取扱説明書 (NH2-100)
Contents
1. 1 1 2 PPPPPPPPPPPPPPPPPPPLPPPPPPPPCCPPPPTPLLPLLPPPPLPFFP 1 3 FPPPPTTPPPPPPPPFFPPPPFTTPPPPYYYTYYTPPPPFFFPPTTTPD 1 4 ee 2 5 POPPPPPPPTPFPPPPLPPPPPYYYYYPPPPPFPPPFPTTPPD 6 6 FPPPPPTPPPPPTPPPPCPLLPPPPLPPPPPPPTYTYFTPLLLLLPPD 6 7 PT 7 8 PT TT 9 9 RE WE ESR SR EE SES EER KRS RNS RE SS 10 10 SHA ERE NE RN RE DE On RE Sa NS 10 11 eeessseseeeeseeseseeeeeeasees 11 12 0 oo 12 132. 12 2 TSKeel NH 100 3 zm TSKeuardgel 2 3 2 a 2 mm X cm mm X cm 0021971 TSKguardgel NHz 100 3 m 2 0 1 TSKgel NHz 100 3 m 2 0X5 15 0021972 TSKguardgel NHz 100 3 m 3 2 1 5 TSKgel NHz 100 3 m 4 6X5 15 1 3 3
3. 50 vol 50 vol 50 mmol pH 6 0 50 50 V V 14 14 1 INSPECTION DATA 14 2 INSPECTION DATA
4. IN N dat i 5 e e At e e 5
5. 7 6 8 8 1 8 2 TSKg
6. 4 4 4 4 1 4 4 2
7. 4 8 4 8 1 4 8 2 3 4 8 3
8. HPLC HPLC HPLC 0 22 xm 0 45 gm 3 7 5 7 0014594 0 45 um 0006280 1 0 mL min 1 5 2 5 MPa
9. 13 1 1 13 1 3 13 1 1 13 1 2 13 1 2 13 1 3
10. 4 8 4 4 8 3 4 8 5 4 8 6 6 1 5 4
11. 4 6 mm 70 h 2 0 mm 40 h 2 0 mm 20 h 5 5 0 5h 1 2 1 13 13 1
12. HLC TSK GEL TSKgel TSKgel SuperMultipore BioAssist Enantio PStQuick Enviropak TOYOPEARL ToyoScreen TOYOPEARL GigaCap TOYOPEARL MegaCap TOYOPEARLPAK TOYOPAK TOSOH 03 5427 5180 G 06 6209 1948 G 052 211 5730 0120 17 1200 105 8623 541 0043 460 0003 252 1123 3 8 2 4 4 9 1 17 13 2743 1 Printed in Japan
13. e e e e e e e e 15
14. lt
15. 6 4 7 7 1 85 5 200 mmol L 95 5 1h LC MS 1 2 1 7 2 pH
16. pH pH pH 20 7 5 pH 7 3 7 4 7 5 7 5
17. N 5 54 Ve Wi Ve min Wi z min h N 11 2 Ve Injection 7 1 10 h As b a As 12 12 1
18. 4 2 0 mmX 1 cm 2 0 mm 3 4 4 1 Column No 4 2 2 3 FELOW 4 3
19. 4 4 2 13 2 INSPECTION DATA 13 2 1 13 2 2 13 2 1 13 1 13 2 2 13 3 13 3
20. BODPPPTPPPPPPFPPPPTTPPPPPPPYYTPPPPPPPP 13 14 CPPCPLPCLLYPYPPLPPLTCPCPPPPPPLYTYYTYYPPEYT 15 15 ii 16 2009 1 1 TSKgel NH2 100 3 zm 2 1 s ionenreeert 1 e INSPECTION DATA ee 1 3 1 gt FLOW PRAT 2 2 3 2 mmX 1 5 cm 4 6 mm 4
21. h 4 mm 4 2 mm i N h 2 mm 4 TSKgel NHz 100 3zm 2 5 5 3 2 0 1 mm
22. lt NM MG A 85 15
23. 4 8 1 10 10 1 10 2 0 45 zm 10 3 pH 11 INSPECTION DATA 11 1 Injection 6
24. a mm X cm 0019308 2 0X1 2 0X1 0019018 3 2X1 5 3 2X1 5 2 2 0019018 12 3
25. 4 EE EE J RR a mm X cm TP Column 0021967 TSKgel NHz 100 34 m 2 0X5 4 000 0 90 1 35 0021968 2 2 0 15 15 000 0 90 1 35 0021969 4 6X5 6 000 0 90 1 30 0021970 4 6X15 18 000 0 90 1 30 14 3 2 2 15
26. 12 3 LC MS 7 1 6 6 1 4 8 3 4 8 5 6 2 6 3
27. 20 cm 4 2 L 8 10 zL 50 ms 1 0 s 40 4 5 4 6 4 7 HPLC
28. 1 2 4 4 3 4 4 4 1 16 F 0 4 mm 1 1 16
29. 1 UV RI UV 7 5 2 7 5 3 25 7 5 4 7 5 5 7 5 6
30. Rev CO066000 TSKgel NHz 100 3m TOSOH
31. el NHs 100 3 zm 6 cm min 2 0 mm 0 20 mL min 4 6 mm 1 0 mL min TSKgel NHz 100 3 m 1 8 3 1 2 NR mm X cm MPa 0021967 TSKgel NHz 100 3 m 2 0X5 15 0021968 2 0X15 20 0021969 4 6X5 5 0021970 4 6X15 15 9 9 1 TSKgel NHz 100 3 um 10 50 50 9 2
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