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1. 10mL 50mL 100mL 10mL 1000 50mL 5000 100mL 10000 50mL 5000 100mL 8000 50mL 100mL 8 10mL
2. 10 ng 50 ng g L 100 ng L 1g GC ng NeedlRx NeedlEx 10ng uL 50ng nL 100ng uL 1 ng nL 1ppm 10 ng 50 ng 100 ng 100mL GC
3. 1 1 NeedlEx 0 5mm 0 7 mm 85mm 4 lt 1 2 NeedlEx 4 2 NeedlEx NeedlEx
4. 5 2 NeedlEx NeediRx 2 4 4 1 Myrcene 2 1 8 Cineole 3 L Menthol 4 Anisaldehyde 2 1 3 3 ee 0 0 0 5 10 15 20 25mm NeedlEx 100 mL 100 g 20 mL Column ULBON HR 1 30 m x 0 32 mm I D 0 25 hm Column temp 50 C 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 C Detector FID 250 C Carrier gas He 2 4 mL min W KORNNYO RIKAGAKU KOGYO 612 8307 a 213 0006 50 2 1 8 28 TEL 075 621 2360 FAX 075 602 2660 TEL 044 833 8900 FAX 044 833 2671 URL http shinwa cpc co jp URL http www komyokk co jp E mail info shinwa cpc co jp E mail qa komyokk cojp
5. 10 ml 100 ng mL 60000 50000 40000 30000 20000 10000 1mL 3 mL hm 9 mL Fas 2641 7923 1320 iass 2azelz64ai sies 3961 2641 7895 1402 1875 2352 24gs 2691 2779 3 Needlfx Q amp A Q 10 50ml 10mL 10mL 5 50mL Q 11 100mlL 50mL 10mL
6. 10 Q 14 3 95 95 Q5 200C 80 Q 15 NeeqlEx GC MS 2 1 GOC MS 1 GC MS Q 16 100 100mL
7. 200C 11 3 NeedlEx Q amp A Q 17 NeedlEx 30 NeedlEx Q 18 Q11 1000ng mL 20mL 100ng mL 10 ng7mL 80mL 1000 ng ml 1000 ng ml x 20 ml 20 ug 100 ng ml 100 ng ml x 80 ml 8 ug 10 ng ml 10 ng ml x 80 ml
8. 100 mL Q 7 NeedlEx 200C 3 Q 8 NeedlEx HzS Q 9 100 ng ml
9. 5 100 Ethyl acetate Toluene 0 2 3 4 5 6 7 8 3 NeedlEx Q amp A Q1 NeedlEx 100 FEID 10 ppb 200 ppb 500 mL
10. 10 3 NeedlEx Q amp A Q 18 NeedlEx 10 10 200ppb 6 100mL 1 80000 60000 40000 n 20000 1 11 14 eo Fmt 36109 37774 34751 37714 51972 53239 51307 45278 n 51136 53114 45935 43644 49751 40365 65401 68648 61463 61420 64232 59199 10
11. 0 4mL 1 mL nn 7 J 0 4mL 100 0 0 1 0 2 0 3 0 4 0 5 0 6 mL 5 2 4 GC NeedlEx 5 10 MT NeediEx GC PZ 4 2222 2 2222 222 2222 112222 222 16222 ET gt Ne
12. 10ng mL 100ng mL 80mL 100 80mL 100mL 50mL 10mL 50 100 50mL 10 50 10mL 120 100 80 60 4 10ng mL 100ng mL 40 _4 1000ng mL 20 0 iongmL 100 loongmL 100 1000ngmL 100 10 mL Q 12 80 80 NeedlEx 80C 80
13. GC 200C 250 180 Ethyl acetate Toluene 150 160 170 180 190 200 210 C 3 Needlfx Q amp A Q 6 100mL 10mL 10 mL 100 mL 10 mL
14. ECD FPD Q 3 NeedlEx NeedlEx Q 4 NeedlEx Q 5 95 GC 95 95
15. 183 3 NeedlEx Q amp A 1 1 10 mg 50 ng 100 ng 75 ng 100m1L 75 ng 100mL 0 75 ng mL ppm 0 75 ng mL 25C 298 0 75 ng mL 92 14 X 22 4 9 ee eoo eo6 eeeeoeo 273 020ppm 1 2 1 mol nL mL 0 278 25C 298 14 4 NeedlEx EE ERE Benzyl Acetate 1 8 Cineole 8 Phenethyl Alcohol Column ULBON HR 1 30 m x 0 32 mm 1 D 0 25 um Column temp 50 C 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 Detector FID 250 Carrier gas He 2 4 mL min NeedlEx 100 mL
16. 2 1 Pam GC 30 1 OK NeedlEx NeedlEx 100kPa GC 30 1 NeedlRx NeedlEx 2 2
17. DOD NeedlEx 3 gw 2 3 2 2 3 4 NeedlRx No 1
18. mm gt G 0 5 10 15 20 25 min lt Thermon 8000 KOH 2 2 Sunpak N 2 1m x 3 2 mm 120C 250 FID 250 C N2 50 mL min 101 x ATT 3 NeedlBx 1 0 02 ppm I i 2 0 49 ppm 19 5 NeedIlEx 16 247 67 93
19. 100 mL 10 15 30 80 RH 1 10 10 mL AP 20N 50 100mL AP 20N AP 20 5 5 6 2 3 GC NeedlEx 1mL
20. 200 ppb 0 100 mL 200 mL 300mL 400mL 500 mL 3415 7090 10528 14440 19011 4803 10068 15032 20166 26511 n 4797 10169 14775 20334 27471 6395 13087 19450 26401 34332 250 ppb 2 800 ml 102 10 2 250 ppb 300000 250000 200000 150000 100000 50000 36429 65476 103863 122839 138897 143898 154334 35500 71000 106500 142000 177500 213000 248500 38 NeedlEx Q amp A Q 2 NeedlEx FID TCD ECD FPD GC MS
21. 50mL 100mL 100mL 10mL 1 3 NeedlExz Q amp A Q 19 200C NeedlRx 200 NeedlEx NeedlEx Q 19
22. 0 8 ug 100ng mTL 10ng mL 100ng mL 100ng mL 100ng mL 10ppm GC FID 100ng 100ng mL 1mL NeedlEx 10ng mL ppm
23. CN1017B ER SR 4 No 2 NeedlEx eedlEx 3 3 NeedlEx Q amp A NeedlEx 8 15 5 QW gi EMICALNDUSTRE im NatISExImetm 1 NeedlEx NeedlEx TBNAX NeedlEx NeedlEx NeedlEx 0 41 0mL
24. L min SS eraniol Perillaldehyde 0 5 10 15 20 25 min 1 8 Cineole NeedlEx 100 mL Anisaldehyde Column ULBON HR 1 30 m x 0 32 mm 1 D 0 25 hm Column temp 50 C 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 Detector FID 250 Carrier gas He 2 4 mL min 0 5 10 15 20 25 min s lsobutanol 1 Propanol Ethanol Ethyl Acetate Ethanol Acetic Acid lsoamyI ALcohol 3 Methylthio 1 propanol 4 NeeqlBx Column ULBON HR 1 30 m x 0 32 mm 1 D 0 25 um Column temp 50 C 200 Program rate 5 min Sprit ratio 10 1 Injection 200 Detector FID 250 C Carrier gas He 2 4 mL min NeedlEx 100 mL Ethyl n Caproate Column ULBON HR 1 30 m x 0 32 mm I D 0 25 um Column temp 50 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 Detector FID 250 C Carrier gas He 2 4 mL min NeedlEx 100 mL 20 25 min 8 4 NeedlEx Column ULBON HR 1 30 m x 0 32 mm LD 0 25 pm Column temp 50 C 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 SS 0 Detector FID 250 C Carrier gas He 2 4 mL min NM NeedlEx 8 100 mL
25. Limonene lsobornyI Acetate Column ULBON HR 1 30 m x 0 32 mm 1 D 0 25 hm Column temp 50 C 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 Detector FID 250 Carrier gas He 2 4 mL min a onone NeedlEx 100 mL 0 5 10 15 20 25 min 15 Je 1 8 Cineole 8 Phenethyl Alcohol ca Pinene 0 5 10 15 a Column ULBON HR 1 30 m x 0 32 mm 1 D 0 25 um Column temp 50 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 Detector FID 250 Carrier gas He 2 4 mL min 20 Myrcene 16 Limonene 10 4 NeedlEx Column ULBON HR 1 30 m x 0 32 mm 1 D 0 25 um Column temp 50 C 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 C Detector FID 250 Carrier gas He 2 4 mL min NeedlEx 25 min 100 mL NeedlEx 100 mL 15 20 25 min 4 NeedlEx NeedlEx 100 mL Tinalool Anisaldehyde Column ULBON HR 1 30 m x 0 32 mm 1 D 0 25 hm Column temp 50 C 200 C Program rate 5 C min Sprit ratio 10 1 Injection 200 C Detector FID 250 Carrier gas He 2 4 m

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