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1. gt PAD PAD SUCREBEAD I SUCREBEAD II REN CAPCELL PAK NH HILIC CAPCELL PAK Cig CAPCELL PAK Cig Y 0 2 an eee NR a E i N 4 O vy 38 European Pharmacopoeia EP Spectinomycin PAD EP C14H24N207 u M W 302 10 HPLC 8 2248 CAPCELL PAK Cis MG S5 2 0 mn2. RHI 10 100 PAD s PAD PAD pKa 1 13 CH20H Hake OD REMERA E SN 7 0 25 pH 7 OH H DKa 12 28 en pKa 12 03 H OH DKa 12 15 e PAD
3. gt 999999 EAN lt gt pS http www j point org shiseido NANOSPACE SI 2 SI 1 PDE Nin reina rs BE SHUYEIDO HATS ean Tr105 0081 1 1 16 FS TEL 03 6253 1412 FAX 03 6253 1416 ES 1601 8037 18 TEL 075 671 0301 FAX 075 671 0302 http www shiseido co jp HPLC NO 17 5000 2011 4
4. NANOSPACE T S NANOSPACE 2 HPLC S S S S
5. A D NANOSPACE PEEK BE 3016 en a E 1 800 000 i PAD HPLC 1 RESORT IO http www shiseido co jp hplc2003 note htmi col_index htm 3 LC cafe No 1 7 BHAT CUINA At ER RA CUL WH BRM BR Cb
6. HPDLC Q amp A HPLC 2 PAD 0473 Al RI pulsed amperometric detector PAD
7. 7 2 Cisa CAPCELL PAK CR PC HILIC Cra LC caf No 10 1 gt Cia
8. 1 100 CHsCN 1 100 CHsCN PPC HILIC 1 CHsCN 609 CHSCN 2 CHaCN CHaCN 50mmol L CH3CN 85 15 H20 CH3CN 40 60 Hs0 CHsCN 85 15 1 H20 CH3CN 10 90 1 Hs0 CHasCN 10 80 ERODTWNDNENIEILCCOS IFE Z1TI3MEIGDD E EA
9. CHaCN CHaOH CHaOH CHaCN CANO CHaOH BI 100mmol L BI 100mmol L CHsCN 85 15 EE AMARO E ASONESO7TS a He0 CH30H 85 15 1 KEOZELZEN 8525 POMO SI alia 1 HaO CHaCN 85 15 AA MARIE CRA EA 00 CHaON BET 1 AP PRES 1009 CHasCN 2 N A PCAPCELL PAK CR 1 CHsCN CHsOH 100mmol L U VENA BI 100mmol L ASEOS AS ASS SS o7 lo N H20 CH3CN 89 15 k aA Saa 1 1 Hao CHaCN 85 15
10. id API 428 of Oxalic acid and 2mL of heptafluorobutyric 6 acid were dissolved into IL of water and then adjusted at pH 3 5 with NaOH The solution and A acetonitrile were mixed at 85 15 Mm JR 200 ul min pH mol L NaOH 400 uL min m E 40C 0 te PAD 2 ul 100 g mL 0 2 4 6 8 10 12 14 16 min TI HAUT gt DDS C18 9 MI 18 a HPLC MA CAPCELL PAK Cig AQ 55 46 mm Id Xx 250 mm HoO jie mL min pH Imol L NAOH 600 uL min m E 200 PAD a 100 ug mL PAD NANOSPACE ANO AD SE HPLC PAD
11. CLAADLOAGE HDS a a TFA pH gt 8 NAAA Cee LIODIESIELERMDPITE
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