原子吸光分光分析による土壌および、植物中の
Contents
1. 139 1 57 min 77 min r 4 Mg 139 Mg 20mA2. Si AL K P 2 logg7
3. 139 1 A Mg 1 3 ppm Mg 2 6 ppm 154 183 09 ogg70 3 Mg 2 6 ppm My 06 PR log 70 3 ho A
4. 1 atomic absorption spectroscopy 1955 A WArsaD 1961 139
5. 10 mA 15 20 mA 15 mA 5 2 20 1 35 40
6. Al 30 ppm 14 Al50ppm Al100 ppm 5 4 P Sr Mg 2 5 ppm HaPO P 3 120 ppm Sr 1 500 ppm 6 P 3 ppm 3 P6 120 ppm 8 P 120 ppm 5 K Sr Mg 2 6 ppm KCI K 30 500 ppm Si1 500 ppm 7 K 100 ppm K 200 ppm 2 KK 500 ppm
7. 0 2N HC1 M X B T 12 3 13 0 3 0 7mg 3 5g 0 03 cc 100g Mg 0 2 mg 1 3 M B 0 3 g Mg 0 6 mg 160 183 11 Mg No 66 66 77 77 99 99 _ log7 0 128 0 141 0 097 0 103 0 197 0 200 M 10 20 0 82 0 7o 1Occ 100cc DDn1 0 82 0 87 1 70 l 70 4g
8. Si Al K P SrCl Sr 1 500 ppm x 1 A WArsm The application of atomic absorption spectra to chemical analysis Spectrochim Acta 7 p 108 1955 2 44 p 1187 1962 3 2 3 HITACHI Scientific Instrument News 6 No 1 p 1 1963 4 44 D 2051 1962 5 pp 54 58 1964 On the Analysis of Mg contained in Soil and Plants with the Aid of Atomic Absorption SpectroscopyY Shiro YokorA Resume The author carried out study on the variation of calibration cure and on the disturbance effect of other elements in the case of the analysis of Mg with the aid of atomic absorpt
9. 3 Si 20 ppm 64 Si Si100ppm Si 200 ppm 9 2 Si Sr Sr 30 000 ppm Sr Si 100 ppm Mg 2 5ppm Sr 900 3 000 ppm 4 Si 3 Al Sr Mg 2 5 ppm AICl Al 0 500 ppm Sr 1 500 ppm 5
10. 1 3 03 09 1 2 A 0 2 3 4 5 6 7 Mg PPW 1 57 min 77 min 0 2mm 15mA CB 2 17 min 10 5 A 1 5 HB min B 2 1 7 min 10 5 7 min 1 Mg
11. 3 2 HC1O4 6 HCIO4 1g 100 HCIO4 0 3 1N IN Na 800 ppm Ca 400 ppm Fe 500 ppm 1 Si Sr MgCl Mg 2 6 ppm Na SiOs5H O Si 0 500 ppm SrCls Sr 1 500 ppm
12. 15 10 5mA 1 2 15 mA 5mA 15 5mA 0 100 155 1 og 7 0 26 0 65 1 30 COAKRSE 6 5 mA 0 041 0 102 0 FINE 8 COARSE 6 10 mA 0 039 0 097 0 194 FTNE 15 mA 0 036 0 089 0 177 COARSE 5 FINE 6 5 1 285 2 mg 2 0 5mm 3 1 57 min 4 77 min 2 log 7 Mg ppm NL 0 26 0 65 1 30 COARSE 6 5 mA 0 055 0 137 0 274 FINE 6 COARSE 6 10 mA 0 053 0 134 0 268 FINE 1 15 mA 0 050 0 127 0 254 COARSE 5 FINE 6 1 20 2 1 3 1 5mA
13. 6 Si A1 Si Al 3 25 139 156 183 HNOs HCIO4
14. 0 06 cc 2 3 2 M X B 0 1g logg 70 005 0 004 0 018 log 70 02 log 70 005 Mg 159 8 Mg PR NN NR 9 00 IS log 7 0 112 0 118 0 109 0 117 0 128 0 117 Mg DDrn 0 993 0 98 0 90
15. Mg 10 ppm 5 25cc 100cc SrCl Mg 0 2 5 ppm Sr 1 500 ppm Mg 0 ppm 8 2 NH4OH pH M X B T Mg 9 3 10 0 001 0 018 0 8g 0 02 cc 0 006
16. Sr 1 500 ppm Si Al 2 Si Al 2 ppm Mg 7 1 2 1g 50cc HNO HC1O4 HCIO 3 cc 100cc 10 cc 100cc Sr 30 000 ppm SrCl 5cc
17. g 139 6 I131 0 122 2 120 9 128 8 128 7 1 014 10cc g 0 292 0 310 0 332 0 336 0 317 0 315 100g Mg mg 37 7 38 7 24 7 25 9 53 1 54 0 Mg Me 39 101 3 18 2 03 2 13 4 36 4 44 1 No 66 24 0 5cm Br d No 77 23 0 5cm Bs No 99 43 0 5cm Bp d 2 4 12 Mg No 9 W 66 66 77 77 99 0 01M EDTA cc 5 56 5 58 3 61 3 77 PA 7 99 ccXE Mg mg 1 355 1 360 0 878 0 920 1 877 1 942 Xx0 243mg 4g g 139 6 131 0 122 2 120 9 128 8 128 7 g 124 7 113 6 106 6 105 3 112 8 114 3 g 3 57 3 46 3 49 3 49 B51 3 56 100g Mg mg 38 0 39 3 25 1 26 3 53 8 54 6 2 Mg Me 3 13 3 24 2 06 2 16 4 42 4 50 EE 1 11 13 Mg No 6 se 7 7 sw 9 Mg mg 37 7 38 7 24 7 25 9 0 54 0 Mg mg 38 0 39 3 25 1 26 3 53 8 54 6 mg 0 8 oe nog P04 5o 7 po 6 _ Me _ 0 025 0 049 0 033 0 033 0 057 0 049 log 7
18. 5 200 ppm 3 Si Sr HI SS 0 20 50 100 200 Gr log 7 0 355 0 355 0 355 0 355 0 325 1500 ppm 0 0 0 0 9 Gr log 7 0 325 0 117 0 108 0 087 0 070 0 ppm 0 64 67 73 79 1 Mg 2 6 ppm 2 HCIO4 3 1 4 Si Sr a ig 0 900 1 500 2 100 Gi og 7 0 097 0 315 0 315 0 315 1500 ppm 71 0 0 0 1 Mg 2 5ppm 2 0 2mm 5 Al Sr Al ppm 0 30 50 100 200 Gr og 7 0 305 0 305 0 305 0 290 0 280 1 500 ppm 0 0 0 8 Gr log 7 0 280 0 240 0 292 0 214 0 192 0 ppm 0 14 17 32 1 Mg2 5ppm 2 0 2mm 6 P Sr SO Gr log 7 0 310 0 3
19. 0 002 log 7 0 005 Mg 1 5 mg log 7 0 002 139 161 1 57 min 7 07 min 15 mA 0 2mm log 7 0 3 Mg 2 5ppm
20. 0 97 1 08 0 97 Mg 0 093 0 098 0 090 0 097 0 108 0 09Z 1 2 2 0 2mm 9 Mg i _ No 13 16 8 20 9 17 0 01M EDTA cc 3 08 3 49 3 69 3 11 4 16 3 61 Mg mg 0 749 0 847 0 896 0 755 1 010 0 876 g 0 816 0 826 0 826 0 832 0 825 0 817 Mg 0 092 0 102 0 108 0 091 0 122 0 107 1 8 10 Mg OO NIINN UI 0 2 23 Mg 0 093 0 098 0 090 0 097 0 108 0 097 Mg 0 092 0 102 0 108 0 091 0 122 0 107 0 001 0 004 0 018 0 006 0 014 1 0 010 8 1 Schollenberger 1 4g 10cc 100cc SrCl 5cc 11 2
21. 10 0 310 0 310 0 310 1 500 ppm 0 0 0 0 0 Gr log 7 0 260 0 245 0 240 0 240 0 240 Oppm 0 6 8 8 8 1 Mg 2 5ppm 2 0 2mm 7 K Sr ee 0 30 50 100 200 lg7 o 335 o ss5 0 335 0 335 o sss 1 500 ppm 0 0 0 0 Gr log 7 0 315 0 315 0 315 0 315 0 310 0 ppm _ 0 0 0 0 1 Mg 2 6ppm 2 0 5mm ce 1 S00 0 310 13 0 060 682 3 000 0 315 S00 0 260 15 0 165 41 120 0 310 0 240 158 183 KK500ppm 2 KK5 000 ppm 5 6 Mg 0 1 0 4 Mg 0 05 2 5 ppm 0 05 0 1g 100cc P 3 ppm K 20 ppm
22. ion spectroscopy Hitachi 139 type The condition of the equipment is as follows Acetylene flux 1 5 l min Air flux 7 0 l min Discharge tube ampere 15mA Slit width 0 2mm The calibration curve is not used exceeding 2 5 ppm Msg The disturbance effect of Si Al K and P was observed but it is removed with the addition of 1500 ppm Sr The aid of atomic absorption spectroscopy is effective in the analysis of Mg contained in soil and plants compared with the chelate titration method
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