タンデム・マイクロリアクター MODEL Rx
Contents
1.2. Fig 4 41 A Fig 4 41 B A Ethylene Propylene Propylene B Ethylene HzO 1 2 1 4 1 6 1 8 2 0 2 2 2 4 2 6 2 6 min Fig 4 41 Rx ZMS 5 Ultra ALLOY 1 30m 0 25mm 0 25um GC 40 C Ver 4 07 4 7 4 7 1
3. A 2 Ver 4 07 2 0 NIS IS 50 C
4. GC 10 kPa 1 5 psi 4 32 Ver 4 0 4 8 Rx Rx Rx 10 mm 40 mm 10 20 mm
5. 2nd A Tools Analytical Modes Stepwise Temp Analysis Stepwise Temp Analysis B Fig 4 21 D 2 A B D 4 D 3 40 900 C 0 1 999 9 min OO kx 3050TR Contro I I File View Tools Dekuq Help C 40 900 C tepwi START STOP Monitor 1st u Reactor 1st InterfaCe 200 8 Max 0 sC Not Ready rp 2nd wR nd MD D nd u Reactor nd Interface carrierGas Step Rate Cmin Temp C Timek Max 300 C 1st 200 10 00 _1st WI 200 2nd 300 10 00 4 REactaTt Gas TON 1 1st Interface 300 4th 500 10 00 200 lt C Actual E 00 Ra Ge 2nd Reactor F a Settings He 2nd Interface 300 we ISamplinq a Sampli Ini
6. LIST 6 1 1 1 1 1 1 1 8 1 1 1 1 N 1 PY1 1035 1 1 1 2 P 6W 2 PY1 2017 20 1 1 3 Rx SUS A 1 Rx1 3540 1 MI 114 6 mm 1 PY1 7911 5 1 1 5 RxITF A 1 Rx1 3534 1 i 1 Rx1 1278 3 1716 1 1 7 1 PY1 3630 1 1 Rx1 1040 1 1 3 1 Rx1 2023 1 1 4 Rx
7. 7 Ver 4 0
8. Fig 4 42 Fig 4 42 1 4 7 2 He Fig 4 43 2 man oN FROMTIER LAB 7 Fig 4 43 Ver 4 0 4 7 3 LF 1
9. Table 4 1 Ver 4 0 Table 4 1 Hz He lsothermal lemp Analysis Linear Temp Real Time Monitoring Linear Temp Selected Zone Analysis SteDwise Temp Real Time Monitoring Stepwise Temp Selected Zone Analysis 4 6 2 X GC MS 4 6 2 1
10. 5 500 kPa 600 kPa ee 5 cm 10 2L 50 C ET TE 305C
11. lt OO bp 4 4 4 2 2 B C1 C2 ClearY 4 4 2 3 1 2 Maintenance
12. 3 3 2 Rx A 3 8 2 3 6 Ver 4 0 3 3 2 2 2 1 Rx ITF A 2 Rx ITF B Fig 3 10 A Rx ITF A 2 Fig 3 10 B A RxITF A B Rx ITF A NN ON Rx ITF A Rx ITF A 1 13 mm 4 Fig 3 10 1 2 RxITF A 2 9 Rx ITF A Rx ITF A 2 Fig
13. 6 4 1 EGA GC GC He 1 3 6 Fig 6 2a P N PY1 2017 6 4 Ver 4 0 e ITF Fig9 6 2b P N PY1 7911 PY1 7921
14. Real Time Monitoring C ON 1 1 D 1 ON 2 D 2 D 3 D 4 2 Rate 0 C 8 F 2 E 0 C 0 C START 4 8 Ver 4 0 GC 2
15. LE 2 GC OFF 1009C 3 GC 3 1 3 1 1 EE RMD 800 CESMRND TI a AC 100 120 V 8A 2 m a OS Windows 8 7 Vista XP GC GC MS PC USB 1 CD ROM RE 1 5 m 178 3 mm Me 400 600 kPa 5 14 L min
16. 190 C 0 25 mm 1 um 1 um 0 Fig 6 1 2 2 HO 0 1 2 min Fig 6 1 6 3 Ver 4 07 6 4
17. 8 F D ON 2 START GC 2 Fig 4 27 ESC Star PC ENTER GC 1 1 Step Fig 4 28 4 19 Ver 4 0 3 Step C 2 Step C 1 Step C GC Stenwise Temp Real Time Monitoring Ready for injection START EN
18. Fig 1 3 1 4 4 6 4 6 1 2 Fig 4 40 GC 10 cm Fig 4 40 GC 400C 200 15
19. TP YR EE ITF Manual Auto 1009C No 90 1009C ITF 6 2 Ver 4 0 6 3 SE
20. COM3 UsB ee _ 3 AN SS EAT 9 i 7 Ey p y BM 0 i OM LPT ECP UPT1 msec gy USB serial Port COM3 4 COM3 GOM1 8 GOMM2 Rs COM23 Ro 9 CoM26 CON2G
21. Fig 4 30 ESC Star PC ENTER C F ON GC GGC 1 1 Step Fig 4 31 Ver 4 0 GC 3 Step C 2 Step C 1 Step C Zone A Zone B Zone d 3 6 GC GC GC Fig 4 30
22. 30 m 0 25 mm 2 0 um UA1 30M 2 0F e 1 mL s 10 uL 5 1 2 GC GC MS GC 200 C 30 5 1 3 GC MS He 50mL min 4 5 He 3 He GC MS START 0 2uL
23. 40 gt 400 C 1 C 2 40 900 C 1 C EN a lt 3 mm 4 mm 78 mm 500 kPa 5 min 40 400 C 1 C DE PD AC100 120V 50 60 Hz 800W AC200 240V 50 60 Hz 800W 4 Aux gas 1 3 Stop 100 mlmin 1MPa PC AT USB 1 CD Microsoft Windows 8 7 Vista XP 512 MB lsothermal Temp Analysis Linear Temp Analysis Stepwise Temp Analysis Real Time Monitoring Selected Zone Analysis 2 1 Ver 4 07 3 GC 1 1
24. C15 2nd A Tools Analytical Modes Linear Temp Selected Zone Analysis Linear Temp Selected Zone Analysis B Fig 4 13 D 2 A B D 3 _5 D 5 0 1 999 9 min C 40 900 C START STOP Monitor 1st Interface 200 s6 Not Ready p 2ndu R 2nd interface NN D1 2nd u Reactor 2nd Interface se Step Rate GC min Temp G Timefin Max 300 C D 4 _1st 200 3 00 s300 1 2009C ET sol oo aml ol 50 1st u Reactor 200 se Actual 1st Reactor 200 C cactant Gas 1st Interface 300 2nd Reactor 200 2nd Interface 300 C
25. Fig 3 7 B Fig 3 7 3 5 Ver 4 07 Rx ITF A 6 mm 12 mm Fig 3 8 12 mm Fig 3 8 RxITF A Rx ITF A Rx ITF A Fig 3 9 A Rx ITF A 6 mm Fig 3 9 B A B 8 mm 6 mm Rx ITF mw 2 Fig 3 9 Rx ITF A Rx A Rx A 20
26. 3 N 1 5 m 1 78 3 mm 400 600 kPa x x 120 x 310 x 310 mm GC 2 m x x 160 x 280 x 150 mm 3 1 Ver 4 07 3 2 2 GC 3 2 1 2 2 Rx ITF A B Fig 3 1 3 2 1 1 2 4
27. START GC MS Fig 5 1 MS 4 6 2 5 1 Ver 4 0 2 2 0 2 uL 1 300 C ITF 200 C 2 300 C ITF 200 C He 50 ml min EN 30 GS 0 GC MS 2009C 1 50 He 50 mL min GC 40 5 min 1 ml min 30 m 0 25 mm 2 0 um UA1 30M 2 0F GC MS ITF 250 C MS 230 C MS
28. 40 C 30 109C min 2 SE 00 6 1 Ver 4 07 6 2 OFF ON N a Re ER TN ITF POWER SENSOR
29. 2 d Fig 4 44 LF SF LF SF LF SF 1st LF SF SF NN LF Fig 4 44 Rx 1
30. a 1 1 Fig 1 1 1 2 1 2 3 Fig 1 2 Ver 4 0 CGC ii SE ee ESI USB a mp a a PC He He
31. 3 2 2 2 2 GC GC 2 GC ITF GC ITF GC 2 2 4 Ver 4 0 3 3 1 2 3 3 1 1 3 3 1 1 1 4 Fig 3 6 Fig 3 6 4 3 Rx SUS A Fig 3 7 A Rx SUS A
32. 4 6 2 5 3 Ver 4 07 XX 0 2 uL 1 300 C ITF 200 C 2 500 C ITF 200 C He 50 ml min GC MS 2009C 1750 He 50 mL min GC 40 5 min 1 ml min 30 m 0 25 mm 2 0 um UA1 30M 2 0F GC MS ITF 250 C MS 230 C MS 10 200 m z 5 sec He 50 ml min GC He 50 ml min 17100 40 Propylene HzO 22 Ethylene 2 3 4 5 min Fig 5 2 ZMS 5 5 4 Ver 4 0
33. Fig 4 11 ESC Star PC ENTER GC 2 1 Step Fig 4 12 Post Heat C 3 Step C 2 Step C 1 Step C Stepwise Temp Real Time Monitoring Ready for injection Cancel GC START END Fig 4 11 Ready for injection START GC Fig 4 12 Linear Temp Real Time Monitoring Ver 4 0 4 3 2 2 Linear Temp Selected Zone Analysis
34. PC Fig 3 14 USB e oe O RS 232C 1 SENSOR Fig 3 14 PC 3 9 Ver 4 0 3 5 3 1 2 IN OUT Fig 3 15 2rd INTRRFACE Fig 3 15 3 5 4 GC Fig 3 16 3 5 5 AS 1020E RS 232C AS 1020E RS 232C RS 232C Fig 3 17 GC
35. MS GC MS ITF ITF OFF ON ITF GETTER A ITF 1ml GC
36. RN NA RN 5 4 A 8 6 4 6 1 6 1 7 2 5 EE 6 1 6 2 SR RS ER NN ES SN Sp 6 2 6 3 OC RN NR 6 3 6 4 Se RS SR NR SN RR 6 4 Appendix A RR RSE Appendix A 1 A 9 Ver 4 07 1 RR GC MS GC MS 1 2 2 1 2 GC
37. START Fig 4 23 Stepwise Temp Real Time Monitoring Ver 4 0 4 3 4 lsothermal Temp Analysis 1st 1sf A Tools Analytical Modes lsothermal Tempt Analysis lsothermal Temp Analysis B Fig 4 24 I ISothermal Temp Analysis START STOP Monitor D 40 9009C rk 1SK u Reactor 1st Interface 200 8 030 min Max 300s6 NN Run Actual 1strReactor 200 sC 1st Interface 300 rk 2ndN Reactor 2nd Interface 0 Max 300G 2nd Reactor 200 lt C Accessories SS MJT AS 2nd Interface 300 ce 0 F Elapsed Set Time 0 00 EN 0 30 i Elapsed Time Fig 4 24 lsothermal Temp Analysis C ON 1 D ON 2
38. Star PC ENTER GC 2 1 Step 4 13 Ver 4 0 Fig 4 20 Fig 4 16 Stepwise Temp Real Time Manitaring Ready for injection Cancel Fig 4 19 200 C min Post Heat C 3 Step C 2 Step C 1 Step C GC START END Ready for injection START GC Fig 4 20 Stepwise Temp Real Time Monitoring Ver 4 0 4 3 3 2 Stepwise Temp Selected Zone Analysis C15
39. Fig 3 16 GC Fig 3 17 RS 232C 3 10 Ver 4 0 3 6 GC EE 20 Fig 3 18 100 mL min 100 kPa 100 kPa Fig 3 18 GC 10 mL min 100 kPa
40. PC ENTER C G ON GC GC 2nd 1st Step Fig 4 15 GC Post Heat C 3 Step C 2 Step C 1 Step C Zone A Zone B Zone C GC GC GC 8 START END Fig 4 14 Ready for injection START Fig 4 15 Linear Temp Selected Zone Analysis
41. 4 4 2 4 D 196C E 90 4 4 3 File Print Ver 4 07 4 5 OFF GC
42. ITF TIC MS m z 28 32 10 mL min 50 ml min GCC ITF N
43. 19I GC 3 8 Ver 4 07 3 5 3 5 1 AUX GAS 1 3 IN Fig 3 13 Rx ITF A 1 AUX GAS OUT Rx ITF A a Fig 1 1 2 3 Fig 3 13 3 5 2 1 2 Fig 3 14 lt IN 1 2 USB PC USB
44. 200C min D ON 2 2 START GC 2 Fig 4 33 ESC Star PC ENTER GC 2 1 Step OO Fig 4 34 4 23 Ver 4 07 200 C min 4 Step C 3 Step C 2 Step C 1 Step C Stepwise Temp Real Time Monitoring Ready for injection Cancel GC START END Fig 4 33
45. D 1 ON 2 D 2 D 3 2 Temp 0cC 8 F 200C min 2 E 09C 0 C START GC 2 Fig 4 19 ESC
46. 2 1 Step 4 25 Ver 4 0 Fig 4 37 GC 2009C min Post Heat 9C a eo 2nd Step CC a Stepwise Te mp Selected IE Analysis ee 8 ZoneA ZoneB ZoneC GC GC GC START END Fig 4 36 Ready for injection START Fig 4 37 Stepwise Temp Real Time Monitoring 4 26 Ver 4 0 4 4 4 4 1 File Save As File Open mrx
47. 4 4 2 Tools Maintenance Fig 4 38 3050 OK Fig 4 39 Passwunrd Input Password Cancel Fig 4 38 A 1 Fig 4 39 Ver 4 0 4 4 2 1 2 2 1 Tune W 2 A 1 lsothermal Analysis A 2 2 Save
48. F 1 A 8 F 2 F 3 START GC 2 Fig 4 36 ESC Star PC ENTER C F ON GC GGC
49. Fig 3 1 2 ITF Fig 3 1 Rx ITF A B M Er 4 ITF Fig 3 1 ITF Rx SUS A Fig 3 2 Rx SUS A Fig 3 2 ITF N 12 mm Fig 3 26 ITF N Fig 3 2 ITF Fig 3 2 Fig 3 2 2 3 2 Ver 4 07 3 2 1 2 2 2 Fig 3 4 2 Rx B Rx A Rx SUS A Fig 3 3 5 4 Rx
50. Ready for injection START GC Fig 4 34 Stepwise Temp Real Time Monitoring 4 3 3 2 Stepwise Temp Selected Zone Analysis C15 1sf A Tools Analytical Modes Stepwise Temp Analysis Stepwise Temp AnalysisS B Fig 4 35 4 24 Ver 4 0 C 2 A B C 4 C 3 40 900 C 0 1 999 9 min C 1 40 900 C Not Ready Run 3rd 400 10 0
51. 4 100 C 800 C 800 C 20 100 C A 3 Ver 4 0 Fig A 1
52. Fig 3 19 USB a SN i Fig 3 19 USB 3 11 Ver 4 07 3 7 2 CD ROM Rx 3050TR control software CD ROM PC CD 3 7 3 COM Fig 3 20 Rx 3050TR Control USB Select the COM port for the controller Press Work Offline when working offline
53. START END Ready for injection START Fig 4 31 Linear Temp Selected Zone Analysis 4 3 6 Stepwise Temp Analysis 1st 2 Real Time Monitoring UADTM 2 5N GC Selected Zone Analysis GC 4 3 6 1 Stepwise Temp Real Time Monitoring 1sf A Tools Analytical Modes Stepwise Temp Analysis Stepwise Temp Analysis B
54. amp ITF IE CR 4 18 5 M3x6 30A 4 19 B 1 PY1 7618 1 Appendix A Ver 4 0 2 1 1 3 4 6 4 5 1 1 4 1 1 1 1 5 1 1 6 2 1 4 2 1 6 2 1 2 2 1 1 2 1 5 or 4 2 2 2 1 Tandemp Reactor Flow Controller 3 2 3 5 3 7 L_ PC FRONTIER LAB L 3 1 4 13 4 14 4 3 Fig A 1 A Ver 4 0 i i A 1 CR Sl es A 1 ERR A 1 SE A 1 NAR NAG oe A 2 52 PSP A 4 NN NN ON hE A 8 1 2 1 1 1 1
55. ON OFF ON F 3 2 ON F 4 2 ON OFF ON G 4 2 Ver 4 0 G 1 ON OFF H J K K 1
56. Ready for injection START Fig 4 27 GC Fig 4 28 Linear Temp Real Time Monitoring 4 3 5 2 Linear Temp Selected Zone Analysis C15 1stff A Tools Analytical Modes Linear Temp Selected Zone Analysis Linear Temp Selected Zone Analysis B Fig 4 29 C 2 A B C 5 C 3 40 9009C 0 1 999 9 min
57. ITF N GC GC 1 1 2 1 Ne 6 6 Ver 4 0 Appendix
58. 1009C F 2 F 4 Auto F 4 300C 2 50 C 500 C Fig 4 6 150 C 1009C 300 C C 300 C gt 150 C 50 C Fig 4 6 Ver 4 0 4 3 lsothermal Temp Analysis Linear Temp Analysis Stepwise Temp Analysis 3 2nd 1st
59. 2 2nd 1sfY 4 3 1 lsothermal Temp Analysis 2nd 2nd A Tools Analytical Modes lsothermal Tempt Analysis lsothermal Temp Analysis B Fig 4 7 VQ C 40 900 C I START STOP O TIMonitor D 40 900 C 1st Interface s Max 300s6 Not Ready 2nd u Reactor k 2nd Interface EatlgliGas NN 200 lo min Max 300 PG Rt 1strReactor 200 F PostHeat Reactant Gas C ost Hea T 3008 1 50 min 1st Interface 300 iG 2nd Reactor 200 lt C Accessories SS MT As Settings bo 2nd interace 300 _ Rn Sampling Zone Elapsed Set Time 0 00 EE 0 30 Fig 4 7 lsothermal Temp Analysis C ON 1 1 D
60. A B C 5 C 3 40 9009C 0 1 999 9 min x START STOP Monitor Step in N Max 300 s6 Not Ready N Run C 4 m 2 1st cae Gas 20 300 600 1 200C sa 0 500 1000 Actual oC CC 200 8 40 _ 900 a 4 Reactant Gas ROR 1 1st Interface 300 2nd u Reactor 2nd Interface lt 00 Ma 3 6 2nd Reactor 200 Accessories E 33 V 2nd Interface 300 l Elapsed Set n t P 1 1 1 0 0 1 w 0D 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 08 0 00 min 38 00 min Time min 1I Elapsed Time Fig 4 26 Linear Temp Real Time Monitoring Fig 4 26 E Settings Real Time Monitoring C 1 ON 1 C 2 C 3 C 4 1 Rate 0 C
61. Fig A 1 Fig A 2 i 50 Pe6 P N PY1 2017 20 LF P N PY1 EC80F 100 Rx SUS A 1 CP N Rx1 3540 1 Rx ITF A P N Rx1 3534 1 P N PY1 7911 5 Rx ITF B P N Rx1 3535 1 Rx ITF A 1716 P N Rx1 1278 3 Rx SUS A a CP N Rx1 3540 1 2 P N PY1 7911 5 ITF N P N PY1 3513 1 Ultra ALLOY CP N UA1 30M 2 0F 1 RE RN PY1 1274 3 phat P N UA EGA 2 5N 1 Fig A 2 1 Rx ITF A 2 P N Rx1 1278 3 S4 P N UV1 7701 10 P N PY1 7911 5 Rx SUS A P N Rx1 3540 1 Rx A ZMS 5 P N Rx1 3542
62. Fe FRONTIER LAB 1 1 2 2 3 1 2 3 Fig9 1 3 Ver 4 0 Tandem nu Reactor Rx 3050TR AC100 115V INPUT 50760Hz 800W rr MADE IN JAPAN ON OFF S 232C AS 1020E
63. M 6 6 1 a 6 4 GC GC GC 200 3009C ITF GC 20 350 C
64. A 2 1 Fig 3 3 2 Rx SUS A go Rx A S4 Rx B Rx B 13 mm 1 4 2 Fig 3 5 RxITF B S4 P N Rx1 3535 P N UV1 7701 P N PY1 7911 Rx SUS A P N Rx1 3540 Rx A P N Rx1 3541 P N Rx1 3542 ITF N P N PY1 3513 ITF N P N PY1 1274 P N PY1 7911 GC Injection Fig 3 4 2 Ver 4 0 3 2 2 GC
65. 2009C 30 5 2 3 GC MS He 50mL min 4 5 He 3 He GC MS START 0 2 uL START GC MS Fig 5 2 MS
66. ON 2 2 E Start E Sampling ON 2 F 09C 0 C G Setting 2 START
67. A B AivCO C He H2 Purge Time in Column 2 0 min D AirCO2 Purge Time in GC MS MS 7 0 min fd Interface Temp Control Auto Manual Auto Manual Sgletive Sampler HeH2 AirCO He H2 Purge Time in columnl 2 0 min Def i AirrCco Purge Time in GCIMS 7 U min Default 0 M roJet Cryo Trap MJT AutoShot Sam
68. E 0 C 0 C F Settings G 1 A 8 G 2 G 3 4 15 Ver 4 0 START GC 2 Fig 4 22 ESC
69. 10 200 m z 5 sec He 50 ml min GC He 50 ml min 17100 Ethylene 1 2 3 min Fig 5 1 ZMS 5 5 2 Ver 4 07 5 2 5 2 1 s 30 m 0 25 mm 2 0 um UA1 30M 2 0F es 1 mL 5 10 uL 5 2 2 30 m 0 25 mm 2 0 um GC GC MS GC
70. ON 1 C 2 C 3 C 4 1 Rate 0 C 8 F D ON 2 2 E Settings F 1 A 8 F 2 F 3 START GC 2
71. Fig 3 24 3 Rx A1 Fig 3 25 1 Rx A1 Rx A1 Rx A2 A3 Ver 4 0 6 Rx A1 Rx ITF Rx A1 Rx A3 i 4 W oF 2 Fig 3 25 Rx A1 2 mm Fig 3 24 Rx A 2 Fig 3 26 A RxITF A B RxITF A 8 mm Rx ITF A 1W 13 mm Rx ITF A 2 Fig 3 26 1 2 Rx A2 A3 Rx A2 A3 Rx
72. Fig 4 32 4 22 Ver 4 0 C 2 C 4 C 3 40 9009C 0 1 999 9 min Rx 3050TR Conxrol START STIOP Not Ready Run rMonitor Actual 1st Reactor 200 c tH As 1st Interface 300 p G40 900 0 Em C 2nd pw Reactor 2nd Interface 200 m Max 300 2ndn Reactor 200 Accessories AS3 2nd Interface 300 EC Elapsed Set TMS 0 00 is 41 50 Elapsed Time Fig 4 32 Stepwise Temp Real Time Monitoring Fig 4 32 E Settings Real Time Monitoring C 1 ON 1 C 2 C 3 1 Temp 0 C 8 F
73. 2 E Start E Sampling ON F Setting VQ Ver 4 07 1 2 START GC 2 Fig 4 25 1st
74. 3 2 2 1 GC Fig 3 5 GC 1 GC 1 1st 2 GC GC Fig 3 5 GC
75. K 2 K 3 2 K 4 2 K 5 K 6 4 2 pu 4 2 1 4 2 1 1 Fig 4 3 F Settings Fig 4 4 1W 2 Fig 4 4 A Auto Manual 4 2 1 3 4 2 1 4 OK
76. B 1 PY1 7805 1 3 7 USB 1 PY1 3751 1 3 8 1 5m 2 PY1 7801 1 3 9 1 5m 2 PY1 7613 1 4 Rx B 1 Rx1 K051 1 4 1 1 1 PY1 7141 1 4 1 4 1 2 12 13 mm 1 Rx1 3531 1 4 1 3 6 8 mm 2 Rx1 3532 1 4 1 5 6 2 mm 1 PY1 7111 1 Rx A 1 Rx1 K040 1 4 2 1 Rx SUS A 2 3 Rx1 3540 1 4 2 2 Rx A 3mm i d 20 Rx1 3541 5 4 2 3 ITF N 3 PY1 1274 3 4 24 1 6 mm 3 4 2 5 P 6W 5 PY1 2017 20 4 2 6 S4 20 UV1 7701 10 4 2 7 0 5 g 1 PY1 5112 1 4 3 GC MS 50 1 MS402180 1
77. COMTI COM2 COM3 COM4 r COMS C COM6 COM7 r COM8 Cancel Work Qffline Fig 3 20 _ COM Windows Fig 3 21 COM LPT USB Serial Port COM COM Fig 3 20 OK 1 8 USB Serial Port Fig 3 22 Fig 3 21 1 8 OK
78. 4 2 1 2 SS MJT AS 1st Interface Temp Control 2nd Interface Temp Control Auto Manual Auto Manual PSS He 2 ipCO Pressure Stability Time 20 sec Default 20 MicroJet Cryo Trab MJT AutoShot Sampler FAS Purge Time 10 sec Default 10 ok canee Fig 4 4 Xa 4 3 Ver 4 0 4 2 1 4 MJT 1030Ex SS 1010E Fig 4 3 F Settings Fig 4 5
79. A Tools Analytical Modes Stepwise Temp Analysis Stepwise Temp AnalysisS B Fig 4 18 D 2 a D 4 p 3 40 900 C 0 1 999 9 min ORx 3050TR Control x C 40 9009C START STOP Monitor 200 se Not Ready Reacto 2nd Interface em ba Step Rate G min Temp C Timg min Max 300 e6 Rt _1st 200 TU 1st n Reactor 200 2nd 300 10 U0 tas 3rd 0 1000 1st Interface 30o c 4th 500 10 00 E ES 9 a 2nd Reactor 200 lt C Accessories F SS MJT _ AS Settings 2nd Interface 300 C Temp Profile i RRR ER RR SEE SE RS son 1 I Sas 1 2200 100 Elapsed Set 9 Time 0 00 i 41 50 Es Elapsed Time Fig 4 18 Stepwise Temp Real Time Monitoring Fig 4 18 F Settings Real Time Monitoring C ON 1 1
80. A 1 Rx1 3578 1 1 5 Rx A 1 Rx1 2501 1 2 2 2 2 1 1 2 1 10 1 2 1 1 Rx ITF B 1716 174 1 Rx1 3535 1 2 1 2 Rx ITF A 1 Rx1 2502 1 2 1 3 Rx SUS A 1 Rx1 3540 1 2 1 4 S4 2 UV1 7701 10 2 2 1 5 Rx A ZSM 5 1 Rx1 3542 1 2 1 6 6 mm 2 PY1 7911 5 2 1 7 ITF N 1 PY1 3513 1 2 1 8 ITF N 1 PY1 1274 3 2 1 9 ITF 3030A 1 PY1 3563 1 2 1 10 30A 1 PY1 3631 1 A 4 Ver 4 0 3 3 1 1 3 2 1 3 3 1 PY1 7808 1 3 4 AC 1 PY1 7023 1 3 4 1 PY1 6034 1 3 6 PY USB 2m A
81. C PC 9 AC 100 115V 100W 2 1 1 Fig 1 4 Ver 4 0 2 RX 3050TR 110 110 V RX 3050TR 220 220 V 1 40 900 C 1 C 500 kPa 5 l min
82. ITF N Fig 6 2b ITF N P N PY1 1274 s Fig 6 2c P N PY1 7811 c a 3 NN Re ITF 2 b ITF Fig 6 2 Ver 4 0 6 4 2 ITF 100 mmin 1 ml min 6 3 1
83. Fig 4 8 Ver 4 0 GC 2 Fig 4 8 Star PC ENTER 4 3 2 Linear Temp Analysis 2nd 2 Real Time Monitoring UADTM 2 5N GC Fig 4 9 Ethanol Ethylene Diethyl ether 60 100 200 300 400 2 C Fig
84. TS SN Ka haKS EEE A Ge 4 1 2 ER ES 1 1 1 3 RN RN NN NR RR EC RE RRS 1 3 2 SC NE CE 2 1 3 hl i 3 1 3 1 NC EN ER EE Sad 3 1 ON CR OM NE NS 3 2 RG 9 2 d MM 3 5 3 4 3 8 3 5 i et Ce EG SE SG 3 9 3 6 NN 3 11 3 7 3 11 38 Rx 3 3 13 4 NE 4 1 4 1 2 M0 4 1 4 2 SN EE A A CR 4 3 4 3 RC ON 3 4 6 44 DS SD ER Te SN SN a SD 4 27 4 5 NE KS 4 29 4 6 4 29 4 7 RF HER 4 31 48 Rx ES aS 4 33 a A RN REE 5 1 5 1 SR NE 1 5 2
85. Star PC ENTER D G ON GC GC 2 1 Step Fig 4 23 GC 2009C min DP O St G at 9 C Il 2 39 Step COO 2 d Step CC TR N 7 gt PStep CY Stepwise emn Selected Zone Analysis i Zone A ZoneB Zone C Ready for injection _ Cancel START END Fig 4 22 Ready for injection
86. 10 20 mm 40 mm 10 mm Fig 4 45 Rx 40 mm Ver 4 0 5 5 1 He ZMS 5 5 2 5 1 5 1 1 s
87. 230 1 1200 09 5 meeE 90 90 fel POOm lm H K 5 K 6 Fig 4 3 A B CA C 2 2 C 1 1W 2 D 1 lsothermal Temp Analysis D 2 Linear Temp Analysis D 3 Stepwise Temp Analysis E F F 1 1 ON OFF ON F 2 11
88. 3 7 3 7 1 USB USB edge 0 eb SW 062 s Update USB FE NNRNET EE PC 0 Rx 3050TR control software CD ROM KSMSS CD CD RRR ET D yg
89. 9 MS 1 5 1 ITF Rx ITF A Rx ITF A 2 2 TF No ITF N 2 GC I EGA 4U GC MS Fig 1 1 MF AUX GAS OUT AUX GAS1 IN _ AUX GAS2 IN _ AUX GAS3 IN Fig 1 2 1 2 Ver 4 07 1 3 1 3 1 AUX GAS Tandemu Reactor Flow Controller Q MF Contr oler AUX L 2 6 AUX GAS 1 mn 7 4 8 x nn
90. A1 A2 Rx A3 Rx 2 mm Rx A2 A3 Fig 3 27 3 14 Ver 4 0 4 4 1 4 1 1 Rx 3050TR Control Fig 4 1 Fig 4 2 4 1 Ver 4 07 4 1 2 Fig 4 3 A NN GoC2 DB2 ps J ile View Tools DebMa Help 1sr a F F 1 co Monitor ET 2 Max Not Ready F 3 i kei mm C 3 EE 1000 1st h Reactor 200 a K 1 F 4 En 1 1st Interface 30 K 2 Ri 2ndn Reactor 200 K 3 G 2nd Interface 300 1 K 4 1 3 G 1 Zone min min CC CM 9 eno Tap Cno Trap 21 A oo
91. C 0 C 4 10 Ver 4 0 F Settings F 1 A 8 F 2 F 3 START GC 2 Fig 4 14 ESC Start
92. _ EE I C 1 START STOP rMonitor 8 300 Not Ready te o C 4 Run 4 1st 00 GTlelG8s 1 2009C nd 20 300 000 3rd 10 500 10 00 Actual 4th 0 500 5 00 1stu Reactor 200 Rsactant as D 40 9009C 1st Interface 300 6 2nd u Reactor 2nd Interface 20 Max 200 2ndh Reactor 200 lt C AccesSsories Setinoe 2nd Interface 300 E sampling MJT AA D rE H TT BS li nital Fnal inital Final e cm 0 amping zo F 1 1 mn mm C NE corap ar A 300 s00f2ssl 30 lt I ioo MC iF Elapsed 0 olm OO Ls el Ke B en J I Set le 0 00 _ 38 00 p mm a NO EE Ime min min F 2 F 3 F 4 Fig 4 29 Linear Temp Selected Zone Analysis 4 20 Ver 4 07 E Settings Selected Zone Analysis C
93. 3 11 ARNING Rx ITF A Rx ITF A ss 3 Fig 3 11 Rx ITF A Rx ITF B Rx ITF B Rx ITF A 1 2 Fig 3 12 Fig 3 12 Rx ITF B Ver 4 0 3 4 1 1 800 C 1 B 1 500 kPa 100 mL min
94. 4 4 RxITF A 1716 2 Rx1 1278 3 4 5 LF 80 pD 20 PY1 EC80F 100 4i6 SF 10 PY1 ES10F 50 4 7 AL 5 PY1 EH10AL 5 0 P 1 PY1 EP55F 1 4 9 5 PY1 2025 20 4 10 1 PY1 7131 1 4 11 350 350 mD 1 UV1 7201 1 4 12 1 UV1 7501 1 1 UA1 30M 2 0F 1 30 m 0 25 mm id 2 0 um 4 14 2 5 m 0 15 mm id 1 UADTM 2 5N 1 A 5 Ver 4 07 Rx A _ SUS 1 5m 1 16 o d 0 8mm i d 1 178 4 15 Brass 1 178 Brass 3 178 1 Rx1 K033 1 Brass 3 4 16 CD ROM 4 17 M2 5x4
95. 4 9 Linear Temp Real Time Monitoring Selected Zone Analysis GC 4 Ver 4 0 4 3 2 1 Linear Temp Real Time Monitoring 2nd A Tools Analytical Modes Linear Temp Analysis Linear Temp Analysis B D 2 A B 40 900 C D 3 0 1 999 9 min I START STOP Monitor O rv 1sf Interface 200 300 se Not Ready gE D 4 2nd u Reactor 2nd Interface _ CarrlahiGas un 0 1 200 C Step Rate 6C min Temp C Timefmin Max 300 sC ti a st Reactor 200 sC E 2nd 20 300 0 00 t Cas 3rd 10 500 10 00 1st Interface 300 4th 0 500 5 00 Post Heat 600 10 00 2nd Reactor 200 Accessories F SS NT ZS 2nd Interface 300 Temp Profile Elapsed Set Time 000 3800 Elapsed Time Fig 4 10 Linear Temp Real Time Monitoring Fig 4 10F Settings
96. CON29 Fig 3 21 COM Fig 3 22 _ COM 3 12 Ver 4 0 3 8 20 2 Rx 3 8 1 2 ITF GC Fig 3 23 ITF AN Fig 3 23 3 8 2 1 Rx A Rx A1 Rx
97. 1 Rx A CP N Rx1 3541 5 P N PY1 5112 0 5 g Fig A 3 2 Appendix A 1 Ver 4 0
98. 4 11 Ver 4 0 4 3 3 Stepwise Temp Analysis 2nd 2 Real Time Monitoring UADTM 2 5N GC Fig 4 16 Diethylether m z 74 00 10 Fig 4 16 Stepwise Temp Real Time Monitoring Selected Zone Analysis GC Diethyl ether Ethanol Ethylene Propylene HzO 2 0 0 300 400 C 1 2 3 4 min Fig 4 17 Stepwise Temp Selected Zone Analysis Ver 4 07 4 3 3 1 Stepwise Temp Real Time Monitoring 2nd
99. Actual D 40 9009C E00 00o 1sty Reactor 200 1st Interface 300 F 2ndu Reactor F 2nd Interface 200 Max 300 Accessories nd os EA bo E SS MJT Settings 2nd Interface 300 Sampling A D TE H Tima Finai tnitial Final 0 mE F 1 1 min min C I 200 Cryo Trap 21 B I EIapsed Set Tc i Time 000 41 50 I _ c F 2 F 3 F 4 Fig 4 35 Stepwise Temp Selected Zone Analysis E Settings Selected Zone Analysis C 1 ON 1 C 2 C 3 2 Temp 0C 8 200 C min D ON 2 2
100. Sampling zone G 1 min min C Cryo Trap 21 300 so 3 6 8 s00 1800 SCs Elapsed Set 0 Final Sampling Crye mp Initial Final Initial 3 18 00 2800 Cs 500 PF Tr 0 ime 0 00 38 00 G 2 G 3 G4 Fig 4 13 Linear Temp Selected Zone Analysis F Settings Selected Zone Analysis C ON 1 1 D 1 ON 2 D 2 D 3 D 4 2 Rate 0 C 8 E 2 E 0
101. Star PC ENTER Ready for injection Fig 4 25 4 3 5 Linear Temp Analysis 1st 1 2 Real Time Monitoring UADTM 2 5N GC Selected Zone Analysis GC 4 3 5 1 Linear Temp Real Time Monitoring 1st A Tools Analytical Modes Linear Temp Analysis Linear Temp Analysis B Ver 4 07 C 2
102. Ver 4 0 MODEL Rx 3050TR FRUIITIER LAB GC MS 1 7
103. pler AS PurgeTime 10 sec Default 10 wcwew Fig 4 5 4 4 Ver 4 0 4 2 2 1 2 Auto Manual Fig 4 4 A Auto Manual Fig 4 3 F 2 F 4 Auto
104. tial Final initial Final N ON 2 GT 0 et 1 Cryo Trap a Al ooo 200jL 2 2 lt 1 NR iioo 1200 3 M Elapsed BN 2200 2 Ne ooo 7 5350 3 min min G 2 G 3 G 4 Fig 4 21 Stepwise Temp Selected Zone Analysis F Settings Selected Zone Analysis C ON 1 1 D 1 ON 2 D 2 D 3 2 Temp 0 C 8 200 C min 2
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