生薬学講座 卒業実験報告書（2008 年度） 学籍番号 PC2005
Contents
1. i2. lt 2008 PC2005 022 7 ge gt S H19
3. gt 2008 PC2004 076 5 wiki
4. 2 10 PGB fr 4B 2763 mg 1X103 gmL fr 4B ODS TLC fr 2G fr 4B column 8 306 mg ODS MeOH HzO 8 1 MeOH HzO 15 1 Acetone MeOH 1 1 Acetone Me column 9 2350 mg 4B 5 fr 9A 282 mg 9B 110 mg 9C 1163 mg 9D 405 mg 9E 22 mg fr 9A 9D PGEs fr 9A fr9 B fr 9C 5X103 g mL fr 9C fr 4B
5. k LS 2008 PC2004 133 3 1 wiki 2 128 300 wiki 60
6. 19 7 TLC A 9C c1 fr 10D 9C c1 1H NMR 3C NMR minor 1H NMR TLC palmitic acid C16 0 oleic acid C18 1 A 92 palmitic acid oleic acid 10 1 1H NMR 9C c1
7. 9C c1 80 mg 9C c1 PGE2 1X X10 4g7mL fr 2H fr 10D 119 mg 9C c1 fr 10D 115 2008 PC2005 125 Polyrhachis dives 7 9C c1 fr 10D aii Polyrhachis res RSmith
8. 117 2008 PC2005 098 6 STY 1 9 wiki 20 6
9. Polyrhachis yes 6 2 4B Polyrhachis dives FSmith 19 dives AcOEt Pd ext 1 PG Ei E fr 2G 4 59g fr 2H 10 1 g fr 2G PG PGE fr 2G fr 4A 4D
10. linoleic acid C18 2 A9Z122 1 0X10 4g mL palmitoleic acid C16 1 A oleic acid C18 1 A 9 1 0X10 33g mL 9 cis 9 116 KS 2008 PC2005 014 4
11. 2008 PC2005 115 Polyrhachis reg 5 2H Polyrhachis res EBM Evidence Based Medicine 19 gyes AcOEt Pd ext 1 PQ Ei Rs 5 ffr 2H PGEz2 ODS small sc
12. 1 9 wiki 5 w i k i 3 5 0
13. 19 lt gt wiki lt H a i
14. 9C c1 GC MS palmitic acid oleic aeid fr 10D 1H NMR 18C NMR 9C c1 1H NMR 13C NMR 6 27 2ppm cis 2 cis TLC fr 10D palmitoleic acid C16 1 A929 minor myristic acid C14 0 fr 10D GC MS palmitoleic acid myristic acid PG 14 18 5 0 X105 g mL
15. 8 NK EN 119
16. ale column 6 1arge scale column 7 fr 7A 7F 6 ODS TLC MeOH HzO 8 1 small scale column 6 arge scale column 7 ff7A fr 7F PGE fr 7B 726 mg fr 7C 389 mg 3X104 mg7mL fr 7B fr 7C TLC fr 7B fr 7B ODS TLC fr 7B 2 Rf ODS TLC MeOH HzO0 20 1 10D 119 mg fr 10F 7 mg fr 7B 1H 18C NMR f 10D TLC palmi
17. toleic acid Rf fr 10D PGE 5X103 mg mL f 10F fr 7B 8X104 mg mL PGE fr 7C fr 10D ODS TLC 7 fr10D palmitoleic acid myristic acid fr 2G 6 114 2008 PC2005 171
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