Agilent Cary 600 Series FTIR Spectrometers and Microscopes
Contents
1. Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Ete Agilent Technologies Notices Agilent Technologies Inc 2008 2010 2013 No part of this manual may be reproduced in any form or by any means including electronic storage and retrieval or translation into a foreign language without prior agreement and written consent from Agilent Technologies Inc as governed by United States and international copyright laws Manual Part Number 8510246800 Edition Tenth edition May 2013 Printed in Malaysia Agilent Technologies Inc Warranty The material contained in this document is provided as is and is subject to being changed without notice in future editions Further to the maximum extent permitted by applicable law Agilent disclaims all warranties either express or implied with regard to this manual and any information contained herein including but not limited to the implied warranties of merchantability and fitness for a particular purpose Agilent shall not be liable for errors or for incidental or consequential damages in connection with the furnishing use or performance of this document or of any information contained herein Should Agilent and the user have a separate written agreement with warranty terms covering the material in this document that conflict with these terms the warranty terms in the separate agreement shall control Technology Licenses Th2. Operation KP o e e 7 0 r e 4 Operation amp Lights 36 j Turning on the system and filling the Dewar 36 gs Performing a collect 40 Turning off the system 42 For additional hardware information see the Resolutions Pro Help If you have purchased the spectrometer only skip all instructions related to the microscope If you have purchased an Agilent Cary 620 FTIR microscope see the User s Guide supplied with that instrument To access the Resolutions Pro Help 1 Start the Resolutions Pro software 2 Press F1 on the keyboard to display the Help 3 Click the Contents tab if necessary 4 Click the plus icon next to About Your FTIR Systems to expand it 5 Click the plus icon next to Agilent 600 Series FTIR to expand it for hardware information on your spectrometer or click the plus icon next to 610 IR for hardware information on your Agilent Cary 610 IR microscope Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 35 Operation Lights There are two LEDs on the front of the spectrometer in the lower left corner The following table summarizes the LED behavior Table 3 LED descriptions Position Condition Comment Top Power Scan Flashing yellow The spectrometer is initializing Solid yellow The spectrometer has not correctly initialized and needs attention Solid green The spectrometer has initialized and is ready Flashing g
3. Room temperature DLaTGS None Cooled DLaTGS Peltier Far infrared DLaTGS None Si None PbSe None InGaAs None Installation requirements Before receiving your Agilent Cary 600 Series FTIR instrument you will have been given a Site Preparation Guide which describes the environmental and operating requirements of the Cary 600 Series FTIR system You must prepare your laboratory according to these instructions before the Cary 600 Series FTIR can be installed You should keep the Site Preparation Guide for future reference If you have misplaced your copy you can obtain a replacement from your local Agilent office Training The software provided with your Agilent Cary 600 Series FTIR spectrometer and microscope includes extensive Help If Agilent installs the instrument s the Agilent representative will demonstrate the basic operating procedures while conducting the installation performance tests during the installation procedure The Agilent representative however is not necessarily experienced in complex analytical routines and is not authorized to conduct extensive training Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 25 Introduction To ensure that your operators benefit the most from witnessing the installation performance tests operator training should be completed before your equipment is installed It is strongly recommended that you take advantage of the special training courses that are con
4. coupled radio frequency energy which is necessary for the internal functioning of the equipment itself Class A equipment is equipment suitable for use in all establishments other than domestic and those directly connected to a low voltage power supply network which supplies buildings used for domestic purposes This device complies with the requirements of CISPR11 Group 1 Class A as radiation professional equipment Therefore there may be potential difficulties in ensuring electromagnetic compatibility in other environments due to conducted as well as radiated disturbances Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Safety Practices and Hazards Operation is subject to the following two conditions 1 This device may not cause harmful interference 2 This device must accept any interference received including interference that may cause undesired operation If this equipment does cause harmful interference to radio or television reception which can be determined by turning the equipment off and on the user is encouraged to try one or more of the following measures 1 Relocate the radio or antenna 2 Move the device away from the radio or television 3 Plug the device into a different electrical outlet so that the device and the radio or television are on separate electrical circuits Make sure that all peripheral devices are also certified Make sure that appropriate cables are used to conn
5. operating procedure practice or the like that if not correctly performed or adhered to could result in personal injury or death Do not proceed beyond a WARNING notice until the indicated conditions are fully understood and met 2 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Contents Contents 1 Safety Practices and Hazards 7 General 9 Ultraviolet radiation 8 Cryogenic cooling 8 Compressed gas cylinders 9 Storage 10 Electrical hazards 10 Laser safety 11 Labeling 12 Laser aperture locations 14 Other precautions 14 Warning and caution messages 15 Information symbols 16 Color coding 17 CE compliance 18 Electromagnetic compatibility 18 EN55011 CISPR11 18 ICES NMB 001 19 2 Introduction 21 Specifications 21 Environmental 22 Fuses 22 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 3 Contents Purge gas Laser Liquid nitrogen Installation requirements Training Documentation Conventions 3 Unpacking and Installation Unpacking Installing the software Spectrometer and microscope connections Spectrometer Microscope Connecting the motorized stage cables Programming accessories for hardware recognition 4 Operation Lights Turning on the system and filling the Dewar Spectrometer Microscope Performing a collect Spectrometer Microscope Accessing the Help Turning off the system 23 23 24 25 25 26 26 27 27 28 28 28 31
6. 32 34 35 36 36 36 38 40 40 40 41 42 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Contents 5 Maintenance 43 Routine 46 Cleaning 46 Spare parts 46 6 Troubleshooting 47 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 5 Contents This page ts intentionally left blank 6 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Safety Practices and Hazards e o o o 0 e 1 Safety Practices and Hazards 0o amp General 8 z j 5 Ultraviolet radiation 8 Cryogenic cooling 8 Compressed gas cylinders 9 Electrical hazards 10 Laser safety 11 Other precautions 14 Warning and caution messages 15 Information symbols 16 Color coding 17 CE compliance 18 Electromagnetic compatibility 18 Your Agilent Cary 600 Series FTIR spectrometers microscopes and accessories have been carefully designed so that when used properly you have an accurate fast flexible and safe analytical system Unless specified otherwise this manual covers the Agilent Cary 660 670 680 Spectrometers and the Agilent Cary 610 FTIR Microscope If you have purchased an Agilent Cary 620 FTIR microscope see the Agilent Cary 620 FTIR Microscope User s Guide If the equipment is used in a manner not specified by the manufacturer the protection provided by the equipment may be impaired Information about safety practices appears throughou
7. 4 Load a sample 5 Runa collect For instructions on how to access the Help which contains information for each of these steps see Page 41 Microscope The basic steps to perform a collect using the microscope are 1 Prepare the microscope 2 Place the sample on the stage 3 Focus and select the analytical area 4 Collect data For instructions on how to access the Help which contains information for each of these steps see Page 41 The shutter should always be in the open position when using the microscope Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Operation To open or close the microscope shutter 1 Look directly at the front of the microscope 2 Gently pull the black handle between the right side of the microscope and spectrometer towards you Figure 15 Side view of closed shutter and handle 3 To close the shutter gently push the black lever away from you Accessing the Help To access the Resolutions Pro Help Start the Resolutions Pro software Press F1 on the keyboard to display the Help Click the Contents tab if necessary Click the plus icon next to Software to expand it Click the plus icon next to Software How To to expand it a oi A Ww N For collect information highlight Perform a Collect and click the links for the required information or highlight Collecting Microscope Data or Microscope Mapping Data for informatio
8. an upright vertical position Before transport remove regulators and install cylinder cap Store cylinders in a well ventilated area away from heat direct sunshine freezing temperatures and ignition sources Clearly mark cylinders so there is no doubt as to their contents Use only approved regulators and connections Use only connector tubing that is chromatographically clean and has a pressure rating significantly greater than the highest outlet pressure from the regulator Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 9 Safety Practices and Hazards 10 Storage Cylinders containing gas under pressure should be firmly secured to a rigid structure and the storage area must be adequately ventilated Never locate gas cylinders near a source of ignition or in a position that is subject to direct heat Gas storage cylinders often incorporate a pressure release device which will discharge the gas ata predetermined temperature usually around 52 C 125 F If gases are to be plumbed from a remote storage area to the instrument site ensure that the local outlets are fitted with stop valves pressure gauges and suitable regulators which are easily accessible to the instrument operator The gas outlets must be provided within 1 5 meters 5 feet of the instrument Bottled nitrogen should not be used for purged systems as the rate of consumption about one bottle per day makes it impractical Electri
9. 215004 or equivalent Agilent Cary 610 FTIR microscope typical 1FS1 72 0 AH 250 V IEC601272 1 Sheet 5 5 x 20 mm Littelfuse 0215020 or equivalent 22 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Introduction Purge gas Purge gas must be water free air dried to dew point of 70 C or dry nitrogen In this manual the term purge gas refers to dry nitrogen or dry air Purge can be supplied to the sample compartment instrument enclosure and microscope in any combination Conversion factors L min cfm x 0 0353 cfm L min x 28 3 Flow rate for purge 10 L min 20 ft hr maximum you must have a flow meter to monitor the flow of the purge gas A regulator is required if the source pressure is greater than 60 psi 420 kPa Tubing should be clean and free of any dust and debris Do not use tubing treated with talcum powder Laser Specifications for the laser light that is accessible during operation are e Maximum accessible power lt 600 uW e Pulse duration Continuous e Wavelength 632 8 nm e Maximum beam divergence Cone of angle 15 degrees or less coming to a focus in the center of the sample compartment and diverging thereafter Specifications for the embedded laser in the spectrometer are e Maximum accessible power lt 1 mW e Pulse duration Continuous e Wavelength 632 8 nm e Maximum beam divergence 1 3 milliradians Agilent Cary 600 Series FTIR Spectrometers an
10. Laser safety warning located on top of internal compartment cover Near apertures The following image shows the laser safety warning located near all apertures on both the Agilent Cary 600 FTIR Series instruments and microscopes Figure 3 Laser safety warning located near apertures Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 13 Safety Practices and Hazards Laser aperture locations WARNING Laser Hazard Avoid exposure laser light may be emitted from this aperture The laser light could cause retinal eye damage if prolonged direct viewing occurs This is a Class 2 laser product It is not powerful enough to harm your skin should your hand intercept it The optical design of the 600 Series spectrometer and the 610 FTIR microscope normally precludes this Always wear appropriate safety equipment and clothing Aperture located directly on the opposite side of the microscope from the laser OEF signal input from the spectrometer Laser signal input from the spectrometer Figure 4 Laser aperture locations on the spectrometer indicated by the circles on the image and microscope Other precautions Infrared sources operate at high temperatures which may burn you Before replacing a source element that has been lit switch off the instrument and ensure that the source has adequately cooled 14 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Safety Pract
11. Resolutions Pro software for you during the installation process it may become necessary to re install it if the computer is replaced The Agilent Resolutions Pro software installation disks will install all files required to run the software See the Agilent Resolutions Pro Software Installation Manual for instructions on how to install and register your software Spectrometer and microscope connections While your Agilent representative will install the spectrometer and microscope for you during the installation process it may become necessary to reconnect cables if you move the instruments Spectrometer Power is connected to the instrument and purge line if used at the rear of the instrument 28 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Unpacking and Installation To connect the power and purge lines to the spectrometer 1 Make sure the power switch on the rear of the spectrometer is in the off 0 position Figure 5 Power switch and socket on the rear of the spectrometer 2 Connect the power cord to the rear of the spectrometer 3 Connect the other end of the power cable to the electrical power outlet 4 Ifyou have a purged spectrometer or you wish to purge the sample compartment connect the gas purge line to the fitting on the rear of the spectrometer Figure 6 Purge fittings on the rear of the spectrometer CAUTION Use only dry air or dry nitrogen to purge the spectrom
12. cal hazards The Agilent Cary 600 Series FTIR spectrometers microscopes and some accessories contain electrical circuits devices and components operating at dangerous voltages Contact with these circuits devices and components can cause death serious injury or painful electrical shock Good grounding earthing is essential to avoid a potentially serious electric shock hazard Ensure that there is an integral ground connection between the metal base of the instrument and accessories and the 3 pin earth grounded receptacle Consult the manuals or product labels supplied with your computer monitor and printer for the relevant grounding requirements The above model is Equipment Class Application of the wrong supply voltage can create a fire hazard and a potentially serious shock hazard and could seriously damage the Cary 600 Series FTIR system accessories and any attached ancillary equipment The Cary 600 Series FTIR instruments have a universal power supply that adapts to the supply voltage However care must be taken to ensure that the correct voltage is used Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Safety Practices and Hazards Consult the manuals supplied with your computer monitor and printer for their specific voltage requirements Replace blown fuses with fuses of the size and rating as stipulated in the text adjacent to the fuse holder or in the manuals where listed Do NOT use power c
13. cifications proper operation and compliance with FDA and CE standards for light emitting products Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 11 Safety Practices and Hazards Labeling Laser safety labels are located on the rear of the Agilent Cary 600 Series FTIR spectrometer and underneath the top cover f DA pias a EE i f le KS foe Sara 1 1 nms J l F C MADE IN AUSTRALLA 8 pm N10149 Ee ChMPFLIED Bild Pi cra ee i LECHFT POE GWA is PUASA TS c u LAJIA Whig ag bi AE Ji ME187904 AGILENT TECHNOLOGIES TAS Detector Purge Air Bearing 165 420kPa 24 G0psi 210 415kPa 30 60psi 9 I min 0 3ft min i 10 l min 0 4Ft min Figure 1 Laser safety label locations on the rear of the Agilent Cary 600 Series FTIR spectrometer The laser safety warning just above the Purge and Air Bearing connections states Laser radiation Do not stare into beam Class 2 laser product IEC 60825 1 2007 Max output 1 mW 600 700 nm If the spectrometer is purchased where a local language is supported the localized warning will be present next to or near the English version Under top cover The following image shows the laser safety warning located on the top of and underneath the interferometer compartment cover 12 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Safety Practices and Hazards Figure 2
14. d Microscopes User s Guide 23 Introduction 24 Laser Hazard The laser light could cause retinal eye damage if prolonged direct viewing occurs This is a Class 2 laser product It is not powerful enough to harm your skin should your hand intercept it The optical design of the 610 FTIR microscope normally precludes this You are never required to remove the protective housing of the 610 FTIR microscope Always wear appropriate safety equipment and clothing Liquid nitrogen Extreme Cold Hazard Liquid nitrogen is very cold and can cause damage to the human body Use appropriate protective equipment when handling liquid nitrogen If you are using the MCT or InSb detector you will need a supply of liquid nitrogen to cool it It takes about 500 milliliters 16 ounces of liquid nitrogen for the initial fill to bring the Dewar to an equilibrium temperature It will take about 20 minutes to reach equilibrium Then add an additional 200 milliliters 7 ounces of liquid nitrogen to top off the Dewar See Page 36 for more information on filling the spectrometer Dewar and Page 38 for more information on filling the microscope Dewar Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Introduction Table 2 Cooling methods for available detectors Detector Cooling method High sensitivity MCT Liquid nitrogen Linearized high sensitivity MCT Liquid nitrogen Linearized broadband MCT Liquid nitrogen InSb Liquid nitrogen
15. ducted at various locations by the Agilent customer support and sales organization In some areas it may be possible to arrange for operator training to be carried out after the installation using your own instrument To investigate this possibility contact your local Agilent sales and service office Documentation 26 This User s Guide provides basic instructions for installing operating and maintaining your Agilent Cary 600 Series FTIR spectrometers and microscopes Where procedures differ for the various instrument models they will be clearly identified Further information and instruction for the Resolutions Pro software analysis methodology operating procedures and various accessories is provided in the Help and electronic manuals loaded onto your computer hard drive during software installation Conventions The following conventions have been used in procedures throughout the documentation e Bolded items indicate an action For example click OK and From the Edit menu choose Copy e ALL CAPITALS indicate keyboard commands For example press ENTER and press SHIFT F8 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Unpacking and Installation KP o e e e 3 Unpacking and Installation Oe amp Unpacking 21 r Installing the software 28 gs Spectrometer and microscope connections 28 Programming accessories for hardware recogn
16. e hardware and or software described in this document are furnished under a license and may be used or copied only in accordance with the terms of such license Restricted Rights Legend If software is for use in the performance of a U S Government prime contract or subcontract Software is delivered and licensed as Commercial computer software as defined in DFAR 252 227 7014 June 1995 or as a commercial item as defined in FAR 2 101 a or as Restricted computer software as defined in FAR 52 227 19 June 1987 or any equivalent agency regulation or contract clause Use duplication or disclosure of Software is subject to Agilent Technologies standard commercial license terms and non DOD Departments and Agencies of the U S Government will receive no greater than Restricted Rights as defined in FAR 52 227 19 c 1 2 June 1987 U S Government users will receive no greater than Limited Rights as defined in FAR 52 227 14 June 1987 or DFAR 252 227 7015 b 2 November 1995 as applicable in any technical data Safety Notices A CAUTION notice denotes a hazard It calls attention to an operating procedure practice or the like that if not correctly performed or adhered to could result in damage to the product or loss of important data Do not proceed beyond a CAUTION notice until the indicated conditions are fully understood and met A WARNING notice denotes a hazard It calls attention to an
17. ect the device to peripheral equipment 6 Consult your equipment dealer Agilent Technologies or an experienced technician for assistance 7 Changes or modifications not expressly approved by Agilent Technologies could void the user s authority to operate the equipment ICES NMB 001 This ISM device complies with Canadian ICES 001 Cet appareil ISM est conforme a la norme NMB 001 du Canada Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 19 Safety Practices and Hazards This page ts intentionally left blank 20 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Introduction g a e e e 2 Introduction a amp Specifications 21 e j Installation requirements 25 gs Training 25 Documentation 26 This manual contains the information required to successfully get started using Agilent Cary 600 Series FTIR spectrometers and microscopes Where mentioned the specifications between spectrometer and microscope differ All other specifications are for both Unless specified otherwise this manual covers the Agilent Cary 660 670 680 Spectrometers and the Agilent Cary 610 Microscopes If you have purchased the spectrometer only skip all instructions related to the microscope If you have purchased an Agilent Cary 620 FTIR microscope see the Agilent Cary 620 FTIR Microscope User s Guide Specifications Agilent Cary 600 Series FTIR s
18. eter and or microscope Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 29 Unpacking and Installation Spectrometer penthouse connections The penthouse connectors include connectors for external accessories external detectors and the data system via USB Do not open the penthouse there are no user serviceable parts inside To access the connectors lift the spectrometer cover Figure 7 Spectrometer penthouse connections 1 EXT DET 1 Used to connect an 2 EXT DET 2 Used to connect 3 Analog Expansion Provides external detector an external detector alternate signal paths and controls 4 FPA TRS Used to connect either 5 USB 2 0 Data system 6 Accessory Used to connect an FPA detector or TRS accessory connector to PC an additional accessory 7 TRIG OUT Located under the EXT 8 USER1IN Usedtoreceivea 9 SIGNAL OUT Used to senda DET 1 connector but obscured in signal from an external device signal to an external device this image Used to trigger to an external device 10 USER 5 IN Used to receive a 11 Beam splitter access cover 12 Metal cover for cable routing signal from an external device for second ADC if fitted 13 Sample compartment connectors not shown 30 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Unpacking and Installation Microscope Power to the instrument and purge line if used is connected at the rear of the instrument To connect the po
19. ices and Hazards Do not block the ventilation grills on the instrument and accessories Consult the manuals supplied with your computer monitor and printer for their specific ventilation requirements Use of the Agilent Cary 600 Series FTIR system and accessories may involve materials solvents and solutions which are flammable corrosive toxic or otherwise hazardous Careless improper or unskilled use of such materials solvents and solutions can create explosion hazards fire hazards toxicity and other hazards which can result in death serious personal injury and damage to equipment and property Always ensure that laboratory safety practices governing the use handling and disposal of such materials are strictly observed These safety practices should include the wearing of appropriate safety clothing and safety glasses Use only spare parts from Agilent with your instrument Warning and caution messages Carefully read all warnings and cautions and observe them at all times A Warning message is used in the text when failure to observe instructions or precautions could result in death or injury Warnings have the following format Hazard Type Nature of the hazard information on how to avoid the hazard and possible consequences if you don t The triangular symbols that appear in conjunction with warnings are outlined in the next section A Caution message is used when failure to observe instructions could result
20. in damage to equipment Agilent supplied and or other associated equipment Cautions have the following format Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 15 Safety Practices and Hazards CAUTION Caution information appears here Information symbols The following triangular symbols appear in conjunction with warnings on the spectrometer and associated documentation The hazard they depict is shown below each symbol gt Electrical shock Extreme cold Eye hazard Heavy weight Heavy weight Hot surface danger to feet danger to hands Laser hazard The following symbol may be used on warning labels attached to the instrument When you see this symbol refer to the relevant operation or service manual for the correct procedure referred to by that warning label 16 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Safety Practices and Hazards The following symbols also appear on the instrument or in the documentation Mains power on 0 Mains power off F fuse oN Single phase alternating current Direct current When attached to the rear of the instrument indicates that the product complies with the requirements of one or more EU directives SP When attached to the rear of the product indicates that the product Cn us has been certified evaluated to CSA 61010 1 and UL 61010 1 Color coding The various indicator lights appearing on Agilent i
21. ition 34 Unpacking As soon as the shipment arrives 1 Locate the shipping list documentation and check that you have received all of the items listed If any of the listed items are missing stop immediately and call Agilent customer service 2 Carefully check the exterior of the shipping containers for any external damage Stains on the containers may indicate exposure to water CAUTION Do not open the shipping containers unless otherwise instructed by your Agilent representative 3 Ifthe shipping container s appear to be damaged water damage crushed package and so on contact Agilent and the carrier within five days Do not accept packages with obvious puncture damage All other damage should be noted on the shipping document and signed by the delivery agent Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 27 Unpacking and Installation 4 Ifyou are sure that all boxes have been delivered and appear to be undamaged place them where their contents can come to room temperature CAUTION Do not unpack any additional boxes or packages or the spectrometer or microscope unless otherwise instructed by your Agilent representative Your Agilent representative will complete the unpacking and installation of your Agilent Cary 600 Series FTIR spectrometers and microscopes If incorrectly unpacked equipment may become damaged Installing the software While your Agilent representative will install the
22. n on using the microscope to collect data Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 41 Operation Turning off the system 42 Unless the system will be idle for some time or will be moved we recommend that the spectrometer not be turned off The computer and peripherals can be turned off if desired Agilent recommends that you disable the screen saver because it may interfere with long data collections If you want to have a dark screen during long periods of disuse it is better to turn off the monitor To shut down the computer module of the system 1 Exit Resolutions Pro and close all other applications 2 Choose Shut down from the Start menu Using the computer s power switch to quit Windows may cause data to be lost Always use the procedure advised by Microsoft If necessary turn off the spectrometer or microscope power switch Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Maintenance KP o e e 0 e 5 Maintenance Oe amp Routine 46 r j Cleaning 46 i Spare parts 46 This chapter includes information on how to access the Agilent Cary 600 FTIR spectrometers and microscopes maintenance procedures that may be carried out by an operator Any maintenance procedures not specifically mentioned should be carried out only by Agilent trained Agilent qualified or Agilent authorized representatives Agilent Cary 600 Series FTIR Spectr
23. nstruments and associated accessories are color coded to represent the status of the instrument or accessory e A green light indicates the instrument is in normal or standby mode e A yellow light indicates that the instrument needs attention e A blue light indicates that operator intervention is required Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 17 Safety Practices and Hazards 18 CE compliance Agilent Cary 600 Series FTIR spectrometers and microscopes have been designed to comply with the requirements of the Electromagnetic Compatibility EMC Directive and the Low Voltage electrical safety Directive commonly referred to as the LVD of the European Union Agilent has confirmed that each product complies with the relevant directives by testing a prototype against the prescribed EN European Norm standards Proof that a product complies with the directives is indicated by e The CE marking appearing on the rear of the product e The documentation package that accompanies the product containing a copy of the Declaration of Conformity This declaration is the legal declaration by Agilent that the product complies with the directives and also shows the EN standards to which the product was tested to demonstrate compliance Electromagnetic compatibility EN55011 CISPR11 Group 1 ISM equipment group 1 contains all ISM equipment in whichthere is intentionally generated and or used conductively
24. ometers and Microscopes User s Guide 43 Maintenance 44 Eye Hazard Near infrared operation The tungsten halogen lamp is extremely bright has high ultraviolet UV output and should not be directly viewed Avoid direct exposure to the lamp In addition appropriate UV filtering glasses are recommended to remove harmful UV radiation This lamp should always be turned off when not in use as it has a limited lifetime Far infrared operation The mercury arc lamp emits harmful ultraviolet UV radiation and must not be viewed by the unprotected eye Appropriate UV filtering glasses are strongly recommended Avoid direct exposure to the lamp This lamp should always be turned off when the instrument is not in use or when the cover is opened This is easily accomplished by selecting the other source position in the software UV visible operation The xenon and deuterium lamps emit harmful ultraviolet UV radiation and must not be viewed by the unprotected eye Appropriate UV filtering glasses are strongly recommended Avoid direct exposure to the lamp The lamps should always be turned off when the instrument is not in use or when the cover is opened This is easily accomplished by selecting the other source position in the software Electrical Shock Hazard Contact with these circuits devices and components can result in death serious injury or painful electrical shock This instrument contains electrical circuits devices and componen
25. ompartment or on the spectrometer or microscope should be immediately wiped up The exterior surfaces of the instrument should be kept clean All cleaning should be done with a soft cloth If necessary this cloth can be dampened with water or a mild detergent Do not use organic solvents or abrasive cleaning agents Spare parts For spare parts and consumables ordering information refer to the Agilent website www agilent com 46 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Troubleshooting ee o Ka o e e 6 Troubleshooting Oe e e For troubleshooting help refer to the Resolutions Pro Help To access the Troubleshooting section of the Help 1 Start the Resolutions Pro Software 2 Press F1 on the keyboard to display the Help 3 Click the Contents tab if necessary 4 Click the plus icon next to Troubleshooting to expand it Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 4 Troubleshooting This page ts intentionally left blank 48 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide www agilent com In This Guide The guide describes the following e Safety Practices and Hazards e Introduction e Unpacking and Installation e Operation e Maintenance e Troubleshooting Agilent Technologies 1997 2000 2004 2010 2013 Printed in Malaysia 05 13 8510246800 Issue 10 aE Agilent Technologies
26. ords with faulty or frayed insulation Use of controls or adjustments or performance of procedures other than those specified in this manual may result in hazardous radiation exposure Laser safety The Agilent Cary 600 Series FTIR spectrometers use a helium neon laser operating in the visible region at 632 8 nanometers The spectrometer is a Class 2 laser product powerful enough to warrant caution in its use Agilent Cary 600 Series FTIR spectrometers and microscopes comply with FDA and CE standards for light emitting products An attenuated portion of the laser beam passes into and through the spectrometer sample compartment Although not powerful enough to harm your skin should your hand intercept it the laser light could cause retinal eye damage during prolonged direct viewing This is not possible given the normal optical layout of the spectrometer However if a highly reflective surface such as a mirror is allowed to intercept the beam the beam could be redirected out of the sample compartment resulting in on axis or direct viewing Care must be taken to avoid this The laser in the spectrometer is operating when the green power indicator of the spectrometer is active The Agilent Cary 600 Series FTIR spectrometers incorporate an interlock switch that automatically turns off power to the laser if the interferometer compartment cover is opened No maintenance of the spectrometer or microscope by users is required to maintain spe
27. ou operate the instrument safely Read each safety topic thoroughly before attempting to operate the instrument and always operate the spectrometer and microscope in accordance with these safety practices Ultraviolet radiation Tungsten halogen source lamps for near infrared analysis emit hazardous ultraviolet UV radiation This radiation can cause serious damage to eyes NEVER look directly at the lamp and always wear appropriate protective equipment and clothing when required Cryogenic cooling Some detectors used with your Agilent Cary 600 Series FTIR instrument MCT or InSb detectors are cryogenically cooled The liquid nitrogen used in this process is extremely cold 196 C 320 8 F and can cause damage to the human body Use appropriate protective equipment when working with liquid nitrogen Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Safety Practices and Hazards Compressed gas cylinders Consult the Agilent Cary 600 Series FTIR Site Preparation Guide for gas pressure requirements Compressed gas cylinders contain highly pressurized gas If storage conditions are outside of the recommended supplier s safety codes the cylinders can explode or rapidly release gas into the environment This may result in injury or death Store and handle compressed gases carefully and in strict adherence to safety codes Secure cylinders to an immovable structure or wall Store and move cylinders in
28. pectrometers and Microscopes User s Guide Unpacking and Installation The connectors are from left to right RS 232 Power USB Joystick Z Stage Connect to a RS 232A serial port on the computer using a RS 232 serial cable Connects to the power transformer Currently not used Connects to the joystick Connects to the Z axis motor used to control the stage height see 2 on Figure 12 using the cable shown below Connects to the X Y stepping motors on the right side of the stage see 1 on Figure 12 Figure 12 Motorized stage connections Where 1 X Y stage control 2 Z stage control Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 33 Unpacking and Installation 34 Programming accessories for hardware recognition While many accessories purchased will be pre programmed some may not Agilent provides the Service Application software to program or reprogram your programmable accessory to work with the hardware recognition capabilities Most components are programmed in the factory however some may require reprogramming See the Resolutions Pro Help for instructions on how to program accessories Specifically click Start gt All Programs gt Agilent Resolutions gt Resolutions Pro Help gt Accessories gt Programming Accessories for Hardware Recognition Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide
29. pectrometers and microscopes are suitable for indoor use only and are classified Pollution degree 2 and Installation Category II EN 61010 1 All specifications are included in the Agilent Cary 600 Series FTIR Site Preparation Guide Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 21 Introduction Environmental For proper operation of your Agilent Cary 600 Series FTIR spectrometers and microscopes these conditions are required e Temperature 20 C to 26 C 68 F to 80 F e Temperature gradient 1 C hr 1 8 F hr maximum e Relative humidity 20 to 50 non condensing e Altitude FTIR spectrometers and microscopes have been thoroughly tested for correct operation at sea level only Please contact Agilent Technologies for advice if you wish to install a system at an altitude significantly above sea level e Free from corrosive and flammable fumes e Free from strong electromagnetic fields e Free from vibrations Performance degradation may result from the exposure of the spectrometer or microscope to strong radio frequency energy If degradation is experienced reorient or relocate the spectrometer or microscope or the radio frequency source Fuses Position the equipment for easy access to the disconnecting switch on the rear of the instrument Table 1 Fuse specifications Instrument Fuse type Agilent Cary 600 Series FTIR spectrometer T4 AH 250 V IEC601272 2 Sheet 5 5x20 mm Littelfuse 0
30. reen The spectrometer is scanning Bottom A D Off Normal operation over range Flashing blue The A D exceeds its maximum value Reduce the sensitivity setting or increase the beam attenuation Turning on the system and filling the Dewar Spectrometer CAUTION This procedure applies to detectors requiring liquid nitrogen Most instruments are supplied with DLaTGS detectors which do not require nitrogen cooling Always check the detector type and cooling requirements before performing this procedure 36 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Operation To fill the spectrometer Dewar with liquid nitrogen 1 Turn on the spectrometer power switch located on the rear of the spectrometer If the spectrometer has been turned off for an extended period it will take about 30 minutes to reach its operating temperature If you collect data before the spectrometer has reached operating temperature your data may not be accurate 2 If you have a cryogenically cooled detector MCT or InSb fill its Dewar with liquid nitrogen as follows Extreme Cold Hazard Liquid nitrogen is very cold and can cause damage to the human body Use appropriate protective equipment when handling liquid nitrogen a Raise the spectrometer cover The Dewar access hole is on the right rear of the detector compartment cover eee Dewar fill hole Detector compartment cover raise spectrometer cover to acce
31. s plug is easily removed by hand Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Operation Figure 14 Top of the microscope showing the liquid nitrogen plug Extreme Cold Hazard Liquid nitrogen is very cold and can cause damage to the human body Use appropriate protective equipment when handling liquid nitrogen 3 Carefully fill the detector Dewar with liquid nitrogen using the provided funnel This takes about 2 5 medium sized Styrofoam cups 475 milliliters 16 ounces of liquid nitrogen Minimize spills by adding half a funnel of liquid nitrogen at a time and allowing it to cool down until the vapor plume dies down Repeat as required 4 Allow about 20 minutes for the Dewar to come to thermal equilibrium 5 Top up the Dewar with about 200 milliliters 7 ounces of liquid nitrogen 6 Replace the plug Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 39 Operation CAUTION Large liquid nitrogen spills can damage the detector and other microscope components Do not fill the Dewar to the top This can freeze the elastomer o ring Dewar seal causing a loss of vacuum This will require the detector assembly to be returned for a pump down Performing a collect 40 Spectrometer The basic steps to perform a collect using only the spectrometer are 1 Setup the hardware based on the experiment you wish to perform 2 Find the centerburst 3 Run a background collect
32. ss Figure 13 Dewar hole on spectrometer Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 37 Operation 38 f g Reach through the hole and remove the liquid nitrogen Dewar plug Carefully fill the detector Dewar with liquid nitrogen using the provided funnel This takes about 2 5 medium sized Styrofoam cups 475 milliliters 16 ounces of liquid nitrogen Minimize spills by adding half a funnel of liquid nitrogen at a time and allowing it to cool down until the vapor plume dies down Repeat as required Allow about 20 minutes for the Dewar to come to thermal equilibrium Top up the Dewar with about 200 milliliters 7 ounces of liquid nitrogen Replace the plug Lower the spectrometer cover Turn on the computer and monitor If you are setting up your spectrometer or if you change the spectrometer detector beamsplitter or source you must configure the hardware before you can collect any data If your hardware is already configured you are ready to collect data Microscope This procedure applies to detectors requiring liquid nitrogen Most microscopes are supplied with MCT detectors which require nitrogen cooling Always check the detector type and cooling requirements before performing this procedure To fill the microscope Dewar with liquid nitrogen 1 Turn on the microscope power switch located on the rear of the microscope 2 Remove the appropriate liquid nitrogen Dewar plug Thi
33. t the documentation both hard copy and online provided with your instrument and accessories Before using the instrument or accessories you must thoroughly read these safety practices Observe all relevant safety practices at all times Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 7 Safety Practices and Hazards General Operation of an Agilent Cary 600 Series FTIR spectrometer and microscope involves the use of compressed gases high voltage energy and hazardous materials including liquid nitrogen tungsten halogen source lamps that emit ultraviolet radiation and a helium neon laser operating in the visible region at 632 8 nanometers The instrument is rated at Class II USA or Class 2 European Careless improper or unskilled use of this spectrometer or microscope can cause death or serious injury to personnel and or severe damage to equipment and property You may choose to wear personal protective equipment such as optical safety glasses but this is not required for this instrument The spectrometer incorporates interlocks and covers that are designed to prevent inadvertent contact with any potential hazards If the instrument is used in any manner not specified by Agilent this protection may be impaired Develop safe working habits that do not depend upon the correct operation of the interlocks for safe operation Do not bypass any interlock or cover These safety practices are provided to help y
34. ts operating at dangerous voltages Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide Maintenance Hot Surface Hazard Burn danger Allow hot parts to cool before proceeding with any maintenance procedure Extreme Cold Hazard Liquid nitrogen is very cold and can cause damage to the human body Use appropriate protective equipment when handling liquid nitrogen Laser Hazard The laser light could cause retinal eye damage if prolonged direct viewing occurs This is a Class 2 laser product not powerful enough to harm your skin should your hand intercept it The optical design of the 610 FTIR normally precludes this You are never required to remove the protective housing of the 610 FTIR Always wear appropriate safety equipment and clothing This section refers only to maintenance procedures for the instrument You should refer to your computer and printer manuals for their maintenance procedures and to Resolutions Pro Help for the maintenance procedures for any accessories you ordered Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 45 Maintenance Routine Routine maintenance information is provided in the Resolutions Pro Help To access the Help 1 Start the Resolutions Pro software 2 Press F1 on the keyboard to display the Help 3 Click the Contents tab if necessary 4 Click the plus icon next to Maintenance to expand it Cleaning Any spills in the sample c
35. wer and purge lines to the microscope 1 Make sure the power switch on the rear of the microscope is in the off 0 position Figure 8 Power switch and socket on the rear of the microscope USB to PC cable also shown 2 Connect the power cord to the rear of the microscope 3 Connect the other end of the power cable to the electrical power outlet 4 For purging of the microscope connect the gas purge line to the fitting on the rear of the microscope upper cover CAUTION Use only dry air or dry nitrogen to purge the spectrometer and or microscope Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 31 Unpacking and Installation 32 Figure 9 Upper rear connectors on the microscope Left to right Purge fitting to gas supply Video out to video capture card installed in the computer Microscope to spectrometer EXT DET 1 or EXT DET 2 connection see Figure 8 5 Connect the Video out connector to the back of the microscope and then to the video capture card installed in the computer Figure 10 Video capture card installed in PC with Video out cable connected 6 Connect the Detector out cable to the back of the microscope and then to the EXT DET 1 or EXT DET 2 spectrometer penthouse connector Connecting the motorized stage cables There are six connectors on the rear of the stage controller Figure 11 Motorized stage controller connections Agilent Cary 600 Series FTIR S
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