A: OPTIC-4 - GL Sciences BV
Contents
1. 2 2 OPTIC 4 OPTIC 4S OPTIC 4SC OPTIC 4D OPTIC 4DC D2. 1 4 11 3 GC dada 530000110959 1 2 d OPTIC 4 Z Standby Cac ELET GC 40 C
3. Page 7 1 OPTIC 4 Issue 1 0 7 2 3 Large Volume Injection GC 2uL 2mL 1uL 1mL 2uL PTV OPTIC 4 OKIE A LVI 150uL
4. CO2 or LN2 Vessel 4 4 OPTIC 4 2 1 8 466 MELE AN OPTIC 4 1 OPTIC 4 2 OPTIC 4 Page 4 10 OPTIC 4 lssue 1 0 5 5 1 Evolution Workstation OPTIC 4
5. rr 1 2 GC 3 4 4 6 1 OPTIC4 SC OPTIC4 DC add ed dM OPTIC 4S OPTIC 4D 22 bL sq st E 4 5 23455 7 3 46 2 GC
6. C 2 3 OPTIC 4 2 4 40 C
7. 18 40 C ig RE 40 70 5 OPTIC 4 EFC 300 700 kPa 99 995 6 GC GC GC MS 7 OPTIC 4 700 kPa 700 kPa 1 3 1
8. 3 Barend lel Page 1 3 OPTIC 4 lssue 1 0 2 GC ITIL OPTIC 4 GC GC 2 OPTIC 4 GC ANGE
9. ST Page 11 4 OPTIC 4 Issue 1 0 12 12 1 OPTIC 4 12 1 1 CS PRT 7 JVDZELAR GIB Cab OO
10. FRVEDSIEHE CH e 100 e e SPE 7 2 4 LINEX
11. 4 3 I 10 I Re ee ll aad Page 4 6 OPTIC 4 Issue 1 0 Column Mounting Tool Cut Column Flush with End of Tool 4 3 3
12. Cooling Valve Mode C Yes No No Delay Time No 9 6 OPTIC 4 4 Configuration System Configuration Auxiliary Outputs 9 7 OPTIC 4SC OPTIC4 DC lL To
13. OPTIC 4 GC OPTIC 4 OPTIC 4SC OPTIC 4DC AE fig OPTIC 4 GC 41 OPTIC 4 OPTIC 4
14. 700 kPa HEH Exhaust SP Exhaust 1 8 PTFE 2 Evolution Workstation Configuration System Configuration Internal Diameter 0 25 mmLength 30 m Evolution Workstation Configuration Standby Parameters C column flow 20 mL min split flow 200 mL min Evolution Workstation column flow 20 mL min Page 11 2 Issue 1 0 OPTIC 4 9 split flow 200 mL min 10 20 mL min T Ed 11 1 ER 11 1
15. PUT EA Apo 2 0 9 AAN C ATAS method mth sequence seq 2 Evolution Workstation Methods Sequences Page 5 1 OPTIC 4 Issue 1 0 5 4 PC USB LAN OPTIC 4
16. 7 4 6 OPTIC 4 9 Evolution Workstation Configuration System configuration Auxiliary Outputs MEL Auxiliary Outputs Page 7 7 OPTIC 4 Issue 1 0 7 4 7 Expert Expert 9 Expert 9
17. e e e Evolution Workstation Clk 5 2 PC Evolution Workstation PC MS Windows XP Vista or Windows 7 512 MB RAM 20 MB OPTIC 4 USB LAN 5 3 Evolution Workstation Evolution Workstation CD ROM CD ROM CD ROM setup exe
18. Add Step Remove Step Inlet Temperature group ZA OA e Initial Inlet Temperature e Delay Time e Ramp Rate 1 9 e Hold Temperature 1 9 e Hold Time1 9 BEA Bi E xU CIECR OMENJA LANTET 9 4 Expert Column Flow group V7 Ai Carrier Control Mode Flow or Pressure Start Column Flow 1 9 Column Flow Time 1 9 End Column Flow 1 9 Split Flow group CX VU v HIS E e Initial Split Flow e Split Flow 1 9 e Split Flow Time 1 9 Auxiliary Flow group 3H ZI XG e Start Auxiliary Flow 1 9 e Auxiliary Gas Control Time 1 9 e End Auxiliary Flow Pressure 1 9 Expert 9
19. DMI 2 OPTIC 4 Page 7 2 OPTIC 4 Issue 1 0 e e 7 2 5 Expert OPTIC 4 iX 8 Expert
20. Start Column Flow Inlet Pressure GH 7 fo E IE 77 End Column Flow Inlet Pressure Ix fA V7 Ai B EF Sample Sweep Column Flow Inlet Pressure IRR BIO ZARB IE 77 LINEX TD DMI LVI Page 7 6 OPTIC 4 Issue 1 0 Desorption Column Flow Inlet Pressure QKR PFR SAM B L7 LINEX TD DMI d Desorption Time i zr FFE c 7 4 4 Vent Mode
21. 3 1 3 1 CPU A PC GC OPTIC ASC OPTIC 4DC OPTiC 4 3 1 OPTIC 4 3 2 OPTIC 4 2 RUN END RUN STANDBY RUN END RUN Waiting for Ready In Waiting for Run In A E wt Page 3 1 OPTIC 4 lssue 1 0 STANDBY Wait
22. GC GC off Page 4 1 OPTIC 4 Issue 1 0 4 1 2 1 OPTIC 4 2 GC2010 7890 6890 GC PERF 3 io 4 AHVAA ZVwOrHUI6 mAw ojsggguWreHOZZAuv vx amp o amp SauDiAAd34 X
23. Evolution Workstation Jus 12 2 7 CRYO OVERPOWER 25 Evolution Workstation 12 2 8 CRYO TEMP ABOVE MAX 400 C Evolution Workstation AE rv 12 2 9 INJ TEMP WARNING IX
24. No part of this manual may be reproduced or transmitted in any form or by any means electronic or mechanical including photocopying and recording for any purpose other than the purchaser s personal use without the written consent of the copyright holder ATAS GL International B V 2010 2011 All rights reserved ATAS GL International B V De Sleutel 9 5652 AS Eindhoven The Netherlands Telephone 31 0 40 254 95 31 Fax 31 0 40 254 97 79 E mail info atasgl com Web site www atasgl com Page i OPTIC 4 lssue 1 0 HE Document Number 2406 8014 Page ii OPTIC 4 lssue 1 0 CE Declaration of Conformity Manufacturer ATAS GL International B V De Sleutel 9 5652 AS Eindhoven The Netherlands Tel 31 0 40 254 95 31 Fax 31 0 40 254 97 79 www atasgl com info atasgl com Model OPTIC 4 Type of Equipment Multimode GC Inlet Application of Council Directives 73 23 EEC Directive as last amended by EC 93 68 EEC Low Voltage Directive amp 89 336 EEC Directive as last amended by EC 91 263 EEC amp 92 31 EEC EMC Directive Certification Body Dijkstra Advies Research amp EMC Consultancy B V Woerden The Netherlands Product Examined to EN 61010 1 1993 EN 61010 1 A2 1995 EN 61000 3 3 1995 A1 2001 EN 61000 3 2 2000 EN 6132
25. Run In 3 GC Run Out 4 Run 4 Run 3 GC OPTIC 4 AutoSampler Ready Ready 2 3 7 OPTIC 4 D Master Run OPTIC 4 OPTIC 4 Slave Mode OPTIC 4 HE OPTIC 4 Slave OPTIC 4 GC Ready In Ed 3 8 Run 3 Run 4 6 OPTIC 4 AutoSampler Ready 1 Ready 2 3 8 OPTIC 4 2 Slave OPTIC 4 Ready Out 1 GC OPTIC 4 Run In 4 GC aee L9 Page 3 9 OPTIC 4 lssue 1 0 4 REO
26. OPTIC 4 OPTIC 4 Page 9 3 OPTIC 4 lssue 1 0 WAITING FOR Instrument EQUILIBRATING RUNNING OPTIC amp GC METHODS Status RUN IN 1 Equilibration Time End Time i 1 uA i Cryotrap High Temperature i 1 Cry otrap Cryotrap Heat Ramp Rate Temperature Cryotrap Low Temperature i t 1 Parameters stable Ready Out Run In Out End Run Time min sec 9 4 9 8 OPTIC 4 ATAS GL www atasgl com OPTIC 4 Page 9 4 OPTIC 4 lssue 1 0 10 10 1 OPTIC 4
27. 12 OPTIC 4 GC OFF 11 1 OPTIC 4 GC 2 100 3 0 4 5 11
28. 4 5 f G300001 LD229 N Page 4 7 OPTIC 4 Issue 1 0 46
29. AN 1 2 5 10mm 3 4 6 5 OPTIC 4 PRET ALTAR BAIL W 150 200 kPa Page 4 9 OPTIC 4 Issue 1 0 Valve control OPTIC 4 Inlet OPTIC 4 1
30. Fixed Time SM Threshold SMLevell SM MP EE 0 4095 SMLevel 1 90 9 1 Vent Time X gt AFD Solvent Monitor Threshold 44 E fA Xf ES UIE d Solvent Monitor Level QRH E 2 Z7HXxf L f 7 4 5 Vent Flow 7f E Split Flow CX UJ v hte
31. COPE 5 45 E OPTIC 4 WME RAT yy Vent Mode 7375 Vent Mode Fixed Time Vent Mode SM Threshold SMLevel Vent Mode SM Threshold threshold 9 1 Vent Mode SMLevel OPTIC 4 9 1 A AR AR SMLevel Instrument WAITI
32. Excel Configuration Save Run Time Data ON OFF Page 6 2 OPTIC 4 lssue 1 0 7 7 1 OPTIC 4 PC Evolution Workstation Evolution Workstation lt 7 2 OPTIC 4 ROD 9 2 1 Split 2 Splitless 3 Hot Split 4 Hot Splitless 5 Large Volume Injection 6 LINEX TD Thermal Desorption 7 LINEX DMI Difficult Matrix Introduction 8 Standard TD Thermal Desorption 9 Expert full control of all parameters 7 2 1 Split OP
33. Evolution Workstation Methods 7 6 2 300 kPa Vl ipii pia PAI 700 kPa 2 E OPTIC 4 3 GC 4 6 2 4 STANDBY LED 5 PC
34. Repeat Apply Up Down File Save 8 2 Evolution Workstation Evolution Workstation Sequence f Execute OPTIC 4 Page 8 1 OPTIC 4 lssue 1 0 9 OPTIC 4 9 1 EHBL REA HEAR P
35. 1 OPTIC 4 2 OPTIC 4 OPTIC 4 GC OPTIC 4 AC 100 240V 50 60 Hz 150VA 450 VA 3 Page 1 1 OPTIC 4 Issue 1 0 4
36. Inlet Gas Lines FEA LH NV XK 3 Split Exhaust SP Septum Purge Exhaust Cooling Air In Cooling Air Out Page 4 2 OPTIC 4 lssue 1 0 OPTIC4 D e Auxiliary Gas In e Auxiliary Gas Out 4 1 4 OPTIC 4 UPnP T 300 700 kPa 99 995 700 kPa regen OPTIC 4 0 on f Carrier In Ex 4 1 Inlet Gas Lines Connection Carrier In Connection za 00 KPA MAX HONITOR Inlet Cooling Valve oit AUTOS
37. 9 9 4 De OFA AA CO Dah a elicit OC 9 IOPTIC 4 7 3 File New 2 5 Method ZSETAL C OK OPTIC 4 7 1 Cancel 7 1 OK 7 2
38. WET Exhaust SP Exhaust 4 1 8 OPTIC 4 50 C 180 C 500kPa 1 OPTIC 4 Air In
39. 350 C 100uL EPA 8270 5 1 Sintered Glass Liner with Taper p no A100133 600 C lt 50 uL recede 5 1 Page E 3 OPTIC 4 lssue 1 0 LINEX DMI Liners LINEX DMI Liner p no L100011 2 DMI 2406 1010 L100012 L100013
40. ELET End Time f amp SAFE GC ac GC Aloe 7 4 2 Initial Temperature JA Ramp Rate ZZ ZEE Page 7 5 OPTIC 4 Issue 1 0 Final Temperature RIEA Hold Time Fg Temperature Control QAAE ffl fal SO Time Solvent Cooling Effect
41. USB 3 9 LED LED e STANDBY Evolution Workstation Standby Parameters e READY GC Ready In READY RUN GC Run In RUN FAULT A E wt Page 3 7 OPTIC 4 Issue 1 0 3 10 PC Evolution Workstation P C OPTIC 4 OPTIC 4
42. OPTIC 4 Be USB COM 5 2 rfe CERCARE F PREMO RO AJAH seen m B LEMOVO 287864 7C DvD GD ROM IDE ATA ATAPI 3 POMCIA PAJA Portable Devices Ex Nokia 6500c Shl Driver USB Universal Serial Bus Hi M H PAPA BB PAA HA Pe e Ps P COM E d wo ORERDERORI EF TIVA He 5 2 Windows XP 7 Evolution Workstation Configuration External Communication X 5 3 USB Serial Port 6 USB OK Evolution Workstation OPTIC 4 Communication Parameters Communication Interface f USB Serial Port C LAK Cancel USB Serial Part LAN Fort IP Address mE 192 168 0 150 Baud Rate bad 5 3
43. ae 9 3 9 4 DE E 10 1 VI REI SAY 10 1 Oy ARP LLL PE 10 1 11 1 ae 11 1 ee 11 1 11 2 Page vi OPTIC 4 Issue 1 0 MS 11 4 12 RE dero E es SS 12 1 1 12 1 12 1 1 p b WM 12 1 12 1 2 S NIB EIE Sy PAARE 12 1 12 1 3 ki 12 12 1 4 12 2 12 1 5 7 Nc 12 2 12 2 12 2 1 ZO Be WA 12 2 12 2 2 12 2 12 2 3 NN NN 12 2 12 2 4 VE AG Yih EDS EBB A C 12 3 12 2 5 DIA ARP YT Tih EY 0 RE ee 12 3 12 2 6 VIL dA AA N 12 3 12 2 7 ASI EM MA AU EA 12 3 12 2 8 12 3 12 2 9 Tu WU 12 3 12 2 10 EI gp 12 4 12 2 11 TAOGE JOS m 12 4 12 2 12 I JIVZEE WADE e 12 4 13 13 1 A OPTIC 4 i A 1 B i TO aa E B 1 C Hi YR REG SREB ccc C 1 D kk D 1
44. End Time Transfer Time Page 7 4 OPTIC 4 Issue 1 0 01 E E239 EZ ESC Evolution Workstation
45. e Method New Optimization Sequence e OK 8 7 7 Expert Expert Method Convert to Export Method Page 7 10 OPTIC 4 lssue 1 0 8 Evolution Workstation 8 1 Evolution Workstation File New Sequence Insert
46. 5 1 LINEX DMI Needle Guide Straight p no L100012 L100011 5 1 DMI Sample Vial p no 2406 1010 DMI L100011 100 1 LINEX Metal Needle Guide p no L1000013 L100011 LINEX TD Liners Fritted Liner with Single Taper and Frit at 20 mm p no L100009 UNEX 25mm 5 1 Page E 4
47. IP A OPTIC 4 System Configuration General Column Parameters GC amp AS 10 Configuration LAN Communication OPTIC IP Address 1952 168 0 150 System Configuration Maximum Temperature enn BE ly Main Gas Channel Iv Auxiliary Gas Channel Pressure Units kPa le Keyboard Beeper Annuleren 5 6 Page 5 6 OPTIC 4 Issue 1 0 5 8 Auxiliary Outputs Configuration Auxiliary Outputs 5 7 Auxiliary Outputs uzila Outputs Mame e Output 1 Valve 1 B Output 2 valve m Output 4 valve Output 4 valve Page 5 7 OPTIC 4 Issue 1 0
48. OPTIC 4SC OPTIC 4DC 1 3 11 1 OPTIC 4 GC 1mm 350 C 60 C sec ZEE WEE RR AEE LURES CRISES OPTIC 4 3 11 2 OPTIC 4 3 3 Cryotrap Heater Cryotr
49. Page 5 3 OPTIC 4 Issue 1 0 5 4 LAN OPTIC 4 IP PRU AIL 192 168 0 150 PC LAN Windows 255 255 255 0 LAN IP 4 IP FRU AC 3 255 255 255 0 IP 1 5 4 1 OPTIC 4 PC USB 2 Evolution Workstation Configuration System Communication 3 IP Ed 5 4 OK
50. Evolution Workstation 12 2 2 INJ EARTH FAULT GC Evolution Workstation 12 2 3 Page 12 2 OPTIC 4 Issue 1 0 INJ OVERPOWER 25 Evolution Workstation
51. Dp Page 7 3 OPTIC 4 Issue 1 0 Evolution Workstation OPTIC Method Method Large Volume ief File Edit view Method Sequence Configuration Window Help 2 m X D cm ud amp Be E General Method Name Method2 Equilibration Time sec 5 en End Time sec 300 E Injector Temperature Initial Temperature C 35 Ramp Rate C sec 5 0 Final Temperature C 200 Hold Time sec 137 Temperature Control Keep Until End El Solvent Venting Vent Mode Threshold Vent Time sec 30 Solvent Monitor Level 10 Solvent Monitor Threshold 25 EJ Column Flow Injector Pressure Carrier Control Mode Flow Transfer Time sec 180 a Sample Sweep Column Flow ml mir 1 0 Transfer Column Flow ml min 1 0 Start Column Flow ml min 1 0 End Column Flow ml min 1 0 Sample Sweep Injector Pressure kF 50 0 Transfer Injector Pressure kPa 50 0 Start Injector Pressure kPa 50 0 End Injector Pressure kPal 50 0 E Split Flow Vent Flow ml min 50 Split Flow ml min 25 E Cryotrap Cryotrap Low Temperature C 30 Cryotrap Hold Time sec 0 Cryotrap High Temperature C 35 Cryotrap Heat Ramp Rate CAsecl 15 0 30 01 00 00 30 00 00 00 30 01 00 01 30 0200 0230 03 00 03
52. 6 Evolution Workstation Evolution Workstation Bd 6 1 7 PC OPTIC 4 7 Page 6 1 OPTIC 4 lssue 1 0 6 3 Evolution Workstation Evolution Workstation 6 1 Evolution Workstation OPTIC Status Viey File Edit View Method Sequence Configuration Window Ow amp B8 E Setpoint Injector Temperature 248 250 Cryo Temperature 334 335 Active Method Method1 Measured Vent Time Actual Solvent Monitor 0 Cryo Temperature 00 00 00 30 01 00 01 30 02 00 02 30 03 00 03 30 04 00 04 30 05 00 05 30 06 00 06 30 07 00 07 30 08 00 08 30 09 00 09 30
53. e FAULT 3 4 3 3 PC GC V v4 Carrier In Inlet Gas Lines Exhaust SP Exhaust Filter Aux In Aux Out OPTIC 4D OPTIC 4DC
54. 7 4 ed D pore 3 MUR IE OPTIC 4 5 7 4 1 Method Name 11 Evolution Workstation Method 1 Equilibration Time FEJ ERF OPTIC 4 Ready
55. 4 1 1 OPTIC 4 OPTIC 4 OPTIC 4 T OPTIC 4 GC
56. 4 4 PC OPTIC 4 Evolution Workstation PC PC USB LAN OPTIC 4 PC USB LAN LAN LAN PC LAN LAN OPTIC 4 Evolution Workstation Page 4 5 OPTIC 4 Issue 1 0 5 4 5 OPTIC 4
57. 4 5 1 dis 2 40 C OFF a O O OPTIC 4 45 2
58. 5 1 On Column Liner for 0 32 mm columns p no A100128 10mm 0 32mm CO KE LINEX 5 1 On Column Liner for 0 53 mm columns p no A100129 A100128 0 53mm CF LINEX 5 1 Fritted Liner with Single Taper and Frit on 20 mm p no L100009
59. OPTIC 4 Access Control Yes No Password String maximum 11 characters Maximum Temperature 100 600 C Communication Interface USB USB LAN Main EFC Yes No Auxiliary EFC No Yes No Cryotrap No Yes No Keyboard Beeper Enabled Enabled Disabled Reset Parameters No Yes No OPTIC 4 Page A 1 OPTIC 4 lssue 1 0 A 3 GC OPTIC Autosampler Ready Out Closed On Ready Closed On Ready Open On Ready OPTIC GC Interface OPTIC Master Master Slave Ready In Closed On Ready Closed On Ready Open On Ready Ready Out Disabled Closed Disabled Open Disabled Closed Ready In Disabled Disabled Ready Out Closed On Ready Closed On Ready Open On Ready A 4 Internal Column Diameter 0 1 mm Column Length 0 100 m Column Outlet Pressure 1 Atm Vacuum Carrier Gas He N H OPTIC 4 Page A 2 OPTIC 4 lssue 1 0 B B 1 6 min DIN poem me ee TTL Out
60. Evolution Workstation Such Evolution Workstation Configuration System Configuration General C Cryotrap ON OK 10 2 9 IOPTIC 4 Cryo Low Temperature 150 C 350 C 150 C O C Cryo Hold Time
61. 0 120 1 5 Cryo Heat Ramp Rate Cryo Low Temperature Cryo High Temperature C sec 1 60 C sec Cryo High Temperature 150 C 350 C 100 C 350 C Page 10 1 OPTIC 4 lssue 1 0 11 OPTIC 4
62. Evolution Workstation 50 C Page 12 3 OPTIC 4 Issue 1 0 12 2 10 CRYO TEMP WARNING i Evolution Workstation E 50 C He etd Cu 12 2 11 NJ PRES WARNING Evolution Workstation
63. OPTIC 4 5 OPTIC 4 Inlet TC Lec 6 External Solvent Monitor 7 Aim GC ae ace GC TC 8 OPTIC 4SC OPTIC4 DC 4 6 OPTIC 4 9 OPTIC 4 GC 1 3 4 1 3 OPTIC 4 Swagelok 1 8 1 16 0 OPTIC 4S Carrier Gas In
64. eo OPTIC 4 GC 1 2 3 4 5
65. PC USB LAN USB No IP Evolution Workstation USB 5 4 1 USB USB OPTIC 4 PC Windows USB 1 2 5 1 ey LDT ETH xxmuy PoP ee bor Pee A bOI USB Serial Port GOM16 6 CD cum ANS RS AUC
66. Page D 2 OPTIC 4 lssue 1 0 D 3 Large Volume Injection KEWA Instrument WAITING FOR Status EQUILIBRATING RUN IN VENTING RUNNING OPTIC amp GC METHODS 1 1 I End Time EE ed 1 i Equilibration Time VentTime Final Temperature lt gt lt P 1 I I I I I Ramp Rate Injector i i P Temperature Initial Temperature i i 10seconds l q Transfer CF End CF M Column Flow Sample Sweep CF i i lt gt Transfer Time Start CF Vent Flow Split Flow Split Flow Split I I rf i Parameters stable Ready Out Run In Run Out End Run Time min sec Page D 3 OPTIC 4 lssue 1 0 D 4 LINEX TD LINEX DMI Instrument WAITING FOR l Status EQUILIBRATING RUNIN VENTING RUNNING OPTIC amp GC METHODS 1 End Time 1 G l l I I I Equilibration Time Vent Time Final Temperature I I I 1 4 Iq D I I I I 1 Injector l f RAMD male I 1 I Temperature Initial Temperature Sample Sweep CF Column Flow K ND Start CF Transfer CF Vent Flow Split Flow Split Flow Split Splitless
67. Page 7 8 OPTIC 4 lssue 1 0 7 5 7 1 OPTICA wl V Standby conditions reached Yes VM E Standby State conditions nd of Method End Run 7 1 OPTIC 4 Page 7 9 OPTIC 4 Issue 1 0 File New Method method type 11 7 5 1 Evolution Workstation Method Execute OPTIC 4 OPTIC 4 Waiting for Run In Method Run RUN
68. 12 1 2 Bs SEES HERE S 12 1 3 OFF Page 12 1 OPTIC 4 Issue 1 0 12 1 4
69. 3 8 3 12 Auxiliary EFC Unit nne tnnt ennt 3 8 3 13 Master Slave ee 3 9 4 5 4 1 4 Tae VN 4 1 4 1 1 I UIGNES CRM 4 1 4 1 2 NS 4 2 4 1 3 4 2 4 1 4 SUA TP ABLE SEMEN 4 3 4 1 5 CSAP S A AjAjA AS SR 4 3 4 1 6 4 3 Page iv OPTIC 4 Issue 1 0 4 1 7 4 1 8 4 2 4 2 1 4 3 4 4 4 5 4 5 1 4 5 2 4 6 4 6 1 4 6 2 4 6 3 4 6 4 4 6 5 4 6 6 5 1 5 2 5 3 5 4 5 4 1 5 4 2 5 5 5 6 9 5 8 5 9 5 10 6 1 6 2 6 3 7 1 7 2 7 2 1 PREGO E7 Nro 7 A E orra erea ENE ENEN NA IEN 4 4 EVENE ES DYER DD i ceeeccccccccescccseccccescecseccecsceceececeeacecscecseacesseecseaceesaceestneeeeaeens 4 4 kk 4 5 INDI et O T fc oos re Dni 4 5 ON D0 SSA Sa 4 5 RE 4 5 as 4 6 4 6 4 6 IE FI OM 4 8 kk 4 8 4 8 IOUT i jj cc 4 9 FF AA TO it excursion seis wneud wosbe dude Vaiss abso scot wac ie otlis 4 9 PSF Y FA TT ABS OBE occ ccccccccccccccscescscescscescscesssccscsccscsecscsecacsesscsusaesesaceusaceesaceasanensas 4 9 kkk 4 10 SETNDUB UD EE SO OQ 5 1 od a
70. OPTIC 4 OPTIC 4 GC 2 4 OPTIC 4 GC GC MS Web www atasgl com Page 2 2 OPTIC 4 lssue 1 0 3 OPTIC 4
71. OPTIC 4 3 11 OPTIC 4 Mama GC Bx TEE LA
72. 12 2 4 NJ TEMP ABOVE MAX 6507 Evolution Workstation 12 2 5 CRYO TC FAULT 2 Evolution Workstation 12 2 6 Cryotrap Earth Fault CRYO EARTH FAULT
73. 500 kPa 150 kPa 12 1 5 INJ PRESSURE WARNING ea Xs 500 600 kPa 7 VAS 12 2 OPTIC 4 Evolution Workstation WET 12 2 1 NJ TC FAULT 2
74. E E 1 Page vil OPTIC 4 Issue 1 0 1 OPTIC 4 1 1 1 OPTIC 4 2 3 ATAS GL International B V 1 2 OPTIC 4 c gite
75. 1 B 2 9 D Ready Out TTL Out OPTIC 4 Page B 1 OPTIC 4 lssue 1 0 B 3 15 D QUA T DAMINEE 1 24 V 20 Max current 250 mA 2 COM 3 NO 4 NC Auxiliary Out 1 Relay output max 30 V 500 mA 5 COM 6 NO 7 NC Auxiliary Out 2 Relay output max 30 V 500 mA 8 COM 9 NO 10 NC Auxiliary Out 3 Relay output max 30 V 500 mA 11 COM 12 NO 13 NC Auxiliary Out 4 Relay output max 30 V 500 mA 15 GND Page B 2 OPTIC 4 c C 1 A100001 A100092 A100049 A100132 A100128 A100129 L100011 L100009 A100060 A100095 Fritted Liner frit 15 mm Liner for Split Injections single necked Liner for Splitless Injections Baffled Liner for Splitless Injections On column Liner for 0 32 mm Columns On column Liner
76. 20mm FELL A 5 1 Page E 2 OPTIC 4 lssue 1 0 KEA VD DFT LVI A type Packed Liner for Large Volume Injections p no A100060 350 C 100uL 5 1 8270 Packed Liner for Large Volume Injections p no A100095
77. 5 OPTIC 4 EFC 700 kPa Page 1 2 OPTIC 4 lssue 1 0 1 4 HIGH VOLTAGE Disconnect power cable before removing any units cover Warning Label 1 5 OPTIC 4SC OPTIC 4DC 1 2
78. Septum Purge Line Carrier Line Split Line mm m m Ce Main EFC Carrier In ZX4 6 E Exhaust yal Column 11 1 0 4 AT UYRIAY IANS tet 6 HAHA 7 R 11 1 Page 11 3 OPTIC 4 Issue 1 0 G300001 LD229 11 AN 11 4 OPTIC 4
79. i 1 Parameters stable Ready Out Run In Run Out End Run Time min sec Page D 4 OPTIC 4 D 5 Expert l Instrument EQUILIBRATING WAITING FOR VENTING RUNNING OPTIC amp GC METHODS Status RUN IN 1 i 1 1 1 1 End Time I I 1 1 1 ISO Time 2 IO Tomp 4 cures d lt P i ISO Time 4 librati lt p EK TN Lg EREMO cd ISO Time 1 ISO Temp 2 Ramp Rate 3 l lt 4 Ramp Rate 4 l l i l Ramp Rate 2 I ISO Temp 3 I 1 7 Injector i i l ISO Temp 1 ISO Time 3 Temperature Initial Temperature Ramp Rate 1 1 I I H I I 1 Dey NME i Sample Sweep CF l La Start CF 2 End CF 2 End CF 3 Column Flow Time 1 Time 2 S 1 1 So lt D lt gt i Start CF 1 ee Start CF 3 NN 1 I 1 l Start CF4 End CF 4 l 1 1 1 1 Time 3 1 1 1 1 lt I 1 I 1 1 1 Initial Split Flow _ Time 1 Split Flow 2 SPUL iw NR Split Split Flow 1 1 Time 2 Split Flow 3 Time 4 1 1 Split Flow 1 lt I I I 1 1 1 1 I Start AF AP 2 End AF AP 2 ARABS 1 1 1 n Time 1 Time 2 Auxiliary Flow Start AF AP 1 l lt j ZuE Time 4 I I Pressure End AF AP 1 Start AF AP 3 Pi E 4 i i i Time 3 End AF AP 4 1 1 1 qA Start AF AP 4 1 1 1 1 1 1 1 1 1 Open Auxi
80. Ed 9 2 Instrument Status EQUILIBRATING CRUNN NENTING RUNNING OPTIC amp GC METHODS End Time Equilibration Time Vent Time Final Temperature Injector Temperature Initial Temperature u Ex m pet I 1 po 4 4 Parameters stable Ready Out Run In Run Out End Run Time min sec Figure 9 2 Te LC In AIR 93 OPTIC 4 Temperature Control Floating C LC Hold Time End Time 9 2 ELOI OPTIC 4 Page 9 2 OPTIC 4 Issue 1
81. e e END RUN STANDBY e OPTIC 4 LED STANDBY LED 3 8 OPTIC 4 OPTIC 4 2 RUN END RUN Waiting for Ready In Waiting for Run In STANDBY Waiting for Ready In Waiting for Run In END RUN STANDBY RUN STANDBY 15
82. Page 4 8 OPTIC 4 Issue 1 0 4 6 3 Gc 1 2 4 6 2 AN 3 G300001 LD229 4 6 4
83. Air In To Inlet Cit PTFE Ad Inlet TC Inlet Heater C Valve GC TC GC OPTIC 4 PC USB LAN Configuration 5 aee L9 Page 3 3 OPTIC 4 lssue 1 0 Inlet Gas Connections Split Line Filter Connections Aux Gas Connections Carrier Inlet Gas Connection Cooling Valve YO P GC and Autosampler Aux Equipment Interface Connections Connections GC Oven TC USB and LAN Ports Connection Inlet TC and Power Connections Cryotrap TC and Power Connections Mains Power Inlet Functional Earth T
84. DMI OPTIC 4 HEAL Windows XP Vista Windows 7 OPTIC 4 5 OPTIC 4S OPTIC 4D l4 jE OPTIC 4SC OPTIC 4DC OPTIC 4PTV OPTIC 4S 2 1 OPTIC 4
85. IP OPTIC 4 15 System Configuration General Column Parameters GC amp 45 1 0 Configuration LAM Communication OPTIC IP Address System Configuration Maximum Temperature 200 C ly Main Gas Channel amp usiliary Gas Channel Pressure Units kPa Crotrap iw Keubnard Beeper Annuleren 5 4 4 OPTIC 4 UsB LAN 8 Ts 5 Evolution Workstation Configuration External Communication TAN 5 3 OK Evolution Workstation OPTIC 4 LAN Page 5 4 OPTIC 4 Issue 1 0 5 5 General Configuration Parameters Evolution Workstation Configuration 5
86. OPTIC 4 Inlet Exhaust lt Split Line Filter Solvent Sensor Auxiliary EFC Aux Aux Flow Column Flow In Out Flow LL 3 4 OPTIC 4 3 6 YEA OPTIC 4 GC GC 4 3 5 C see L9 Page 3 5 OPTIC 4 lssue 1 0 O0 ten UN RES ze 0 Pd 3 5 Page 3 6 OPTIC 4 Issue 1 0 3 7 OPTIC 4 OPTIC 4 OPTIC 4 PC Evolution Workstation OPTIC 4 2
87. OR GC OPTIC 4 GC GC CC Page 2 1 OPTIC 4 lssue 1 0 2 3 OPTIC 4 BE 7 OPTIC 4
88. SORRIR 2 eli 25 kPa 12 2 12 AUX FLOW WARNING ete a maa Evolution Workstation 2 Po M MAN X42 mL min ITHEELZRVIER iene Page 12 4 OPTIC 4 lssue 1 0 13 fi e KS 34cm x 15 cm x 34 cm hx w x d e HX 8 4 kg OPTIC ADC 18 40 C 40 70 e 100 240 VAC 50 60 Hz e 150 VA e 450 VA e The European Low Voltage Directive The Electromagnetic Compatibility Directive e RoHS Compliant EA e Full electronic pressure flow control e 600 C GC 35 C e AH 35 C HUE
89. Equilibrating Evolution Workstation 7 5 2 Evolution Workstation JE ir 73 Initialise Method Waiting for Ready In Equilibrating Waiting for Run In Method Standby OPTIC 4 Running OPTIC Method Running OPTIC amp GC Methods Method End Run END RUN Initialise Method 7 6 Evolution Workstation ECR IMB CU CAT YT EZTAIT ALEC
90. 3 4mm 5 1 Liner for Splitless Injections p no A100049 1 0mm 1 gb SPME 5 1 Page E 1 OPTIC 4 lssue 1 0 Baffled Splitless Liner p no A100132 1 0mm 1 pl
91. international OPTIC 4 mutinodec OPTIC 4 www atasgl com OPTIC 4 lssue 1 0 ATAS GL International B V ATAS GL International B V 2 ATAS GL International B V makes no representations or warranties with respect to the contents or use of this manual and specifically disclaims any express or implied warranties of merchantability or fitness for any particular purpose Further ATAS GL International B V reserves the right to revise this manual and to make changes to its content at any time without obligation to notify any person or entity of such revisions or changes The instruments are similarly subject to change without notice
92. ZAR TA AIF EEC LO da RI Ie REC 25 2caxiEUX s XHICOV Cu 9 21 Cooling Valve Mode tH LZ ORE No No 7 4 3 Carrier Control Mode 4 FAX Bl BIO FE Pressure JE Flow Transfer Time JEX EAT Transfer Column Flow Inlet Pressure f amp EE 7 AAIE
93. 0 Instrument gt _ WAITING FOR Status EQUILIBRATING RUN IN VENTING RUNNING OPTIC amp GC METHODS 1 1 End Time 1 1 I 1 Equilibration Time Vent Time Final Temperature lt __ _ re lt P 1 l 1 1 Ramp Rate amp Injector i p CENE Temperature Initial Temperature l Floating Final Temperature i 1 1 1 1 i I i 1 1 1 i Parameters stable Ready Out Run In Run Out End Run Time min sec 9 3 9 4 Expert OPTIC 4 Expert 9 4 OPTIC 4 OFF DA Hold GC GC 9 5 OPTIC 4
94. 11 2 11 3 H SPLITLESS vecccccccccccccessssccesssscecessssscessesssecessssuecesstauecesssasecessanees 7 1 LARGE VOLUME INJECTION kk 7 2 LINEX TD LINEX DMI i 7 2 EXPERT 7 3 7 3 ITI 7 5 AY YVRINF SEP PES 1745 vee cccccccccccccccccceccscecccecscsececcsecssecssscssssevscsesesauavscuasasasevscs 7 5 dps cw 27 n E 7 5 7 6 7 7 cocccccccccccccsccccsececsseccesececseeccsececsssessesersseseasessrsusesaseseusueesesesens 7 7 NT NNNM A O 7 7 EXPERT RD 7 8 7 9 EVOLUTION WORKSTATION kk 7 10 EVOLUTION WORKSTATION kb 7 10 7 10 Expert ki 7 10 VA DLE E A aii 8 1 Evolution Workstation eese nnne nnne 8 1 Evolution Workstation eese 8 1 OPTIC 4 9 1 VASE RI ERN 9 1 Eee 9 2 SE Ao 9 2 Expert A 77 F COA OME FIM ee 9 3 ak 9 3 9 3
95. 2 ve i 1 Evolution Workstation Configuration Standby e Split valve state Split e Injector temperature 600 C e Column flow 0 5 mL min e Split flow 200 mL min 1 2 ST Page 11 1 OPTIC 4 Issue 1 0 EAD OASAREOIZIL 1 2 OPTIC 4
96. 6 Standby Parameters Configuration Standby Parameters General X 5 5 Standby Timeout A OPTIC 4 Standby Timeout OPTIC 4 SHEER OL FI IFD ETAL E OUI figo bm CRE SPMD EME BERIE NI EPIC RYE 0 0 mis RET SEE F ELE E CREE INA EIR I LEBDYVES Standby Parameters General Advanced Injector Parameters Temperature 35 JE Iw InjectorTemperature Control Injector Cooling Gas Control Parameters Column Flow Septum Purge Flow Ausihary Flow 1 0 ml min ml min ml min Split Flow Split Valve State ml min Splitless Cryotrap Parameters Temperature B5 Standby Timeout Timeout 0 00 ms Annuleren Page 5 5 OPTIC 4 Issue 1 0 5 7 System Configuration Parameters Configuration System Configuration General X 5 6 C
97. RBR 50 C LN 180 C e 1 0 60 C sec 9 e Merlin MicroSeal e lt 500 kPa e 2 HAIL e JEAUY Y 7 700 kPa e 5 500 mL min He 2 100 mL min He OPTIC 4D OPTIC 4DC e HE 1 full scale 0 2 full scale e Ke 1 full scale 10 full scale 1 0 mL min 0 2 of full scale e 9 e He N H 700 kPa e e Page 13 1 OPTIC 4 LAN USB 4 30V 500 mA max DC24 V 250 mA max GC Evolution Wo
98. SO TALIA TREAT ESL io 77 cL ura nd GERD iit alld D BOO LES CES 5 1 Windows XP 3 Evolution Workstation CD USB Serial Drivers PET Ec 4 Windows USB Page 5 2 OPTIC 4 lssue 1 0 5 Evolution Workstation CD USB Serial Drivers Ere 6 ee
99. TD LINEX DMI OPTIC 4 LINEX TD LINEX DMI Difficult Matrix Introduction 2 DMI 30 uL GC GC MS
100. jp GG Gj Su sc 5 1 PCR cl i 5 1 Evolution Workstation 5 1 se 5 2 USB lt 5 2 LAN 5 4 General Configuration Parameters Lesser nnns 5 5 Standby Parameters i cceccccsecenscessscessecsnsecssssessessnsessssessesensesereesesesens 5 5 System Configuration Parameters 5 6 Auxiliary Outputs o E 5 7 External Communication kk 5 8 Access Control ciccccccccccccccccccesscsecsccccccessesccsceccccesessetascececseseesctaseeeeeeesns 5 8 Dc 6 1 dq VPE SENE 6 1 ee 6 1 Evolution Workstation ee 6 2 NT Gp RA 7 1 nuo 74 Ge 7 1 SPLIT EMEN 7 1 Page v OPTIC 4 Issue 1 0 7 2 2 7 2 3 7 2 4 7 2 5 7 3 7 4 7 4 1 7 4 2 7 4 3 7 4 4 7 4 5 7 4 6 7 4 7 7 5 7 5 1 7 5 2 7 6 7 7 8 1 8 2 9 1 9 2 9 3 9 4 9 5 9 6 9 7 9 8 10 10 1 10 2 11 11 1
101. 10 00 Time min sec GC amp OPTIC methods are running No errors Save run time data OFF Method run time 01 21 C run time 01 12 JE be uu Eo L m L prc nu ON OFF 6 1 Evolution Workstation Save Run Time Data OPTIC 4 OPTIC Method Run Time GC GC Run Time 3x
102. 30 04 00 04 30 0500 Time OPTIC is standing by No errors Save run time data OFF Method runtime 00 00 GCruntime 00 00 7 2 OPTIC 4 LVI Method gt Execute 25 OPTIC 4 Method gt Execute 11 Evolution Workstation Method Final Inlet Temperature Initial Inlet Temperature
103. 4 1 2 OPTIC 4 To Inet PTFE TE 4 2 ELT a 4 2 OPTIC 4 Page 4 4 OPTIC 4 lssue 1 0 4 2 4 2 1 1 4 2 2 OPTIC 4PTV Ex
104. 5 9 External Communication OPTIC 4 Configuration External Communication 5 6 USB LAN Evolution Workstation OPTIC 4 5 10 Access Control Configuration Access Control EE Evolution 2 User Manager 5 7 software Access Control Software Access Control Change Software Password Level Password Page 5 8 OPTIC 4 lssue 1 0 6 6 1 OPTIC 4 Evolution Workstation 5 6
105. 6 1997 A1 1998 A2 2001 Class B EN 55022 1998 A1 2000 Class B Certificates Certificate of Conformity to Low Voltage Directive 73 23 EEC No Certificate of Conformity to EMC Directive 89 336 EEC No ATAS GL International B V hereby declares under our sole responsibility that our OPTIC 4 Multimode GC Inlet when installed in accordance with installation specifications is in conformity with the above Directives and Standards NV obs N Gribov Product Development Manager Date March 31 2011 Declaration of Conformity Page iii OPTIC 4 lssue 1 0 1 d MM RC E 1 1 1 1 E E E E EE S E 1 1 1 2 1 1 1 3 1 3 TV 1 3 15 1 3 2 DOO D 2 1 2 1 Po eV 2 1 2 2 pe nme M 9002 2 1 2 3 E CD cl a E NE E ee 2 2 2 4 aa 2 2 3 SUM 3 1 3 1 er 3 1 3 3 LED 6 3 2 3 4 hh Lia v 3 3 3 5 Oaea Ene 3 5 3 6 EX ee 3 5 3 7 OPTIC 4 3 7 ee 3 7 3 9 LED i 3 7 3 10 PC Dro OFFAL DO OpjjjbADpAjjjj A 3 8 311 FIA AZ UZ Va fi 3 8 3 11 1 3 8 3 11 2
106. AMPLER GE External Solvent dem Monitor Connection 4 1 OPTIC 4 gt 4 1 5 OPTIC 4 EFC Inlet Gas Lines X 4 1 EFC 0 3 431 6 OPTIC 4PTV Ext Solvent Monitor B 4 1 Page 4 3 OPTIC 4 Issue 1 0 441 7 Exhaust SP Exhaust
107. NG FOR Status EQUILIBRATING RUN IN VENTING RUNNING OPTIC amp GC METHODS 1 1 Equilibration Time 1 Vent Time i End Time 1 SM Zero Level 1 N Actual Solvent Monitor A 1 Split Flow Transfer Time 1 1 z Split Flow Save Split Flow E Split 1 1 1 Parameters stable Ready Out Run In Run Out End Run Time min sec 9 1 OPTIC 4 Page 9 1 OPTIC 4 Issue 1 0 9 2 TREO RAE OT OPTIC 4 Solvent Cooling Effect Yes
108. OPTIC 4 Split Line Filter Assembly OPTIC 4 Injector Assembly Base OPTIC 4 Main EFC Channel OPTIC 4 Aux EFC Channel Issue 1 0 OO UU UU UU Ul Ul Ul 25 20 10 10 10 10 10 U Uu Uu e PRP RP RPP PW Page C 1 OPTIC 4 C 4 2406 4034 Interface Cable for PAL Autosampler 2406 4035 Interface Cable for Shimadzu GC2010 2406 4036 Interface Cable for Agilent 7890 2406 4037 Interface Cable for Trace GC C 5 2406 4150 2406 4151 2406 4152 2406 4153 2406 4154 2406 4155 2406 4156 2406 4157 2406 4158 2406 4159 2406 4160 Upgrade kit OPTIC 4 S to OPTIC 4 D Upgrade kit OPTIC 4 S to OPTIC 4 SC D Upgrade kit OPTIC 4 D to OPTIC 4 DC D Upgrade kit OPTIC 4 S to OPTIC 4 DC D Upgrade kit OPTIC 4 S to OPTIC 4 SC CO2 Upgrade kit OPTIC 4 D to OPTIC 4 DC CO2 Upgrade kit OPTIC 4 S to OPTIC 4 DC CO2 Injector Heat Exchanger Cooling Option LN2 Tee Joint for Injector Backflush OPTIC 4 Injector Cooling Kit Direct LN2 OPTIC 4 Injector Cooling Kit CO2 C 6 2406 4124 2406 4125 2406 4126 OPTIC 4 Installation Kit for Shimadzu 2010 GC OPTIC 4 Installation Kit for Agilent 7890 GC OPTIC 4 Installation Kit for Thermo GC Issue 1 0 PRP PRP RP RP R
109. P RP RPP PR Page C 2 OPTIC 4 lssue 1 0 D D 1 Split i Instrument EQUILIBRATING WAITING FOR RUNNING OPTIC amp GC METHODS Status RUN IN Equilibration Time End Time lt gt lt S Final Temperature 7 i Injector Ramp Rate Temperature Initial Temperature i i i Transfer Column l 1 Flow l Column Flow 1 1 1 1 Transfer Time l lt t ___ ee Start CF 1 1 Split Flow Split Flow Save Split Flow Split Splitless l t 1 Parameters stable Ready Out Run In Out End Run Time min sec Page D 1 OPTIC 4 lssue 1 0 D 2 Splitless WAITING FOR Instrument E EQUILIBRATING RUN IN Status RUNNING OPTIC amp GC METHODS End Time m s Final Temperature Equilibration Time Ramp Rate Temperature Initial Temperature Transfer Column Flow V4 End CF 2 Transfer Time sa p Start CF I Split Flow I I l I l Injector 1 I l l Column Flow Split Split Flow Splitless f Parameters stable Ready Out Run In Out End Run Time min sec
110. TIC 4 Hot split Split 50 C e e e 7 2 2 Splitless OPTIC 4 Hot Splitless Splitless
111. ap TC Cryotrap C Valve 3 12 Auxiliary EFC Unit OPTIC 4D OPTIC 4DC Aux In Aux Out alot WA Page 3 8 OPTIC 4 Issue 1 0 3 13 Master Slave OPTIC 4 GC OPTIC 4 Evolution Workstation Configuration Master OPTIC 4 Master Mode OPTIC 4 233 OPTIC 4 Mater OPTIC 4 GC Ready In 1 X 3 7 Ready In OPTIC 4 Ready Out 2
112. erminal 3 3 OPTIC 4 DC A E wt Page 3 4 OPTIC 4 Issue 1 0 Configuration DO B OPTIC 4SC OPTIC 4 DC Cryotrap C Valve Ee Cryotrap TC Cryotrap Heater 3 5 3 4 C OPTIC 4 OPTIC 4D OPTIC 4DC Main EFC Septum Purge Line 6 Fen j Carrier In gt Septum Purge ro Exhaust lt Carrier Line
113. for 0 53 mm Columns DMI Liner with Taper Fritted Liner 20 mm with Single Taper A Type Packed Liner for Large Volume Injections 8270 Packed Liner for Large Volume Injections C 2 2406 1002 3007 11605 2406 1003 2406 1004 2406 1005 2406 1006 2406 1007 OPTIC Low Bleed White Septum 11 mm pk 25 High Resistance Silicon O Ring OPTIC Graphite Ferrule for 0 53 mm ID Column pk 10 OPTIC Graphite Ferrule for 0 1 0 32 mm ID Column pk 10 OPTIC Injector Metal Ferrule Column ID 0 25mm pk 10 OPTIC Injector Metal Ferrule Column ID 0 32mm pk 10 OPTIC Injector Metal Ferrule Column ID 0 53mm pk 10 C 3 2406 2047 2406 2048 2406 2049 2406 2010 2406 2012 2406 2013 2406 2015 2406 2016 2406 4020 2406 2250 2406 2051 2406 2056 2406 2257 2406 2269 2406 2270 2406 4025 2406 4005 2406 4016 2406 4017 OPTIC Stainless Steel Injector Bottom Nut pk 5 OPTIC Key Injector Bottom Nut OPTIC Injector Bottom Nut for Metal Ferrule pk 5 OPTIC 4 Injector Septum Nut Standard OPTIC 4 Injector Top Boss Clamp Nut OPTIC 4 Injector Clamp Nut Insulator OPTIC 4 Injector Septum Nut Shimadzu type OPTIC 4 Injector Septum Nut Insert Shimadzu type OPTIC 4 Solvent Monitor Assembly OPTIC 4 Injector Cooling Valve OPTIC 4 EFC Fitting 1 8 tubing Shimadzu aluminum packing type G pk 10 Fuse Slow Blow 230V 6 3A pk 5 OPTIC Injector Bottom Insulation Cap Agilent 7890 GC OPTIC GC Oven Thermocouple
114. ing for Ready In Waiting for Run In END RUN STANDBY PC Evolution Workstation 3 2 RUN END RUN STANDBY STANDBY READY RUN OPTIC 4 Multimode GC Inlet 3 2 OPTIC 4 3 3 LED LED e STANDBY Evolution Workstation lt Standby Parameters e READY GC Ready In e READY A E wt Page 3 2 OPTIC 4 Issue 1 0 e RUN GC Run In e RUN
115. liary Outputs Time 1 d 7 P a ips gt s m Closed Time 2 l I L H 8e f l Time 3 i qp E l Time 4 etc 1 dT YS i l 1 Parameters stable Ready Out Run In Run Out End Run Time min sec Issue 1 0 Page D 5 OPTIC 4 lssue 1 0 E DALTE A100060 A100095 s f A100001S Fritted Liner Frit at 15 mm p no A100001 25mm FA 5 1 Single Necked Liner for Split Injections p no A100092
116. rkstation 2 150 C 350 C 1 0 60 C sec 150 200 kPa GC Issue 1 0 Page 13 2 OPTIC 4 lssue 1 0 A OPTIC 4 A 1 Timeout 30 00 min sec 0 500 min Inlet Temperature Control Yes Yes No Inlet Temperature 35 C 180 600 C Standby Column Flow 1 0 mL min 0 20 0 mL min Standby Split Valve State Split Split Splitless Standby Split Flow 50 0 mL min 0 0 450 mL min Inlet Cooling OFF ON OFF Standby Septum Purge Flow 5 0 0 0 10 0 mL min Standby Auxiliary Flow OPTIC 4D and OPTIC 4DC 10 0 0 0 100 mL min Cryotrap Temperature Control No Yes No Cryotrap Temperature 35 C 150 350 C Auxiliary Output 1 Open Open Closed Auxiliary Output 2 Open Open Closed Auxiliary Output 3 Open Open Closed Auxiliary Output 4 Open Open Closed A 2
117. t Solvent Monitor 3 Inlet TC cae ee 4 GC GC TC N GC 4 3 OPTIC 4 GC D mini DIN BI OPTIC 4 GC
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