F-Search System
Contents
1. E 101 1 2 F Search 2 3 F Search oe 3 3 1 Hi ra1 E ARON E is ai 3 3 1 1 ASA DE AC atada 3 3 1 2 1 18 3 3 1 3 2 0x 4 3 2 A A A aa 5 3 2 1 F Search2. 200V E GC 73 207 287 GC
3. MRC CAE RS UAB A 47 C MS 29 550 10 50 TIC Total lon Chromatogram
4. E Fab B MS EGA 1 1 10 MS EGA EGA MS 100 300KB GC MS EGA 1MB S N C
5. http www frontier lab com jp PYT 017E 018E 4 A1 A2 A3 A1 A2 A4 A1
6. 1992 1998 TG MS
7. A2 0 1 mm 2 A1 A4 A3
8. AS B MS 30 10 10
9. 21 Peak Assignment Polymerfadative Enyo rtf Rtrmel ww Gual 1 BisphendA Poly p phenylenes3 4 diphenylene ether terephthala P FL 114 2200 1400 228 89 2 Bisphenol A Palysulfone PSF P FL 132 2198 13 98 3 Bisphenol A Polyethersultone PESF P FL 135 2203 13 99 que 4 BA Bisphenol A Polyarylate PAR P FL 120 2202 14 00 5 BA Bisphenol 4 Polycarbonate mett method MM PC P FL 127 6 BA Bisphenol 4 Polycarbonate solution method SM PC P FL 128 99 7 BA Bisphenol A Polycarbonate thermally stabilized P FL 130 99 8 BA Bisphenol A Epoxy resin EP P FL 105 98 a RA Hisnhennl A Rismaleimide triazine resin AT resin PfFI 107 AA Le T T 10 11 12 T T T T T T T T ky 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 i rma 17 18 19 20 21 22 23 24 25 26 27 28 29 30 13 A 1 1 13 ge EE A 5 AA HE Bisphenol 4 Poly p phenylene 3 4 diphenylene ether terephthala PCFL 1
10. EGA PFTBA Perfluorotributylamine 44 7 Py GC MS 7 1 Py GC MS Py GC MS 7 1 600C GC splisplitless 1 10 17100
11. Delete Insertl 26 PyGC MS Make INT SUM Mass Spectrum INT SUM OK INT SUM Chromatographic Peaks Chromatogram Peaktt 6 5 658 0 217 Abundance Top 7 800 0 142 7000000 7 975 0 183 6000000 9 750 0 125 9 908 0 100 1 E 5000000 E Delete 4000000 11 650 0 133 11 567 11 700 BB 12 975 0 200 12 842 13 042 BB 3000000 13108 0 108 13 042 13150 BB 2000000 13 233 0125 13 150 13 275 BB 14 467 0 117 14 417 14 533 BB TORON Start End 14 583 0 092 14 533 14 625 BB 0 14 700 0117 14625 14742 BB 11 40 1150 11 60 15 858 0175 15 750 15 925 BB Time min
12. 5 24 ADD MS 8 41 003 D F Search File View PyGC MS EGA MS Library Options Help AA AAA Aa Search Unknown Mass Spectrum of A1 003 D 10 171 min 2 100 80 6 20 41 B7 77 91 115 128 145 154 177 189 er miz O 50 100 150 200 250 Reference of 4 Methyl 2 6 di ter butyiphenol BHT Dibutyitin maleate polymer 8 1 80 60 20 a Sr 91 115 128 195 1 177 220 0 a de a a 4 A L miz gt O 50 100 150 200 250 view Arint MS Spectrum Displayed Results Print E Chromatogram Thermogram Top 5 Hits _ gm copy _ use Reference Records Details 1 4 Methyl 2 6 di ter butyl Dibutyltin maleate polymer D 49 110 2 4 Methyl 2 6 di ter butyl Dibutylin bis butyl maleate D 43 120 1520 10 14 220 3 4 Methyl 2 6 di ter butyl 2 5 Di ter butyl 4 methylphenol Butyl hydro 4 1 003 1484 10 18 220 4 4 Methyl 2 6 di ter butyl Dibutyltin dimaleate D 4 1 nn 1522 10 15 220 5 4 Methyl 2 6 di ter butyl Cyclicneopentane tetrayl bis 2 6 di ter butyl 4 2 093 1525 10 63 220
13. 14 5 1 3 BESAN KILIT Y PROCESAN 5 1 4 5 1 5 5 1 3 5 1 4 A
14. GC splisplitless 17100 GC MS 600 C 400 C 340 C He Ultra ALLOY 5 MS HT 30 m 0 25 mm id PpP Vent free GC MS MS 9 1 Py GC MS 52 9 2 ADD MS 8 2 1 ADD MS F Search PyGC MS NIST Wiley MS MS TIC
15. F Search EGA MS14B PyGC MS14B ADD MS13B Pyrolyzate MS13B Py GC MS Py GC MG ADD MS13B PY 1114E 131 600C 600C
16. 4 EGA 300C MS 200C 43 EGA C4 MS
17. PFTBA Perfluorotributylamine 49 8 THM GC MS 8 1 THM GC MS THM GC MS 8 1 400C GC splisplitless 1 10 17100 MS 400 C as
18. 48 7 2 21 5 69 21 5min 81 ar 55 100 200 m z 5 10 15 20 min 7 2 F Py GC MS GC GCC MS
19. GC PY MS MS C1 GC C2 GC 1 8 6 UY C3 EGAF ETU F1 TD5 R MS EGA 2 5 m 0 15 mm
20. F1 GC TF TEO F2 GC GC GC 30 cm 17 8 6 F3 MS
21. F gt earch selected library Program Files HFoearch L ib El 5 51 k ls not avallable because the version ie 17 5 rg vou sure that vou convert this library to 47 97 Select Library Type x Save irc a Lib 0am Select library type i PyChro C EGA cancel mo MET Save as type Frcemer Lab Library M X Cancel a Library Select ILbrary for Search EGA Int Sum Compound Select Library for Search Frontier Lab s Library 1 13 EGA 3 Z 40D MS088 1 M Pyrolyzate MSO9B fl as iak Int Sum Compound 7 EGA MS 2 fl i PyChro MS 2 fl fl 1 1 3 a Aj aj Aa cee o lt Remove
22. 10 29 lt MENTIRA 28 32 10 50 CO02 550 D MS GCIMS
23. MS 600 C Ultra ALLOY 5 MS HT 30 m 0 25 mm id He Vent free GC MS MS 7 1 Py GC MS 7 2 PyGC MS Pyrolyzate MS PyGC MS Pyrolyzate MS 7 2 1 PyGC MS Integration Summation INT SUM
24. 5 1 4 5 25 Pyrolyzate MS IEN EPDM D F Search File View PyGC MS EGA MS Library Options Help AA AE aa Search Unknown Mass Spectrum of EPDM D 6 733 min x 3 100 80 70 6 83 T A SL 111 140 miz O 50 100 150 Reference of 1 Decene CH2 CH CH2 7CH3 Polyethylene high density PE HDPE 26 Ei 60 40 29 83 97 111 f L 140 miz O 50 100 150 r view FI rint MS Spectrum Displayed Results Tm rint C Chromatogram Thermogram C Top 5 Hits Copy _ ose P FL 004 1 2 eS 3 C10 1 Decene CH2 CH Polyethylene ionomer lO PCFL 009 4 c10 1 Decene CH2 CH Ethylene propylene diene rubber EPDM PCFL 003 5 C10 1 Decene CH2 CHC Polyundecanoamide nylan 11 P FL 083 6 C10 1 Decene CH2 CH Novon P FL 165 7 c10 1 Dece
25. PcID Serial Number cs frontier lab com FAX 024 935 5102 024 935 5100 3 4 B OK 3 5 Protectine PF Search ls now protected Pleaze let Frontier Lab know Pell to get password to Use this system Pell 21215151100259501 0025954001 61 732ED60 Pleaze enter password Pa ww T A PcID 3 4 Ief No data is loaded F Search File View PyGC MS EGA MS Library Options Help SAA A EE El mE Ready EDIT LIB Not selected NUM 2 3 5 F Search 3 2 2 PY 1110E 141 PY 1111E 141 PC F Search Uninstall
26. EGA MS 1 2 3 PyGC MS5 C1 C10 C1 C20 C1 C40 3 INT SUM A EGA analysis 36 b 78 250 700 C averaged 1 91 128 mass spectrum i a 6 dl 100 200 300 400 500 600 700 C 50 100 150 200 250 m z B Py GC analysis 36 HCI 4 0 Ce Benzene 78 Toluene Naphthalene 51 91 128 7 T 7 T T N ih NN a 5 10 15 min 50 100 150
27. F Search 3 1 I 5 1 12 PyChro EGA EGA F Searcn 5 1 12
28. 40 6 2 1 A 3 E RS Wi GC MS ITF B PY PY GC ITF GC GCI Am GC GC MS ITF MS AE EGA PY 3030D GC MS EGA 2 5 m 0 15 mm P N UADTM 2 5N 0 1 0 3 mg LF 80 ul P N PY1 EC80P 100 20C min 700C 300C 300C 300C 280C Helium 1 50 1 ml min m z 29 550 6 0 13 scan S N
29. IR F Search 3 2 3 PY 1112E 141 PY 1113E 141 PY 1114E 131 PY 1115E 131 CD ROM CD ROM F Search Lipb 3 2 4 PY 1112E 141 PY 1113E 141 PY 1114E 131 PY 1115E 131 4 F Search 4 1 EGA Py GC 4 1 1 Evolved Gas Analysis E
30. OK Library Edit Library Header 29 5 6 2 2 Name UserLibrary Path C Program FilesiFSearchiLibWiserLibrar 5 26 EGA MS EGA MS 5 2 03 YN o Library Add New Entry EGA MS a 2 5 27 b Advancedd Edit Defaull 5 28 EGA Analytical Method Direct EGA MS
31. 36 Retention Index Scan Time Misc Information 5 6 6 0 5 I 5 Library Edit Existing Entry View Existing Entry 5 36 1 GC Entries Compound 2 INT SUM Entrtesl Int Sum Edit Advanced hS Edit Default
32. b Y 3 1 1 13 3 1 3 2 0x 2 0x F Search 3 2 F Search 5 1 12 EGA PyGC Additive 2 F Search C Program Files FSearch Lib 5 1 2 F Search F Search Selected library Program FileskFSearch libkEGA MS06 fl
33. Viewl Mass Chromatograms 5 6 6 5 7 TIC TIC Viewl TIC 100 X Axis Display Range Erom min Whole mY Scaling Scale each plot to the largest peak in that plot 16 Y 5 6 Pe Yon paces EGA MS Library Options Hep Sw w imel DOG IBEGE MS
34. Cut intensity ratio lt 3 X Axis Display Range Erom 2 45 m Y Axi ling Scale each plot to the largest peak in that plot on To 5 8 17 2 7 r9040102 D F Search File View PyGC MS EGA MS Libr ry Options Help AMES MERA EA ro a igg TIC bn TIC TY90401 q mz Em El Acetic acid 55 B 44 a c enzene 44 20 40 60 80 m z b c O Acetic acid 98 MS gt 20 40 60 80 m z c a Benzene 98 O MS 40 60 80 a b Pyrolyzates MS 5 9 2 5 1 12 Z TIC View Overlayed TIC MS 5 10 a 5 10 b
35. GC MS Py GC MS GC MS TD GC MS MS 0 1 Py GC MS Py GC MS TD GC MS 9 1 9 2
36. 5 418 o Library Add New Entry N 5 27 a m Synonyms Ethyl 701 Ethyl Corp lonox 99 Shell MP 37 C 5 33 Py GC MS X 5 5 Py GC MS 9999 10000 0 5 5 RU DEEE Y 31 TOO NOE R 2 5 27 b Advancedl
37. 200 Autotune 41 6 2 2 EGA MS 0 1 mg mg
38. MS ADD MS Retention Index RI 1 R 100 9 2 1 Py GC MS TD GC MS A E gt EGA PY 3030D GC MS GC MS Ultra ALLOY 5 5 diphenyldimethylpolysiloxane B
39. OK 5 6 6 Entry Information Pyrolyzate MS09B fl Polymer addtive Acrylonitrile EPDM styrene copolymer AES IV Include in search Compound 4 Phenylpent 4 enenitrile hybrid dimer C C Ph C C CN Ref No 11332 Mol Formula C11H11N Mol eight 157 Entry ID P FL n26 Peak ID SA Retention Index 1422 Ret Time Miscellaneous Information Advanced gt gt OK 5 35 Py GC MS 9 800 min R 5 6 Py GC MS Polymer Additive Compound Mol Formula Mol Weight DIE 9999 Entry ID Peak ID Ref No 10000 Include in search
40. 5 6 2 5 6 3 Deletel E EPDM D F Search File View PyGC MS EGA MS Library Options Help Sa AE E Ea Edit Library Entries Int Sum 0 Hide Assignment Col Chromatogram Thermogram Compound 2993 Ret P Assignment Potymersadaitive Enyp 100 11456 B 1 Butene CH2 Acrylonitrile acr P FLI 025 11320 A Acrylonitrile Acrylonitrile acr P FL 025 80 11457 BO n Butanol Acrylonitrile acr P FLI 025 11458 T Toluene Acrylonitrile acr P FLI 025 211321 S Styrene Acrylonitrile acr P FL 025 60 11459 al alpha Methylsty Acrylonitrile acr P FL 25 11460 AA 2 Methylenepen Acrylonitrile acr P FL 025 11322 AS 2 Methylene 4 Acrylonitrile acr P FL 025 40 11323 SA 4 Phenylpent 4 Acrylonitrile acr P FL 025 211461 SA 4 Phenylpentan Acrylonitrile acr P FL 025 11324 SS 3 Butene 1 3 di Acrylonitrile acr P FL 025 20 11462 A 2 Methylene 4 Acrylonitrile acr P FL 025 11325 A 2 Methylene 4 Acrylonitrile acr P FL 025 11326 A 2 Methylene 4 Acrylonitrile acr P FL 025 0 11327 S 4 6 Diphenylhe Acrylonitrile acr P FL 025 0 10 20
41. GC MS OK 5 6 6 5 29 Calcl 5 3 OK 5 6 6 30 Advanced 9 y 9 a EGA MS b 1
42. 5 4 Options Color Defaulll Colors of Chromato Chart Labels of Spectrum Ghart Sample Colors M a ass Labels TIC and Mass chromatogram Id i E e Show Labels for Major Spectrum Peaks 100 Background ma T por Sp 0 Profile E Offset fo 00 05 10 15 Hilight B Set to Defaut Cancel 5 4 BIE 5 5 5 21 5 5 Options Peak Label ON OFF Offsetll 5 1 10
43. View Merged Format TIC A2115 OSD FS 1310144 TIC A 2I115 4D F S 1310144 TIC A 2115_05 D F S 1310144 TIC 4 21115_03D F S 1310144 0 Ll fa in gt 16 16 4 16 8 17 2 17 6 18 TIC 4 2115_04 D F S 1310144 0 in gt 16 16 4 16 8 17 2 17 65 18 1100 TIC 4 21115_05 D F S 1310144 O lo fa n267 1569 1571 1573 1575 15 77 1579 in gt 16 16 4 16 8 Lr 17 6 18 a TIC b TIC 5 10 5 1 13 18 File Subtract Background MS
44. EGA MS Make Mass Spectrum 5 17 A B C OK 5 1 4 A Make Snectrum From min 18 oK To min 26 Background min 17 5 B C 5 17 EGA MS Search 5 18 5 1 3 24 62 PE D F Search File View PyGC MS EGA MS Library Options Help SL E REGA EE TIC Search Unknown Chromatogram Thermogram of PE D 18 348 to 20 114 min 2 100 n min O 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 R
45. EGA Py GC PVC PVAc PVA EGA 2 Py GC 10 2 EGA PVC EGA
46. PC autoimp msd 39 6 6 1 EGA 6 1 spliYsplitless 1 50 300C EGA MS 100 700 C EGA Ultra ALLOY DTM 2 5 m 0 15 mm id He Vent free GC MS MS N GC 300 C 6 1 EGA 6 2 EGA MS EGA MS 6 2 1
47. MS MS F Search View Mass Chromatograms B2 EGA 20 54 L 1 2 7 99 GIIGW EBINRRRRERERSEHESRRRRRSRRSERGSRRS3 32 34 35 AVANT Nana dana aan 23 30 32 34 35 37 COMPOLNd ana AN
48. 70 lscarr 25611005 time 4922 8743 min EDIT HB Pyrolyzate MSO98H 5 7 5 1 11 2 mz Viewl Mass Chromatograms 5 8 TIC 5 9 2 57 100
49. PyGC MS14B 390 ADD MS13B MS 358 600 70 400C Pyrolyzate MS13B 165 33 TMAH 38013
50. SB File Subtract lons 6 m z MS SB TIC 22 P GS 374 S2D F S 927389 0 8 1 12 14 16 1 8 2 22 24 26 32 TIC 022 P 6S 374 S2 1 bsd F S 869207 m z gt 0 8 1 12 14 16 18 2 22 24 26 5 11 TIC 5 1 14 5 1 5 2 EGA 5 2 Int Sum 5 3 Compound 5 4 3 F Search
51. EGA 11 PHPy GOA TIA B10 UBA CHARLA CAD ARUC ELO GC EGA 10 20C min Py GC 600C 20msec 1 800 000C min EGA Py GC EGA Py GC PMMA PTFE
52. He Ultra ALLOY 5 MS HT 30 m 0 25 mm id Vent free GC MS MS 8 1 Py GC MS 8 2 PyGC MS Pyrolyzate MS PyGC MS Pyrolyzate MS 7 2 1 PyGC MS5 Integration Summation INT SUM 50 8 2 1 PyGC MS A E rB RE T GC MS B C PY Mae PY GC ITF
53. Copyj 2 5 1 19 Detailsj 5 15 Polymer Additive 2 5 Di ter butyl 4 N N dimethylaminomethyphenol IZ Include in search Compound Dimethylamine RefNo 10060 Mol Formula C2H7N Mol WWeight 45 06 Entry ID 401 050 Peak ID A 4 Retention Index 1 Ret Time 1 570 min ddd Miscellaneous Additive Synonyms Ethanox 7O3CEthyl Corp MP 94 C Information Pyrolyzer PY 2020iD Analytical Method Pyrolysis GCMS Sample Amount 003 mg Sample Heating Program GC Oven Temp Program nt Temp Init Time Rate Final Temp Final Time Int Temp Init Time Rate Final Temp Final Time C min Cimin C min C min Cimin min 600 D 0 O 0 40 2 20 320 14 0 B q Heated Zone C Column Carrier Gas Detector PY GC ITF 320 Name Ultra ALLOY S MS HT Name He Mass Range 29 to GC Injector 320 Len
54. A Py GC MS 0 1 mg 46 4 A1 A2 AS3 A1 A2 A1
55. 4 50 A Py GC B A B 4 5 A EGA 400C 2 HN 4 5 B Py GC EGA Py GC EGA MS PyGC MS
56. TIC TIC MS MS O B 0 1 B1 Py GC MS
57. Edit Default 5 34 GC MS OK 5 6 6 35 Edit Header Defaults Pyralyzer Py 2020p Analytical Method Pyrolysis GCMS Sample Amount 0 03 mg Sample Heating Program GC Oven Temp Program Int Temp Init Time Rate Final Temp Final Time Int Temp Init Time Rate Final Temp Final Time min Cimin min min Cmin min a a a ao o o gt m j HE HE m Heated Zone C Column Carrier Gas Detector PY GC ITF 320 Name Lltra ALLOY S MS HT w Name He X Mass Range 29 Ma GC Injector 320 Length 30 m Inlet Pressure 34 kPa 800 amu GCMS ITF 280 Column Flow 1 mimin Split Ratio 1 100 Miscellaneous Information ome 5 34 Py GC MSRIERIFODA D Inner Diameter 0 25 mm Scan Speed 2000 amu sec Detector 230 Film Thickness 0 25 um 5 35 5 6
58. EGA MS14B 700 PyGC MS14B 733 ADD MS13B 428 Pyrolyzate MS13B 198 RS CD ROM 1 PC Microsoft Windows 8 32 64bit 7 32 64bit Vista 32 64bit XP HD 200MB MS Agilent ChemStation HAS MS NetCDF AIA 2 3 F Search 3 1 3 1 1 F Search Ver 3 4 PY 1110E U14x PY 1111E U14x F Search fl 3 1 2 1 13 1 13
59. PY 1110E 141 PY 1111E 141 5 3 2 2 PY 1110E 141 PY 1111E 141 7 3 2 3 PY 1112E 141 PY 1113E 141 PY 1114E 131 A a E 7 3 2 4 PY 1112E 141 PY 1113E 141 PY1114E 131 PY 1115E 1931 RR kk 7 4 F Search MMi 8 4 1 EGA Py GC 8 4 1 1 A T e E E EE A 8 4 1 2 A EIA A FIDA E A A ei A ida 8 4 2 8 4 2 1 7 A EA A 8 II A A A E ESS 8 4 3 F Search 8 4 3 1 MIS AMD AAA O ata did dios 8 4 3 2 EGAMSIAB SA 2 NN 8 4 3 3 PYECMSIABS TTD US a Ai ii 9 4 3 4 ADO MSISB 217 TS RR 10 4 3 5 Purolyzate MS13B 11 4 4 EGA MS Py GC MS 11 E o MEA A A A 14 5 1 F Search i 14 5 1 1 MS 14 5 1 2 5 1 3 5 1 4 5 1 5 5 1 6 9 1 7 5 1 8 5 1 9 5 1 5 1 5 1 5 1 5 1 5 1 5 1 5 1 5 2 5 3 5 4 5 5 5
60. C Mol Weight 9999 Retention Index 0 4 3 4 ADD MS13B ADD MS13B 4 3 10 4 3 ADD MS13B 4 3 5 Pyrolyzate MS13B Pyrolyzate MS13B 4 4 o 4 4 Pyrolyzate MS13B 4 4 EGA MS Py GC MS
61. 5 12 20 EGA Int Sum Compound EGA Int Sum Compound Ief No data is loaded F Search File View PyGC MS EGA MS Library Optid EAN EA ME mol 5 13 5 1 15 5 2 5 5 5 14 Search Quality Qual 100
62. 5 27 gt rafeAvs yl TRARRE penea e fe zl E E x em 5 28 EGA 31 Entry Information EGA MS06 fl Polymer i AdgWive Acrylonitrile styrene copolymer AS V Include in search RefNo 10022 Compound Mol Formula CH2CH CN Jm CH2CH Mol Weight 9999 Entry ID P FL 022 Retention Index 0 Ret Time min Start 12 700 Top 15 758 End 17 700 Temp C Start 354 Top 415 End 454 Calc Miscellaneous Information 5 29 5 3 EGA Polymer Additive Mol Formula Mol Weight S 9999 Entry ID Peak ID Ref No 10000 Include in search Retention Index Ret Time Temp Misc Information EGA 0
63. A2 0 1 mm 2 A1 A4 A3 42 AS
64. 4 3 3 PyGC MS14B PyGC MS14B C1 C10 C1 C20 C 1 C40 INT SUM INT SUM 4 2 Entry Information PyGCG MSOD6B f x Eyere vm acon copolymer Pev cereo O 0005 rcracz mtoocol o Engo roos a E 0 a a E CAS No 25067 34 9 4 2 PyGC MS14B A C1 C40 INT SUM B Entry ID FLT GC MS PY GC
65. B PyGC MS Subtracl EGA MS Subtractll A E B PyGC MS EGA MS 5 1 6 MS 5 3 Viewl Mass Table Scan 4529 38 742 min PYT0012 D a Base Peak Intensity 31776 miz Intensity 5 3 MS 5 1 7 File Printl TIC 5 1 8 File Copyl Power 15 Point 5 1 9
66. Re 5 6 3 INT SUM O Py GC MS INT SUM E 5 3 Library Add New Entry 5 27 a 2 E 5 27 b Advanced Edit Default 5 30 GC MS OK 5 6 6
67. earch File View io EGA MS Library Options Help Sil E EL EL TIG TIC PED F S 1611010 100 ari 90 80 13809 433 17 53 7 37 9 58 12 92 k 8 02 ds 1 836 8 58 3 16 60 8 90 0 54 e 19 97 50 pe 20 85 40 2 26 2189 20 23 13 3 44 431 7A 20 E a pg Fiia 4 5 pe 56 S A i Ml LT LA HI OS 1 23 A 5 5 7 8 9 IRead E of detected peaks 61 EDIT LIB Pyrolyzate MSO09B fl NUM Y 5 21 5 19 Addd Savel Loadd 5 21 OK PyGC MS List Results 5 22
68. emen 5 22 INT SUM Y PyGC MS Search 5 23 5 1 3 File View PyGC MS EG MS Library Options Help AAA AE AAA Search Unknown Mass Spectrum of PE D 0 094 to 30 000 min 3 100 43 E 69 83 az 40 111 a 125 139 453 168 182 196 211224236 250 264 278 292 306 320 334 348 362 199 miz O 50 100 150 200 250 300 350 400 450 Reference of Polyethylene high density PE HDPE C1 C40 21100 ha En 69 83 y 40 111 z0 125 139 153 168 182 196207 224236 250 264 278 292 306 320 334348 362 390 404 418 949 miz 50 100 150 200 250 300 350 400 450 view Print MS Spectrum Displayed Results Print e Chromatogram Thermogram C Top 5 Hits oemt Copy _ goss Reference Records Details 1 Polyethylene high density PE HDPE C1 C40 P FL 0C 2 Novon C1 C40 P FL 1E 3 Polyethylene ionomer IO C1 C40 PCFL OC 4 Ethylene ethyl acrylate copolymer P CE EA C1 C4 PCFL OC 5 Ethylene methyl methacrylate co
69. 32 o Edit Header Defaults Pyrolyzer Py 2020p Analytical Method Pyrolysis GCMS Sample Amount 0 2 mg Sample Heating Program GC Oven Temp Program Int Temp Init Time Rate Final Temp Final Time Int Temp Init Time Rate Final Temp Final Time min Cimin C min C min Cimin C min o K E e e za r m Heated Zone C Column PY GC ITF 320 Name Utra ALLOY 5 MS HT Name He Mass Range 29 to Inlet Pressure 34 kPa 800 amu Column Flow 1 mlmin Split Ratio 1 100 2E alla GC Injector 320 Length 30 m GCMS ITF 280 Inner Diameter 0 25 mm Film Thickness 0 25 um Miscellaneous Information Scan Speed 2000 amufsec Detector 230 cera 5 30 _Py GC MS N 5 31 R 5 4 OK 5 6 6 Entry Information PyGG MSUGB fl Polymer additive Polystyrene PS 01 010 Y Include in search Ref No 10
70. C Program Files FSearch Lip F Search Library Select Libraries for Search 5 12 5 13 EGA Int Sum EGA MS GC MS Py GC MS GC MS THM GC MS GC MS Py GC MS GC MS THM GC MS GC MS Py GC MS GC MS TD GC MS EGA Int Sum Compound EGA Frontier Lab s Library EGA C EGA MS13B fl I PYGC MS13B fl ADD MS
71. 30 m 0 25 mm BE 0 25 um P N UA5 MS HT 30M 0 25F MS HT 0 03 mg ds Sa E a san y a o e LE 80 ul P N PY1 EC80F o C PY e 600C Ala 400C 340C PY GC ITF 300C 93 RI MS calas GC GC 40C 2min 320 20 min 14 min GC 300C GC MS ITF 2800 Helium 1 100 DIAM 1 ml min MS m z 29 550 2 3 scan 200 Autotune 200V 9 2 2 A ADD MS13
72. 7 2 1 PyGC MS A pa IANN MRS E Ja YFA ld EGA PY 3030D Wi 45 GC MS B GC MS Ultra ALLOY 5 5 diphenyldimethylpolysiloxane 30 m 0 25 mm E 0 25 um MS HT P N UA5 MS HT 30M 0 25F 0 1 mg SAN DAMA 6 2 2 LF 80 ul P N PY1 EC80F TASAS C PY 600C PY GC ITF 300 C GC GC 40C 2min 320C 20 min 14 min GC 300 C GC MS ITF 280C Helium 1 100 1 ml min MS m z 29 550 2 3 scan 200 Autotune 200V 7 2 2
73. GC GC GC GC MS ITF AP IER MS w EGA PY 3030D GC MS Ultra ALLOY 5 5 diphenyldimethylpolysiloxane 30 m 0 25 mm JS 0 25 um MS HT P N UA5 MS HT 30M 0 25F 0 1 mg DAYA 6 2 2 LF 80 ul P N PY1 EC80F 400C 300C 40C 2min 320C 20C min 14 min 300C 280C Helium 1 100 1 ml min m z 29550 2 3 scan 200 Autotune 200V 51 9 Py GC MS 9 1 Py GC MS ADD MS
74. F Search MS Evolved Gas Analysis EGA Pyrolysis Gas Chromatography Py GC ARI RJJ FIC dJ EGA Py GC EGA EGA MS14B
75. F Search PY 1110E 141 PY 1111E 141 CD ROM F Search CD ROM F Search F Search E 3 4 3 4 B http www frontier lab com pp 3 4 A PcID CD Serial Number F Search E
76. 6 2 5 Di ter butyl 4 methyl 2 6 Di ter butyl 4 methylphenol W1 018 1526 10 26 220 7 4 Methyl 2 6 di ter butyl 1 1 3 Tris 2 methyl 4 3 3 5 di ter butyl 4 h 4 1 322 1526 10 24 220 3 2 4 Di ter butyl 6 methyl Tetrakis 2 4 di ter butyl 5 methylpheny 4 4 4 2 305 1651 11 31 220 3 2 4 Di ter butyl 6 methyl Organic phosphate complex O 3 800 1573 11 45 220 10 2 6 Di ter 4 methylphenol Tetrakis 2 4 di ter butyl 5 methylphenyl 4 4 4 2 305 1670 11 41 220 11 1 2 4 6 Triisopropylphenol 2 6 Di ter butyl 4 methylphenol Butyl hydro 4 1 003 1504 10 34 220 12 Unknown Cyoclicneopentane tetrayl bis 2 6 di ter butyl 4 2 093 1552 10 79 220 13 2 5 Di ter butyl 1 4 benz 2 5 Di ter butylhydroquinone WU1 31 1454 9 99 220 5 24 Py GC MS Pyrolyzate MS MS Pyrolyzate MS13B f 28 5 1 3
77. Polymer MS_List pdf 4 2 2 358 C Program files Fsearch List ADD MS _List pdf 4 3 F Searchn 4 3 1 GC MS 4 3 2 EGA MS14B EGA MS14B EGA 4 1 Entry Information EGA MS06Bf Polymer Additive Polyethylene ionomer 10 A noludeinsearch Compound E a Ref No 10009 Mol Formula Structure see atachmer MojWWeight 9999 E
78. 200 250 m z 45 PVC EGA Py GC 13 5 F Search 5 1 F Search 5 1 1 MS 5 1 Optionsj MS Data Type Agilent UEOL Shimadzu NetCDF ERE O DED F Search File View PyGC MS EGA MS Library Options Help EN HR ER lor kE T a e u A LEJE RE EE Ms Data Type 51 5 2 File Load MS OK SR PED F Searct Eie View PyGO MS EGA MS Library i mw Options He AAA Aa 5 2 _ MS 5 1 2
79. 30 11328 S 2 Phenethyl 4 p Acrylonitrile acr P FL 025 Time min 11463 S 5 Hexene 1 3 5 Acrylonitrile acr P FL 025 11329 A Acrylonitrile Acrylonitrile EP P FL 026 Spectrum RT 9 800 11464 T Toluene Acrylonitrile EP P FL 026 11330 S Styrene Acrylonitrile EP P FL 026 100 11465 al alpha Methylsty Acrylonitrile EP PCFL 026 11466 AA 2 Methylenepen Acrylonitrile EP P FL 026 211331 AS 2 Methylene 4 Acrylonitrile EP P FL 026 80 2 SA 4 Phenylpent 4 11333 SA 4 Phenylpentan Acrylonitrile EP P FL 026 11334 SS 3 Butene 1 3 di Acrylonitrile EP P FL 026 60 11335 A 2 Methylene 4 Acrylonitrile EP P FL 026 11336 A 2 Methylene 4 Acrylonitrile EP P FL 026 11337 S 2 2 Phenylallyl Acrylonitrile EP P FL 026 40 1133A A Dhdethslene 4 Arrylaonitrile FP PrFI y Entry Info 11332 Measured 2006 07 06 11 25 00 Data Path 0 Delete Edit Close 50 100 150 m z Ready E EDIT LIB Pyrolyzate MSD9BAI DO INUM y 5 36 37 5 7 5 7 1 Library Password Pr
80. INT SUM ANA A O rn 32 epa as a ME O a ID E IAE MUI 34 NOS D ANO A REZA O DANDO oia 35 a Ao 37 a aaa a 38 AE A E E E A E EET 38 38 5 8 NIST nn nnnnnnn anna 38 EII SO 40 6 1 KEDAI EDITE toto 40 6 2 EGAMS 242 II 0O MER ti o a 40 6 2 1 EA IEO Er F aaas 41 6 2 2 2 42 B F PrGC MS A 45 7 1 Py GC MS ki 45 7 2 PyGC MS Pyrolyzate MS LL 45 7 2 1 PES MS AD PIE FEI oran Eo 45 7 2 2 A Os A 46 32 TEM CGOMSA RDA SDE TN 50 8 1 THM GC MS A0 it sia 50 8 2 PyGC MS Pyrolyzate MS 50 8 2 1 PIES MS AD MES es o ei 51 Poa PyGO MISA RDA AE Ga a 52 9 1 Py GC MS kk 52 9 2 ADD MS Ri 53 9 2 1 Py GC MS TD GC MS MMM 53 9 2 2 coccion 54 215 F Search
81. 015 LcH2cHPh n Mol eight 9999 Entry ID Pero 016 Peak ID Retention Index O Scan Time min Start 0 097 End 7 000 Compound Mol Formula Miscellaneous Information 5 4 Py GC IMST7 IDD05S5G Polymer Additive Mol Formula Mol Weight Entry ID Peak ID Ref No Include in search Retention Index Scan Time Misc Information CAS No 9003 53 6 5 31 Py GC MS DFE 9999 10000 0 33 5 6 4 0 Py GC GC MS 5 4 Library Add New
82. 138 1l Pyrolyzate MS13B fl Select Library for Searc 5 1 EGA SITUAR EGA MS14B fl Int Sum SDF PyGC MS14B f Int Sum PyGC MS14B f Compound Pyrolyzate MS13B fl en Compound Pyrolyzate MS13B fl Compound ADD MS13B f Compound ADD MS13B f 5 2 EGA Int Sum Int Sum Compound h Pyrogram Polymer Search Compound pa Eira Pyrogram Polymer Search Compound user1 1 yA owen Remove
83. 14 2200 14 00 Bisphenol A Palysulfone PSF P FL 132 2198 13 98 Bisphenol A Polyethersulfone PESF PCFL 135 2203 lass 2 Bisphenol A Polyarylate PAR P FL 120 2202 14 00 228 Bisphenol 4 Polycarbonate melt method MM PC P FL 127 14 00 Bisphenol 4 Polycarbonate solution method SM PC P FL 128 ud 14 15 18 Bisphenol 4 Polycarbonate thermally stabilized P FL 130 BA Bisphenol 4 Epoxy resin EP P FL 1n5 BA Bisphenol A Bismaleimide triazine resin BT resin P FL 107 I Inidertifieri Palvfether ether ketanei PEFK PrFI 113A 5 14 5 1 16 Displayed Results l Print 2 22 5 1 17 Top 5 Hits Prinl 1 5 5 5 1 18
84. 55 E 6444979 B1 2 F Search 700 EGA MS 700 PyGC MS 33 165 Pyrolyzate MS 33 Pyrolysis GC MS Data Book of Synthetic Polymers Pyrograms Thermograms and MS of Pyrolyzates TSUGE Shin OHTANI Hajime WATANABE Chuichi 2011 ADD MS 3581237 70 400 94 95 ME 1994 GC MS EGA MS14B 1381 PyGC MS14B 2014 ADD MS13B 3370 Pyrolyzate MS13B 3173
85. 6 10 dl 12 13 Dl 15 16 17 18 19 9 6 1 9 6 2 9 6 3 9 6 4 9 6 0 9 6 6 5 7 5 7 1 9 7 2 TRAIN RE Se GS 14 AI A A E AEE 15 15 A AA Rk ER 15 SS VOR NN ki 15 IATA EE ISO OE lao 15 SA e ASA IA AD E a aai 15 16 Er ER DOI ta 16 2 EE E A R 17 ESE A IN RR Po 18 JOY ETA DOE DS P UI A 18 Pp A A A ETE 19 A A E E PE E TETE 21 ro E EEN A A 22 BeF Aa aaa Ai 23 a DY INSI DER ai is dd 23 a AE E E E A kc 23 EGA MS uuu 23 PyGC MS 25 ADD MS 27 Pyrolyzate MS 28 29 2a P TO SODA EM dd 29 EGAMSS JI TDT IDAS OR a a T 30
86. EGA 5 18 EGA 5 3 PyGC MS Py GC MS PyGC MS14B fl PyGC MS Detect Peaks E 5 19 Py GC 2 9 0 04 min xi M Global Settings Retention Time Range Min Intensity 2 21 From 0 088 fmin Peak Width 0 04 min To 99 998 min Time Event Start min End min Detection Min Inetensity Peak wicthlmin 5 19 25 Start Time min 1 End Time min sz Cancel V Detect Peaks Min Intensity 96 Peak Width min 0 04 5 20
87. Entry 5 27 a 2 5 27 b Advancedd Edit Default 5 32 Py GC MS GC MS OK 5 6 6 Edit Header Defaults Pyrolyzer Py 2020p Analytical Method Pyrolysis GCMS Sample Amount 0 03 ma Sample Heating Program GC Oven Temp Program Int Temp Init Time Rate Final Temp Final Time Int Temp Init Time Rate Final Temp Final Time min C min min min C min min o _B A A A a Pa m j
88. F Search System All in One PY 1110E 141 O FRONTIER LAB Mrina 2013 Frontier Laboratories Ltd sm F Search All in One PY 1110E 141 Somo E F Search Ver 3 4 PY 1111E 141 EGA MS14B PY 1112E 141 PyGC MS14B PY 1113E 141 ADD MS13B PY 1114E 131 Pyrolyzate MS13B PY 1115E 131 kkk 1 F Search 1 CD ROM PC2 3 Copyright Frontier Laboratories Ltd 2014
89. GA International Confederation for Thermal Analysis ICTA 4 1 2 Pyrolysis Gas Chromatography Py GC GC 400 800C He GC 4 2 4 2 1 700 C Program files Fsearch List PDF
90. N 37 o A A A 21 BGA DD e El o O O nn A A A 12 MS Tanatorio 2 NISTD So NN 38 A A A EEEE EE 16 O E E NO ERRE 43 44 47 48 49 E A A A A A A A 24 SR A A AA AAA AAA ARA 15 23 NON 15 16 18 O TE E EE E A 21 23 53 A E E E E A q A E O AE 15 24 PP a a a A A 45 PA o a a a A a a aaen 43 47 A A 43 49 8 15 17 18 24 43 48 A necio ledibdlc oddldidcol ici ddr li Osea 26 E A CI CAPO PE UA O E OR O E 10 11 12 15 24 28 29 30 32 48 SS A nn N 16 17 18 NS A E EE EEEE ON OT 16 NESO 9 10 12 27 32 37 45 50 56
91. ected Current Password Current Password Aii Wew Password MM Contirmm Per Password Apply Cloze 5 37 5 38 5 8 NIST PC NIST EPA NIH Mass Spectral Library National Institute of Standards and Technology 5 39 F Search 38 K Detect Peaks List Results w Make Mess spectrum 1 la Subtract Search 80 Search NIST 70 Em search Wew Tools Qptiora Window Heip 18 x C A E N 2 Propercic acid 2 methyt methyl este 5 Formata C5HeO2 MAL 100 CASA 80 62 46 METE 107749 IDE 746 Other Dos Fire TSCA RTEOS EPA HOODOO h Continmaor Chuck Anderson Aldrich Chemical C 10 largest penis 5 39 NIST NIST C NISTxx MSSEARCH autoimp msd Cannot start NIST NIST
92. eference of Polyethylene high density PE HDPE 21100 n min 1 2 3 4 5 7 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 6 8 MS Spectrum Displayed Results S mt Close Chromatogram Thermogram Top 5 Hits erre cuy cose Reference Records Polymer f Additive 3333 0 0 0 lgErtyp tri Toa Enarci auaf al 1 Polyethylene high density PE HDPE P FL n 1 436 456 534 99 2 Ethylene propylene diene rubber EDPM P FL 003 398 464 524 95 3 Ethylene acrylic acid copolymer P E 44 P FL 005 400 463 518 94 4 Novon 15 21 min P FL 165 412 473 520 94 5 Ethylene ethyl acrylate copolymer P E EA P FL 007 386 459 524 93 6 Hydrogenated natural rubber P FL 075 384 453 520 93 7 Ethylene propylene copolymer P E P P FL 002 408 464 528 92 8 Polyethylene onomer IO P FL 009 412 473 516 91 9 Polypropylene atactic at PP 1 21 min P FL 11 100 468 512 390 10 Ethylene yinyl acetate copolymer EW A 15 24 min P FL 006 396 450 604 90 11 Ethylene methyl methacrylate copolymer P E MMA4 P FL 004 388 461 520 89 12 Polypropylene atactic at PP 10 21 min P FL n11 300 4685 512 39 13 Polypropylene syndiotactic syn PP P FL 12 404 472 512 89 14 Polypropylene isotactic iso PP P FL 1n 404 466 506 87 1 Dalunranulanalatartii gt a DD f1 2 mimi DrFI A ni 1 ann IH San aT
93. gth 30 m Inlet Pressure 34 kPa 500 amu GCMS ITF 280 Inner Diameter 0 25 mm Column Flow 1 mlmin Scan Speed 2000 amu sec Detector 230 Film Thickness 0 25 um Split Ratio 1 100 5 15 Advanced A A B 5 2 EGA MS EGA EGA MS14B fl EGA MS Display Temperature 23 M 5 16 A D OK EGA Temperature gt Initial Temp C 100 Initial Timefmin fo B Rate Cmin 20 C Final Temp C FOO Cancel 5 16 MERT
94. m Heated Zone C Column Carrier Gas Detector PY GC ITF Name Utra ALLOY 5 MSHT y Name He y Mass Range 29 to GC Injector 320 Length 30 m Inlet Pressure 34 kPa 800 amu GCMS ITF 280 Inner Diameter 0 25 mm Column Flow EN ml min Scan Speed 2000 amu sec Detector 230 Film Thickness 0 25 um Split Ratio 1 100 Miscellaneous Information cono 5 32 Py GC MSRIERIFODA D RICA 5 33 5 5 OK 5 6 6 34 9 6 5 Entry Information ADD MS0SB fl Polymer Additive 2 6 Di ter butylphenol Y Include in search Compound 2 5 Di butylphenol Ref No 10009 hMol Formula C14H22O Mol Weight 206 17 Entry ID 213 001 Peak ID Retention Index 1455 Ret Time 9 908 min Miscellaneous Information Polymer Additive Compound Mol Formula Mol Weight Entry ID Peak ID Ref No Include in search Retention Index Scan Time Misc Information Py GC
95. ne CH2 CH Paly dadecamethylene adipamide nylon 12 6 PCFL 088 8 c10 1 Decene CH2 CH Chlarosulfonated polyethylene CSM P FL 055 3 C11 1 Undecene CH2 C Polyethylene high density PE HDPE P FL3 001 10 C11 1 Undecene CH2 C Paly dadecaimethylene adipamide nylon 12 6 P FL 088 11 C11 1 Undecene CH2 C Ethylene methyl methacrylate copolymer P CE P FL3 004 12 c10 1 Decene CH2 CH Ethylene winyl acetate copolymer EVA P FL3 006 13 C10 1 Decene CH2 CH Chlorinated polyethylene CM P FL n53 s 2 L 5 25 Py GC MS 5 6 5 6 1 Library Create Savel 5 26
96. ntey ID FLT 009 Retention Index o0 Ret Jeffin Start 15 600 Top 18 568 Endaf 20 800 Temp C Start 412 Top 473 End 516 Calc i OK Cancel B Pyrolyzer PY 2020iD Analytical Method DirectEGA MS Sample Amount 0 2 ma Sample Heating Program GC Oven Temp Program Int Temp Init Time Rate Final Temp Final Time Int Temp Init Time Rate Final Temp Final Time min Cimin min min Cimin min 100 0 20 700 0 30 0 0 0 0 0 0 0 0 0 Heated Zone C Column Carrier Gas Detector PY GC ITF 320 Name Ultra ALLOY DTM Name He Mass Range 29 to GC Injector 3on Length 25 m Inlet Pressure 50 kPa 550 amu GCMMS ITF 280 Inner Diameter 0 15 mm Column Flow 1 mimin Scan Speed 70 amu sec Detector 230 Film Thickness 0 um Split Ratio 1 50 Edit Default Print Y 4 1 EGA MS14B A Entry ID FLT GC MS PY GC B Mol Weight 9999 Retention Index 0
97. otection 5 37 5 38 New Password Confirm New Password Apply cs frontier lab com FAX 024 935 5102 024 935 5100 Current Password New Password Confirm New Password Applyj 5 7 2 5 38 Current Password New Password Confirm New Password Applyl Fassword Protection Password Protection Status Mot protected Status Frot
98. polymer P E MMA CC1 C40 PCFL OC 6 Ethylene yinyl acetate copolymer EY A CC1 C40 PCFL OC 7 Hydrogenated natural rubber C1 C40 PCFL 07 3 Ethylene acrylic acid copolymer P E 44 C01 C40 PCFL OC 9 Polybutene 1 isotactic C1 C40 P FL 01 10 Polyethylene high density PE HDPE C1 C20 P FL 0C 11 Polybutene 1 isotactic C1 C20 P FL 1 5 23 Py GC MS 5 4 ADD MS Py GC TD GC ES 27 5 5 Py GC MS ADD MS13B fl 5 1 3 5 1 4
99. xs is not available because the version is 11 8 Are you sure that you convert this library to 11 9 Library type EG4 MSO6 fl EGA C PyGC C Additive Cancel 3 2 2 0x 1 F Search F Search C Program Files FSearch Lib 2 F Search Library Select Libraries 3 3 Select Library for Search Frontier Lab s Library EGA Int Sum Compound A Fa PLP b mr Convert Lib to EGA Type Convert Lib to Comp Type EGA MS065 tl M2095 fl 3 3 3 2 3 2 1
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