the User Settings of the SampleJet Different Storages IconNMR can display different SAMPLEJET carousels by choosing the number of holders 0 30 47 or 99 of the open shop Waste Rack and Status IconNMR can decide if a tube is finished or if other jobs on this tube are submitted The customer can choose if a specific tube should be returned to waste rack when measurement on a tube is finished Preheating Controlling 33 IconNMR is submitting information about subsequent tubes in queue to be put in the preheating In addition IconNMR can overwrite the conditioning time set in the Heater Commands BRUKER IconNMR software recognizes the SAMPLEJET from version 4 2 in cluded in TOPSPIN 2 1 From this IconNMR version the SAMPLEJET can be de fined as a SAMPLEJET or a BACS See Setting up IconNMR on page 116 for details 80 183 BRUKER BIOSPIN Users Manual Version 4 0 SAMPLEJET Together with IconNMR Figure 12 1 The SAMPLEJET storage overview in IconNMR bal KON MMH Automaten Aprzz
71. ion 12 1 The SAMPLEJET can perform some basic actions on its own but is normally con trolled by the TOPSPIN or IconNMR software This chapter describes the interac tion of those NMR software with the SAMPLEJET SAMPLEJET Together with TOPSPIN 12 2 You can insert and remove any probe in the SAMPLEJET trough commands on the command line Use the sx command followed by a number to empty the magnet and insert the probe with the given holder number If you just want to remove the probe use the SX ej command If the SAMPLEJET user settings were correct the SAMPLEJET will perform a change of the operating mode if needed If the operating mode cannot be changed to the desired mode the system will abort with the No sample in posi tion message Table 12 1 TOPSPIN Commands Command TOPSPIN Description sx 123 All versions Remove the current sample if there is one in the magnet Then insert the sample in position 123 sx ej Eject the sample from the magnet and place it back in storage Shows a link to the SampleJet web page Users Manual Version 4 0 BRUKER BIOSPIN 79 183 Using Bruker NMR Software SAMPLEJET Together with IconNMR 12 3 Table 12 2 IconNMR Features for SAMPLEJET Feature dH Description in TOPSPIN P All Versions IconNMR can be configured as working with a BACS Storage Overview 4 2 2 1 An overview of the storage can be obtained In this overview the state of every sample is displayed with d
72. irur osc L The leading dots are wildcard characters for the number of the rack BRUKER BIOSPIN 149 183 Users Manual Version 4 0 Printout Section Figure 19 3 H1 G1 A1 and Jump to H2 IBIQ OS Figure 19 4 H1 H2 H12 and Jump to G1 II The leading dots are wildcard characters for the number of the rack 4 0 Users Manual Version BRUKER BIOSPIN 150 183 Rack Enumerations Figure 19 5 A12 B12 H12 and Jump to A11 9ogg9g9o9o9 M GO EXE X B EX GO GGG JO Jag Joao A OG GG GO GO GG JoJo Mo G8 8 GG l2 CO COGO GO SOOO FIIO GG GG monooiuiLu ocT 9 Figure 19 6 A12 A11 A1 and Jump to B12 8 G0 808 8 8 RIESE C2 GO GO GO G0 GO QU i 2 0 O8 000 G0 2 260060 0 VDE I 2 GO GO G0 G0 G0 8 i co 8 9 i 2 COCOS BOO OOS I 8 G0 8 0G 4 O OAO u LL The leading dots are wildcard characters for the number of the rack BRUKER BIOSPIN 151 183 Users Manual Version 4 0 Printout Section Figure 19 7 H12 G12 A1 and Jump to H11 GGG GG Dota Ui S20 S OS amp G0 8 00 osoo oi S O ee ee ee O Figure 19 8 H12 H11 H1 and Jump to G12 LS DOOOOOE mononiuirur oc The leading dots are wildcard characters for the number of the rack Users Manual Version 4 0 BRUKER BIOSPIN 152 183 Content of a Rack Content of a Rack 19 4 Table 19 3 General information mea 00 o A e 1 T Tabl
73. ld the shuttles when not in use Shuttles will therefore no longer occupy any holders for tubes Waste Rack Being able to put measured short tubes from the openshop ring into a rack leads to very easy unloading of the openshop You just have to remove one single rack instead of searching and removing measured tubes from the open shop ring one by one Figure 9 2 The CAROUSEL 99 5 storage 5 rack slots 96 holders for openshop tubes without spinners 6 shuttles storage holders 3 holders for openshop tubes with spinners 66 183 BRUKER BIOSPIN Users Manual Version 4 0 Using the Carousel 99 5 Using the Carousel 99 5 9 2 The firmware will recognize the CAROUSEL 99 5 option if it is set in the System Configuration The new storage requires a new storage calibration Depending on what tube diameter you work with the setting can be changed in the User Settings on page 53 to suit the diameter of the openshop ring The SAMPLEJET will make sure the system is in the right operating mode when using tubes from the ring Table 9 1 The CAROUSEL 99 5 holder numbers Holder numbers Number of slots Used for 1 96 96 96 Short or long samples without a spinner in the open shop ring 97 99 Long samples sealed reference tubes with a spinner in the openshop ring m EE EN IT ere ee Fors samples in rack 2 or usod as waste a nen o orator sapien rack or used as a waste reco dem Farah samples inrack 4 rud
74. le the SAMPLEJET GRIPPER ARM 2 21089298 to function it has to be listed in the System Configuration If it is listed all of the coordinates and the camera need to be calibrated If matrix codes are to be read a software key and calibration is required 8 2 1 The barcode reading can be used to identify racks to the BRUKER IconNMR soft ware This creates to the possibility of setting up your IconNMR runs from the BRUKER SAMPLETRACK software to a specific rack This feature needs at least firmware 5 Since the SAMPLEJET requires more commands for communication with the IconNMR older IconNMR versions cannot be used To use the VISION you need at least TOPSPIN 2 1 to be installed containing IconNMR 4 2 Bar Code Reading Behavior 8 2 2 60 183 SAMPLEJET LIGHT AND DOOR SWITCHES are recommended for a SAMPLE JET equipped with the VISION option The device can detect if a rack has been changed Therefore all of the racks are read only as long as the doors are closed If one door is opened all racks tubes and shuttles are flagged as ID not reliable and every rack tube and shuttle accessed has to be verified again If the door stays open the continuous verification of the racks slows down the working speed Always close the doors when using the VISION option to make more efficient work possible BRUKER BIOSPIN Users Manual Version 4 0 Using the VISION for Bar Codes If a bar code could not be read the first time S
75. led tubes must be dried first in the pre heating unit before measuring them Switching on and off the cooling 10 5 The cooler and the temperature control inside the carousel are connected togeth er You can not switch on the cooler when the power supply for the carousel is switched off This is to protect the system from under cooling and getting clogged Figure 10 4 Open the cooler to switch on or off The power switch for the power supply of the carousel independent The power switch of the cooler depending on the power supply 74 183 BRUKER BIOSPIN Users Manual Version 4 0 Cleaning the Heat Exchanger Cleaning the Heat Exchanger 10 6 If a tube in a rack breaks the liquid and broken glass will fall down in to the heat exchanger In this case you have to take out the heat exchanger in order to clean it Figure 10 5 The special tool 1 Loosen two screws with the allen key 2 5 found in the SAMPLEJET tool kit 2 Lift out the Heat exchanger with the special tool coming with the cooling 3 Clean the heat exchanger and the rack slot 4 Put it back again and screw it to the carousel Figure 10 6 Remove the heat exchanger i Loosen the two screws Lift out the heat exchanger with the special tool Users Manual Version 4 0 BRUKER BIOSPIN 75 183 Cooling option 76 183 BRUKER BIOSPIN Users Manual Version 4 0 Carousel 47 5 What is the Carousel 47 5 11 1 This carousel was the first
76. llow a shuttle transport with the gripper This de pends on the inner lip of the shuttle Figure 5 7 Transporting a shuttle Inner lip transportable 1 No inner lip not transportable 32 183 BRUKER BIOSPIN Users Manual Version 4 0 Loading and Unloading Probes Loading and Unloading Probes 5 5 To gain access to the probes the Load Sample and Load Rack functions have to be used in the main menu on the display If the SAMPLEJET is equipped with a remote control accessing a sample is even easier Read the chapter Remote Control Option on page 95 The tray will rotate quickly if no sample is in the magnet If there is a sample in the magnet the tray will rotate very slowly to not disturb the NMR experiment This speed reduction can be switched off in the User Settings Read the chapter Us er Settings on page 53 Figure 5 8 Racks and openshop ring Samples in the AP Won Ai 5 racks in use openshop ring 7 Users Manual Version 4 0 BRUKER BIOSPIN 33 183 Using the SAMPLEJET System Locked by User 5 5 1 Display options to load and unload the SAMPLEJET will lock the system for 60 seconds for the user During this time the user can safely access carousel and the SAMPLEJET will not move During the last 15 seconds of this countdown the user can repetitive lock the SAMPLEJET for another 60 seconds by choosing Get more time Figure 5 9 The countdowns before unlock Change Sample Re
77. m time for a sample to stay in the PREHEATING option This will make sure your sample will reach the target temperature and com pletely dries Set the time to a start value of 3 minutes and optimize it if re quired If you set the Minimum conditioning time too short water from wet tubes may get into your probehead Users Manual Version 4 0 BRUKER BIOSPIN 89 183 Extension Option Examples of Preheating Settings 13 6 2 Example 1 Short NMR time The first example shows a set up with a short NMR time 4 sample tubes were au tomatically allocated into the heater slots for at least 3 minutes After the first sam ples the conditioning time is defined as four times the NNR time The time between following tubes in the magnet is very short Table 13 3 Heater settings for example 1 Setting Value Heater allocation Minimum conditioning time Figure 13 7 Example 1 Short NMR time starting at tune 101 Minimum conditioning Regular conditioning time 103 106 Heater slot 19 il ll T1 110 tenier iici FO EIL LI MEE Heater slot 18 101 JL NEUES II e a Ll nne Errem cim mm to Hl maa MM L1 ter BEE eee LL 1 Tel D dll Ll Ll Ll EZ time Heater slot 23 Move 101 from the magnet to the rack Move 106 from the rack to the heater Move 102 from the heater to the magnet 90 183 BRUKER BIOSPIN Users Manual Version 4 0 Preheating Settings Example 2 Long NMR time The
78. maining time to finish sect Touch to get more time 10s 15 123 system Idle system Idle The system can be locked either from display actions or from remote control If locked by one of these actions on the other device will lead to a Command re fused Other user active message These actions will lock the system Rotating the carousel from display Rotating the carousel with the remote control option The Load Rack function The Load Sample function he Remove Measured Samples function Opening the front door will not lock the SAMPLEJET for user actions Figure 5 10 System Locked by User System State system lacked by user 5Us 123 system Idle 34 183 BRUKER BIOSPIN Users Manual Version 4 0 Loading and Unloading Probes Rotating the Carousel 5 5 2 The carousel in the SAMPLEJET can be rotated with two hidden buttons on the oystem State page on the Display For directly accessing a specific sample or rack the functions described in the next chapters will be more convenient and fast er Figure 5 11 The hidden buttons System State a c EM ee NL ee o o Rotate clockwise FK o4 grow ges qo wu y y Rotate counterclockwise L Sample r magnety 7 Ko ew EEE The first press on one of the hidden buttons will Brighten the display if dimmed The second press on one of the hidden buttons will Lock the system e Switch on the light Move away the gripper
79. mm This is the start value of the insertion depth that can be set either shuttle or rack dependent Operating Modes Enabled Operating Modes default all enabled Choose the modes to work with from the list This will affect the available oper ating modes on the SAMPLEJET display when using the function Change Op erating Mode Let system decide to change operating mode automatically default disabled If this option is set the SAMPLEJET will change the operating modes automat ically This means the system has to know where the shuttles are stored when not used Read Shuttles on page 54 for the shuttles homes If the SAMPLEJET can not change the mode when needed for a sample No sample in position xx is returned to TopSpin or IconNmr Table 7 1 Automatically mode change restrictions Mode Restriction Manual The SAMPLEJET will never leave the Man mode ual Mode automatically for safety reason Spinner The SAMPLEJET will not change from Spin mode ner mode to a shuttle mode if the racks are defined as mixed for technical reason Touchscreen Touchscreen service code default 0 gt A numerical service code can be entered to override the default value to pro tect critical functions on the SampleJet This service code will be requested when functions are chosen from the display The service code will not be re quested when it has the default value Backlight brightness when dimme
80. ning Solids MAS No Sample Changer Hardware Manual Inject Eject Start ICON NMR wt Open Configuration Window haul On Express Set up Welcome to au uis R 4 5 b 8 Express Setup for First Time Use Which Automation Setup will you avail of COSampleXpress BACS Sample Changer Sample Jet OBEST Flow NMR CLC NMR GNMR Case OSix Pack Magic Angle Spinning HR MAS Magic Angle Spinning Solids MAS ONMR BioToals OSampleTrack SampleXpress BACS SampleTrack Sample Jet SampleTrack BEST ONo Sample Changer Hardware Manual Inject Eject Start IconNMR Open Configuration Window 28 Change the Default Number of Sample Holders to 596 in the Automation Window menu See The number of sample holders on page 119 Setting up the IConNMR if already in use 29 Enter IconNMR in TopSpin 30 Select Configuration in the IconNMR start window Figure 16 9 IconNMR start window HH ICON NMR av500 Eile 16 8 31 Select the Automation Configuration menu or Master Switches to change the Default Automation Mode to the desired automation mode See Select ing the Automation Mode on page 116 Users Manual Version 4 0 BRUKER BIOSPIN 117 183 Initial Configurations Hi W N HHNH Config ari Ele B User Settings zer Manager Thee Experiments Additeral pers riginnitpr Her Automnmion Veindew Teaibice Setup Figure 16 10 Selecting the automation device J St
81. nserted Users Manual Version 4 0 BRUKER BIOSPIN 155 183 Printout Section Loading a Sample Using the Display 19 7 1 Navigate to the main menu and press the Load Sample button 2 Select the sample to be exchanged it will then move to the front Figure 19 13 Change sample System Stat Load Sample 1 of 3 4 JIE sample in magnet 123 CC system Idle System Idle system Idle 3 Open the front door 4 Insert the new sample 5 Close the front door 6 Press Done The SAMPLEJET may start moving after 60 seconds inactivity 156 183 BRUKER BIOSPIN Users Manual Version 4 0 Loading a Sample Using the Remote Control Loading a Sample Using the Remote Control 19 8 1 Open the front door 2 Press a button on the REMOTE CONTROL to rotate the sample to the front Figure 19 14 The REMOTE CONTROL Rotate Tray system locked SAMPLEJET 3 Insert the sample A Close the front door The SAMPLEJET may start moving after 60 seconds inactivity Users Manual Version 4 0 BRUKER BIOSPIN 157 183 Printout Section Changing the Operation Mode 19 9 1 Navigate to the main menu and press the Change Operating Mode button Figure 19 15 Change operating mode System State ra Change Operating Mode Sample in magnet Load Sample Load Rack 1mm Shuttle 1 mm Shuttle 1 2 3 Change Operating Mode Smim shuttle 5mm Shuttle System Idle system Idle system Idle 2 Select the desired mode
82. ny common web browser located on the spec trometer computer An administrator or super user password is required to configure the hosts file If you can not change the hosts file the IP has to be used In this case a short cut has to be created on the web browser to this IP The shortcut should be named oampleJet 9 Check if the hosts file contains an entry for the SampleJet The SAMPLEJET uses the fixed IP address 149 236 99 55 This IP address is only valid in the 110 183 BRUKER BIOSPIN Users Manual Version 4 0 Setting up the Service Access with a Web Browser spectrometer network Table 16 1 Where the hosts file are located Operating System Path to the hosts files C WINDOWS system32 drivers etc hosts Figure 16 1 Hosts file E hosts notepad TE File Edit Format View Help 236 99 1 ASP ST2 Second Ethernet card 236 99 99 spect av300 av400 av500 av600 av700 av800 av900 Ethernetcar 236 99 89 drul DRU entry 236 99 88 dru2 DRU ay 205 48 6 deliver Address for delivering 236 99 55 samplejet 10 Just type samplejet in any Web browser to get access to the service web if the hostfile is modified correctly The Main Window 16 3 1 Figure 16 2 Web server start up window Bruker SampleJet Device Information Documentation AboutUs SampleJet Login testa 2 Brukor Biaspin AG Switzerland Operating Mode Users Manual Version 4 0 BRUKER BIOSPIN
83. og in to the web page as a user password bruker 3 Click on Download Logfiles on the Basic Service menu 4 Follow the instructions shown on the webpage 15 6 2 Information about the software the hardware and the user settings are stored in the system files The files are textfiles containing data in xml Extensible Markup Language structure Three files are stored BIS xml Contains information about the SAMPLEJET hardware Base xml Contains default settings and software data and will be replaced with every firmware upload User xml Contains the user settings the statistics and the calibration e Patch xml This optional file can be used for customer specific hot fixes or special tests e icDMatrixDSLinux dat The matrix code library registration file is used if you want to read matrix codes with the VISION option dmesg txt This file contains the operating system log messages The files can be downloaded through the web interface 1 Open a web browser and type in samplejet or http 149 236 99 55 2 Log in to the web page as a user password bruker 3 Click on Download System Data on the Basic Service menu 4 Follow the instructions shown on the webpage BRUKER BIOSPIN Users Manual Version 4 0 Loading new Firmware Loading new Firmware 15 7 A SAMPLEJET firmware has a deb extension and is an archive file The filena me contains some information about the software package
84. on inserts a rack they may forget to remove the cover or to check if the rack stands flatly If you switch on this option the gripper will check the rack every time a new rack is accessed e Sample insertion depth for samples in clampable shuttles default 20mm gt With this value you can set the insertion depth rack wise This is helpfully if your racks does not have the same filling height of the tubes OpenShop Ring e Sample type in slot 1 96 default 1mm to 5nm Samples gt If your system is equipped with the CAROUSEL 99 5 option you can preselect the allowed tube diameters in the openshop ring This will have an influence on the automated change of operating modes and of the sample security if you have the vision option If you choose the 1mm to 5mm Samples option without having a VISION op tion the customer is responsible for selecting the right operating mode for the tubes being used In this case there are no safety checks for the right diameter e Sample insertion depth for samples in clampable shuttles default 20mm If your system is equipped with the CAROUSEL 99 5 option you can set the in sertion depth for the openshop Users Manual Version 4 0 BRUKER BIOSPIN 55 183 User Settings 56 183 Probehead Probehead Sample Diameter default Undefined If you choose your current probehead the system will take care to allow only the valid operating modes Default Sample Insertion Depth default 20
85. on the web interface This delays could be caused of the system waiting for a previ ously cooled tube to gets warm or the gas supply to reach a minimum pres sure New light mode in user settings some users like to observe the SampleJet running sometimes The new light mode observe will switch on the interior light whenever the SampleJet is working New counter for gate and clamp slider With those two additions on the statistic counters every actor has now an indi cation of how intense this hardware was used in past New look for the System Database page The system database contains new data about if a tube was measured The web page is restructured to remain still clearly arranged Minor bug fixes Of course we are fixing any known problems as soon as we learn about BRUKER BIOSPIN Users Manual Version 4 0 Upgrading to Firmware 7 Upgrading to Firmware 7 3 2 There are some important things to know when updating to Firmware 6 They are listed below e Since Firmware 7 has a new lift algorithm all the lift calibrations needs to be re peated Without those calibrations the system will refuse working Repeat all the lift calibrations you may have from an older firmware f the software runs into a Hardware Offline see Hardware Offline on page 45 after restarting the SAMPLEJET the System Configuration may be wrong or has not supported hardware Contact BRUKER BIOSPIN for assis tance To u
86. open shop Tubes in the open shop ring will be marked as measured after they where in the magnet or even more intelligent controlled by IconNMR A new menu on the display will now help you to remove those already measured tubes Static warnings added The system will now show warnings if critical states where detected but the SampleJet is currently still able to operate normal Those static warnings are filling the last gap in exception reporting between dynamic warnings in the log files dynamic failures errors and static failures hardware offline Insertion depth can be set now rack and shuttle dependent oince different racks may have different filling heights of the tubes and since the optimal insertion depth of a tube in the probe head is related to this filling height the insertion depth can now also be set per rack Long tubes in carousel 99 5 Labeling now allowed Since long tubes will no longer be inserted into the shuttle entirely labelling on the glass below the cap is not problematic anymore New safety stops for tubes with spinner added The system will stop when a tube with spinner in the openshop exceeds the upper height of 60mm or if the shuttle will be detached on the way from the storage to the magnet Users Manual Version 4 0 BRUKER BIOSPIN 17 183 Firmware Hints 18 183 Countdown when waiting for preheating or gas pressure shown If a sample transport gets delayed this will be shown on the display and
87. page you have to press the Save Settings button at the bottom of the list You can only store a changed value on the User Settings page when the SAM PLEJET is in the Idle state and no sample tube is in the magnet Settings for optional hardware are shown only if that option is installed on your SAMPLEJET These settings are labeled with option in this chapter Users Manual Version 4 0 BRUKER BIOSPIN 53 183 User Settings SampleJet User Settings 7 2 Sample Security for Racks e Rack Occupied position default disabled If the content of a rack changes during the NMR experiment a crash may re sult when returning a tube to the rack With this option the position in a rack is checked first before a sample is returned to it If there are door sensors indicating the doors were not opened between the in serting and removing of a sample into and from the magnet the check will not be proceeded We recommend not to change the rack contents during NMR experiments Deny user access to rack if sample of the rack is in magnet default enabled The SampleJet will not bring a rack to the front door if one of the tubes of that rack is in the magnet Check sample diameter with matrix code option default disabled If you have the VISION option you can choose if the diameter of the tubes in the Racks corresponds with the preset diameter of the option Racks on page 55 Sample Security for OpenShop
88. pgrade to new firmware read the instructions in Loading new Firm ware on page 107 After the installation you should check the User Settings for your original val ues and set the new options Users Manual Version 4 0 BRUKER BIOSPIN 19 183 Firmware Hints 20 183 BRUKER BIOSPIN Users Manual Version 4 0 First Steps Getting Familiar with the SAMPLEJET 4 1 This chapter describes the SAMPLEJET for users working with the device for the very first time Of course you will find more detailed information in the following chapters Caps Every tube transported with the SAMPLEJET needs a special cap The SAMPLE JET will hold the tube on this cap when transported This makes the system ver satile it can transport different sample diameters with the same gripper Shuttles In addition to the well known spinners the SAMPLEJET works with special shut tles A shuttle always remains in the magnet and simply transports the tubes up and down For every sample diameter a specific shuttle must be used Operating Modes The SAMPLEJET has particular operating modes Basically every diameter has it own operating mode and associated shuttle types Modes can be changed manually but also automatically Storing Tubes The NMR tubes are stored in the round tray In the centre 5 slots for racks with 96 tubes each are located The outer ring the so called openshop ring contains sin gle tubes States The SAMPLEJET alway
89. ptured by the VISION eeeseeeeeeeeeee 62 9 Carousel 99 5 65 Figure 9 1 The CAROUSEL 99 5 20 0 cece cece ec ec cece memes nnne 65 Figure 9 2 The CAROUSEL 99 5 storage esses 66 Figure 9 3 A 1mm shuttle in the Shuttle Storage sssuss 67 Figure 9 4 Hanging tubes on their caps into the grate 68 10 Cooling option 71 Figure 10 1 The carousel 30 5 cooled c ccc cece eee ee eens nsec ee eeeeeeeenens 71 Figure 10 2 The heat exchanger cccccccceececeeeeeeeeeeeseaesseeeaeeseananenes 73 Figure 10 3 Carousel cooled top view c ccc cceccce eee eeeeceeeeeeaeeeeeeaeenenes 73 Figure 10 4 Open the cooler to switch on or off uuueseussse 74 Figure 10 5 The special tool ccccccccccececeececeeeeseeeaeeseaesseeeaeeneansnenes 15 Figure 10 6 Remove the heat exchanger cccccecececeeeeeeeeeeeeeeaeeeeeeeens 75 11 Carousel 47 5 77 Figure 11 1 The CAROUSEL 47 5 00 0 cece cece ec ec eee eeeeseseeeaeaeaeenees 77 Figure 11 2 The CAROUSEL 47 5 storage esee 78 12 Using Bruker NMR Software 79 Figure 12 1 The SAMPLEJET storage overview in IconNMR 81 13 Extension Option 83 Figure 13 1 The PREHEATING UNIT esee 83 Figure 13 2 Shuttles in the parking ccc cc ccecece eee eeeee ee eeeeaeeeeeeaeeeenes 85 Figure 13 3 Set
90. r apply any force to the drives axis or rotary tray of the SAMPLEJET Ap plying force may lead to a misadjusted calibration which may result in a crash and or sample destruction 46 183 BRUKER BIOSPIN Users Manual Version 4 0 Operating Modes Introduction 6 1 The operating modes the installed hardware the carriers the caps and the tubes are all related in someway This chapter describes all the relations modes and parts SampleJet Operating Modes 6 2 The SAMPLEJET has the following different operating modes 1mm Shuttle e 1 mm Shuttle e 3mm Shuttle e 5mm Shuttle e Spinner Manual The operating modes are named after the carrier spinner shuttle they use In the User Settings one can disable the unused operating modes to simplify the handling when changing the modes manually and also protect the system from going into a wrong mode Users Manual Version 4 0 BRUKER BIOSPIN 47 183 Operating Modes The X Xmm Shuttle Operating Mode 6 3 In the shuttle operating mode of a specified diameter the samples will be stored without a spinner in the rack or the openshop ring There will only be one shuttle remaining in the shim system for all the samples The clampable shuttles 3mm and 5mm clamp the tube that allows it to spin and adjust the insertion depth of the tube The shuttles for the smaller diameters 1mm and 1 7mm do not clamp the tubes Therefore spinning is not possible and t
91. ra Most probably the gas supply Change the lift presetting by clos tion is too weak for your lift preset ing some bypass holes with screws ting or enhance the gas supply to the Calibration feedback over 80 SAMPLEJET Then repeat the cali bration Carrier hitting the sliders on top Too many bypass screws Change the lift presetting by open of the shim stack hard closed ing some bypass holes with screws Then repeat the calibra tion Carrier hitting the turbine on the Corrupt lift calibration or Repeat the lift calibration bottom of the shim stack hard unstable gas supply 126 183 BRUKER BIOSPIN Users Manual Version 4 0 Vision Calibration Vision Calibration 17 5 oystems which are equipped with a camera require this calibration The calibra tion is available when the appropriate gripper arm is listed in the System Configu ration The calibration routine can be started from the display or the web interface To start a vision calibration do the following Calibrations Gripper camera for bar codes This procedure calibrates the position of a bar code on a rack This will take around thirty seconds Gripper camera for matrix codes This will calibrate the matrix code reading For this calibration the vision cali bration shuttle is needed and has to be set in the User Settings This calibra tion will take around thirty seconds For the matrix code calibration you need to have the vision
92. rking with priorities of measure ments e g nighttime daytime experiments Read more in chapter SAMPLE JET Together with IconNMR on page 80 Through the web interface you can have a overview of already measured samples on the System Database page from the Device Information menu To reset the status flags you can press the All measured samples removed on the Basic Commands page from the Basic Service menu Figure 5 14 Removing Samples Remove Measured Samples Measured Samples Pod 5 5 samples Removed system Idle see also the detailed description of how to use this function from the display in chapter Removing Measured Samples on page 159 Users Manual Version 4 0 BRUKER BIOSPIN 37 183 Using the SAMPLEJET Loading Racks 5 5 5 Figure 5 15 Loading Racks The rack mode uses the samples stored in the five racks in the carousel Since these samples are not stored with a spinner a shuttle is used Use the Load Rack function in the Main menu of the SAMPLEJET display for inserting or removing racks This will rotate the chosen rack position to the front door Figure 5 16 Bring the desired rack to the door Load Rack 1 of 3 Select Rack System Idle See also the detailed description in chapter Loading a Rack Using the Dis play on page 154 A check of the rack cover and positioning is activated in the User Settings 38 183 BRUKER BIOSPIN Users Manual Version 4
93. rs Manual Version 4 0 BRUKER BIOSPIN 143 183 Supplies and Accessories Table 18 5 5mm Parts for the SAMPLEJET Attribute Label color Diameter Clamping the tube Rotatable Transportable No Max temperature 120 C For operating modes Spinner Manual em Spinner Pme tO feo 144 183 BRUKER BIOSPIN Users Manual Version 4 0 Limitations Limitations 18 10 Table 18 6 Limitations on the SAMPLEJET Part Attribute Value Standard Caps Manual mode only Description These are not SAMPLEJET caps Only the SAMPLEJET caps have the right geometry to guarantee successful sample transport with the SAMPLEJET 1mm Shuttle for BACS Limitation Manual mode only Description This is a 1mm carrier designed for the BACS sample changer You can not use them as a 1mm shuttle for the SMAPLEJET Match System Limitation Manual mode only Description Match spinners and samples should not be used in the spinner mode of the SAMPLEJET o Users Manual Version 4 0 BRUKER BIOSPIN 145 183 Supplies and Accessories Table 18 6 Limitations on the SAMPLEJET Part Attribute Value Older Spinners Limitation Manual mode only Not recommended Description Older spinners without a yellow mark must not be used in the spin ner mode of the SAMPLEJET It is possible to use them in the man ual mode but not recommended For Operating Mode Manual 146 183 BRUKER BIOSPIN Users Manual
94. rtly dinero TTE 11 Figure 1 4 SAMPLEJET Hardware esses nene 11 Figure 1 5 Different Carousels for the SAMPLEJET 12 2 Safety 13 Figure 2 1 Warning hazardous area 20sessssenennnensnnenennnennnnennnnnnnen 13 Figure 2 2 Warning LASER hazard ccccccceceeeececeeeeeeaeseeeeesseaeas 14 3 Firmware Hints 17 4 First Steps 21 5 Using the SAMPLEJET 23 Figure 5 1 The simplified states as a diagram sususse 23 Figure 5 2 Navigating through the menu cc cece ce ee cece eee eeeeeeeeaees 24 Figure 5 3 The System State window ccccce eee ee ee eeeeeeeeeneeeeeaeaes 24 Figure 5 4 The display menu tree eeeeseeeeeeenenn 26 Figure 5 5 The SAMPLEJET web page seem 27 Figure 5 6 The web page menu tree 2sssusenensnnennnnnnennnennnnen nennen 29 Figure 5 7 Transporting a shuttle 0u2u22220020nanennnnnnnnnnennnnnnnnn nenn 32 Figure 5 8 Racks and openshop ring esses 33 Figure 5 9 The countdowns before unlock cc cece cece ec ec eee eeeeeeeeaees 34 Figure 5 10 Figure 5 11 Figure 5 12 Figure 5 13 Figure 5 14 Figure 5 15 Figure 5 16 Figure 5 17 Figure 5 18 Figure 5 19 Figure 5 20 Figure 5 21 Figure 5 22 System Locked DY User 2 ici a see ebene 34 Tne nidden DUNO rcp 35 Loading Samples s extestirsutae
95. s Manual Version 4 0 Replacing the Pincer Mounting a new pincer 6 Insert the new pincer until a click sound can be heard Make sure the orientation of the pincer is correct There is no gap between the pincer and the black pen Figure 15 3 Inserting the pincer Check the orientation of the pincer Close the Cover 7 Remount the back cover Restarting the system 8 Release the emergency button by turning it clock wise The application will be restarted Users Manual Version 4 0 BRUKER BIOSPIN 103 183 Basic Service Cleaning the SAMPLEJET 15 5 If a sample tube is broken all the glass has to be removed from the SAMPLEJET otherwise the racks will not stand properly on the rotary tray Stop the SAMPLEJET operating before you start cleaning the device Don t forget to stop the submitted jobs in IconNMR Pay special attention to the toothing of the rotating tray If it is not clean the drive cogwheel may be damaged If proper cleaning is not possible through the front door remove one of the side covers Angled allen key 2 5 If the gripper arm disturbs the cleaning it can be moved away Choose the Load Rack or Load Sample function from the display 104 183 BRUKER BIOSPIN Users Manual Version 4 0 Storing the System Data and Log Files Storing the System Data and Log Files 15 6 If troubleshooting an unknown error BRUKER BIOSPIN may ask you to send the log files and system
96. s indicates a state Before a command is sent it is in the idle state then it changes to busy when transporting a sample If something goes wrong the system changes to error state Human Interfaces There is a touchscreen on the front of the SAMPLEJET It is mainly used for load ing and unloading tubes With a standard browser you can access a web inter face This is used for setup and installation Running the Device You can use sx commands from TopSpin or set up jobs from IconNMR Users Manual Version 4 0 BRUKER BIOSPIN 21 183 First Steps 22 183 BRUKER BIOSPIN Users Manual Version 4 0 Using the SAMPLEJET Introduction 5 1 In this chapter the handling of the SAMPLEJET for standard use is defined SampleJet states 5 2 Before operating the SAMPLEJET it is important to know the general behavior of the device It works as a state machine that means it jumps from one defined state to an other These are the simplified states Booting Idle Busy defined action Recovering Error defined error e Shutting down Hardware offline During operation the SAMPLEJET jumps from the idle to busy state and back again Figure 5 1 The simplified states as a diagram Hardware offline r Users Manual Version 4 0 BRUKER BIOSPIN 23 183 Using the SAMPLEJET Accessing the SAMPLEJET 5 3 In addition to the display on the front of the SAMPLEJET there is also a built in
97. safer faster and more convenient work with the SAMLEJET 10 183 BRUKER BIOSPIN Users Manual Version 4 0 SampleJet Overview SampleJet Overview 1 3 The SAMPLEJET is based on modules which are shown below Figure 1 2 SAMPLEJET front view with closed casing CASING i CONTROL UNIT with LCD touch panel SAMPLE MOUNTING UNIVERSAL It is mounted onto the magnet with the MAG MOUNTING It accommodates the different heights of the BST shim upper part and magnet Figure 1 3 An inside view of the SAMPLEJET with the casing partly removed CASING CONTROL UNIT USC LIGHT AND GRIPPER ARM DOORS SWITCHES or GRIPPER ARM 2 3 AXIS SYSTEM CAROUSEL DRIVER hidden CAROUSEL BST ADAPTER DESEE DE DER POWER SUPPLY The SAMPLEJET will be placed on top of the MAG MOUNTING and tightened with 4 star screws Figure 1 4 SAMPLEJET Hardware The rack A shuttle A short tube with cap Users Manual Version 4 0 BRUKER BIOSPIN 11 183 Introduction Inside the SampleJet 1 4 Figure 1 5 Different Carousels for the SAMPLEJET CAROUSEL 99 5 CAROUSEL 30 5 COLLED 12 183 BRUKER BIOSPIN Users Manual Version 4 0 Safety Warnings and Notes in this Manual 2 1 There are two types of information notices used in this manual These notices highlight important information or warn the user of a potentially dangerous situa tion The following notices will have the same level of importance throughout this manu
98. sage over and over again the system has serious problems you can not handle without assistance from BRUKER The system will go to the manual mode to enable at least manual insertion of samples Figure 5 21 The states of an error recovery q Full Error Recovery Action 1 2 3 Startup Error Error during System in Error PENES State uM Message j Error Recovery System Idle 1 Fast Error Recovery Action 1 2 Fast and Full error recovery Depending on the Error the SampleJet chooses a fast or a full error recovery A fast error recovery will be performed if The error recovery was started from the display and not from the web inter face The BST is in a defined state 7 lower BST adapter slider closed Starting a error recovery from the web interface will always choose the full error recovery Users Manual Version 4 0 BRUKER BIOSPIN 43 183 Using the SAMPLEJET Figure 5 22 Floating Shuttle in Error Recovery Hint If a shuttle is towering the BST adapter as shown in Floating Shuttle in Error Recovery on page 44 the action Assure that BST is empty in the full error re covery can skipped by just pressing the Done button 44 183 BRUKER BIOSPIN Users Manual Version 4 0 Hardware Offline Hardware Offline 5 8 The system goes into to the Hardware Offline state if an error occurs during ap plication startup These errors cannot be handled with the Error Recovery
99. se quence There are 3 possible reasons for the Hardware Offline state If no hardware or firmware was changed 1 There is a defective hardware If firmware was changed 2 The new firmware does not support the old hardware If hardware was changed and hardware is not defective 3 The System Configuration has wrong values If you have a Hardware Offline situation contact your local BRUKER BIOSPIN representative You cannot solve the problem on your own except after loading new Firmware In this case try to load the old firmware again In the Hardware Offline state the web interface is operational for functions which do not access the SAMPLEJET hardware e g loading firmware Users Manual Version 4 0 BRUKER BIOSPIN 45 183 Using the SAMPLEJET Emergency Stop 5 9 The red emergency button on top of the SAMPLEJET disconnects the power sup ply to all the drives This will immediately stop any movement of the carousel and the gripper The emergency button can also be used to restart the application If the emergency stop has been pressed the application is restarted when the button is released This will then lead to an error recovery in any case Important Things to Keep in Mind 5 10 e Never interrupt the busy state of the SAMPLEJET Just wait until the opera tion is finished and the state is idle before sending commands to the SAM PLEJET from the display or the web interface Neve
100. second example shows a set with long NMR times No sample tubes were automatically allocated into the heater slots But because of the 3 minute condi tioning time every tube will go to the heater before going into the magnet The time between following tubes in the magnet is longer than in the first example but short in comparison to the NMR time This setup will not put any tube into the heater during the long NMR time Table 13 4 Heater settings for example 2 Setting Value Heater allocation Minimum conditioning time Figure 13 8 Example Long NMR time starting at tube 101 Minimum NMR time Minimum D Magnet 15 Heater slot 18 Heater slot 19 Heater slot 20 Heater slot 21 Heater slot 22 Heater slot 23 Heater slot 24 Heater slot 25 Move 101 from the magnet to the rack Move 102 from the rack to the heater Users Manual Version 4 0 BRUKER BIOSPIN 91 183 Extension Option Preheating on a Power Failure 13 7 The SAMPLEJET recognizes all the sample tubes in the preheating slots as long as the SAMPLEJET is turned on The Emergency Stop button makes the appli cation restart The system remains the information about the samples in the heat er at that time because the SAMPLEJET did not lose current If the SAMPLEJET ever loses its power supply you have to empty the pre heating slots before starting up the system again Since there is a fixed order of placing the tubes in the preheating slo
101. solution partner Bruker BioSpin provides a world class market leading range of analysis solutions for your life and materials science needs Our ongoing efforts and considerable investment in research and development illustrates our long term commitment to technological innovation on behalf of our customers With more than 40 years of experi ence meeting the professional scientific sector s needs across a range of disciplines Bruker BioSpin has built an enviable rapport with the scientific community and various specialist fields through understanding specific demand and providing attentive and responsive service Our solution oriented approach enables us to work closely with you to further establish your specific needs and determine the relevant solution package from our comprehensive range or even collaborate with you on new developments O lt N Mm N Q o S Mm S X 2 Mm Bruker BioSpin Group info bruker biospin com www bruker biospin com
102. t blinking Tubes automatically allocated in the preheating Tubes configurable Minimum conditioning time configurable Users Manual Version 4 0 BRUKER BIOSPIN 169 183 Technical Data 170 183 BRUKER BIOSPIN Users Manual Version 4 0 Bruker Biospin Contact General Questions 22 1 Submit your inquiries regarding SAMPLEJET sales and service to your local BRUKER BIOSPIN representative Use the following address to acquire further information Contact for Sales Information 22 2 For further technical assistance please do not hesitate to contact us directly at BRUKER BIOSPIN AG SAMPLEJET Info Industriestrasse 26 8117 Fallanden Switzerland Phone 41 44 825 98 80 E mail samplejet info bruker ch Contact for Additional Technical Assistance 22 3 For further technical assistance please do not hesitate to contact us directly at BRUKER BIOSPIN AG SAMPLEJET Service Industriestrasse 26 8117 Fallanden Switzerland Phone 41 44 825 98 90 E mail samplejet service bruker ch FTP ftp ftp bruker ch pub NMR download SampleJet Users Manual Version 4 0 BRUKER BIOSPIN 171 183 Bruker Biospin Contact 172 183 BRUKER BIOSPIN Users Manual Version 4 0 Figures 1 Introduction 9 FIOUTE Tel SAMPLEJE T Systemi cack cateceutcess amet mida rds Sp IE I E eine bis 9 Figure 1 2 SAMPLEJET front view with closed casing 11 Figure 1 3 An inside view of the SAMPLEJET with the casing pa
103. t connected to any other networks such as the company internal net work Do not connect the SAMPLEJET to another network because the fixed IP addresses may cause problems The only computer that can access the web interface is the spectrometer comput er from the NMR system One of the two installed ethernet cards belongs to the closed network of the spectrometer Every SAMPLEJET has the IP 149 236 99 55 which is defined in the hostfile of the spectrometer computer as samplejet Figure 5 5 The SAMPLEJET web page Bruker SampleJet The current state SampleJet Bruder BioSpin AG Switzerland The operating mode The pending action Operating Mode ati The user status Users Manual Version 4 0 BRUKER BIOSPIN 27 183 Using the SAMPLEJET To access the SAMPLEJET just enter samplejet or http 149 236 99 55 in a web browser window The web pages are dynamically created on the web server the web browser will receive html pages only Therefore no java extension is needed Always use the mouse to press the buttons on the web page instead of hitting the Enter key The SAMPELJET shows different pages depending on the user level The user account should be used only by the NMR system administrator Table 5 1 Login table Login Password Rights out If you log in as a User you can harm the system if you are not careful 28 183 BRUKER BIOSPIN Users Manual Version 4 0 Figure
104. tessutesese iso a ea ea ues 36 Bring the desired tube to the door cccecceceeeeeeeeeeeeees 36 REMOVING Samples eee tet vba a 37 ILeOAGING RACKS uesmetareudtadittant vn eT td mam arsaamenaieeees 38 Bring the desired rack to the door sesssus 38 Remove the cover of the rack cccccececeeeeceeeeeeseeeeeeaeas 39 How to insert a rack correctly esseseeeseeseeeee 39 The enumeration of the rack ccccccececeeeeceeeeceeeeseeeaeaes 41 An error message nase 42 The states of an error recovery cece cece eee e cece ee eeeec eases nenn 43 Floating Shuttle in Error Recovery eeeseesese 44 6 Operating Modes 47 Figure 6 1 Users Manual Version 4 0 Limitation in the spinner mode seeeeeeeee 49 BRUKER BIOSPIN 173 183 Figures 174 183 Figure 6 2 The open sliders sese mme 50 Figure 6 3 The door on the back cccccc cscs cceececeeceseaeeseeeaeeneanasenes 50 Figure 6 4 Changing the operation mode on the display 51 7 User Settings 53 Figure 7 1 Cycle time vs axes speed 2 0 cece ec ec cece eeeeeeeeeeseeeaeaeeeeneas 57 8 Vision 59 Figure 8 1 The GRIPPER ARM 2 for the VISION option o9 Figure 8 2 Bar code and matrix code ununesesesenennnenenennennnnnnnnenenen nenn 59 Figure 8 3 A picture ca
105. the SAMPLEJET e Storing the system data e Storing the log files Loading new firmware Calibrating the Device 15 2 The calibrating is described in chapter Calibration on page 121 Changing the O Ring 15 3 The O ring on the Gripper should be changed once a year If the rubber loses its elasticity caps can not be held anymore Spare O rings can be found in the SPARE PARTS KIT Figure 15 1 Change O Ring Change this O ring once a year Users Manual Version 4 0 BRUKER BIOSPIN 101 183 Basic Service Replacing the Pincer 15 4 If the SAMPLEJET should crash for any reason the pincer is the weakest point and should break first to prevent the system from serious damage Once a pincer loses one or more of its four legs it has to be replaced Even an undamaged pincer should be replaced after 3 years The drives have to be switched off for this procedure Switching off the drives 1 The system has to be in the idle state 2 Press the red emergency button 3 You can now move the gripper arm manually Open the Cover 4 Remove the back cover to access the gripper arm Removing the broken pincer 5 Try to remove the pincer with your fingers Pull the blue pincer down firmly while holding the gripper arm with the other hand The older design pincer could not be removed by hand Use gripping pliers and be careful of the magnetic field Figure 15 2 Replacing the pincer 4 102 183 BRUKER BIOSPIN User
106. the same diameter will be labeled with the same color Every diameter has its own color The colors refer to the BRUKER match system as close as possible Table 5 2 The defined colors Color Diameter Black DEB ec The colors on the shuttles and caps serve as a visual check of having the right shuttle for the right tube diameter BRUKER BIOSPIN Users Manual Version 4 0 Caps and Carriers Caps 5 4 2 BRUKER BIOSPIN delivers factory assembled sample tubes and caps There is a hole in the cap where sample liquid may be filled through The Gilson liquid han dler s needle fits through this hole It can be closed once with a pellet If the cap does not hold onto the sample with sufficient force 6 Newton the sample could be lost during transportation in the SAMPLEJET The SAMPLEJET caps are consumables they can only be used once If caps are used over again they might not sit tight enough on the tubes Users Manual Version 4 0 BRUKER BIOSPIN 31 183 Using the SAMPLEJET Carriers 5 4 3 Carrier names Shuttle A shuttle is a carrier which stays in the shim system during operation It simply transports a sample up and down Some of the shuttles clamp the sample for sample spinning Spinner All the rest of the carriers are named spinners Check if existing carriers can be used with the SAMPLEJET See Supplies and Accessories on page 129 Transportable Shuttles Some of the first shuttles will not a
107. ting the shuttles in the parking esse 85 Figure 13 4 The Heater Commands cece cece eee ee ee eeeeeeeaeeseaeeaeenens 86 Figure 13 5 Heater window on the display eseeeeeeeeessee 86 Figure 13 6 The Basic Commands page csse 87 Figure 13 7 Example 1 Short NMR time starting at tune 101 90 Figure 13 8 Example Long NMR time starting at tube 101 91 Figure 13 9 Order of putting next tubes in the slots 92 Figure 13 10 Top view on the extension cccccccce eee eeeec eases eaeeeeeeeeeeenes 93 14 Remote Control Option 95 Figure 14 1 The REMOTE CONTROL e 95 Figure 14 2 Where to connect the REMOTE CONTROL 96 BRUKER BIOSPIN Users Manual Version 4 0 Figures Figure 14 3 The pads zen ansehen 97 Figure 14 4 Using the REMOTE CONTROL sese 97 Figure 14 5 System locked by REMOTE CONTROL eese 99 Figure 14 6 The standard sequence ccc cece cece eee eeececeeeeeeaeeeeseeeeeaeas 99 15 Basic Service 101 Foure 19 1 Change O RING es eu 101 Figure 15 2 Replacing the pincer 22204222020 00 nenne nennen nenne nennen nenn 102 Figure 15 3 Inserting the pincer 2u202022220n0nnnnennnnennn en nn nennen nenn 103 Figure 15 4 Filename nomenclature
108. ts one can find out what tube is in which slot in case of a power failure Figure 13 9 Order of putting next tubes in the slots 22 23 24 25 92 183 BRUKER BIOSPIN Users Manual Version 4 0 tensi EP side z 7 9 11 en Users Manual Version 4 0 BRUKER BIOSPIN dd NS Extension Option 94 183 BRUKER BIOSPIN Users Manual Version 4 0 Remote Control Option What is the Remote Control used for 14 1 The REMOTE CONTROL allows the changing of openshop samples without dis turbing a running NMR measurement Furthermore the exchanging of a rack or an openshop sample is very easy Only two buttons are used the users do not have to know the menu on the display This is useful if many users are placing racks and samples in the SAMPLEJET A minimum of SAMPLEJET firmware version 4 is used to operate the REMOTE CONTROL It is not possible to harm the SAMPLEJET by uncontrolled pressing of the buttons on the REMOTE CONTROL Figure 14 1 The REMOTE CONTROL Users Manual Version 4 0 BRUKER BIOSPIN 95 183 Remote Control Option How to Install the Remote Control 14 2 The installation of the REMOTE CONTROL is simple and can be easily carried out by the customer if the REMOTE CONTROL is ordered after the installation of the SAMPLEJET 1 The SAMPLEJET has to be in idle state 2 Remove the cover on the right side gt Angled allen key 2 5 3 Feed the plug through
109. turn DATE FAILURE OCCURED SYSTEM ORDER NO DISPATCH NO The customer signatory confirms that the returned product is absolutely free of any hazardous substances e g toxic corrosive explosive biologically dangerous or radioactive Signature COMPANY INSTITUTE NAME X MAILING ADDRESS CITY POSTAL CODE COUNTRY PHONE NO This form is a corrected copy of the original ZFQS0083 form version 02 162 183 BRUKER BIOSPIN Users Manual Version 4 0 Technical Data Shipping 21 1 The SAMPLEJET is packed in a single cardboard box on a standard euro pallet Tilt and impact indicator stickers can be located on the sides of the box Table 21 1 Shipping Data Value Unit en Supply on Operation 21 2 The SAMPLEJET requires electricity and compressed air or nitrogen Table 21 2 Supply on operation Data Value Unit Electrical power active approx 50 eese 1 SE 1 Standard conditions for gas 20 C 101 3kPa 65 rH ANR norm liters after ISO R558 2 3 and ISO R554 2 2 2 Work pressure supply pressure 1bar Gas flow at work pressure after ISO 1217 Users Manual Version 4 0 BRUKER BIOSPIN 163 183 Technical Data Required Place in the Lab 21 3 Figure 21 1 SAMPLEJET dimensions Magnet side view wo gg uiu wo g KEW Magnet top view 145 cm i 103 cm 164 183 BRUKER BIOSPIN Users Manual Version 4 0 Display Display 21 4 There is a touchscreen on the
110. ty and Repair Declaration 20 2 This safety and repair declaration is applicable for NMR probes e Shim systems e Sample handling systems Bruker s analytical instruments may be exposed to hazardous substances when used by customers Whenever a customer returns a system or its components to Bruker e g for repair upgrade loan returns exchange etc the customer accepts the following obligation It is the explicit responsibility of the customer to make sure that the returned products are absolutely free of any hazardous substances In case of omission to do so Bruker will hold the customer liable for any result ing personal injuries and or damages caused to Bruker employees and or to other persons exposed to the hazardous substances The customer is liable for all damage caused to Bruker e g with the cleaning up of hazardous substances decontamination security measures etc The customer is also liable for any other direct and or indirect damages that may be caused to Bruker by the hazardous substances Q I ACCEPT THIS OBLIGATION The completed and signed form has to be attached to the returned product Otherwise customer returns for the above mentioned products cannot be processed The safety amp repair declaration form has to be signed by a Bruker service engineer if the system was never operated by the customer e g prior to completion of the installation PRODUCT PART NO SERIAL NO FAULT DESCRIPTION reason for re
111. up of a IconNMR version 4 The setting up should be done analogical to the description like with other versions IconNMR version 4 2 or later supports SAMPLEJET specific functions Depending on the IconNMR version different automation modes are available Table 16 3 Selecting the Automation Mode IconNMR Version Standard BACS Working by referring to positions Automation Mode Description referring to bar code ID s on the racks Only with the VISION option gt 4 2 sample Jet Working by referring to positions sample Track Sample Jet If a SampleTrack is installed you can work by If the customer is using IConNMR for the first time the setup is slightly different than if IconNMR is already in use If IconNMR is in use continue with Setting up the IconNMR if already in use on page 117 Setting up IconNMR for First Time Use 16 7 1 26 Enter IconNMR in TopSpin 2 Select the automation mode in Express Setup for First Time Use See Se lecting the Automation Mode on page 116 116 183 BRUKER BIOSPIN Users Manual Version 4 0 Setting up the IconNMR if already in use Figure 16 8 IconNMR Express Setup Window CON NMR Express Set up Welcome to snl u NM Express Setup for First Time Use Which Automation Hardware will you avail of 9 BACS Sample Changer BEST Flow NMR O LC NMR O NMR Case O Six Pack O Magic Angle Spinning HR MAS Magic Angle Spin
112. web server accessible The web interface is used for setup and service the dis play for normal operation Both of them depend on the firmware and can be differ ent in any versions Access from the Display 5 3 1 The Display on the SAMPLEJET is equipped with a touchscreen The menu is built as a tree shown in The display menu tree on page 26 all functions are guided Figure 5 2 Navigating through the menu Enabled function Example 1 of 2 Go to the superior Disabled function menu if any Go to the next Go to the previous function panel function panel in this menu in this menu State of the device Logged in for service It is possible to protect the service menu by setting a code in User Settings on the web interface If no password is set you do not have to log in and out The Lo gout button is then disabled If the display is not accessed for 3 minutes it shows the System State and is dimmed The dimming options can be set through the web interface in the Basic oervice menu on the User Settings page Dimming the display will increase the lifetime of the background light Figure 5 3 The System State window System State sample in magnat 123 system Idle 24 183 BRUKER BIOSPIN Users Manual Version 4 0 Accessing the SAMPLEJET Hint The background light of some of the displays is getting darker and darker with increasing operating hours If it is unreadable contact BRUKER BIOSPIN

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