TSKgel H タイプカラム取扱説明書
Contents
1. i 15 i EIEN2. i o
3. 0 y a e e N e e e e
4. 13 13 1 NSPECTION DATA 13 2 Hxr Hur SuperH SuperHZ 8 1 mm X cm TP Column TSsKgel SuperHZ1000 SuperHZ4000 TSKgel SuperHZM N SuperHZM M TSKgel SuperHZM H 4 6X15 9000 4 6X15 16000 4 6X15 16000 TSKgel SuperHZ1000 SuperHZ4000 TSKgel SuperHZM N SuperHZM M TSKgel SuperHZM H 6 0X15 9000 6 0X15 16000 6 0X15 16000 8 2 mm X cm TP Column TSKgel SuperH1000 SuperH5000 TSKgel SuperH6000 SuperH7000 TSK
5. i 1 1 2 FCCPPPPYTPTYTFPPFFFPPPPFPPPPYYYPPPPPFFFFFPFTPTPFPYYYYYPYYPPPPPPFF 1 3 cesseeeeeseseneeeeeeeneeeeeeeeseseneeeeeeeneneeeeeee 1 4 ee 2 5 cesseeeeeeseseneeeeeeeneeeeeeeeeeseseeeeeeeseseseeeee 5 6 tete 6 7 FPPPPPPPPPTPPPPPPPTFTPTCPPPPPPPPYPPPPPPPTTPLLPPPPPPPPYPLPPLLPLLPLYYPD 9 8 TT TY 13 9 0 RE ERE EE SEKI SAE ES ERE ER 13 10 14 11 oo 15 12 RPCPPPTYYTPPFFFPPTPPFPPPPFTPPYTYYFPPPFFTFPFYY
6. 4 10 2 3 4 10 3 4 10 3 3 H 5 5 1 4 10 5 2 5 3
7. J 5 4 6 3 SuperH SuperHZ 6mm 0 2mm 60cm 4 6mm 0 2mm 20cm 0 2mm 10cm 4 6 4 SuperH 4 2 1 8 10 L RESPONSE FAST
8. 14 HLC TSK GEL TSKgel TSKgel SuperMultipore BioAssist Enantio PStQuick Enviropak TOYOPEARL ToyoScreen TOYOPEARL GigaCap TOYOPEARL MegaCap TOYOPEARLPAK TOYOPAK TOSOH 03 5427 5180 G 06 6209 1948 G 052 211 5730 0120 17 1200 105 8623 541 0043 460 0003 252 1123 3 8 2 4 4 9 1 17 13 2743 1 Printed in Japan
9. 4 5 4 5 1 4 5 2
10. 12 1 3 4 5 2 12 2 1 1 12 2 1 12 2 3 12 2 1
11. DMF DMSO n N NMP 2299 MEK ODC HEP CHCls FC 113 m CH HFIP CHCls dPTb10 THF DMSO 6 2 2 Ham His HzO0 MeOH 3 4 THF DMF
12. 21 5mm oc GPC HT GPC GPC 15 i A i i
13. 5 7 3 1 MPa TSKgel SuperHZ1000 5 5 TSKgel SuperHZ2000 TSKgel SuperHZ2500 TSKgel SuperHZ3000 TSKgel SuperHZ4000 TSKgel SuperHZM N TSKgel SuperHZM M TSKgel SuperHZM H E mm X cm mL mn mL min 0 15 0 35 TSKgel SuperHZ1000 TSKgel SuperHZ2000 TSKgel SuperHZ2500 TSKgel SuperHZ3000 TSKgel SuperHZ4000 TSKgel SuperHZM N TSKgel SuperHZM M TSKgel SuperHZM H 0 25 0 60 mm X cm mL min mL min 1 MPa TSKgel SuperH1000 TSKgel SuperH2000 TSKgel SuperH2500 TSKgel SuperH3000 TSKgel SuperH4000 TSKge
14. 12 1 12 2 2 4 9 30 12 3
15. 11 1 a s d 11 2 7 H 16 TSKeuardcolumn H Hsk L Hs H 3 a HH 7 mm X cm TSKguardcolumn Hxr L TSKgel G1000Hxi G4000Hxr 6 0X4 0 OX TSKguardcolumn Hixr H TSKgel G5000Hxr G7000Hxr GMHxr 6 0X4 0 Oi gt gt TSKguardcolumn Has L S TSKgel G1000Hgs G4000Hus 7 5X7 5 TSKguardcolumn Hms H S TSKeel GMHrs H 7 5X7 5 TSKguardcolumn Huir L TSKgel G1000Hrk G4000Hns 6 0X4 0 TSKguard
16. a s 8 3 8 2 9 9 1 9 2 0 45 xm
17. N e e e e e e e e e
18. 6 2 1 6 2 3 SuperH SuperH Hms Hm 6 2 2 3 SuperH Hm CHCls DMF DMSO n NMP m CHCls MEK ODCB TCB HFIP HFIP CHCls o CHCls CHCls FC 113 4 SuperH Hua THF mL min CP Hm lt gt
19. 12 1 12 1 1 12 1 3 12 1 1 12 1 2 12 1 2
20. HH 9 3 10 INSPECTION DATA 10 1 Injection 6 TSK GEL N 5 54 Ve Wi 2 2 Ve min Wi min h N 10 2 Injection 7 TSK GEL 1 10h As b a
21. 8 0 5 3 0 0 59 20 8 0 6 3 5 0 43 20 CHC13 MI 0 5 DMF 0 4 2 5 SuperH DMSO 8 0 2 1 0 8 0 2 1 0 1 20 25 n 8 5 0 0 31 25 NMP 1 0 1 65 8 M 0 5 3 00 30 MEK 8 4 0 0 39 22 ODCB 1 0 1 32 25 HFIP 8 5 70 20 9 6 0 95 20 8 1 0 97 20 1 8 0 45 20 1 06 25 8 2 94 20 THF 0 55 20 25 C 7 7 1 7 2 5
22. 5 4 6 6 1 H HixrL Hs SuperH SuperHZ THF 21 5mm CHCls GPC TSK GEL GMH HT HT o ODCB SuperH Hrk H Hxr
23. G PC TSK GEL H TOSOH i i i i i i
24. 25C 7 4 0 2 100 0 02 6 6 mm X cm 4 6X15 10 z L 5 L 6 0X15 20 zL 10 gL 7 8X30 100 L 50 gL 8 8 1 Hxr Hs SuperH SuperHZ 25 C Hxr SuperHZ G1000H G2000H G2500H G3000H MultiporeHxr M 60 G4000H G5000H G6000H G7000H GMH 80C Hxr GPC GMH HT His SuperH 140 8 2 4 10 1
25. 2 _ HH Ha gt gt ll LT TOSoH FLOW TSKgel SuperH coumn No 3 SuperH SuperHZ 4 4 1 SuperH SuperHZ 4 2 2 3 ELOW 4 3 4 4
26. 0 3mL min 7 5 7 8mm 0 5mL min 3mL min 5 100 20 30 i 1 THF CHCls 1 DMF HFIP CHCls ODCB 2 2 HxL
27. 17 13 PCCPPCPPPCPTPPPPPPPTPYPYEPPPYPPLPPPYEYPYYPPYYEYKKY 19 14 21 2004 4 1 TSK GEL TSK GEL H GPC H 2 1 mu eeeeeeeeee 1 i INSPECTION DATA SRE IRR EEN 1 3 gt
28. 0 05s STD 1 0s 70 80 4 7 4 8 4 9 _ 4 10 4 10 1
29. CHCls DMF HFIP THF 6 2 6 2 6 2 1 HxL SuperHZ Hxr SuperHZ THF 1 Hxr SuperHZ 1 HxLu SuperHZ THF CHC1s G1000H ij 4 6mm 0 15mL min 6 0mm
30. As HLC 11 4 9
31. 0mm 11 3 A NN i 12 TSK GEL
32. 4 5 3 4 6 4 6 1 1 16 4 SuperH SuperHZ 2mm 4mm h Hm H Ha Hi h 4 mm h SuperH SuperHZ h 2 mm 4 4 6 2 5
33. column Hir H TSKgel G5000Hak G7000Hnsk GMHrs L N M amp H 6 0X4 0 NIRNS AS AS NNS NN dN TSKguardcolumn Has S el GMHrn M S amp H S 7 5X7 5 GPC TSKguardcolumn SuperH L TSKgel SuperH1000 SuperH4000 4 6X3 5 GPC TSKguardcolumn SuperH H TSKgel SuperH5000 SuperH7000 SuperHM L N M amp H 4 6X3 5 GPC TSKguardcolumn Hm 30 30 20 7 5X7 5 GPC TSKguardcolumn Hrm 30 HT GPC 30 20 7 5X7 5 GPC TSKguardcolumn Hur S HT GPC S 7 5X7 5 GPC TSKguardcolumn MP XL TSKgel MultiporeHxr M 6 0X4 0 GPC TSKguardcolumn SuperHZ L TSKgel SuperHZ1000 SuperHZ4000 SuperHZM N amp M 4 6X2 0 4 6mm 2 4 6X3 5 6 0mm TSKguardcolumn SuperHZ H TSKgel SuperHZM H 4 6X2 0 4 6mm 2 2 4 6X3 5 6
34. gel SuperHM L N M H TSKgel G1000HxL G4000Hx GMHxr L TSKgel G5000Hxr G7000Hx GMHxr TSKgel G1000Hnn G7000Hrs GMHmn L N M amp H 6 0X15 16000 0 7 1 6 6 0X15 10000 07 1 6 6 0X15 16000 07 16 7 8X30 14000 0 7 1 6 7 8X30 14000 0 7 1 6 7 8X30 16000 0 7 1 6 TsKgel GMHrs M S amp H S 7 8X30 8000 07 16 TSKgel GMHms H 30 HT 4000 TSKgel GMHrm H 20 HT 6000 TSKgel GMHrs H S HT 8000 TSKgel GMHmn H HT 16000 TSKgel G2000Hrs 20 HT 6000 TSKgel GMHmn H 30 4000 TSKgel GMHrs H 20 6000 TSKgel MultiporeHxr M 7 8X30 16000 TSKeel GMHxr HT 7 8X30 5500 TSKgel G1000Hnn G4000Hrs S 16000 GMHm H a 13 3 2 2
35. l SuperH5000 TSKgel SuperH6000 TSKgel SuperH7000 TSKgel SuperHM L TSKgel SuperHM N TSKgel SuperHM M TSKgel SuperHM H 5 mm X cm 3 mL min mL min 7 0 1 MPa TSKegel G1000Hxr TsKgel G2000Hxr TSKeel G2500Hxr TSKeel G3000Hxr TSKeel G4000Hxr TSKeel G5000Hxr TSKeel G6000Hxr TSKeel G7000Hxr TSKgel GMHxr L TSKeel GMHxr TSKgel GMHxr HT 1 0 5 0 mm X cm mL min mL min 1 MPa TSKgel G1000Hms TSKgel G2000Hms TSKgel G2500Hms TSKgel G3000Hms TSKgel G4000Hms TSKgel G5000Hms TSKgel G6000Hms TSKgel G7000Hms TSKeel GMHn L TSKgel GMHn N TSKgel GMHrr M TSKgel GMHn H TSKgel GMHms M S TSKgel GMHms H S TSKgel GMHmn H 30 TSKgel GMHmn H 20 TSKgel GMHrs H 30 HT TSKgel GMHrms H 20 HT TSKgel GMHrs H S HT TSKeel GMHns H HT TSKeel G2000Hrms 20 HT TSKgel MultiporeHxr M TSKgel G1000Hr TSKeel G2000Hr TSKgel G2500Hr TSKeel G3000Hr TSKeel G4000Hrs TsKgel GMHnns H 21 5X30 H Hxr Hrm SuperH SuperHZ 25 THF HT ODCB
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