913KB
Contents
1. 450nm 1 1 8 ppb a os 2 FR PR 2 lt 1 EES BLD HA Ze BT WL AY 3 4 12. 1 7 5 16 EL 1 SA 12HHHHHHH O
3. E FE RAR FIV bP NGG v FE 17 10 28 17 12 14 IIHHHHHHHHHH ELISA ELISA 96 HU 1 ELISA 6
4. EHSAIHHHHHHHHH 430 Lot No I 0 CORAL Lot No Ll 9 440000000 ELISA
5. ELISA ELISA ELISA ELISA ELISA
6. TECAN 450nm 3 4 parameter logistic fitting LS PLATEmanager 2001 A O HHHHHHHHHL 10
7. 4 4 1 441 0 1 2 4 8 g L DH ERE FR OE TI DEE 0 oF ey 0 0 1 1 10 100 ug L 0 4 10 25 60 mg L HHHHHH 3 3 8 SD MA SD 3SD 10SD
8. HHHHHHH 3 50 50 50 X100 50 50 20 10 11 HHHHHH GFC
9. E E FLN 0011 17 9 21 8 1 8 ug L 17 10 31 9 00 11 45 5 22 CC caveman Rak ores nos LS PLATEmanager 2001 BY HHHH HHHH 1 109 1 gL 3 8 3 8 SD 3SD 10SD OUI 2 0 10 SD 3SD 0
10. 0 02mg L 0 2mg L 2mg L
11. 50mg 1466 1 10mg L 102 113 3 2 6 3 GC MS SIM 3 3 3 31 1 2 3 PER HHHHHHHHI Flutolani1 N 3 1 methylethoxy phenyl
12. ELISA ELISA 1 1 2 3 4 5 6 7 2 1 2 43000000000000050 1 ELISA ELISA 4 3 ELISA OELISA OELISA 2 ELISA OELISA OELISA
13. FR MRR gE RFE lt lt lt lt my 25mL NN 85 MeOH J 1nL 7 VHRIT EY 7 5mL 8 5 gt 8 3 3 4 30 25C 6mL 106 1 0mL 7 3 8 2 SAT 2
14. ELISA REED 3 ELISA 4 ELISA 5 ELISA Os TAA Ca LCRA ELISA
15. 100L we11 25 C 1 ut 3 100 L we11 25C 10 100 L we11 450nm 3 5 3 6 3 8 HW A 2 1 ppb A B C 4 9 RG SE fin Mh cn 3 BS KS BS ts KO KO oo lo Cee ENE ETS i 5 BR 3 2 1 2 2 4 8 6 0 1 2 5 4 2 BE 1 8 2
16. 2 21 5 2 7 Dries U 5 26 HHHHHHHHH fe JO fy BIT RAT Le 1 487 1 425 1 379 1 427 1 388 1 338 1 432 1 397 1 380 U iF ggL uel 3 ggr uel mr g L ELISA 1 0 12m g L 2 0 77 gu g L GC MS MDL 0 008g g L 527 0000000000000000 2hgLHHHHHHHH ND XD XD me 1 EL 9 95 g L ELISA 1 0 12 rg L 2 0 77g L GC MS MDL 0 008 u g L 30 6 HHHHHHHHHHHH 7 1 8 g L
17. 6 ee ee 15 CONES S60 RC I ee 15 2 16 3 18 4 19 5 we ee 21 6 ee we 23 OTL 9 RO ESE ESHER HG REESE SOE Se 26 5 2 ee ee we ew ee 27 1 6 6 27 2 29 6 31 1 31 31 3 31 7 1 1 HHHHHHL 1 1 HHHHHHHHHH
18. 2 1 1 EST A DR CR RS NS ND Dd CE ee Me EOI ks Eee ee EE SE er ee I ON te ee ee ee eee ee ee ee ree 3 1 ODES ea ee RR EG BS DEE O 3 2 eee ee ee EE CE RAE OR SRS 4 1 4 2 6 4 3 tt E EN 1
19. 12 43000000 1 OOOO HOOD UW 43 1 000000000 EEA F 1 068 02023 YPH8125 5 RE 7S OES 120860050 A0207160001 LS PLATE manager 2001 5 8 yk OR 0432 HHHHHIH 81 HIE ID FR IT 111 2801 51 ll 7 2 COD 2 0m OOD GEC 1 2 2 g L
20. 0 S113HHHHHHHHHHHHHI AYR S1 PAYER S2 TAYE S3 PAYER S4 AK S5 3 IEEEIEIEIEE 1 302 1 228 1 2350 97310 87910 88610 64610 0000 By 57 7 1 59611 417 1 30911 21211 1370 98610 69110 86610 6540 54110 53110 32910 27710 4 gl 953 224112817 145 4 005 8 053 TE em TS 5 00000 N N OO N OO N N O2 N N CO E gt CA N 3 CA N e Not HHHHHHH 15 1141 HHHHHHHHHHHHHHHHHHH 9 TERE ull 0 1 2 4 s xe 2 Le75 1178 086 0 585 0 207 WOR 3 1 57 1218 0943 0 565 0 320 15 1142 HIHHHHHHHHIYHIH HIHHHHH HIHHHHI 2 lt 2 1 671 1 276 2 076 0 073 0 993 21 a A EF Cre 8 0 52 Flet Seance d ae 1 15709 179E 00 211550 73220 ST 515 1 U 5 1 15 1 UW UU ie TERE 6 1 2 s N 2 1250
21. 50mg L 146 24 g L 0 1 5 10 50mg L 0 5230000000000 0 g 0 1 5 1 3 3 3 0 744 0 794 0 733 i 1 5 3 3 3 0 4 0 794 0 733 0 712 A 0 D2 OTB ot 6 07 3 ono oe es 0 720 vo ozo 0766 0 738 0 718 28 00000 1 53 24 HHHHHHHHHHHHHL 0 STD1 STD2 STD3 STD4 ee TE em 2 oso 0674 056 058 022 RE 3 oss 0654 0529 0 368 6 DA DD XN QI BI mak 4 C P 5 5 MF f it iT E A f GF EI 8 1 AZ CPi Sram 819 v SIEM BED SRE 1 813 WE 522 G00 29 0000 ELISA GC MS ME
22. Re 3 OO UW 42300000000000 E E FLN 001F 17 9 21 1 8 ug L 17 10 31 9 00 5 5 6 lt TH A RSE AE BEAT Le ER Ean 068 02023 5 LS PLATEmanager 2001 5 AE BRIE Sa 0000 2 527 10 XB 17 UT 2 u g L EMH Le MIRE Le 2 3 8 8 4 000
23. RE RD Be est REE SCTHETOC 2 REDE 300 wL 3 Ti BR 1 100 ul 15 25C 10 Sk 100 nL V EA raw pote lt 01 ET Ol 9 pe LT2 8 EY i ee 10
24. Cl1 C2 C3 C4 10 1ml C1 04 1 2 4 8ppb 3 6 mL 4 450 mL CUA CHAR L BRA E LET 2 78 1 Enzyme linked Immunosorbent Assay ELISA Es
25. 1 10me L 102 113 CA UY MR 3 Be BRT ESE DE EME 3 2 6 3 GC MS SIM 3 3 3 IV 1 Lt Sa a Oe eS ae ee WW ee 0 1 2 Si 2 1 2 9 ies 3 3 2 1 3 2 2 3 2 3 3
26. e ue ELISA 14 5 5 1 HHHHHL 1 OOOO HHHHHHL 5 1 1 5 STD1 STD2 STD3 STD4 a Le et sem 2 1622 285 0 992 0 607 037 ween 8 1614 1 307 0 980 0 500 037 2 z Da DF Cre i 4 i ma i 2 156532EH000 12897 E00 0 2352 00 1 5 11 15 U00000 DD 2 13000000000000050 el ee 1 0 1 298 0 997 0 692 0 334 1 5 1 9 0 986 0 654 0 329 oo We 1 mw
27. ELISA 00 IIHHHHHHHHHHHHHHHHHHHHHHHHHHHL 31000000000 ELISA ELISA 96 32U000000000 3 2 HHHHHHHHHHH sate AHD Km
28. 3830 25C 1 3 2 4C 30 25 J 7 A 7K 6mL CLA ME LL 832221 2 ey Ue 1 3 3 10mng 10mnL 1000ppm 10 10ppm eee arrested REDA HE DT 245 5 TK KAT mL 10 40 1 1 3 4 100 rrL we11 25 C 1 3 100 L well J e 25C 10 100 L we11 J 450nm 1
29. lt e e lt e lt lt my gt 8 25mL NR MEK A ROT YU YS CALE 85 MeOH J 1mnL 7 5mL 8 5 3 3 4C 30 25C J 6mL 106 1 0mL 2 3 4 10 MeOH J 100L we11 25 C 1 J 3
30. Ss a NNS es A ieee Srey ae I ES O 2 E ee 1 TT ZA TEBEK FE BU IEE DHE Fi HB Te 2 Y TICS IT SIV
31. OE 12 1 10 2 1 3 2 3 2 ELISA
32. 7 OOOOOG HH 0427 HHHHHHHHH I PMP SVE YE NEA LAD 17 11 7 14 50 18 20 5 LS PLATEmanager 2001 EE D42 8000000000 aia RT Ci U4290000U000 5 CA 110 100 wer 0 ORE 6 4 10295 60 mez 0000 3 50 50 50 X 100 50
33. 2 BE 1 2 r NE AO Ae SV 5 6 PIII SRT ay TES 9 10 PAP 11 MEP 3 Tis 3 1 via 4mL 10 40u1 3 2 LA E LF RIN HE LUT Bese tii amp LF amp FR HEEE TRIAS RK SJ J 100 uw L well Ne Dor RE LT 100 L we11 J 25C 10 100 L we11 450nm
34. E T 682 0704 526 1 17 10 28 17 12 14 E EL105 01 Hitt 350g 99 750 ZI 7 IV AD KEE toh HD HB ERD 15 C 25C 40 0 10 46 n 2 1 12 1 QUOD He DH FERE BE ae AR A BHA 1 2 4 Su g L 95 101 1 3 7 49 B BO 0 8 0 2 1 8ppb lu g L Cae Bk n 8 SD 1 3SD 0 12 g L FE 10SD
35. 3 4 IC ICsg ICE X100 2 4 3 DIAS pA aD PN I ee EN Yale a Sa 0 ST aT ee OIE VW TI PAP MEP 5 BB 30 1 2 1 2 1000ppm FE ZX FX 7 IEEE 3 3 1 RIN HEE ENED THE 0 1000ppm 50ppm 3 2 RN SS SIM FR EK CLC 1 811002602 L 2 3 ORIN
36. 2 3 Fae 3 1 8 30 25C UM 6mL 10 1 0mL 092 Fea BARE REAM SE EEE SARE AU CLOW RA FX 7 100L we11 25 C 1 Al 25C 1027818884 Le 1 100 L we11 450nm Vleet 2 A 4 1 1 3 1 1 PC 28 90 180 270 300 330 360 0 878 0 939 0 764 0 808 0 038 0 043 0 029 60 040 44 46 38 60 100 0 93 7 101 7 99 0 105 9 86 1 91 1 0 727 0 645 0 658 0 709 0 724 0 635 0O 637 _ 0 81 0 77 0 83 079 SD 0 017 0 027 0 019 0 031 0 028 0 025 0 0171 CV 24 43 29 44 38 401 gt 27 90 5 97 5 99 6 87 3 61 0 204 0 1 5 0
37. 1 4 0 065 0 3SD 1 524 0 195 1 329 2 0 77 pg L 17 3 HHHHHHL U 3127 HHHHHHHHHHHHHH fe a FH YEE YA ir STD1 STD2 STD3 STD4 zgL 0 1 2 4 8 Li 0868 052 0 283 1500 2 wen 3 1 603 i1223 0925 os 0 309 0518 HHHHHHHHHI HH HHHHH q A 1 572 1 213 2 042 0 9 0 988 0 1 3 5 ti 8 T Be BOF hee Sora A 1 Gi I Feo ORC Stands HEEE WW 15 maEa 1 2132 ASAD EDO EN Does 1513000 HH 519 HHHHHHHHHHHHHH S2 u g L Pe 2 2 2 2 2 2 2 pr 21 fe 7 fs 3 2 1 1 2 1 OB 1 895 4 00000 1 5 1 10 1
38. 1 HHHHH ELISA 2 Fy KIC 2 7 27 22 118 amp FAV Blt DDB SC DTT KIT K 3 000000 TECAN 4 HHHHH 3 4 parameter logistic fitting 5 ae alee LS PLATEmanager 2001 5 00000000 4 42000000 1 OOOO OOOO 0 421000
39. 0OD 0 2 6 4 3 1 1 5 10 49 10 HHHHHHHH 1 8 g L 2 AC 1 B 3 1 2 6 69 OND 36 6 lt 0 1 30 1 6 lt 0 19 2 000000 OO OK CA Ee FO RATE Ou g L 1 50mg L 102 146 a 111 5 160 9 OOOO PUK Aw 7K 3 3 ELISA GC MS ELISA 1 0 12 g L 2 0 77ug L GC MS 0 0
40. 1 1 8 X12 ay pa EE EER 9A a 5 E YEAH C1 2 ppb E YESE SEK C1 4 ppb E YEAH C1 8 ppb RE 0 5 6 OF 7 E 1 ee 38 3 10918015 PURER LF 9 EET ED wal ee 150L 8 1504L 1 E 7 1 2 181218515 FP TIZ CIEE PRE LET 1 3 feds LASS Eh ort dete 5 9 100 gL 8 A Re 55 COL ho REE ee 2 25C 1
41. CO O2 0 Oo 3 ah ms A CC B AA NCHA 7 0000000 000000 U 24410000000000000D IR RA ETA HK 2 STD1 STD2 STD3 STD4 E EIT sea 2 lo 100 695 05 O2 WORD 3 1 639 1 3900 02967 os 6sn mok A aa C 5 re ii 1 1 1 1 1 i i i i i i 1 1 1 1 i i 1 i i i 1 i 8 a 1 8 Ff i i i i i ee 1 1 1 1 1 1 Lit ii i i i i LI LI LI id i i tpt ti i tw iii ila ic i i 1 i a i i i i 8 a a i 5 0 i 0 a a i a a i i 8 a a i a a 1 a a a 1 0 a 1 1 i 1 ta 1 0 a 0 5 DB i ne od eee EEE 1 1 1 8 a ie a a of Fr ee ee mm mmm mm mm i i i i 1 1 a Fe a 1 1 1 ed 1 1 1 1 as i i i i i WM ca uz i i i i a i L i 0 i f D 4A rie GFE A 0 Hz Flot MME V1 aE 2305TExDGO 19076E 002 0R 05 163 000 HHHHHL 0 5 14221 0000000000 TT rir gt 2 1222000000000000 unl 0 52 s xm
42. O UU 421HHHHHHHL 41 00000000 082 0704 990 kei Gort toto jp T 601 8315 48 ae Shigekazu ito horiba com 2420000 A U Z2 HHHHHHHHH 2 3U00000000000 43 HHHHHHHHHHHH ELISA ELISA
43. 2 1 8 ppb 8 ppb 10 LCN SUS Q 30 1 O WHERE 7601 8315 48 TEL 075 692 1786 FAX 075 692 0 http Wwww horiba biotech Co jDp 1 1 1 1 Bo 20 80 1 2 7 TMB 1N 1 3 oT Vn 4C
44. E EL105 01 99 750 DER OIL 15 25 AC 8C 10 46 2 3 42 HHHHHHHHHHH 1 1 8 ppb 1 0 16 0 29 4 8 6 0 1 0 06 0 22 1 2 5 4 2 2 30 1 2 2 113 120 2 GO Te 1 5 1 2 2 7 410000000 17 10 17 11 U41 HHHHHHHHHHHHHHH li ee ee
45. 0 1 5 10 50 mg L 50 60 55 3 13 1 433 0000000050 Ha hE E FLN 001F 17 12 12 17 30 21 00 17 12 13 18 00 0 12 12 21 RE 12 13 21 LS PLATE manager 2001 atk AV Be 143 4 WAR AID 17 12 9 BIRT CEI 17 12 9 AT GEND 17 12 9 0000
46. O A E G 1 ies OP int Stendard ATE 1 V_ 11802 118592000 318212010 7 HESSEN om 5162 00000000 BJ 24 25 0 28 0 286 Re S5 0 102 0 55210 287 0 53510 2610 0 ey DT 0 55910 0 543 PAYER S4 SE 1 0 536 0 49410 Ye 051191 HHHHHHHHHHHHH UHHHO ABTA 00 0 691 PAY S3 2 oR IH 139110 155 1 222 0 S2 1 WF ESTED 1351EEHDU PEGHEHO 4O71OF 003 18 147 1 05163 HHHHHHHHO 1 1 526 1 543 1 1 0 21L20000000000000060 1 400 1 450 Ay1 oO x S o S A oN CO OO CN 3 1E Ci F i YAW SI gt 0 5119 2 OUD A DODO dd HDD KA 5 c 5 ol il 1 489 Flot Standard 9 5 1 fees 0U000060 0 918 1 5541 5841 5711 25611 22311 2810 52610 55910 8340 50610 56310 5090 25410 286 09 0 905 0 843 519 11 478 1 o47 1 196 1 172 1 24710 85810 8586 0 8810 51210 555 0 54210 267 10 285 CO lt 00 CO CO oo LO oo OO LO ST e OO ap N O2 CO Cc N CN OO LO CYO 3 LO
47. t ai cad eee CC SC ey eee eee ee ee See et SSCS wea Ol enh Sree a a ae Gye ee ea ae ee es RNN Neesstoes 07 ee Soi es esha ie ea gi ss 6 CDSE re ee ee ee ee 0 Se a PO ee Oli See eee ee eee ee eet ee ere CE sg a Ge a lt a Sb E fete wee oo OD OI Ls Zs 3 4 0 1 2 3 4 1 1
48. 1006 3 2 HHHHHHHHHH 514 HHHHHHHHHHHHHH 3 sem 2 1 507 1 208 099 os576 029 wee 3 1 573 1 245 0 951 0 558 0 252 0 5 1 5 DA DD TH A B CD R2 1 627 1 242 2 2 0 051 0 996 16 Oe A Ra A O 12423E 000 d SECON B14BGE DOG 996 18366 dA V OPO 0512000 U00000 0 5 161 HHHHHHHHHHHHHHHHHHHHH 0 S2 wet 1 1 1 1 1 111 1 1 2 3 4 5 6 7 gs Es Ree ee ae ee fea 2I0 Pos cats 1l a LE es ao os ao we 20 3SD 0 12 1 g L 10SD 0 40 g L 05162 0U000000000000000000005 RSI 1 ELISA 1 571 1 538 1 624 1 573 1 461 1 473 1 581 1 418 1 520 1 478
49. ELISA 1 Ale 6 2 1 1 ELISA ELISA 2 HHHHHHHHHHHL E EL105 01 g 350g 99 750 A 15C 25 4
50. HHHHHHHL 3 8 3 8 10 n 8 HHHHHHH 1 3 3 HHHHHHH 2 1 HHHHHHHHH 2 1 3
51. 1 4 7 B Bo B Bo 0 8 L 1 ppb B Bo 0 2 WELT 100 B Bo 10 ppb E 1 UU HHHL 0 1 1 AE HL 8 ppb 1 2 2 1 1 ppb 8 ppb Bo 2 2 2 3 2 3 1 4C 30 25 6mL 10 1 0OmL L H lt 2 352 7 EA EEA CL HD 10 1 100L we11
52. 100 L we11 J ee 25 C 10 100 L we11 J 450nm 4 4 ppm ppm a NO MR6 6 5 BB 4 113 3ppm 131 5ppm 7 100 1 10 7 2 4 2 0 Analytical Chemica Acta 376 1998 93 96 Development of a competitive enzyme linked immunosorbent assay based on a monoclonal antibody for a fungicide flutolanil 2
53. 3 5 OO U 4250000000000 B E FLN 0017 17 9 21 Lee tet 17 10 30 0 20 11 45 17 11 30 8 50 13 00 5 10 30 22 11 30 19 Yl E Fr 068 02023 YPH8125 LS PLATEmanager 2001 me AR AR 0000 2 1 1 1 1
54. OD GEE 6 HHHHHHHH HHHH 0426 HHHHHHHHHH I E FLN 001F E FLN 002F EE HE cre 17 11 2 8 50 0 5 5 7 FEE TE 068 02023 5 LS PLATEmanager 2001 8 nN 1 4 MRSS SA 0U0000000 2 1 3 1
55. We STD1 STD2 STD3 STD4 ERK nl o 1 1 gt 4 1 8 0337 0607 699 1235 162 12 WORD 3 Le 130 Ge 0 590 037 HHHHHUHHIHIUH HHHHHH BII RR A Dp 85 fi so amp irra 13 Ds A B i oi Ro OP inti Sirdar REE V BRED 1 FEO 2 BREE 11 0 5 1 4 1 0010 51111 3000 eee ae ee eee gu 0 1 2 1 5 ELISA 1 1760 1276 02881 0 540 0 823 am 2 1675 1 178 0 865 02555 0 297 wee 3 LST 1912 0 943 0 565 os20 Hea SAUL IU HUA HEIDI BHI 1 671 1 276 2 076 0 073 0 993 19 Fa D CE A 8 b 52 Pel Shanda 113 Vo ISTE ERED 2075500 TE AT 15142000 1 5 112 1 HHHHHHHHHHHHHHHSHHH _ meme uel 0 1 2 4 8 2 149 iiss 089 0 554 0 281 3 1 462 1 162 0 85 0 539 0 287 5112 2 6 XN QC BII Rome A 5 bp gz oe bt AA fey tl i 1 Da tet CPi rarer REE FE a Fi 0 1 HITED 11012 ZE 74270 PTI 5 143 0 20 D000000
56. 25C 1 3 100 L we11 J BR 25C 10 100 L we11 J 450nm 2 3 3 Bo L H t 2 5 0 05075 6 28E 0o 8 H 0 218625 0 000215 8 0 000139 0 14 28 51185 4 21 4 1 761309 8 41E 14 2 144789 1 2 4 1 1 1 2 Bo L HH Bo L 1 038375 0 8185 0 002334 0 002208 8 8 0 002271 0 14 1 9 227799 1 PT lt t 1 25E 07 P T lt t t 1 761309 t P T lt t 2
57. 0 40g L 0 10 SD 3SD 0 2 0 77g L 1 g L 2u g L 3 8 4 3 0 082 g L n 8 0 16 0 29 4 8 6 0 00000 1 8 g L 3 1 3 0 2 8 49 0 004 0 715 g L 3 0 06 0 22 1 2 5 4 OOD 8 g L 2 1 2 3
58. Sa el SOE ORS Re oO eA ee Bare SS 1 I ITT TTT TT ET ETT TTT TTT EET 4 Bi ea RS Seine ee Ra ee oy 4 3 ip es a ae I BS we SS Bee AA Ge 5 5 ww ww we ww JELISAYE ENC a IEDC NE 5 5 OR RF A REPO dB 6 6 6 6 6 6 66 6 6 6 5 DOSES Bk RS Oo oS Ge Bo 14 DAS 5 Dee Olen oe REE RS eh ee ee oe DSCs 5 SSeS OE eee ees owe eR eS eS we GE 5 6 4 2 6 1 eens 7 2 CO ai as Ses ng DA ests Me TT elas eS ee ee Ses Se 8 9 4 10 5 ew we we ww 11 ee 6 12 7 1 N CD EE HSS SS ESSE 13 CA ep eae Si a ah ae Se pa ch ae ee ae ee a 13 NEES E eh eee RN ee 14 eee 15 5 1
59. g ie OD a 10 2 3 3 00000000 3 J00000050 B E REE 7680 0011 1 220 0857 26 7876 F A X 0857 22 4240 e mail yanagawan pref tottori jp 3200000050 B E BLISA 682 0704 5 2 6 1 0858 35 5421 0858 35 5413 A yamane ka pref tottori jp 3300000000 1 UD00000 00000 3400000000 17 10 28 17 12 14 8 4 0000 41 0000000000 14 2 14 3
60. im 3 3 3 s 3 2 1 658 1 270 0 932 os2 0 282 wien 3 reed is50 0 982 0 81 0 207 26 2 1 23 UIHUUUHUUUHL a TS 3 rgm ran os0 vow 2 1645 1588 LI oe ooo ween 3 1578 149 i331 0 583 6o9 5 1224000000000000000 RES EES ERE uel 0 4000 io 25000 60000 gama oa 3 3 s sm 2 1494 1 486 rs06 1368 ween 3 L557 1602 1437 1432 rs 00000 m 00000000 ra w 900000 od 1 10 100 1000 10000 100000 Qu HL 517 HHHHHHHHH 5 2 000000 1 OO HHHHHHH 035241 00000000000000 0 STD1 STD2 STD3 STD4 om oar 0234 109 13396 2 wen 3 13920 rod Go od oz 27 1522 1 DA DDO CI BI A B C D R 2 1 363 1 3583 2 6 0 012 0 995 FE A 8 3 0 CFint Stand W 1 36322000 138E 241805000 118126 02 OT 5 2 1 000 ONE
61. 00 074 Go 0212 7 wpe 3 1167 097 675 oar 0219 05131 2 8 8 8 8 0 0 0 0 Ooo HHHHHH g 1 1224 1376 259 0006 0996 1 1 2 2 1 5 fi 1 9 Yeora Os d sore A E D SPE Glandand RIB VY 12426000 Er TED SHE0E 09 IEE 0 5 15 2 00001000 02 U00000 S116HHHHHHHHHHHHHIL S1 AS S2 AS S3 AK S4 AS S5 zale zale ira o ra o ir E aCe ER ER eS eS Eee E3 1 585 1 152 1 214 0 917 0 884 0 717 0 546 0 404 0 284 0 213 1 608 1 156 1 228 0 958 0 879 0 702 0 525 0 4 0 274 0 206 Ba 41 8 EES E RE IL Pugh 1O18 1 054 1 998 2 079 4 145 4 063 9 8 uot 0 043 0 110 0 067 0 046 0 187 282 0 247 ESKERE 25 ml fae rs 6 0U00000000 SWS NTT Duan 5117 1 A Omni Sa mS meme zg Ll 0 1 2 4 8 sem 2 1601 1 215 0913 0 562 0 279 3 160 1 237 099
62. 1 2um 4 4 2 3 4 42HHHHHHH 0 1 5 10 50 mg L HHHHHH 3 ELISA
63. 185 0 201 0 197 0 178 0 166 B Bo 023 002M 021 023 021 023 0 20 SD 0 011 0 027 0 013 0 016 0 003 0 004 0 009 CV 54 15 4 69 7 7 1 6 2 5 e 2 100 0 85 8 90 7 98 5 96 6 87 3 89 5 0 888 0 808 5 1 4 1 000 93 107 4 89 0 80 9 4 2 2 3 2 RTE PM 28 90 180 270 300 330 360 0 01 2 100 1 101 7 95 1 102 8 99 4 102 3 0 217 0 23 CVG 31 5 1 68 49 42 6 2 4 8 60 1 237 0 909 1 120 1 193 1 054 1 039 1 039 ee SD 0 063 0 021 0 049 0 069 0 026 0 025 0 043 1 CV 96 5 1 24 44 58 24 22 4 141 Aa 100 0 73 5 90 5 96 4 85 2 840 84 0 0 0 B Bo 5 BR 2 2 28 Bop 73 59 360 2 Boa n 80 2 8 360
64. 2 trifluoromethyl benzamide a a a trifluoro 3 isopropoxy ortoluanilide IUPAC 66332 96 5 CH O CH CH i ue mp 102 103 C 1 77mPa 20 C TT 4 Log Pow 3 7 1 2 9 6mg 1 20C 3g 1 65g 1 238g 1 606g 1 20C Al 60 FC REK TILT Spiess CEH SIV SO BRIS LOK AG ca 2 3 1997 32 1 18 HHHHHHH IHHHHHHHHHHHHHHHHL HHHHH SHHHHHHHHH HUHUHHUHU HHHHH HHHHHHHHHHHE HHHHHHHL 2 17 5 16
65. 50E 07 P T lt t t 2 144789 t Bo FLD t t gt t Bo L HH t t gt H 2 5 BB t Bo L H 2 1 2 1000ppm 3 3 1 IN HEE ENED THE A 1000ppm J SIN RED tre PE Pe 8 eB 3 2 em 5g SOL BUC SINCE
66. C 8 C HUES 10 46 n 2 1 2 3 E SRT 1 1 18 g L 95 101 8 E 1 3 7 4 Tgz g L SD 38D 0 12 pzg L 1u g L 10SD 0 40 ug L 0 0 77 g L 21 g L YA FEY BE 2 0 3 9u g L 4 9 0 16 0 29 pg L 0 082 ug L 4 8 6 0 1 8 g L 2 0 3 9p g L OR MEINE RIM 0 2 8 4 sS 0 004 0 715 ug L 18u g L 1 2 0 2 6 43
67. J 13 0 MTT TT E el 1 E 10 10 2 a 50 200 uL 1000 nL 500 mL 10 mL ADVANTEC GLASS FIBER FILTER GA 55 3 ORR E e Pe RUS SAS hy U 1 2
68. 0 580 0297 MUU ODI UAH DA O EAN 1 608 1 205 2 872 0 096 0 998 23 15 ee a a E E TE a 1 1 E a 1 he 1 2 jee ee eee 12 nne yy ets Te EE ee eee i een Ta eae E a i Rs ener DE et ee 1 eet a RRR RR RR E SEE i i ERE EE 4 SERE is a E EER NER ER ea ge RE EES fener ee Page ve he ON er sass Fa ee 4 2 i 0 1 2 5 B i fa 5 tA FN RSC A E h FR 8 OF Girde dR Vv LORE 12047E m0 287158 00 SEES U 5 161 00000000 Al 0 5 118 1 0000000000000040000 B 3 STD1 STD2 STD3 STD4 uel 0 1 2 4 8 en 2 LSI ite 0898 6s 0 209 ween 3 1450 ii 0901 6s9 0 323 5 1 18 2 DTT ROTTS TALS SIT IY E
69. 00 OO 0424 HHHHHHHHH E E FLN 00117 17 9 21 1 8 ug L 17 10 28 15 40 19 00 17 10 30 9 20 11 45 17 11 1 10 00 0 5 10 28 24 10 30 22 ILL DLN 2 068 02023 YPH8125 LS PLATEmanager 2001 0000 1 3 Ho AY 1 1
70. 000000 lt UEFA FERRER 2 E E FLN 00117 17 9 21 1 8 ug L 17 10 28 15 40 19 00 5 2 6 5 lt TH A RSE AE BEA LCT BOR 068 02023 YPH8125 LS PLATEmanager 2001 ae AR pes iia 0000 10 8 NK FARIA L LUT A 0 1 2 4 8uge L 3 3 0000000000 wo OO 42HHHHHHHHHHHHHHH NE
71. 08u g L 3 2 g L ELISA 2 6 9 8 96 1149 GC MS 4 4 6 0 95 96 24 HHHHHHHHHHHHHHHHHHHH 21HHHHL 0 7601 8315 4 8 075 692 1786 F A X 075 692 1790 e mail Shigekazu ito horiba com NJ 2 E LISA 23HHHHHHHHHHHHHHHHHHHHHHHHHL 2 3 D23 B EL105 01
72. II 19 7 3 2 3 4 1 2 3 3 1 14 O _ mEemHDR of J O Mn Letom oO Tel el ol hl 0 O0 O ii 0O 42U000000 4 2 2HHHHHHH ELISA Do ELISA
73. IM INE HHHHHHUHHHHL HHHHHHL 1 7 5 1 6 2
74. eX 1 0 Var 2 30 lt 8
75. pene Mi 1 1 5 10 4 t 1 84 g L O7 2 1 126 6 36 6 30 1 lt 0 1 i 0 1 a 2 2u g L 0 1 5 10 50mg L 113 120 102 146 ELISA 2 g L ELISA 96 114 3 0 2 6 9 8 GC MS 95 96 4 4 6 0 1 7 1 8 g L 2 50mg L 146
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