1100 Installation Manual.pub
Contents
1. Remove the column and direct the pump output tubing to a beaker Flush the Vacuum Degasser first with water and then with isopropanol Turn off the vacuum degasser Disconnect the tubing between the vacuum degasser and solvent reservoirs and the vacuum degasser and pump Plug all of the ports on the vacuum degasser Store the vacuum degasser in a clean dry location b2ibo SPd KS GGid RKT 2S Y L E LIM 16 AKUS GN SRS TENGS ily y oSPNG Pyy I iS Ganly y ryR N KS 6 Maintenance Removing and Refitting the Top Cover Tools required e Screwdriver Pozidriv 1 Preparations e Switch OFF the vacuum degasser at the main power switch e Disconnect the power cable and remote cable e Disconnect all solvent tubes from the ports of the vacuum degasser e Remove solvent cabinet from the vacuum degasser e Remove vacuum degasser from the stack WARNING Toxic and hazardous solvents The handling of solvents and reagents can hold health risks gt When opening capillary or tube fittings solvents may leak out gt Please observe appropriate safety procedures for example goggles safety gloves and protective clothing as described in the material handling and safety data sheet supplied by the solvent vendor especially when toxic or hazardous solvents are used 1 Remove the front panel 2 Unclip the clips on the top cover 54 1200 Series VD User Manual Maintenance Introduction to Maintenance and Repair 4 Unscrew t2. Installation Instructions Part Number 0001 1019 1100 Degasser Retrofit Kit Europe Global Headquarter North America Japan Biotech AB Biotech USA LLC BioNik Inc Telephone 46 0 300 56 91 80 Telephone 01 0 612 703 5718 Telephone 81 545 38 9125 info biotech se bmathieu biotechusa us info bionikinc com doS 27 2yibyito NEKO CUCU OM aeann aaa Getting Started 1 Safety i annines ere rt Removing Original Gon Donen eee Installing Biotech Kit Components MEERE 3 Finish sede E 4 Technical Sippo ee err SCLC COW I saiora tyasateecsted aac ences 5 This manual covers the Installation of the Biotech Degasser Retrofit Kit for the Model 1100 Degasser This kit is a drop in replacement for the original 1100 internal components that is based on Teflon AF membrane technology and closed loop vacuum control The original power supply control board and pressure sensor are retained so that communication with the instrument stack and software is maintained The following procedures should only be performed by a quali fied technician Sika ENGR Kit Components Qty 1 PN 9000 0002 Degassing Tray Assy Qty 1 PN 9000 0001 Power Cable Assy Qty 1 PN 8000 0032 Sensor Mounting Bracket Equipment Required Model 1100 User Manual for cover removal and reinstallation instructions 1 Phillips Screwdriver Bie tNfyEo Warning The original vacuum chamber membranes should be flushed to remove any potentially hazard
3. PC board assy into the sensor mounting bracket as shown with the mounting hole relief facing up and the solder side of the sensor board facing up until sensor locks in place Note when sliding the assembly in place be careful to support the sensor by holding the sensor with your index finger on one side with your thumb on the backside of the board to prevent breaking the bond between the sensor and PC board 4 Secure the Sensor Bracket to the post on the drip tray that it was removed from earlier using an M3 x 6 screw Saved earlier 5 Connect the tube from the sensor to the TEE on the Degasser Tray Assy Page 3 lyak iid R KY 2Y LPySyia 2yio 6 Disconnect the power cable from the original control board 7 Connect this cable to the supplied cable as shown 8 Connect the other ends of the supplied cable to the original control board and control board on the new Degasser Tray as shown The figure below is a representation of how the unit should look when the Install is complete Re install all of the covers that were removed at the beginning of this instruction again refer to the 1100 Users Manual or Appendix A For ordering and technical support please call Europe Global Headquarter North America Japan Biotech AB Biotech USA LLC BioNik Inc Telephone 46 0 300 56 91 80 Telephone 01 0 612 703 5718 Telephone 81 545 38 9125 info biotech se bmathieu biotechusa us info bionikinc com www biotech se
4. he screws on the top plate and remove the plate by lifting its back and then sliding the plate to the front 3 Lift the cover away Screws 5 Place the metal cover onto the housing Lower the front of 6 Replace the top cover Ensure the clips are seated the plate first then slide panel to the back Assure the correctly four metal tabs of the panel slide underneath the Z plane Fix the two holding screws Metal Tabs Screws 1200 Series VD User Manual 55 6 Maintenance 7 Reinstall the front cover For ordering and technical support please call Europe Global Headquarter North America Biotech AB Biotech USA LLC Telephone 46 0 300 56 91 80 Telephone 01 0 612 703 5718 info biotech se bmathieu biotechusa us www biotech se www biotech se 56 8 Reinstall the vacuum degasser in your system stack and connect the cables and capillaries and turn on the vacuum degasser Japan BioNik Inc Telephone 81 545 38 9125 info bionikinc com www bioikinc com 1200 Series VD User Manual
5. ous solvents that may be remaining Protective gloves and face protection should be worn and the operation performed in a properly ventilated area Consult your company s Safety Director for more information Make sure that the power cord is unplugged from the unit before proceeding Page 1 vY 2yh NJi 2Y LPySyi o 1 Remove the outer cover and top plate refer to the 1100 Operators Manual See Appendix A for these instructions if the manual is not available 2 Disconnect the tube running from the sensor from the chamber port leaving the tube connected to the port on the sensor Remove the screw holding the small bracket holding the sensor PC board from the post on the drip tray and set the sensor assy behind the drip tray You do not need to disconnect the cable from the Control Board ay 3 Remove the screws holding the Vacuum Chamber Vacuum Pump and the Vacuum Valve Disconnect the cables for the pump and valve from the control board These items can be discarded but retain the screws that were securing these for future use Qty 2 M3 x 6 and Qty 2 M3 x 16 will be needed 4 Loosen the two screws securing the cover over the power supply and control board a few turns and remove this cover Unit after original components removed Page 2 yta RiBKYN 2Y LPySyiao 1 Install the new Degasser Tray assy slide the bulkheads through the openings in the front panel and set in position 3 Slide the original sensor
6. www biotech se www bioikinc com Page 4 Ky TENK KUGR26 yn CENAKLI yR SS SyRexc b2iboh Geol MELISS didye LENG Aviva KINE y byROENG Ob Pibyia kN KN TERLI 2NGEL PRG ar To shutdown the degasser a b c Remove harmful mobile phases from the vacuum degasser and other instruments in the system Flush the column according to the instructions supplied with the column Flush the degasser If the solvent contains buffer salts flush with water If the mobile phase is allowed to evaporate salt crystals that may form harmful deposits fr ww Ww A w Dr rl pahi PETE Select T EERI lN y t d e If the mobile phase contains chloroform or other solvents that can decompose to form hydrochloric acid remove all traces of the mobile from the system using a suitable solvent After removing any potentially harmful mobile phases prepare the detector by flushing it with isopropanol To avoid contaminating the system refilter or discard solvents including water that were exposed to the environment for more than 24 hours before use For weekend storage we recommend flushing 60 40 MeOH Water through the Vacuum Degasser pump column flow cell provided your column is compatible with MeOH Water for a few minutes before you turn off the Vacuum Degasser pump and detector 2y Ky To shut down the system for a long period of time a b c d Follow steps a and b in the short term shutdown procedure
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