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USER MANUAL MODEL 653 TWO-WIRE pH/ORP

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2. 18 Entering a Dassword sss 18 pH CALIBRATION sscisstintouabsietieasthaminesiaietantic 20 Standardizing Single Buffer Calibration 21 Calibrating Two Buffer Calibration 22 Grab Sample Standardization 24 Selecting a Buffer 25 Electrode Mamtenamnce 26 Replacing Blectrodes 26 Output Hold in Calibration Mode 26 IC Controls Manual Calibration of Offset and Slope 27 Temperature Compensation for pH 27 Manual Temperature Compensation Sm nie E 27 ORP CALIBRATION Fur E Ua LOREMS 28 Selecting a Standard for Calibration 28 ORP Standardization 29 Blectrode a u ette 29 ORP Manual Calibration 29 4 mA to 20 mA OUTPUT SIGNAL 30 Reversing the 4 mA to 20 mA Output 30 Simulated 4 mA to 20 mA Output 30 Output Dampmg eeeeeeeeeeeeeeeeeeeeeeeeaee 31 CAUTION AND ERROR MESSAGES 32 Error and Caution Messages for pH 32 Error and Caution Messages for ORP 34 Error Messages for Temperature 34 CONFIGURATION OF PROGRAM 35 TROUBLESHOOTINGO eee 37 Transmitter Problem Troubleshooting 38 pH Electrode Troubleshooting 39 ORP Electrode Troubleshootng 40
3. ELECTRONIC HARDWARE ALIGNMENT Instrument Shop Procedure The following instructions are intended for instrument personnel to adjust the transmitter if necessary This procedure should be performed in an instrument shop or safe area location Do not perform electronic adjustments in the field Devices referred to in the following descriptions are shown on component location drawings D5990188 and D5990189 Proper field wiring for hookup is shown on drawing D5990196 These instructions assume 24 VDC power is hooked up the calibration of input electronics are operational and field wiring is in place Calibration of pH Input Input for measurement circuit zero is 0 00 V at high impedance BNC connector normally found in the wiring chamber in the back of the model 653 or on preamp in field J Box Measured voltage at pH test point TP pin 7 of U100 should be 0 600 VDC No adjustment required as the unit is factory set with 2 000 V in and pH set point set to 2 29 V via constant set in eeprom not field adjustable NOTE There is no span adjustment because the chemical calibration always varies it to suit the electrode Calibration of Temperature Input The temperature input of the 653 is so reliable that no adjustable electronic parts are needed The stability and repeatability of the 1000 ohm RTD temperature circuit typically needs no adjustment Adjustments often lead to lower accuracy due to the difficulty of knowing the true
4. and keys to move between digits and use the T and keys to adjust each digit When ENTER is pressed to go into edit mode two things will happen First the last digit will start blinking to show that this digit can be changed Second any blank spaces will change to zeros and a plus or minus sign will appear Now each digit can be accessed Change between positive and negative numbers by switching between plus and minus sign using the 1 or key when the plus minus segment is blinking Press ENTER again to leave edit mode Before the new value is changed the transmitter will check the new value to make sure that it is within range If the new value is lower than the lowest value allowed for that frame then the transmitter will use the lowest allowable value instead of the new value entered Likewise if the new value entered is higher than allowable then the highest allowable value is used instead The transmitter will display whatever value it has stored in memory Example Change the output low setting from 0 pH to 2 pH From the menu select out LO The current set point e g 0 00 will be displayed Press ENTER to select edit mode The display will change to 00 00 and the last digit will start blinking Press lt twice to move left two digits The third digit from the end will now be blinking Press the f key to change the 0 to 2 Press ENTER again and the display will change from 400 00 to 02 00 indicating th
5. key to display Err and press SELECT to view the error codes detected by the transmitter Calibration Settings If the transmitter was calibrated previously then the transmitter will use the calibration settings from the last successful calibration otherwise default settings are used Error and caution messages generated during the last calibration will remain in effect For pH transmitter IC Controls recommends a full two buffer chemical calibration after initial startup Refer to the pH Calibration or ORP Calibration section as required Transmitter settings and parameters can be viewed and or changed at any time Refer to the menu on page 3 the areas shaded in dark orange indicate program settings Serial Number Display The transmitter s unique serial number can be reviewed at any time Press the D AG key or the SAMPLE key 4 times to call up the startup display routine above This does not change any of the settings The serial number is the 10 digit number that scrolls across the screen um 653 211 www iccontrols com Page 11 EASY MENU IC Controls EASY MENU The layout of the program is shown in the menus found on page 3 The menu can be used as a quick reference guide to all the transmitter functions Remembers Where You Were The transmitter remembers where home base is which areas of the menu were used last and it will loop around the columns in the menu The menu can be explored using the arrow keys to find any parameter
6. part number A1100052 A1100052 6P blue 10 0 pH buffer part number A1100053 A1100053 6P These buffers come in 500 mL bottles and are also available in six packs 6P um 653 211 www iccontrols com Page 19 pH CALIBRATION IC Controls Standardizing Single Buffer Calibration Standardizing the transmitter causes the transmitter to calculate the offset for the pH electrode which can be viewed both before and after standardization The electrode slope value determined during the last buF2 calibration will be maintained Press SAMPLE to display the pH reading Press SELECT to reach the main menu then use the 7 or key to display CAL Press SELECT then use the f or key to display buF1 Press SELECT again to reach the next menu A buffer needs to be selected with which to calibrate the transmitter Use either automatic detection a custom value or one of the standard buffers 4 7 10 For further details refer to Selecting a Buffer for an explanation of the buffer selection process Place the electrode in the buffer solution then press SELECT to start the calibration process The display will show a flashing pH reading to indicate that the transmitter is reading pH in calibration mode and is waiting for the operator to press ENTER once the pH has stabilized As soon as the electrode has stabilized and the ENTER key is pressed the display will stop flashing the electrode offset will be calculated and the new offset
7. procedure For further details refer to Selecting a Buffer for an explanation of the buffer selection process Press SELECT again to start the calibration process The calibration with the second buffer works similar to a standardization except that additional error checking is possible and the slope efficiency cust will be calculated If an error occurs at this point the settings from the j standardization buF1 selection will be kept Either retry the calibration Auto with a second buffer buF2 or resume normal operation with the settings 401 from the standardization 4 01 J 7 00 J 10 0 j CALIBRATE pH Ka ENTER Illustration 16 Second buffer um 653 211 www iccontrols com Page 21 pH CALIBRATION IC Controls Example Assume the process normally has a pH in the caustic region above 7 pH Calibration will be performed using 7 pH and 9 pH buffer values the 9 pH buffer was chosen to demonstrate the full functionality of the 653 Press SAMPLE to go to the pH display Press SELECT then use the or keys to select CAL Press SELECT again to reach the calibration menu Use the f or keys to select buF1 then press SELECT again to select a buffer from the menu First use auto buffer recognition AUTO prompt Put the electrode s in the first buffer Start with 7 pH buffer solution then press SELECT to start the calibration process The display will flash the pH readi
8. the output response to the change in the input signal can be observed This is useful for verifying program settings and for testing the hardware calibration To simulate a different 4 mA to 20 mA output signal press ENTER to enter edit mode Edit the displayed mA value to display the desired output needed for testing the output signal Press ENTER to select the displayed value The output signal will be adjusted to put out the desired current This process can be repeated as often as necessary The output signal is held at the displayed level until the program leaves this part of the menu um 653 211 www iccontrols com Page 29 4 mA to 20 mA OUTPUT SIGNAL IC Controls Output Specifications pH ORP Maximum Span 0 pH to 14 pH 2000 mV Span Adjustment 0 01 pH mV Output Resolution 0 01 pH 1 mV Table 2 Output specifications Output Damping The 4 mA to 20 mA output can be damped to provide the user with a means to deal with rapidly varying or noisy signals Damping range is 0 seconds to 40 seconds With 0 seconds there is no output damping and each reading the transmitter makes is used to directly update the display and 4 mA to 20 mA output The factory default 5 seconds adds the next 4 seconds of readings to the first and divides by 5 giving very fast response Selecting 40 seconds adds the readings for all 40 seconds and divides by 40 providing an excellent smooth damping out of turbulent readings Any s
9. 3ADN33 JL AWHD 201 HLIM 34d3IHS aza NY 0337 3H AYW 3394331N 009 Y NDILVSVd3s 438A TvNv H SN3S ONO 303 CHAD NOD E 3S LON XD4 INA O1 NOJ123MND2O 133314 SI SNISIA S USN3S SVINVIS El w GLHA O Nar 291 CR Aa Atr2 5 Ug di E ven 3s 20 xni 207 9 mon cn 9 9 gt EP EERE 20 IER an S mn in Se Elend eg a sina 9155 Y HA 438 NO Q T3IHS HD 33 WV 3dLN323 NO 55419 b co E ono C438 El a oam 3N8 001 41 1fid1nD LAANI GK di INGWNaLSNI XxOoH 009 ALONAY YOSNYS um 653 211 www iccontrols com Page 48 IC Controls DRAWINGS um 653 211 www iccontrols com Page 49 DRAWINGS D4850015 600 Interface Installation Page 50 IC Controls MODEL 600 RECOMMENDED INSTALLATION WEATHERPROOF EXPLOSIO 4 5000 4 5000 LII 600 N PROOF J BUX 3 4 4 RECOMMEND DUAL U BOLT CLAMP TU SUPPORT PLATE FOR SUBMERSIBLE APPLICATIUNS LIQUID LEVEL WAA 3 4 CPVC SUBMERSION SUPPORT PIPE COR SENSOR BODY Se Seel TYPICAL SENSORS ALTER WEATHERPROOF SURFACE TYPE J BOX MODEL 600 71 NATE INSTALLATION 6 8900 600 71 gt LN 4 9200 sch 1 T 1 L T CONDUIT TO ANALYZER ES RECOMMENDED 3 4 AND FI
10. 47 in x 5 47 in refer to drawing D4990070 The 653 option 8 P N A2500267 pipe mounting kit may also be used to mount the transmitter by using the 2 inch U bolts refer to drawing D4990069 The 653 option 7 P N A2500268 wall mounting kit may also be used to mount the transmitter by using the holes in the mounting plate for wall studs using customer supplied studs refer to drawing D4990073 Field Mounting Orientation The 653 can be field mounted in any 90 degree increment from standard When panel mounted this is generally not applicable Use the procedure below to select the desired field mounting orientation 1 First calibrate the transmitter to the desired range in the instrument shop and install in field mounting kit provided Take transmitter to field to check orientation If the transmitter is in the correct orientation go to step 8 If the transmitter is not in the correct orientation take it back to instrument shop Q vc N Loosen the panel mount screws on either side of the 653 then remove from the mounting kit panel 6 Move the 653 in desired direction 7 Reinstall using step 5 in reverse order 8 Mount transmitter with the hardware provided Page 6 www iccontrols com um 653 211 IC Controls INSTALLATION Transmitter Wiring The transmitter requires 24 VDC power via the 4 mA to 20 mA TB200 terminals 1 and 2 Refer to drawing D5990189 for component location For stable operation the trans
11. ERROR key function ENTER Key The ENTER key is used to access the ability to change values or edit settings DIAG ENTER SAMPLE gt SELECT ERROR CANCEL Illustration 11 transmitter keypad um 653 211 www iccontrols com Page 13 EASY MENU IC Controls EDIT MODE Edit mode is used to change a numeric value or to select between different options The values and settings which can be edited are identified by the darker shading in the menus Any frame which has a white background cannot be modified by going into edit mode but can be viewed Editing by Selecting a Setting Examples of selecting a value are on off settings and switching between different units e g metric or imperial Editing a value is like picking an option from a list only one item on the list can be viewed at a time Example Turning output off From the menu select out ON OF The transmitter will now display either ON or OFF which are the two choices To change the setting press ENTER to go into edit mode The display will start blinking Use the 7 or keys to switch between the possible options which in this case are ON and OFF When ON is displayed press again to accept the new setting and leave edit mode Editing a Numeric Value Numeric values such as an alarm set point are adjusted by going into edit mode and then adjusting each digit until the new value is displayed Use the
12. LO from the menu The current value will be displayed Press ENTER to go into edit mode The transmitter will display PASS for 2 seconds because a password needs to be entered first Level 1 security is needed to change this setting Select PASS from the main menu again Change the displayed value to 0001 which is the level 1 password and press ENTER The transmitter will display good followed by ACC 1 indicating that the password is valid and that level 1 access has been achieved Try changing the output low setting again This time edit mode can be attained unhindered Select PASS from the main menu again Enter the level 2 password which is 0002 Change the level 2 password to 0000 in order to disable password security Password 2 is found in the configuration menu and therefore requires level 2 access before it can be accessed Select CONF PAS 2 from the menu Press ENTER with 0000 displayed Both passwords are set to 0000 again and password security is disabled um 653 211 www iccontrols com Page 17 SECURITY Page 18 ENTER PASSWORD PASSWORD 2 ENTERED NO PASSWORD 1 ENTERED 0000 ENTERED YES YES ACCESS ACCESS ACCESS ACCESS LEVEL 0 LEVEL 0 LEVEL 1 LEVEL 2 VIEW ONLY VIEW ONLY OPERATOR COMPLETE DISPLAY DISPLAY DISPLAY DISPLAY bAd good good ACC 0 ACC 0 ACC 1 ACC 2 IC Controls Illustration
13. and consumable items electrodes and all solutions being stored at temperatures between 5 C and 45 C 40 F and 110 F in a non corrosive atmosphere IC CONTROLS consumables or approved reagents must be used or performance warranty is void Accessories not manufactured by IC CONTROLS are subject to the manufacturer s warranty terms and conditions Limitations and exclusions Industrial electrodes and replacement parts are warranted to be free from defects in material and workmanship for a period of three 3 months from the date of installation or eighteen 18 months from the date of shipment when used under normal operating conditions and in accordance with the operating limitations and maintenance procedures given in the instruction manual and when not having been subjected to accident alteration misuse abuse freezing scale coating or poisoning ions Chemical solutions standards or buffers carry an out of box warranty Should they be unusable when first out of box contact IC CONTROLS immediately for replacement To be considered for warranty the product shall have an RA Return Authorization number issued by IC CONTROLS service department for identification and shall be shipped prepaid to IC CONTROLS at the above address In the event of failure within the warranty period IC CONTROLS or its authorized dealer will at IC CONTROLS option repair or replace the product non conforming to the above warranty or will refun
14. isolated max load 500 Q Convertible to 1 VDC to 5 VDC um 653 211 www iccontrols com Page 45 IC Controls DRAWINGS DRAWINGS D5990188 O 48a8us 3 053s gtl Ada 88106650 6ap spe CG8 cco cGy NIQ Z 1 w pasn YOLVIOT LN3NOdWOO ivo AV 1dSIG S3I383S NIG Z 1 SW 3 iIL 0p9uoj3 O 401u aen eBuvupg STOULNOD Jj ddo HYD 90 e tt 243 4P a yop AG on lay Component Locati Disp we 30 ou 108 Ir saf HH uL e CN La TI9H89 N Um S ee L FOI nb T Rm E mou 401 a D CD ACEP 2 MMS432N q OrdSIGQ en SL A3u 9F0LS8 N Nd AV 1dSIG 11 TOT WO wo s eoooooooooooooo I d I 2 d I d I d I 8 3013933135 39NV V 012313S 39nYa SS HOLY DN um 653 211 www iccontrols com Page 46 DRAWINGS IC Controls Se FEIS 3j 05s A 29 681066S0e s spe Nia Z L S9 ul pasn NOILVOO ONISIM LN3NOdNWOO 59 3dONW 3M 0p0uoj O J401u aj aBuoap STOULNOD 9 Wiring 8 Component Location SNE dd et ENEE 152524 ma II oe TR W DOO xe Via 8 SEN e OOQ gt vive DOO OOOO OOD D5OOOO0000QI 9 DOO 2 2 RBMOOQOOOOOd e O
15. mV Temperature 5 C to 105 C 23 F to 221 F Keypad 8 pushbutton entry keys Enclosure Le DIN aluminum panel mount Case Dimensions 144 mm x 144 mm x 132 mm 5 7 in x 5 7 in x 5 5 in Weight 1 4 kg 3 0 Ib Shipping Weight 1 8 kg 4 0 Ib Shipping Dimensions 46 cm x 30cm x 23 cm 18 in x 12 in x 9 in Environmental Data PROPERTY CHARACTERISTIC Temperature Operational 5 0 C to 45 C 41 0 F to 113 F Storage 10 0 C to 55 C 14 0 F to 131 F Relative Humidity 80 Yo maximum non condensing Enclosure Ratings IP65 Nema 4X when installed in panel RFI EMI resistant Electrical Ratings 24 VDC min 16 VDC max 40 VDC lift off voltage 16 VDC 4 to 20 mA Electrical Requirements 16 VDC to 40 VDC 24 VDC nominal Quality ground required for microprocessor Operational Data PROPERTY CHARACTERISTIC Accuracy pH 0 5 Yo of measured range ORP 0 5 Yo of measured range Temperature 0 3 C Precision pH 1 digit 0 01 pH ORP 1 digit 1 0 mV Temperature 1 digit 0 1 C Response Time 90 within 5 s default function of flow and temperature Damping adjustment 0s to 40s Temperature Automatic 1000 Q RTD Compensation Auto 5 C to 105 C 23 F to 221 F Manual 5 C to 105 C 23 F to 221 F Output One continuous programmable 4 mA to 20 mA output
16. mV then the transmitter looks alright c If the reading is far from 7 pH or 0 mV do a single point calibration and note the pH ORP reading and the offset value FOURTH Problem isolated If the offset is within 10 mV of zero then the transmitter wiring and preamp are good If the transmitter and the equipment are good then the problem is in the probe refer to the Electrode Troubleshooting section If the offset is greater than 10 mV the problem may be in the equipment transmitter wiring or preamp refer to the Transmitter Problem Troubleshooting section A x l III BNC Fitting Paper Clip Short Illustration 24 BNC fitting Illustration 25 Paper clip short test on BNC fitting Page 36 www iccontrols com um 653 211 IC Controls TROUBLESHOOTING Transmitter Problem Troubleshooting If the offset is higher than 10 mV check the wiring between the preamp and its terminal block to see if there are any loose or faulty connections Frayed corroded or broken wires here are the most common cause of equipment problems If the wiring looks good and after recalibration a large offset is still present a Use the paper clip U at the transmitter terminal block and short between the reference common and the signal This procedure bypasses the preamp and wiring b A new single point calibration can be done to see if there is a
17. messages Error and Caution Messages for pH Error Description Causes Solutions E1 2 Offset gt 1 3 pH units Large offset in electrode To calibrate select 4 7 10 or This error generated by custom buffer to allow for offsets auto detection of 4 7 10 of up to 4 pH units buffers only Previous offset istelained Wrong buffer used Only Specify correct buffer and redo 4 7 10 pH buffers can be calibration auto detected E1 3 Offset gt 4 pH units Wrong buffer used Select correct buffer Previous offset retained Bad electrode Perform maintenance Electrode not detected Check connections um 653 211 www iccontrols com Page 31 CAUTION AND ERROR MESSAGES IC Controls Error Description Causes Solutions E1 4 Electrode efficiency less than 60 or greater than 110 Nernstian response slope is too flat or too steep Previous calibration is retained buF2 calibration done before buF 1 calibration Use buF 1 for first buffer then buF2 for slope Buffers used in buF1 and buF2 are too close together or are the same buffer Select buffers which are further apart Do buF 1 calibration only and use old slope Wrong buffer selected Redo calibration with correct buffer E1 5 Temperature Process outside of TC Use manual temperature compensator is off scale operating rang
18. or pH 10 if needed NOTE Required for pH selection only Before putting the transmitter into operation verify the settings to ensure that they agree with the intended setup 10 For the 4 mA to 20 mA output set high limit and low limit 11 Set preference for temperature units C or F in CONF unit 12 Set desired input signal damping if known default is 5 second 13 The transmitter is now ready for field installation um 653 211 www iccontrols com Page 9 INSTALLATION IC Controls NOTICE OF COMPLIANCE US This meter may generate radio frequency energy and if not installed and used properly that is in strict accordance with the manufacturer s instructions may cause interference to radio and television reception It has been type tested and found to comply with the limits for a Class A computing device in accordance with specifications in Part 15 of FCC Rules which are designed to provide reasonable protection against such interference in an industrial installation However there is no guarantee that interference will not occur in a particular installation If the meter does cause interference to radio or television reception which can be determined by turning the unit off and on the user is encouraged to try to correct the interference by one or more of the following measures Reorient the receiving antenna Relocate the meter with respect to the receiver Move the meter away from the receiver Plug
19. 13 Password validation www iccontrols com um 653 211 IC Controls pH CALIBRATION pH CALIBRATION The pH transmitter is calibrated using one of several methods A one point standardization adjusts the electrode offset while maintaining the previous slope The two point calibration combines the results of the standardization with the results of the buF2 calibration and calculates the slope as well as the offset The grab sample calibration is a convenient method to adjust the electrode offset in cases where it is not possible to physically remove the pH electrode from the process A calibration is easily accomplished by selecting an appropriate buffer placing the electrode in the buffer solution and letting the sensor stabilize typically around 3 minutes Once the value is stable press ENTER The internal diagnostic tests will activate warning or error messages if faulty operation is suspected or detected Errors detected during calibration will not cause the transmitter to lock up Slope Yo efficiency Offset mV pH CALIBRATE pH Illustration 14 pH menu The 653 features an automatic output hold Output hold goes into effect as soon as SELECT is pressed with CAL displayed The output hold feature avoids false alarms and erratic signal output caused by a routine calibration Buffers automatically recognized by the 653 are red 4 01 pH buffer part number A1100051 A1100051 6P green 7 00 pH buffer
20. 15 A9120098 Terminal strip 6 CKT A2101513 Explosion proof J box only 600 71 pH Interface Wall Mount A2500178 pH ORP preamp D5990196 D4850015 A2100049 Preamp holding bracket A9120050 Terminal block 6 CKT A2101514 Weather proof wall mount J box only Consumable Supplies A1100051 4 0 pH buffer red 500 mL A1100051 6P for 6 pack A1100052 7 0 pH buffer green 500 mL A1100052 6P for 6 pack A1100053 10 0 pH buffer blue 500 mL A1100053 6P for 6 pack A1100054 Mixed 6 pack 2 each of A1 100051 A1 100052 A1100053 A1600050 pH calibration kit 1 year supply A1100083 263 mV ORP standard 6 calibrations A1100084 66 mV ORP standard 6 calibrations A1100087 476 mV ORP standard 6 calibrations A1600061 ORP calibration kit 1 year supply A1100192 Deionized rinse water 500 mL A11000192 6P for 6 pack A1100090 Electrode storage solution 500 mL A1100090 6P for 6 pack A1100091 Electrode wash solution 500 mL A1100091 6P for 6 pack A1100092 pH renew solution 500 mL A1100092 6P for 6 pack A1100094 Gentle scale remover 500 mL A1100094 6P for 6 pack Page 44 www iccontrols com um 653 211 IC Controls Appendix C 653 Specifications Appendix C 653 Specifications Physical Data PROPERTY CHARACTERISTIC Display Four and one half LCD digits 1 5 cm 0 6 in displays for pH or ORP temperature error codes prompts and diagnostic information Display Ranges pH 0 pH to 14 pH units ORP 2 000 mV to 2 000
21. ELECTRONIC HARDWARE ALIGNMENT 41 DISPLAY PROMPT S sizani 42 GLOSSARY EE 43 Appendix A Default Settings 44 Appendix B Parts List 45 Appendix C 653 Specifications 46 ITT 47 D5990188 Display Component Location 47 D5990189 Wiring amp Component Location 48 D5990196 600 Interface Wiring 49 D4850015 600 Interface Installation 51 D4990069 Pipe Mount Kit 52 D4990070 Panel Mount Kit 53 D4990073 Wall Mount Kit 54 INDUSTRIAL PRODUCTS WARRANTY 55 INDEX eegene eeh 56 O Copyright 2006 IC Controls Ltd All rights reserved Page 2 www iccontrols com um 653 211 IC Controls 653 MENU pH ORP SAMPLE home base CHANGES Areas shaded in dark orange indicate program settings which can be changed by the user Menu areas shaded in light blue indicate view only um 653 211 CONTENTS SLOP Slope Yo efficiency OFFS Offset mV pH CALIBRATE Un lr ir gt E S gO HHO Ye main menu OLd HOLd SEt C F Auto 3 F Offset mV er mv CALIBRATE 66 mv HOLD mv Err See list of error and caution messages ERROR ON OF Output damping sec ge cur CONF See Configuration Menu Accessible on
22. Equation which relates the voltage signal produced by the electrodes to the pH of the sample The equation is temperature dependent ORP Oxidation Reduction Potential The potential developed by a metallic electrode when placed in a solution containing a species in two different oxidation states Oxidation The loss of electrons by a molecule or ion RAM Random Access Memory Memory in RAM can be both written to and read from The contents of RAM will disappear as soon as the RAM chip loses power Redox Reaction A chemical reaction involving transfer of electrons from one element to another ne element is being oxidized another element is being reduced Hence the word redox Reduction The gain of electrons by a molecule or ion TC Temperature Compensator Temperature Compensation Correction for the influence of temperature on the sensing electrode The transmitter reads out concentration as if the process were at 25 C regardless of actual solution temperature Page 42 www iccontrols com um 653 211 IC Controls Appendix A Default Settings Appendix A Default Settings The following program settings are the default settings for the transmitter New transmitters will have these settings unless the setup has already been customized for the user s specific application Outputs pH ORP Input to be transmitted pH ORP Low setting 0 00 2000 mV High setting 14 00 2000 mV ON OFF switch ON ON Global units Metri
23. GRAM IC Controls CONFIGURATION OF PROGRAM The 653 transmitter has been designed with ease of use in mind In most cases the transmitter has oa A int Jj E Initialize analyzer settings been configured to ordered specifications at the factory and no configuration of the transmitter is pH option ORP option necessary However several hardware options are available and if pH jd y S mec camping sec they are changed the program ap kr dA j DEEN trout damping sec configuration settings need to be set accordingly for the program to CONF j ck dA E Eh input damping sec function properly Corrs y QUE onse on Selecting the pH or ORP option i G Use metric units The 653 is designed as a single input TE Use imperil unts pH or ORP Transmitter It can be field configured to change from the Set level 1 password pH option to the ORP option by a PAS 2 Set level 2 password and enable security simple menu selection When pH is selected the ORP menu will disappear Also when ORP is Illustration 23 Configuration menu selected the pH menu will disappear Initializing All Program Settings Occasionally it may be desirable to reinitialize all of the program s settings to bring them back to defaults Executing the initialization procedure will cause the transmitter to reset all the program variables and settings to factory defaults and then proceed with the normal startup display The initialization proce
24. MPLE key 14 Security access level 17 disabling 18 enabling 17 password 18 password 17 password 2 17 SECURITY 17 selection 27 Sensor mounting 8 wiring 8 Serial number 11 Simulated current output 30 Slope 27 efficiency 23 IC Controls manual adjustment 27 Nernstian response 23 Specifications 46 Startup 9 diagnostics 11 display 11 error checking 11 loss of power 11 program initialization 35 shop test 9 STARTUP 11 Temperature 27 Temperature calibration 36 default value 27 displaying 27 offset 36 Temperature compensation 27 43 Temperature compensation manual 27 standard buffers 25 Temperature dependence curves 25 Timer 15 minute time out 12 security time out 12 Troubleshooting 38pp electrode 39p isolating the problem 37 preamp 38 transmitter 38 wiring 38 TROUBLESHOOTING 37 Units 36 Version 11 Wiring 7 10 Page 56 Www iccontrols com um 653 211
25. Pressing SAMPLE key will return display to home base Pressing the key will return the user to exactly the area of the menu most recently accessed Home Base Press SAMPLE The SAMPLE key s function is to give the user a known starting point displaying the home sample or home input The SAMPLE key is usable from anywhere in the menu The pH ORP display is the home base display for the transmitter The transmitter s two inputs pH ORP and temperature are arranged underneath each other at the left hand side of the menu Use the f or key to display each of the readings in turn From anywhere in the menu the SAMPLE key can be used to return to the pH ORP reading or home base display The program will safely abort whatever it was doing at the time and return to displaying the pH ORP sample reading SAMPLE SAMPLE home base home base PH ei 7 51 orP 125 j E L LS Zei Illustration 8 pH home base Illustration 7 ORP home base Features 1 The transmitter has a built in timer which returns the program to displaying the home base if no key has been pressed for 15 minutes This time out has the same effect as pressing the SAMPLE key 2 If security has been enabled the time out will change the access level back to 0 or 1 automatically which gives the user read only access The user will have to enter an appropriate password to go to a higher access level 3 Whe
26. Q a ve DOOOQ DOO E zon Ge OO e OQ a DOOOQ Lafe lt SR e 5050401 DOO B bdl OOO e OQ EE DOOOQ e Lee p zdL 8017 duo Hd 5090901 e Lee dal 00901 e 0 e eieiei H DOOOQ R20 e OOOOQDOOOOCOOCOOCOOUDOOOOUCOOCOOCOOCOOCOOCOOCOD K x 060509050 0505050506060606060606060606060606060606060605 ete QO0O0O0Q0O00 LvOLGSEN Nd GL Aan 99 1300N 11 A 6S Zeie BX SO OOO OOO DOO OOO ote o 105262 OQ emo cem O D vw 52528 w opa P Safe DOO ora 01 OOO OOD z 9 DOOC DOO aet OOO OOO m eeh DOO OOO OQ m E eeh DOO m 2 OO OQ FA 3 DOOC DOO 2 2 OOO 2522 eet OQ Oo DOOM DOO A OOO OQ 22 DOCOC oe EE ee OQ sE DOOC DOO OOO OQ DOCOC DOO SOO OO DOOC DOO OOO ote ettet ote Dv vw OOK 001481 y I d I 2 d I E d I d I 8 80123 13S 39NV3 V 3013317135 39NV SSH21V1 OWDI QDAE D5990189 Page 47 trols com Www iccon um 653 211 IC Controls DRAWINGS iring 600 Interface WI D5990196 jo 43345 et Mn S9 009 1v31 MUSN3S ANY a007 D2 v HiD8 NO AGB 96106650 aap pel g t 2 Jay S7435 LINGNOD ONILYY v54d NIbINIYW Di H3ZA bus 59 00 2100529 EZIDZ6Z Nd SV STDMINDS JI wOad 3 786 TAY 3IN3NMD23N 0 1099 DAD34 318v2 AITANS YSHOLSNI JIVASAINI 00 Kam ad COD 8000D0269 Nd Sv STDMINDO JI Wai 3789 TVA ONISIA Jun pw 66 N30 T38 31892 30N3MMOU233 03 lad0S YIWOLSNI GEO oj wiug niabung Feel 273 YA SIOHLNOS dl aoe Aer Jl TNA3IN SPH 3OSN3S 3I
27. TOYULNOD 9j zeg Kal AJIA ACIS of LS EEN 0000 EIS di ol DES E ir 08EE 9 S310H ONILNNOW 917 ANDA SeIE T A3IA N L 8 EIEZ E 091271 091271 B m q sgssroqss V l 91 X SIZE LIAIN dd 31DN ae E E nee I I I 2 H tL H Sr8z 8 b d EN I C b mi S ESH MM SAN g I A3IA IN o KS _ A aji BS all WW pall WE EES E 1 gt T TP ex ei i IC EES E Iessen sanas es J silts _ 41 89St 4 site s B aCrt Page 53 www iccontrols com um 653 211 INDUSTRIAL PRODUCTS WARRANTY IC Controls INDUSTRIAL PRODUCTS WARRANTY Industrial instruments are warranted to be free from defects in material and workmanship for a period of twelve 12 months from the date of installation or eighteen 18 months from the date of shipment from IC CONTROLS whichever is earlier when used under normal operating conditions and in accordance with the operating limitations and maintenance procedures in the instruction manual and when not having been subjected to accident alteration misuse or abuse This warranty is also conditioned upon calibration
28. TTINGS RECOMMEND 90 ELBOW PIPE TO HELP LIFT SUBMERSION SENSOR FOR 600 71 RECOMMENDATION FOR EASY FLEX CONDUIT TO SENSOR SHOULD BE 4 THAN SENSOR PLUS S LIQUID TIGHT FLEX CONDUIT GRIP AT TOP OF SENSOR REMOVAL AND CALIBRATION LONGER UPPORT PIPE 63E SENSOR LEAD LENGTH RECOMMENDATIONS 643 ND 22 gt FOR 600 LENGTH OF SUPPORT PIPE PLUS 0 3 METER FT 605 NU 22 ge min FOR 600 71 2X LENGTH DF SUPPORT PIPE PLUS 15 METER 617 ND 22 FD m by jdate JB CONTROLS dr E F C 9 9 99 Orangeville Ontario Canada chk TITLE INSTALLATION app INDUSTRIAL pH INTERFACE MODEL 600 de dwg no coe Om pa4gsoois IRE V scole sheet of 1 0 www iccontrols com um 653 211 DRAWINGS IC Controls 0 T jO 48aus 91025 Add 69006670 Gump apo ul Basen LIX LNAUW Jdld Scd t6 66 90 01 O 4 JALIL opouvg olaogup wW A Buo4 J 66 90 10 CO lt STOYLNOD amp l 830p AQ Mount Kit ipe Pi S1 E Co LJAJVveug I CH a Sr DwuccT r9 wut Z28 0 WWZET SZ S DIE 0527 S DIE 0S2 I uu 2 S2901 Dwwucor Set y uucG 1 re H uueg 00878
29. USER MANUAL MODEL 653 TWO WIRE pH ORP TRANSMITTER 1 2 DIN HOUSING um 653 211 53 SERIES TRANSMITTER EA J le YA I YA HA LIA WA v Ld d d ID CONTROLS CONTENTS CONTENTS CONTENTS ui 2 SEN Le LEE 3 INTRODUCTION giereg 5 AA AAA 5 Eeatutes ergeet 5 INSTALLATION E 6 Transmitter Mounting 6 Field Mounting Orientation 6 Transmitter Wiring 7 Electrical Installaton esses 7 Sensor Mounting 8 Sensor WIPE iere tete redes sasa 8 Instrument Shop Test Startup 9 STARTUP ccna cis laitaijnaresos EROR NO Rp o PRORA bends 11 Transmitter Startup Tests 11 Calibration Settings 11 Serial Number Display 11 EASY LE EE 12 Remembers Where You Were 12 Home Base Press SAMPLE 12 ATTOW KEYS inorena tee tenete ere eus 14 DIAG and ERROR Keys 14 ENTER K y 5er eerte 14 EDITMODE EE 15 Editing by Selecting a Setting 15 Editing a Numeric Value 15 Key Functions in Edit Mode 16 SECURITY waa MER o ane a 17 Enabling Password Security 17 Disabling Password Security
30. al temperature compensation has been selected then the manual temperature compensation set point is used Other Buffer Values or Custom Buffers IC Controls 4 01 pH BUFFER 15 28 5 45 55 65 75 B5 95 105 Temperature Degrees Celsius Illustration 18 Temperature compensated pH buffer 4 I 7 16 7 14 2 12 7 10 7 08 a 7 06 7 00 pH BUFFER 7 04 7 02 7 00 6 98 8 98 7 m 15 25 35 45 55 65 75 B5 95 105 Temperature Degrees Celsius S lustration 19 Temperature compensated pH buffer 7 10 0 pH BUFFER 8 7 9 6 15 25 35 45 55 65 75 B5 95 105 Temperalure Degrees Celsius 5 Illustration 20 Temperature compensated pH buffer 10 If a buffer with a pH value other than 4 7 or 10 pH is to be used select cuSt custom value then enter a value between 0 and 14 pH Buffer values entered this way are not temperature compensated the buffer is assumed to have the specified pH value at the current temperature Offsets of up to 4 pH units are allowed Page 24 www iccontrols com um 653 211 IC Controls pH CALIBRATION Electrode Maintenance The electrodes need to be calibrated periodically to maintain an accurate pH measurement IC Controls recommends that the transmitter and electrodes be calibrated every 30 days Depending on the process they ma
31. ansmitter program automatically returns to the configuration menu With only password 2 set to a non zero value level 2 access is required to make changes in the configuration menu but all other settings are unprotected Effectively the user will always have at least level 1 access At this point password 1 is still 000 You may optionally enable operator access control or level 1 security by changing the level 1 password from 000 to a non zero value Change the password by selecting CONF PAS 1 from the menu then entering an appropriate 3 digit password Write down the passwords set and store them in a secure place once a password has been set there is no way to redisplay it Since passwords are set in the configuration menu level 2 access is required to change either password If the level 2 password has been forgotten there is no simple way to regain access to the transmitter Contact the factory if you find yourself locked out of the transmitter Page 16 www iccontrols com um 653 211 IC Controls SECURITY Disabling Password Security Password security can be disabled by setting the level 2 password to 0000 In order to change the password level 2 access is required to enter the program Select CONF PAS 2 from the menu then press ENTER when the program displays 0000 Both passwords 1 and 2 are set to 0000 and security is now disabled The main menu will be changed to exclude the PASS frame and the c
32. at the new value has been stored in memory The 4 mA to 20 mA low set point has now been changed from 0 00 pH to 2 00 pH Press the key to display LO out etc Page 14 www iccontrols com um 653 211 IC Controls EDIT MODE Key Functions in Edit Mode ENTER t SELECT lt CANCEL Illustration 12 um 653 211 Enters edit mode The entire display or a single digit will blink to indicate that the transmitter is in edit mode Press the ENTER key again to leave edit mode and accept the new value Adjusts blinking digit upward or selects the previous item from the list If a 9 is displayed then the digit will loop around to show 0 Adjusts blinking digit downward or selects the next item from the list If a 0 is displayed then the digit will loop around to show 9 Numeric values only move right one digit If blinking is already at last digit display will loop to the sign on the left Numeric values move left one digit If blinking is at the 4 sign then blinking goes to the last character Settings restore the initial value if it was changed Otherwise leave edit mode without doing anything Transmitter keys used in edit mode www iccontrols com Page 15 SECURITY IC Controls SECURITY The 653 has a built in password protection system This security system is disabled by default and does not need to be enabled if no password protection is
33. c units temperature in degrees Celsius C pH in pH units ORP in millivolts mV Security Not enabled Temperature compensation method for pH Automatic TC using temperature input Temperature compensation method for ORP calibration with quinhydrone standards Automatic TC using temperature input Input signal damping Signal damping for pH 5 seconds ORP 5 seconds Temperature 5 seconds um 653 211 www iccontrols com Page 43 Appendix B Parts List Appendix B Parts List IC Controls Part Number Description Reference Drawing Number 653 pH ORP transmitter A9051060 Assembly 653 pH ORP main PCB D5990189 A9051058 Assembly 653 micro display board D5990188 A9141022 Assembly 653 case complete A9201014 16 wire interconnector cable two end A3200097 Hardware set 53 series display board 4 each of standoff lock washer 4 40 nuts A3200098 Hardware set 53 series 4 20 board 4 each of bracket lock washer 4 40 D4990070 screws and nuts A2500270 2 inch pipe mounting kit 53 series D4990069 A2500267 Panel mounting kit 53 series D4990070 A2500268 Wall mounting kit 53 series D4990073 540 24 VDC power supply Interconnect Cable to 600 Interface A9200008 pH ORP cable 6 conductor with shield per foot D5990196 600 pH Interface Pipe Top Explosion Proof A2500178 pH ORP preamp D5990196 D48500
34. cal reasons the first temperature input is identified as C throughout this instruction manual and in the menus To select imperial units for the transmitter select unit from the configuration menu then go into edit mode and change the C prompt to F um 653 211 www iccontrols com Page 35 TROUBLESHOOTING IC Controls TROUBLESHOOTING When trying to determine what the problem is with a pH ORP loop there are a few simple steps to follow ISOLATING THE PROBLEM FIRST Write down the symptoms a pH ORP reading b temperature reading c pH offset and slope or ORP offset SECOND Separate the sensor from the transmitter so that the problem can be isolated Disconnect the sensor from the transmitter at the BNC fitting refer to illustration 24 In this way it is much easier to test and determine if the problem is in the pH ORP sensor or in the transmitter THIRD See if the transmitter reads correctly by inputting 0 mV 0 mV 7 pH a Bend a paper clip into a U shape or use a BNC shorting strap if one is available b Insert the paper clip in the transmitter input BNC connector shorting between the center pin and the outside ring see illustration 25 This will produce a 0 mV input which is the same as pH 7 If using a BNC shorting strap simply attach it to the input BNC connector Note the pH reading if it is approximately 7 pH then the transmitter looks alright Note the ORP reading if it is approximately 0
35. cent of Nernstian theoretical response Confirm the second point calibration precision by repeating the calibration There should be close agreement between the reading and the buffer however small adjustments may be handled by repeat calibrations Note Jf the temperature is far from 25 C and auto was used the transmitter will be displaying the compensated pH value of the buffer Refer to Selecting a Buffer section for more information Page 22 www iccontrols com um 653 211 IC Controls pH CALIBRATION Grab Sample Standardization The grab sample standardization method provides an easy way to single point adjust the pH sensor without removing the electrode from the sample Grab sample standardization requires the user to determine the actual pH of the sample using an alternative method For example if the transmitter is reading 3 55 pH and laboratory analysis determines the actual pH of the sample to be 3 42 pH the grab sample method can be used to adjust the offset so that the previous 3 55 pH reading changes to 3 42 pH The precision of standardization using the grab sample method is only as accurate as the values supplied to the transmitter by the operator 1 Take a grab sample of the process which is representative of the solution the pH electrode is in preferably from just beside the electrode 2 Store the current pH reading in memory by selecting PH CAL GrAb GEt from the menu Press ENTER at the flashing do at a
36. d the purchase price of the unit The warranty described above is exclusive and in lieu of all other warranties whether statutory express or implied including but not limited to any implied warranty of merchantability or fitness for a particular purpose and all warranties arising from the course of dealing or usage of trade The buyer s sole and exclusive remedy is for repair or replacement of the non conforming product or part thereof or refund of the purchase price but in no event shall IC CONTROLS its contractors and suppliers of any tier be liable to the buyer or any person for any special indirect incidental or consequential damages whether the claims are based in contract in tort including negligence or otherwise with respect to or arising out of the product furnished hereunder Representations and warranties made by any person including its authorized dealers distributors representatives and employees of IC CONTROLS which are inconsistent or in addition to the terms of this warranty shall not be binding upon IC CONTROLS unless in writing and signed by one of its officers Page 54 www iccontrols com um 653 211 IC Controls INDEX Automatic recognition wrong buffer 25 Automatic temperature compensation 27 selecting 27 Battery backup 11 Buffers 20 automatic recognition 20 25 custom value 25 purchasing 20 selecting 22 25 standardize 21 temperature dependence 25 Calibration 20 29 error checking 21 error me
37. djustments made Slope and offset warnings are given however whenever the adjustments fall outside the preset safe regions Unlike a normal calibration the manual adjustments will allow slope adjustments outside 6096 to 11096 slope efficiency or offset adjustments greater than 4 pH units about 240 mV The usual error messages will come up but the specified new values will be installed nonetheless IC Controls advises that the operator use one of the regular calibration procedures whenever possible Temperature Compensation for pH pH is the product of the concentration of the H ion and the temperature of the solution This means that the pH of a solution will change with temperature even if the makeup of the solution stays the same To arrive at an accurate pH reading both the concentration measured by the electrodes and the solution temperature measured by the temperature probe need to be known The 653 transmitter has been programmed to provide automatic temperature compensation The temperature probe can read temperatures from 5 C to 105 C The process temperature can be displayed directly by selecting C or F from the menu If no automatic temperature compensator is available or needed manual temperature compensation can be used If the process temperature is constant set the manual temperature compensator to the process temperature If the process temperature varies or is unknown a default temperature of 25 C i
38. dure is not to be used unless the user is absolutely sure that they want to restore the transmitter to factory default configuration Refer to Appendix A for factory default settings After the transmitter program has been initialized the user will need to re enter the output signal settings as well as the program configuration if it was different from the factory default settings For the user s convenience the transmitter will remember the most recent menu selections Input Damping Both the measurement and the temperature can be damped to provide the user with a means to deal with rapidly varying or noisy signals Damping range is 0 seconds to 40 seconds With 0 seconds there is no damping and each reading the transmitter makes is used to directly update the display and 4 mA to 20 mA output The factory default 5 seconds adds the next 4 seconds of readings to the first and divides by 5 giving very fast response Selecting 40 seconds adds the readings for all 40 seconds and divides by 40 providing an excellent smooth damping out of turbulent readings Any selection between 0 seconds and 40 seconds can be made Page 34 www iccontrols com um 653 211 IC Controls CONFIGURATION OF PROGRAM Select CONF pH or orP or C dA 5 from the menu Press ENTER then change the input damping to the new number of seconds Press ENTER again to leave edit mode Temperature Calibration The temperature compensator in the sensor can sometimes s
39. e A simple OHMS s SSS device is either a passive device such as an RTD or a component with such a small signal that a se spark is not possible Simple devices do not u T gt D require certification as they are safe by nature SUPPLY VDC Illustration 4 Maximum loop resistance Sensor Mounting Flow sensors can be in any orientation but should be mounted tip down at an angle anywhere um 653 211 www iccontrols com Page 7 INSTALLATION IC Controls from 15 degrees above horizontal to 15 degrees from vertical 15 degrees above horizontal is best because air bubbles will rise to the top and grit will sink both bypassing the sensor Submersion sensors should not be mounted where a lot of air bubbles rise in the tank they will cause spikes in the pH ORP readout If a bubble is allowed to lodge in the sensing tip electrical continuity between the sensitive glass and the silver silver chloride element may be disrupted Sensor Wiring Ensure 24 VDC power is disconnected at supply end Sensor connection to transmitter configured with integral preamp model 653 is direct connect via a BNC connector on the main board refer to illustration 5 and drawing D5990189 for BNC connector location Sensor Wiring Legend TB100 1 V unused 2 REF unused 3 V unused TB101 1 SIG unused 2 T Red 3 T White BNC direct connect pH Illustration 5 Sensor wiring direct connect For sensor connection to transmitter co
40. e of 5 C to compensation 105 C TC not connected Check TC connections install TC CA1 6 Offset gt 1 3 pH units Large offset in reference Check electrode service or electrode or electrode replace if necessary depleted Bad buffer used for Use fresh buffer calibration CA1 7 Slope efficiency less Poor electrode pair Check both the reference and the than 85 or greater than performance glass pH electrode The glass 102 Nernstian may need to be cleaned or etched EES Bad buffer Use fresh buffers Buffers too close together Use buffers that are further apart Electrodes did not stabilize Allow more time for the before calibration entered electrodes to stabilize Use buffer closest to 7 pH as first buffer Er pH reading off scale Process too caustic for Verify process pH 14 accurate measurement Large electrode offset Service or replace electrode Err pH reading off scale Electrode not connected Check connections pH lt 0 Electrode not responding Etch glass electrode Clean reference electrode Replace electrode if necessary Process too acidic to be measured Verify process Page 32 www iccontrols com um 653 211 IC Controls Error and Caution Messages for ORP CAUTION AND ERROR MESSAGES 50 mV higher or lower than the offset for the previous calibration electrode or electrode depleted Error Description Caus
41. ectrode to the transmitter and then turn on the power The transmitter will go through its automatic startup procedure any time power to the transmitter was lost for more than a few seconds The startup procedure will initialize the transmitter program perform error checks scroll the unique 10 digit serial number of the unit and then proceed to display the pH ORP and function normally All program settings calibration settings and default values will have been retained by the transmitter as the memory has battery backup Transmitter Startup Tests The startup procedure will begin by scrolling a flashing IC CONTROLS across the display while performing memory tests The transmitter will proceed to display in sequence the transmitter model number in this case 653 any software option numbers and the program version number e g 2 10 The program then moves on to perform display tests each of the implemented display segments will light up in turn If the transmitter passes all the startup tests then the hardware is functioning properly and the transmitter will proceed to display pH ORP or error messages if detected If the transmitter displays Err or Err this indicates that the input is off scale An off scale error can indicate that the electrode is not in solution is off scale or is not connected properly If the display periodically flashes Err go to the error display section press SELECT key to access main menu and use f or
42. eld mountable using optional 2 inch pipe mount kit P N A2500267 or wall mount kit P N A2500268 3 Keypad adjustable microprocessor functions such as calibration plus independent 4 mA to 20 mA zero LO and span HI controls 4 Automatic temperature compensation 5 Standard inch NPT feed through conduit provides ample space for wires to pass 6 Steering diode protects 4 mA to 20 mA power from damaging electronics For complete transmitter specifications refer to Appendix C um 653 211 www iccontrols com Page 5 INSTALLATION IC Controls INSTALLATION Transmitter Mounting The sensor is typically supplied with a 1 5 m 5 foot lead as standard The transmitter should be kept within this distance The transmitter should be positioned to allow the sensor while still connected to be removed and the electrode tip placed in a beaker on the floor for cleaning or calibration Assume the safest place for the beaker is on the floor the service person stands on The electrical openings are on the case bottom the electrode connections on the right and the 4 mA to 20 mA on the left when viewed from the front Horizontal separation between rows of transmitters should allow for periodic replacement of electrode leads and the electrical connections IC Controls recommends 10 cm 4 inch minimum separation between rows columns As standard the 653 comes with panel mounting components Enclosure mounting cutout dimensions are 139 mm x 139 mm 5
43. election between 0 seconds and 40 seconds can be made Select out dA from the menu Press ENTER then change the damping to the new number of seconds Press ENTER again to leave edit mode Page 30 www iccontrols com um 653 211 IC Controls CAUTION AND ERROR MESSAGES CAUTION AND ERROR MESSAGES Detected errors and or cautions are displayed by the transmitter From the keypad press ERROR or from the main menu select Err If there are no error or caution messages NONE will be displayed otherwise scroll through the error list using the T or keys Errors and or cautions cannot be removed from this list directly each error caution will be removed automatically when appropriate e g errors associated with improper calibration will be cleared after a successful calibration Caution and error messages are numbered Messages 1 through 5 are identified as En e where n is the input number and e is the error number Messages 6 through 9 are less serious and are identified as cautions instead e g CAn e Off scale errors are not numbered but are identified as Err and Err depending on whether the input is at the top or the bottom of the scale The off scale error is displayed instead of the sample reading and does not show up in the error menu with the numbered error messages if any Input Source Input Number for Error Caution Messages pH ORP l Temperature 2 Table 3 Input values for error caution
44. electrode wash solution P N A1100091 Rinse thoroughly and ensure that after cleaning response is not more than 3 minutes REFERENCE If pH 7 0 reads between 6 pH and 8 pH then the reference is good If pH reading is out of this range then the reference is poor or has failed pH GLASS Subtract pH 4 0 reading from pH 7 0 reading a If the result falls between 2 5 to 3 0 the glass is good b If the result is less than 2 5 then the pH electrode is failing and should be replaced Less responsive failing pH electrodes can sometimes be regenerated using P N A1100092 electrode renew solution THIRD If electrodes pass tests then they are good Place electrode back in the loop and then perform a 2 buffer calibration FOURTH If the electrode fails the tests a Replace the pH electrodes b Consider returning electrodes to IC Controls for failure analysis if electrode life seems short IC Controls offers a free cause of failure and application analysis that may help increase electrode life in your application Page 38 www iccontrols com um 653 211 IC Controls TROUBLESHOOTING ORP Electrode Troubleshooting In order to troubleshoot an ORP electrode it is very important to be certain that the transmitter used for troubleshooting is functioning correctly IC Controls manufactures a portable calibrator model 659 for this purpose The calibrator can be used to prove the ORP transmitter before use or it can be used to prove the ORP
45. erious error message is displayed the electrode exhibits signs of major problems e g the buffer selected was not the buffer used so the offset would be large then the standardization was not successful The transmitter has retained the values from the last successful calibration Press any key to acknowledge the error The transmitter will return to the buffer selection menu and display the selected buffer e g Auto Refer to the Caution and Error Messages section and follow appropriate corrective action retry the calibration Press any key to resume normal operation after a caution or error message has appeared Calibrating Two Buffer Calibration Fully calibrating the transmitter involves calculating both the offset and the electrode efficiency or slope to match a particular electrode pair which can also be viewed both before and after two buffer calibration The electrode slope will be calculated as a percentage of Nernstian response First calibrate the offset with buF1 by following the procedure for Standardizing Single Buffer Calibration Secondly return to the calibration menu and display buF2 to calibrate the pH glass efficiency or slope Press SELECT to reach the buffer selection menu Use the f or keys to select either automatic buffer recognition a custom value or one of the standard buffers 4 7 10 The second buffer should be at least 1 pH unit higher or lower than the buffer used for the standardize
46. es Solutions E1 2 Electrode has stabilized Large offset in electrode Check electrode connection but offset gt 1000 mV pair The previous offset has Perform electrode maintenance been retained Refer to the electrode manual Use a different ORP standard Wrong standard specified Specify the correct ORP value for for calibration the standard and redo calibration Electrode not connected Check electrode connection and redo the calibration CA1 7 The offset is more than Large offset in reference Check electrode service or replace if necessary Incorrect standard used for calibration or standard not specified correctly Use fresh standard and redo the calibration ensuring that the correct custom mV value is specified Repeating the calibration should clear the caution message Error Messages for Temperature Error Description Causes Solutions E2 1 Temperature reading Temperature less than Verify process and sensor off scale Temperature 5 C location Ee Electronic calibration Follow procedure in Hardware shows Err necessary Alignment section E2 2 Temperature reading Temperature compensator Verify process and sensor off scale Temperature not attached location E than 105 C Electronic calibration Follow procedure in Hardware Display shows Err necessary Alignment section um 653 211 www iccontrols com Page 33 CONFIGURATION OF PRO
47. et password 1 operator access PAS 2 Set password 2 complete access PASS Enter password to change access level PH pH input SEt Set point manual temperature compensation value OR pH grab sample value SLOP Slope given as Nernstian response tc Temperature compensation unit Unit selection um 653 211 www iccontrols com Page 41 GLOSSARY IC Controls GLOSSARY Electrode Both a sensing and a reference electrode are needed for the transmitter to measure the process Commonly these are combined into one and referred to as a combination electrode The temperature sensor may be built into the electrode as well EPROM Erasable Programmable Read Only Memory The EPROM chip holds the program which determines the functioning of 653 transmitter Replacing the EPROM chip with a chip containing a new or an updated program changes the way the transmitter functions The EPROM chip is programmed by the manufacturer EEPROM Electronically Erasable Programmable Read Only Memory The EEPROM chip holds the customer settings for the program which determines the site functioning of 653 transmitter The customer settings in the EEPROM chip will not disappear even if the chip loses power Menu The series of prompts which determine the layout of the program used by the transmitter Microprocessor An integrated circuit chip which executes the program in the EPROM and controls all the input output functions Nernst Equation
48. how a small variance in its offset To make the sensor read correctly without adjusting the electronic calibration of the transmitter use the following procedure The current temperature as measured by the temperature sensor needs to be known If the sensor is in the process the known temperature of the process can be used Select CONF in C OFFS from the menu A frame showing the current temperature offset will be displayed Use the following formula to calculate the new offset value new geg D T usse offset t offset current For example if the temperature input is reading 24 6 C but it should be reading 25 0 C and the current offset is 0 2 C offset 25 0 C 24 6 C 0 2 C 20 6 C The calculation works both for Celsius and Fahrenheit units Select CONF in C OFFS from the menu Press ENTER then change the temperature offset to the new offset value Press ENTER again to leave edit mode Return to the sample menu and verify that the temperature input is now displaying the correct temperature Metric or Imperial Units By default the transmitter will use metric units This means that temperature will be displayed using degrees Celsius and that the prompt for the temperature input will be C However the transmitter can be made to use imperial units Using imperial units temperature will be displayed using degrees Fahrenheit and the prompt for the temperature input will be F For practi
49. loop transmitter where the problem has been detected Before testing your ORP sensors be sure your test transmitter is known to be good FIRST Inspect electrodes and if dirty or scaled a Clean with soft cloth b Acid clean to remove scale P N A1100094 gentle scale remover is recommended SECOND Perform electrode calibration but do not adjust transmitter a 66 mV quinhydrone standard record reading and response time b 263 mV quinhydrone standard record reading and response time Slow response Clean again or acid clean overnight in electrode wash solution P N A1100091 Rinse thoroughly and ensure that after cleaning response is not more than 3 minutes If the readings in the two standards do not differ by about 197 mV 263 mV 66 mV then there is a problem with the electrode Slow response can be due to coating of the electrode ORP and or reference or to a failed or poor reference electrode e g dried or depleted THIRD If electrodes pass tests then they are good Place electrode back in the loop and then perform a calibration FOURTH If the electrode fails the tests a Replace the ORP electrodes b Consider returning electrodes to IC Controls for failure analysis if electrode life seems short IC Controls offers a free cause of failure and application analysis that may help increase electrode life in your application um 653 211 www iccontrols com Page 39 ELECTRONIC HARDWARE ALIGNMENT IC Controls
50. ly when Bass function is activated Illustration 1 Menu overview www iccontrols com Page 3 CONTENTS Page 4 IC Controls Initialize analyzer settings PH option ORP option Input damping sec o Offset C F Use metric units Use imperial units U gt n Set level 1 password gt n N Set level 2 password and enable security Illustration 2 Configuration menu www iccontrols com um 653 211 IC Controls INTRODUCTION INTRODUCTION The model 653 pH ORP transmitter as shipped from the factory is calibrated and should not reguire recalibration other than a minor software zero and span adjustment to match the receiver or recorder being used As received the transmitter s span has been calibrated to 0 pH to 14 pH or 2000 mV to 2000 mV which covers most common processes General The 653 is one of a series of DIN panel type two wire transmitters It is considered to be a two wire device because both the power and signal use the same two wires In the case of pH or ORP a pH or ORP signal corresponding to the actual pH or ORP is converted to a 4 mA to 20 mA signal which is carried along the same two wires as the 24 VDC power used to power the device Features The 653 pH ORP transmitter has the following features 1 Instrument housing which is 1 2 DIN aluminum panel mount type IP 65 NEMA 4 watertight dust tight rating RFI EMI resistant 2 Fi
51. mitter needs a good ground a good ground connection can typically be made by using a shielded 4 mA to 20 mA wire connected to ground in the transmitter and to a local earth rod or earth at the 24 VDC power supply The transmitter requires 24 VDC to operate properly The on board regulation allows the supply to vary to any level between 16 VDC to 40 VDC without affecting the transmitted signal To hook up power to the transmitter perform the following wiring procedure 1 Unscrew and remove rear cover 2 Using 18 AWG to 22 AWG wire hook up the 4 mA to 20 mA power connections to TB200 24 VDC and RETURN terminals as shown in illustration 3 4 20 mA Loop Power Wiring Legend TB200 1 24 VDC Black 2 RETURN White 3 GROUND Shield Illustration 3 Power wiring Electrical Installation Installation should be performed in compliance with all applicable local electrical safety codes The 653 uses 24 VDC supply generally considered low hazard in general purpose applications However IC Controls recommends that the following safety practices be followed e Flex conduit should be installed within 18 inches of the enclosure Ensure all covers are on and firmly in place before power is applied Disconnect power before opening covers NOTE pH ORP sensors and RTD temperature gt compensators are passive and meet the intrinsic ROP mo safe definition of a simple devic
52. n in doubt as to what the transmitter is displaying pressing the SAMPLE key will ensure it is displaying the pH ORP reading When home base is displayed pressing the key will show the sample parameter being displayed Pressing the key will return to displaying the sample reading Page 12 www iccontrols com um 653 211 IC Controls EASY MENU Arrow Keys The four arrow keys on the keypad are used to move around the menu The same keys can have other functions as well however when moving from frame to frame in the menu these keys work as expected Example Press SAMPLE key to ensure that home base is displayed Press the key One of the prompts from the main menu will be displayed Use the f or keys to display the prompt above or below If the prompt at the top or the bottom is displayed the program will loop around Press the f or keys until CONF is displayed Press SAMPLE to return to the pH ORP sample display Press the key again and CONF will be displayed again Main Menu Main Menu PH orP je Er E Err ou out CONF CONF PASS h PASS ki Illustration 9 pH main menu Illustration 10 ORP main menu DIAG and ERROR Keys The DIAG and ERROR keys are used to access the diagnostic and error or alarm intelligence resident in the transmitter Pressing the D AG key will display program information and performs a display test Refer to Caution and Error Messages section for a description of the
53. necessary If the password protection system is not enabled then the user will have unrestricted access to all transmitter settings available through the menu as described in this manual Having security disabled provides the same access to the program as being at access level 2 at all times With security enabled anyone can view settings anywhere in the program When proper access rights are not warranted the program will display PASS for 2 seconds indicating that a proper password must be entered before being allowed to proceed Access Level Description e e 0 View nly cdessto all settings 1 Access to all settings except for configuration menu Usage Operator access No changes can be made to configuration and passwords cannot be changed 2 Access to all settings This allows the same access to program as when password security is not enabled Usage Installation management Table 1 Security access levels Enabling Password Security When security is disabled both password 1 and password 2 are set to 0000 Security is enabled by setting password 2 to a non zero value Select CONF PAS 2 from the menu The transmitter will display 0000 Use the arrow keys to change the display to the desired password for level 2 Pressing SAMPLE at any time will safely cancel password entry Press ENTER to enter the password into memory and to enable password security The tr
54. nfigured with remote preamp in a model 600 14 J box refer to drawing D5990196 The sensor connects to the preamp in the remote 600 14 junction box using P N A9200008 interface cable The 600 14 junction box is then hardwired into TB100 and TB101 on the main board of the transmitter as per illustration 6 600 Interface Wiring Legend TB100 1 V Orange 2 REF Red 3 V Black TB101 1 SIG White 2 T Brown 3 T Blue Illustration 6 Sensor wiring remote preamp in 600 J box Page 8 www iccontrols com um 653 211 IC Controls INSTALLATION Instrument Shop Test Startup 1 NH tn gt U Apply 24 VDC power to the transmitter Hook up the sensor via TB100 and TB101 or direct connect via BNC and remove the orange protective cap Select either pH or ORP program configuration depending on your sensor and application Place the pH sensor in 7 0 pH buffer ORP sensor in 66 mV standard The 653 pH ORP transmitter should come up reading near 7 pH or 66 mV Perform a standardize calibration for a reading of pH 7 00 0 02 pH units or 66 mV 2 0 mV allow 30 minutes warm up time for the electronics to stabilize To check for general performance place the pH sensor in pH 4 or pH 10 buffer The display should read approximately pH 4 or pH 10 For ORP place the ORP sensor in 263 mV standard the display should read approximately 263 mV Run the second buffer SLOP span calibration to trim the reading to pH 4
55. ng to indicate that the transmitter is reading pH in calibration mode and is waiting for the operator to press ENTER once the pH has stabilized When the electrode has stabilized and the ENTER key is pressed the display will stop flashing the electrode offset will be calculated and the new offset standardize will be entered into memory The transmitter will adjust its calibration settings and show 7 00 pH To calibrate with the second buffer press CANCEL twice to return to the buF1 display Press the key to display buF2 Press SELECT to select the second buffer This time select cuSt custom or non standard buffer from the menu The transmitter would not recognize a 9 pH buffer in auto buffer recognition mode only 4 7 or 10 With cuSt displayed press SELECT then use 7 or key until you get 9 00 on the display and press ENTER Then press SELECT to start the calibration As soon as the electrode has stabilized and the ENTER key is pressed the display will stop flashing the electrode slope will be calculated and the new slope efficiency will be entered into memory The transmitter will adjust its calibration settings and show 9 00 pH Press SAMPLE to return to the main pH display Verify that the slope has been calculated press SELECT twice then use the 1 or keys to display SLOP in the pH menu Press SELECT again to display the slope efficiency A good electrode will have an efficiency or slope of between 85 and 102 per
56. nsated value of the standard should be used um 653 211 www iccontrols com Page 27 ORP CALIBRATION IC Controls ORP Standardization Performing an ORP calibration or standardization causes the transmitter to calculate a new offset for the ORP electrode To start the calibration select orP CAL from the menu The user needs to select a standard with which to calibrate the transmitter Select either a custom value or one of the IC Controls quinhydrone standards Place the electrode in the standard solution then press SELECT to start the calibration process The display will show a flashing ORP reading to indicate that the transmitter is reading ORP and is testing for stability Once a stable value is observed press ENTER The display will stop flashing and the ORP electrode offset will be calculated and the new offset will be stored in memory The calibration may be redone or started over at any time Press SAMPLE to display the ORP reading then SELECT as needed to restart the calibration If the transmitter detects any problems during calibration a caution or error message will appear Refer to the heading Caution and Error Messages for a description of each message If an error occurs then the standardization was not successful The transmitter retains the offset value from the previous calibration Press ENTER to acknowledge the error The transmitter will return to the calibration menu and display the selected standard e g CUSt o
57. ny problem in the transmitter alone independent of the preamp and field wiring Problem identified a If the offset is within 10 mV of zero then the transmitter is good and either the wiring or the preamp is faulty and will have to be replaced or re done b If the offset is greater than 10 mV from zero then the problem is in the electronics The transmitter should go back to the service shop for electronic alignment or repair um 653 211 www iccontrols com Page 37 TROUBLESHOOTING IC Controls pH Electrode Troubleshooting In order to troubleshoot a pH electrode it is very important to be certain that the transmitter used for troubleshooting is functioning correctly IC Controls manufactures a portable pH transmitter and pH calibrator model 659 for this purpose The calibrator can be used to prove the pH transmitter before use or it can be used to prove the pH loop transmitter where the problem has been detected Before testing your pH sensors be sure your test transmitter is known to be good FIRST Inspect electrodes and if dirty or scaled a Clean with soft cloth b Acid clean to remove scale P N A1100094 gentle scale remover is recommended SECOND Run buffer tests on the electrodes but do not adjust transmitter a Immerse probe in 7 0 pH buffer write down reading and response time b Immerse probe in 4 0 pH buffer write down reading and response time Slow response Clean again or acid clean overnight in
58. onfiguration menu will no longer have the PAS 1 frame Entering a Password With security enabled select PASS from the main menu The transmitter will display 0000 Using the arrow keys edit to display level 1 or level 2 password then press ENTER The program will display good followed by the access level before returning to the main menu If an incorrect password was entered the program displays bAd instead Refer to illustration 13 to see how the program validates a password Level 1 or level 2 access is now acquired for as long as the transmitter is being operated The access level will automatically be restored to level 0 after no key has been pressed for 15 minutes This 15 minute time out will also redisplay the main sample It is good practice to return the transmitter to level 0 access or level 1 access if password 1 is set to 000 once the access level user has finished using the transmitter This is accomplished by selecting PASS from the main menu then pressing ENTER with 0000 displayed Password Example a Quick Tour With security disabled select CONF PAS 2 from the menu Set the level 2 password to 0002 Select CONF PAS 1 from the menu Set the level 1 password to 001 Security is now enabled Select PASS from the main menu Press ENTER with 0000 displayed The transmitter will display ACC 0 to indicate we are now at access level 0 Try changing the output low setting Select out
59. ontamination and or poisoning of the electrode surface or by a change in the reference electrode OFFS Offset mV E CALIBRATE 263 j HOLD mV Illustration 21 ORP menu Calibration is easily accomplished by selecting the proper standard placing the electrode in the standard solution and letting the transmitter do the rest The transmitter tests for electrode stability and performs diagnostic tests during calibration Automatic stability testing takes most of the guesswork out of deciding when a reading is acceptable or not The internal diagnostic tests will activate warning and or error messages if faulty operation is suspected or detected Errors detected during calibration will not cause the transmitter to lock up Selecting a Standard for Calibration The most common ORP standards are buffered pH solutions saturated with quinhydrone Two quinhydrone standards available from IC Controls are P N A1100083 with an ORP value of 263 mV at 25 C and P N A1100084 with an ORP value of 66 mV at 25 C If one of these standards is used select 263 or 66 from the calibration menu directly For any calibration standard selected the transmitter can be calibrated by selecting CUSt from the calibration menu then entering the ORP value in mV of the standard The oxidation reduction potential of most standard solutions is at least somewhat dependent on temperature If high accuracy is required the temperature compe
60. pproximately the same time that the grab sample is taken It is important that the pH value recorded in memory represents the pH of the sample This is easy to accomplish if the transmitter has a stable reading but difficult if there is a lot of fluctuation in the pH reading This step can be repeated as often as necessary 3 It is possible to view or even change the pH value recorded in memory Select PH CAL GrAb OL d 4 Analyze the grab sample to determine the actual pH For maximum accuracy the temperature of the sample should be the same as it was at the time the old value was recorded using GEt A significantly different pH could result if there is a temperature difference 5 Select PH CAL GrAb SEt from the menu Edit the old pH value and change it to the new pH value Press SELECT and press ENTER with the flashing do prompt displayed The offset will be adjusted according to the difference between the old and new pH values The error checking done for the grab sample calibration is similar to that done for a buF1 standardization An offset warning CA 1 6 is given if the new offset is greater than 1 3 pH units from theoretical behavior If the new offset would be greater than 4 0 pH units then Err1 3 is generated and the new offset will not be recorded GrAb Illustration 17 Grab sample standardization um 653 211 www iccontrols com Page 23 pH CALIBRATION Selecting a Buffer Automatic buffer detec
61. r 66 etc Take corrective action and retry the calibration If a potential problem has been detected e g there is a large change in the offset a caution message will appear and the transmitter will complete the calibration The caution message simply informs the user that poor ORP electrode performance is suspected Press any key to resume normal operation after a warning or error message has appeared To see the new offset that has been calculated press SAMPLE then select orP OFFS from the menu to display the ORP electrode offset in mV Electrode Life The electrodes need to be calibrated periodically to maintain an accurate ORP measurement checking the calibration at least once once a month is recommended Depending on the process the transmitter may need to be calibrated more frequently e g weekly or daily More frequent calibration is important where high accuracy ORP measurements are required Over time electrode performance will degrade The sensing electrode can become contaminated and dirty while the reference electrode becomes depleted Depending on the harshness of the process the electrodes will need to be replaced after a few months or after several years of use ORP Manual Calibration It is possible to bypass the regular calibration procedures and edit the offset directly When the offset is edited there is no way for the transmitter to verify the accuracy of the adjustments made IC Controls advises using
62. return to pH reading Note This procedure is the same for ORP select ORP from the main menu and proceed as per above Output Hold in Calibration Mode The 653 features an automatic output hold Output hold goes into effect when CAL is displayed as soon as SELECT is pressed The output hold feature avoids false alarms and erratic signal output that would be caused by a routine calibration Output hold has the following effect the 4 mA to 20 mA output signal is frozen at its current level If the output signal for pH is not acceptable at the value found it can be changed for the duration of the calibration Select Hold from the menu to display the pH value used by the transmitter to determine the output signal Use the normal editing procedure to change the pH value used for output hold The output hold remains in effect for the duration of the calibration the output hold is disabled when the CAL prompt is displayed the SAMPLE key is pressed or after no key has been pressed for 15 minutes um 653 211 www iccontrols com Page 25 pH CALIBRATION IC Controls Manual Calibration of Offset and Slope It is possible to bypass the regular calibration procedures and edit the slope or offset directly Offset and slope are protected by level 1 security which is the same security as the other calibration procedures When the offset or slope are adjusted directly there is no way for the transmitter to verify the accuracy of the a
63. s normally used Manual Temperature Compensation If the temperature compensation method for the pH input needs to be changed press SAMPLE to display the pH Press SELECT to reach the main menu then use the T or keys to display PH Press SELECT again then use the f or keys to display tc At this point either Auto for automatic temperature compensation or SEt for manual temperature compensation set point will be displayed depending on the current setting To change the setting from Auto to SEt press ENTER to edit the current setting The display will start blinking indicating that a selection needs to be made Use the f or keys to display SEt Press ENTER to select manual temperature compensation With SEt as the current display press SELECT to display and or adjust the temperature setting to be used with manual temperature compensation If the current value needs to be changed press ENTER to edit the current setting The display will start blinking Use the f or keys to display the desired temperature for manual temperature compensation Press ENTER to accept the currently displayed value Page 26 www iccontrols com um 653 211 IC Controls ORP CALIBRATION ORP CALIBRATION Redox electrodes the sensing electrode theoretically do not undergo changes of zero point nor of characteristic slope as do glass electrodes used to measure pH Nevertheless incorrect redox potentials can be measured usually caused by c
64. ssages 22 example 22 grab sample 20 24 offset 21 output hold 20 26 settings 11 single point 20p slope 20 22 standardize 21 29 temperature input 27 36 two point 20 22 Celsius 36 Configuration program 35 units 36 CONFIGURATION 35 Current output 30 output hold 26 output hold during calibration 26 reversing 30 simulating 30 specifications 31 Custom buffer 25 Damping inputs 35 output 31 Default settings 44 Diagnostics calibration 20 um 653 211 www iccontrols com INDEX memory test 11 startup procedure 11 Edit mode 15 change settings 16 key functions 16 numeric values 15 Electrode 29 43 Electrode maintenance 26 Replacing 26 troubleshooting 39p Error messages 32 acknowledging 22 CA1 6 33 CAI1 7 33 calibration 22 clearing 32 E1 2 32 E13 32 El 4 33 E15 33 E2 1 34 E2 2 34 Err 33 Err 33 Fahrenheit 36 Grab sample 24 Home base 12 Installation 6p 11 Keypad 14 arrow keys 14 CANCEL key 16 DOWN key 16 ENTER key 16 SELECT key 16 UP key 16 Maintenance 26 electrode 26 Manual temperature compensation 27 selecting 27 set point 27 Memory test 11 Menu 3 Menu Page 55 INDEX home base 12 MENU 12 Nernst equation 43 Offset 27 manual adjustment 27 ORP 43 ORP standards 28 ORP standards selecting 28 Output damping 31 Output hold 26 Output signal damping 31 Password 18 PH current output 30 temperature dependence 25 PROMPTS 42 replacing electrodes 26 SA
65. standardize will be entered in memory Note The ENTER key may be pressed before the electrode has stabilized forcing the transmitter to calibrate using the current pH input resulting in a low precision calibration Confirm the single point calibration precision by repeating the calibration There should be close agreement between the readings and the buffer however small adjustments may be handled by repeat calibrations Calibrations may be redone or started over at any time Press CANCEL to display the selected buffer e g Auto then SELECT to restart the calibration Note f the temperature is far from 25 C the transmitter will display the temperature compensated pH of the pH buffers Refer to Selecting a Buffer section for more information zd o e 10 0 If the transmitter detects or suspects any problems during calibration a caution or error message will appear Refer to the Caution and Error CALIBRATE Messages section for a description of each message If a potential problem has been detected e g a large offset then a caution message will be appear The caution message simply informs the user that poor performance is suspected and will be compensated for by the microprocessor Nevertheless the transmitter has successfully completed the calibration m 2 5 m x Illustration 15 First buffer Page 20 www iccontrols com um 653 211 IC Controls pH CALIBRATION If a more s
66. temperature without a controlled temperature bath Any necessary minor adjustments are handled by the software To adjust the temperature input refer to the heading entitled Temperature Calibration in the Configuration of Program section Page 40 www iccontrols com um 653 211 IC Controls DISPLAY PROMPTS DISPLAY PROMPTS Acc n Access level for security Displayed after password entered by user Auto Automatic buF1 Buffer for standardizing or first buffer for calibration buF2 Second buffer for calibration C Temperature in degrees Celsius temperature input CAL Calibrate transmitter CONF Configuration of program to match hardware cur Signal output in mA or current cuSt Custom standard value dA Damping of input output signal do Do press ENTER to do reset clear action donE Done reset clear action has been accepted Err Error F Temperature in degrees Fahrenheit GrAb Grab sample calibration GEt Get sample of process for grab sample calibration HI High limit 20 mA for 4 mA to 20 mA output window Hold Output hold during calibration init Re initialize transmitter to default settings LO Low limit 4 mA for 4 mA to 20 mA output window OFF Off OFFS Offset OLd Old grab sample value from previous grab sample calibration ON On ON OF On Off switch OPtn Input option select ORP ORP input out 4 mA to 20 mA analog output channel PAS 1 S
67. the meter into a different outlet so that the meter and receiver are on different branch circuits If necessary the user should consult the dealer or an experienced radio television technician for additional suggestions The user may find the following booklet prepared by the Federal Communications Commission helpful How to Identify and Resolve Radio TV Interference Problems This booklet is available from the U S Government Printing Office Washington D C 20402 Stock No 004 000 00345 4 CANADA This digital apparatus does not exceed the Class A limits for radio noise emissions from digital apparatus set out in the Radio Interference Regulations of the Canadian Department of Communications Le present appareil num rique n met pas de bruits radio lectriques depassant les limites applicables aux appareils num riques de la class A prescrites dans le R glement sur le brouillage radio lectrique dict par le minist re des Communications du Canada Page 10 www iccontrols com um 653 211 IC Controls STARTUP STARTUP If the transmitter is new and has not been installed then follow the procedures described in Installation Electronic Hardware Alignment and Configuration of Program before mounting Mounting and wiring procedures for new installations vary with equipment options refer to drawing section for instructions If the transmitter has been previously installed all that is required is to attach the el
68. the regular calibration procedures whenever possible Page 28 www iccontrols com um 653 211 IC Controls 4 mA to 20 mA OUTPUT SIGNAL 4 mA to 20 mA OUTPUT SIGNAL A 4 mA to 20 mA output is provided over the 24 VDC power leads The output has an on off switch and adjustable low and high span or scale adjustments This ONIOF makes it possible for example to OFF transmit short span pH signals such as 4 pH to 10 pH using the high and low adjustments out To adjust the output span or output window for pH signals set LO to correspond to the low end of the scale or 4 mA output and set HI to correspond to the high end of the scale or 20 mA output The transmitter will automatically Illustration 22 Output menu scale the output according to the new settings Reversing the 4 mA to 20 mA Output The low scale setting will normally be lower than the high scale setting It is possible to reverse the output or flip the window by reversing the settings of the low and high scale Example Define an output window from 7 5 pH to 6 5 pH with 7 5 pH corresponding to 4 mA output and 6 5 pH corresponding to 20 mA output Set LO to 7 5 and set HI to 6 5 Simulated 4 mA to 20 mA Output Select cur from the menu to display the output current in mA that is presently being transmitted by this output signal The display will be updated as the output signal changes based on the input signal and the program settings From here
69. tion provides the simplest and most accurate method of calibrating the 653 transmitter The transmitter has been programmed to recognize the three buffers most commonly used for calibration 4 pH 7 pH and 10 pH The electrodes need to be submersed in the buffer solution and the transmitter will detect the correct buffer value allowing for an offset of up to 1 3 pH units Temperature Dependence of Buffers The pH of a solution is dependent on temperature To achieve greater accuracy the temperature compensated values for the 4 pH 7 pH and 10 pH buffers are calculated by the transmitter If manual temperature compensation has been selected then the manual temperature compensation set point is used as the buffer temperature The graphs show the temperature dependence of the standard buffers The tc curves have been programmed into the transmitter The actual pH value of each of the three standard buffers will be used Example Calibrate with the 4 01 pH buffer at 25 C The temperature of the buffer is 50 C The transmitter will use the pH value of 4 05 Incorrect Buffer Selection by the transmitter If the offset is known to be greater than 1 3 pH units or if the transmitter selected the wrong buffer using automatic buffer recognition it is necessary to specify which buffer is being used When 4 01 7 00 or 10 0 is selected temperature compensated values are used and an offset of 4pH units is allowed If manu
70. y need to be calibrated more frequently e g weekly or even daily Frequent calibration is especially important if an accurate pH measurement is required Over time electrode performance will degrade The glass bulb becomes less responsive to pH and the reference electrode becomes depleted The electrodes will need to be replaced after several years of use or depending on the harshness of the process after several months Replacing Electrodes When the electrodes have been replaced or serviced follow this procedure to return the calibration settings to their default values For pH the offset should be set to 0 0 mV and the slope set to 100 Nernstian response For ORP the offset should be set to 0 0 mV Also any errors relating to calibration will be cleared Select PH from the main menu From the pH menu select SLOP Yo Efficiency Press SELECT to display the current value Press ENTER and the display will flash the current value use the arrow keys to edit to read 100 0 Press CANCEL to abort the operation or press ENTER to reset the calibration to 100 Nernstian response Press SAMPLE to return to pH reading Select PH from the main menu From the pH menu select OFFS mV offset Press SELECT to display the current value Press ENTER and the display will flash the current value use the arrow keys to edit to read 0 0 Press CANCEL to abort the operation or press ENTER to reset the calibration offset to 0 0 mV Press SAMPLE to

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