VALVEMATE® II Valve Actuator User's Guide
Contents
1. 1 Set the valve selector to the appropriate value for the replacement valve Refer to Valve Selection on page 2 5 Ensure that the coupler on the collar is oriented so the notch in the coupler is aligned with the pin on the top as shown below If the coupler is not oriented correctly remove using needle nose pliers Rotate to the correct orientation and re install Ny LI pin coupler _ collar Allen screw front of VALVEMATE II with valve removed Place the valve on the instrument and tighten the Allen screw Note The locating hole on the top of the valve should line up with the pin on the front of the collar Reconnect the power supply to the VALVEMATE II Gilson VALVEMATE II Valve Actuator User s Guide locating hole O back of valve 4 3 yUaWarde day AJLA Troubleshooting 5 If you encounter a problem while operating the VALVEMATE II refer to the following pages If you cannot solve or isolate the problem contact your Gilson authorized representative See Before Calling Us on page 5 5 Gilson VALVEMATE II Valve Actuator User s Guide 5 1 Error Messages Troubleshooting Error Messages If an error message appears on the VALVEMATE II refer to the following table Error Description Possible Cause and Solution 0 No error 1 Unknown command Unknown command Clear the error and send a known legal command 2 Invalid NV RAM address Attempt to write to an NV R2. The arrow keys can be used to rotate the installed valve Use this arrow key to rotate the valve counterclockwise Cv Use this arrow key to rotate the valve clockwise If You See an Error If an error message appears on the display refer to Chapter 5 Troubleshooting Gilson VALVEMATE II Valve Actuator User s Guide Maintenance 4 The VALVEMATE II was designed to require minimal maintenance Keep the unit clean Wipe the unit with a soft cloth dampened with a mild detergent and disinfect as needed Gilson VALVEMATE II Valve Actuator User s Guide 4 1 Valve Replacement Maintenance 4 2 Valve Replacement Follow these directions to replace the currently installed valve VALVEMATE ll compatible valves are listed in Appendix A Replacement Parts and Accessories Before You Begin Locate the following e replacement valve 9 64 Allen wrench supplied with the VALVEMATE II Removing the Installed Valve To remove the currently installed valve 1 Home the valve by pressing both of the arrow keys on the front panel at the same time 2 Disconnect the power supply from the VALVEMATE II 3 Using a9 64 Allen wrench loosen the Allen screw on the bottom side of the valve to remove the valve from the instrument Allen screw front of VALVEMATE II with valve installed Gilson VALVEMATE II Valve Actuator User s Guide Maintenance Installing the Replacement Valve To install the replacement valve
3. Check connections for proper pin assignments on the device supplying input to the VALVEMATE II Confirm that device supplying input to the VALVEMATE II is turned ON and working properly Make sure that the pulse to the VALVEMATE II is at least 0 1 second in duration Fluid flowing from wrong port or not flowing from any port The valve may be misaligned turn power OFF then ON to the VALVEMATE II The valve may not have been in home position when installed in the VALVEMATE II Refer to Placing the valve in its home position on page 2 8 The valve may be incorrectly plumbed Fluid may not be reaching the valve if connected to a pumping system lower system pressure and disconnect the valve s inlet tubing to determine if fluid is reaching the valve Gilson VALVEMATE II Valve Actuator User s Guide 5 3 Bulyooysajqnoly Troubleshooting Troubleshooting Low flow rate Check for leaks in tubing High back pressure 5 4 The valve may be incorrectly plumbed Gilson VALVEMATE II Valve Actuator User s Guide Troubleshooting 5 Repair and Return Policies Before Calling Us Gilson authorized representatives will be able to serve you more efficiently if you have the following information e theserial number and model number of the instruments involved The serial number is located on the bottom of the VALVEMATE II the installation procedure you used e list of concise symptoms e list of operating procedures a
4. a small Phillips screwdriver into the selector on the rear panel and turn it 2 Align the white dot with one of the indicated numbers The unit ID is 30 plus the selected number Gilson VALVEMATE II Valve Actuator User s Guide SUOI DBUUD 311399 Electrical Connections Installation 2 4 Contact Connections ROTATE HOME The VALVEMATE II can receive contact closure input from other devices to rotate and home the valve To make contact connections use the remote cable ordered separately part number 33035261 This cable has a 3 conductor plug that connects to the ROTATE HOME port on the rear panel refer to the diagram on page 2 2 The other end of the cable contains four tinned wires ROTATE green W D M o sree HOME Connect the tinned wires to the contact closure outputs of the device according to the instrument s user s guide To determine the state of the ROTATE or HOME input contact use the appropriate GSIOC command refer to Appendix C GSIOC Commands Gilson VALVEMATE II Valve Actuator User s Guide Installation Valve Selection The valve selector identifies the type of installed valve Refer to the table below for valve information To change the valve selector 1 Gently insert a small Phillips screwdriver into the selector on the rear panel and turn it 2 Align the white dot with one of the indicated numbers Setting Part Number Positions 494C22006 494C2
5. long for 1 16 OD tubing package of 10 490318021 1 Valco ZF1S6 10 Type 316 stainless ferrules 1 16 package of 10 499311519 2 Stainless steel tubing 0 010 ID x 0 062 1 16 OD x 5 ft 494LZN1 10 1 Valco LZN1 10 stainless steel nut 1 16 0 75 long package of 10 490318021 1 Valco ZF1S6 10 Type 316 stainless ferrules 1 16 package of 10 49953059 2 PEEK tubing 0 030 ID x 0 062 1 16 OD x 5 ft 494LZN1PK 10 1 Valco LZN1PK 10 PEEK nut 0 87 long for 1 16 OD tubing package of 10 490318051 1 Valco ZF1PK 10 PEEK ferrule 1 16 package of 10 49951059 2 PEEK tubing 0 010 ID x 0 062 1 16 OD x 5 ft 494LZN1PK 10 Valco LZN1PK 10 PEEK nut 0 87 long for 1 16 OD tubing package of 10 490318051 1 Valco ZF1PK 10 PEEK ferrule 1 16 package of 10 495032 1 TFE Tubing 1 5 mm ID x 3 0 mm OD 1 8 10 ft pkg 49041017P 1 Upchurch P 301 NUT FLANGELESS 1 8 IN 1 4 28 DELRIN ACETAL BLACK pkg of 10 49041015P 1 Upchurch P 300 FERRULE FLANGELESS 1 8 IN Gilson VALVEMATE II Valve Actuator User s Guide TEFZEL ETFE YELLOW pkg of 10 2 9 suol 229UUOD Huiquinid Plumbing Connections Installation 2 Plumbing Setup Plumb the VALVEMATE into your system as required by your application The fittings you will use depend on the OD of the tubing connected to the valve Tubing and fittings are included with each of the plumbing packages listed on page 2 9 Slide the nut and ferrule onto t
6. 0 005 020 ID tubing can be used up to 5000 psi for a limited time and 0 030 to 3000 psi Larger IDs are typically good to 500 psi These limits will be substantially reduced at elevated temperatures and in contact with some solvents or acids Its mechanical properties allow PEEK to be used instead of stainless in many situations and in some environments where stainless would be too reactive However PEEK can be somewhat absorptive of solvents and analytes notably methylene chloride DMSO THF and high concentrations of sulfuric and nitric acid This tubing is highly prone to kinking or sealing off if held in a sharp bend over time Gilson VALVEMATE II Valve Actuator User s Guide B 5 sjen zew pue swesbeig y ed MOJ4 AJLA Valve Flow Path Diagrams and Materials Appendix B 6 PPS Polyphenylene sulphide It is very resistant to all solvents acids and bases Valcon E Apolyaryletherketone PTFE composite Standard specs are 400 psi at 225 C but higher pressure ratings are possible at reduced temperatures However this polymer cannot be used in prolonged contact with high concentrations of sulfuric and nitric acids DMSO THF or liquid methylene chloride Valcon E2 A proprietary reinforced TFE composite Valcon E2 works well at lower pressures and is suitable for temperatures up to 75 C This material is resistant to most chemicals but should not be used in prolonged contact with high concentrations of sulfuri
7. 0 016 ID ports 1 16 tubing 1 16 ZDV fittings 494C5H2000 High pressure stainless steel multi position valve 10 position 10 port with Valcon H rotor 0 016 ID ports 1 16 tubing 1 16 ZDV fittings 494C52346 High pressure PEEK multi position valve 6 position 6 port with Valcon E rotor 0 016 ID ports 1 16 tubing 1 16 ZDV fittings Gilson VALVEMATE II Valve Actuator User s Guide A 1 Replacement Parts and Accessories Appendix Valves Continued Part Number Description 494C5H2340 High pressure PEEK multi position valve 10 position 10 port with Valcon E rotor 0 016 ID ports 1 16 tubing 1 16 ZDV fittings 494C53006 High pressure stainless steel multi position valve 6 position 6 port with Valcon H rotor 0 030 ID ports 1 16 tubing and fittings 494C 253186 Low pressure PPS multi position valve 6 position 6 port with Valcon E2 rotor 0 030 ID ports 1 16 tubing 1 4 28 fittings 494C256186 Low pressure PPS multi position valve 6 position 6 port with Valcon E2 rotor 0 060 ID ports 1 8 tubing 1 4 28 fittings 494C256188 Low pressure PPS multi position valve 8 position 8 port with Valcon E2 rotor A 2 0 060 ID ports 1 8 tubing 1 4 28 fittings Gilson VALVEMATE II Valve Actuator User s Guide Appendix A Rotors Part Number Description 494C220R6 Rotor Valcon H for 6 port analytical valve part number 494C22006 1 16 fit
8. 3006 494C22Z3186 494C2H2000 494C23000 494C22Z3180 494C52006 494C53006 494C52346 494C253186 494C256186 494C256188 494C5H2000 494C5H2340 Gilson VALVEMATE II Valve Actuator User s Guide 2 5 SUOI DBUUD eI11 99 5 Electrical Connections Installation 2 6 Power Connection Use the DC power supply and power supply cable supplied with the VALVEMATE II to make the connection between the 24V DC power receptacle and a power source Gilson VALVEMATE II Valve Actuator User s Guide Installation Valve Installation Follow these directions to install a valve if it was not factory installed by Gilson VALVEMATE Il compatible valves are listed in Appendix A Replacement Parts and Accessories Before You Begin Locate the following gt valve 9 64 Allen wrench supplied with the VALVEMATE II Installing the Valve To install the valve 1 Home the VALVEMATE II by pressing both of the arrow keys on the front panel at the same time 2 Disconnect the power supply from the VALVEMATE II 3 Set the valve selector to the appropriate value Refer to Valve Selection on page 2 5 4 Ensure that the coupler on the collar is oriented so the notch in the coupler is aligned with the pin on the top as shown If the coupler is not oriented correctly remove using needle nose pliers Rotate to the correct orientation and re install 5 Place the valve on the inst
9. 59 Os Koxey nO O Ov 494c256186 OoOO P 301 P 300 OO 0 060 ID x 1 8 OD TFE tubing 494C 256188 Gilson VALVEMATE II Valve Actuator User s Guide 2 13 suol 229UUOD Huiquinid Connector Plate Installation Installation 2 Connector Plate Installation A connector plate part number 3303522 ordered separately is available for stacking multiple VALVEMATE II units To install the connector plate 1 Place the connector plate on the top of the VALVEMATE II The back of the connector plate has one edge that goes up and one edge that goes down this should be placed at the back of the VALVEMATE II 2 Place the thumbscrews through the connector plate to the holes on the VALVEMATE II and tighten 3 Place the second VALVEMATE II on the connector plate connector plate C C thumbscrews connector plate installed on the VALVEMATE II rear panel 2 14 Gilson VALVEMATE II Valve Actuator User s Guide Operation 3 This section describes how to control the VALVEMATE II You can control the VALVEMATE II using TRILUTION Software the front panel contact closures or Gilson Serial Input Output Channel GSIOC Gilson VALVEMATE II Valve Actuator User s Guide 3 1 Front Panel 3 2 Operation Front Panel The front panel contains two arrow keys and an LED display that shows valve position
10. AM address that doesn t exist Contact Gilson for information regarding correct NV RAM addresses 3 Move while busy Attempt to switch the valve while the valve is still moving Wait for the current command to execute before sending another 4 Positioning error The VALVEMATE is having difficulty rotating the valve Ensure that the correct setting is selected on the valve selector 5 Invalid command parameter A numerical parameter was out of range Clear the error using the buffered e command Then enter a numerical parameter within the range 6 Homing error Error occurred during homing Ensure that the appropriate number is selected on the valve selector on the rear panel Turn power OFF then ON to the VALVEMATE II 7 Move while unhomed Attempt to move before the valve was homed Send the buffered H command to home the valve 8 Invalid setting Invalid setting on valve switches or user defined parameters 5 2 Gilson VALVEMATE II Valve Actuator User s Guide Troubleshooting 5 Troubleshooting Unit not operational Check power cord connection Try different outlet Check all connections VALVEMATE II making an erratic noise when moving the valve The valve may not have been in home position when installed in the VALVEMATE II Refer to Placing the valve in its home position on page 2 8 Input functions not operating Check 3 conductor plug connection to the ROTATE HOME port Make sure wire connections to the other device are secure
11. ELRIN ACETAL BLACK pkg of 10 49041015P Upchurch P 300 FERRULE FLANGELESS 1 8 IN TEFZEL ETFE YELLOW pkg of 10 A 4 Gilson VALVEMATE II Valve Actuator User s Guide Appendix Cables and I O Accessories Part Number Description 36078143 GSIOC cable 59444524 power supply 24V desktop universal 7080318107 power cord 110V 7080316106 power cord 220V 33035261 VALVEMATE II remote control cable assembly Miscellaneous Part Number Description 4311402 9 64 Allen wrench 3303522 VALVEMATE II connector plate Gilson VALVEMATE II Valve Actuator User s Guide A 5 Salossad2y pue s ieg JUaWAaDL day Valve Flow Path Diagrams and Materials B Valve Flow Path Diagrams Part Number Description Analytical stainless steel valve 494C22006 2 position 6 port with Valcon H rotor 0 016 ID ports 1 16 tubing and fittings Analytical stainless steel valve 494C2H2000 2 position 10 port with Valcon H rotor 0 016 ID ports 1 16 tubing and fittings Preparative stainless steel valve 494C23006 2 position 6 port with Valcon H rotor 0 030 ID ports 1 16 tubing and fittings Position 1 Position 2 Gilson VALVEMATE II Valve Actuator User s Guide B 1 Valve Flow Path Diagrams and Materials Position 2 Appendix Part Number Description Preparative stainless steel valve 494C23000 2 position 10 port with Valcon H rotor 0 030 ID ports 1 16 tubing and fittings Preparativ
12. VALVEMATE Il Valve Actuator User s Guide World Headquarters Gilson Inc 3000 Parmenter Street P O Box 620027 Middleton WI 53562 0027 USA Telephone 608 836 1551 Fax 608 831 4451 Gilson S A S 19 avenue des Entrepreneurs F 95400 VILLIERS LE BEL France www gilson com sales gilson com service gilson com training gilson com 2006 Gilson Inc All Rights Reserved 4 Aoisong LT3332 01 Table of Contents 1 Introduction Unpacking Standard Equipment Documentation Accessories Valves and Plumbing Packages Other Accessories Customer Service Technical Specifications 2 Installation Electrical Connections Rear Panel Contact Connections ROTATE HOME Valve Selection Power Connection Valve Installation Before You Begin Installing the Valve Checking Valve Position and Liquid Flow Placing the valve in its home position Plumbing Connections Plumbing Setup Stainless steel plumbing package prep 0 030 ID x 1 16 OD tubing Stainless steel plumbing package analytical 0 010 ID x 1 16 OD tubing PEEK plumbing package prep 0 030 ID x 1 16 OD tubing PEEK plumbing package analytical 0 010 ID x 1 16 OD tubing TFE plumbing package 0 060 ID x 1 8 OD tubing Connector Plate Installation Gilson VALVEMATE II Valve Actuator User s Guide 3 Operation Front Panel If You See an Error 4 Maintenance Valve Replacement Before You Begin Removing the Installed Valve Inst
13. alling the Replacement Valve 5 Troubleshooting Error Messages Troubleshooting Unit not operational VALVEMATE II making an erratic noise when moving the valve Input functions not operating Fluid flowing from wrong port or not flowing from any port Low flow rate High back pressure Repair and Return Policies Before Calling Us Warranty Repair Non Warranty Repair Rebuilt Exchange Return Procedure Unit End of Life A Replacement Parts and Accessories Valve Flow Path Diagrams Materials Nitronic 60 Stainless steel Type 316 Gilson VALVEMATE II Valve Actuator User s Guide C GSIOC Commands GSIOC Commands GSIOC Command List Gilson VALVEMATE II Valve Actuator User s Guide Introduction 1 The Gilson VALVEMATE Il is a small footprint valve actuator that provides automatic rotation of a 2 position or multi position low or high pressure valve The VALVEMATE Il is controlled by TRILUTION Software as well as the front panel contact closures and Gilson Serial Input Output Channel GSIOC Gilson VALVEMATE II Valve Actuator User s Guide 1 1 Unpacking Introduction Unpacking Unpack the VALVEMATE Il and accessories carefully from the carton Cross check the contents against the standard equipment checklist shown below and against your purchase order s optional accessory list to verify that all parts are included and undamaged Do this now even if the VALVEMATE II will not be used immediately Ma
14. als Refer to Appendix B Valve Flow Path Diagrams and Materials for more information Nitronic 60 N60 Valcon H Valves 494C22006 494C2H2000 494C23006 494C23000 494C52006 494C5H2000 494C53006 PPS Valcon E2 Valves 494C2273186 494C2273180 494C253186 494C256186 494C256188 PAEK Valcon E Valves 49452346 494C5H2340 Manufacturing standards Meets applicable Safety and EMC certification standards UL and CE certified Physical space requirement 8 3 x 15 6 x 9 8 cm 3 3 x 6 2 x 3 9 in Power requirements 24V DC at 2 0A supplied via a 2 1 mm ID power plug center contact is positive Valve switching speed msec lt 200 msec depending on valve Weight Gilson VALVEMATE II Valve Actuator User s Guide 1 04 kg 2 29 Ibs No valve installed suoljerdijinads jediuyra Installation This section takes you through the steps for setting up your VALVEMATE II Gilson VALVEMATE II Valve Actuator User s Guide 2 1 Electrical Connections Installation 2 Electrical Connections Rear Panel Please read this entire section and refer to the rear panel diagram below before making any electrical connections Do not turn on power to the VALVEMATE II until all connections have been made Stee He a Gore VALVEMATE II rear panel 1 GSIOC 2 UnitID 3 ROTATE HOME Contact Connection 4 Valve selector refer to page 2 5 for inf
15. c and nitric acids DMSO or liquid methylene chloride Valcon H This composite a carbon fiber reinforced PTFE lubricated inert engineering polymer has long been the standard for typical HPLC applications in which pressures are around 5000 psi and temperatures are not more than 75 C Information provided by Valco Instruments Company Inc Gilson VALVEMATE II Valve Actuator User s Guide GSIOC Commands C The Gilson Serial Input Output Channel GSIOC is an asynchronous serial communications interface that enhances the power of your Gilson equipment The GSIOC incorporates an EIA RS 485 interface and allows up to 32 slave devices to be controlled from a single master in a multi drop configuration Each slave device is identified by a unique number which must be known to the device and to the controller The default ID code of the VALVEMATE II is 35 Using the computer and software you e specify the VALVEMATE II as the device you want to control issue commands that set operating parameters control operation or request information from that device Gilson VALVEMATE II Valve Actuator User s Guide C 1 GSIOC Commands Appendix C 2 GSIOC Commands There are two kinds of commands that you can send over the GSIOC Buffered commands send instructions to the VALVEMATE Il These commands are executed one at a time Immediate commands request status information from the VALVEMATE II These commands are exec
16. e Introduction Customer Service Gilson Inc and its worldwide network of authorized representatives provide customers with the following types of assistance sales technical support applications and instrument repair If you need assistance please contact your Gilson authorized representative Specific contact information can be found on the Gilson website at www gilson com To help us serve you quickly and efficiently please refer to Before Calling Us on page 5 5 Gilson VALVEMATE II Valve Actuator User s Guide S 4aWO sSN gt D DIIAIO Technical Specifications Introduction Technical Specifications Please be aware of the following before operating the VALVEMATE II Warning Changes or modifications to the VALVEMATE II not expressly approved by Gilson could void the factory authorized warranty The VALVEMATE II has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FCC commercial environment The VALVEMATE II generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instructions may cause harmful interference to radio communications Operation of the VALVEMATE Il ina residential area is likely to cause harmful interference in which case the user will be required to correct the interference at the user s own expense Shielded cables must be used with the VALVEMATE II to ensure compliance with the Class A FCC li
17. e PPS valve 494C22Z3186 2 position 6 port with Valcon E2 rotor 0 030 ID ports 10 32 fittings 1 16 tubing Preparative PPS valve 494C22Z3180 2 position 10 port with Valcon E2 rotor 0 030 ID ports 10 32 fittings 1 16 tubing High pressure stainless steel multi position valve 494C52006 6 position 6 port with Valcon H rotor 0 016 ID ports 1 16 tubing 1 16 ZDV fittings High pressure stainless steel multi position valve 494C5H2000 10 position 10 port with Valcon H rotor 0 016 ID ports 1 16 tubing 1 16 ZDV fittings B 2 Gilson VALVEMATE II Valve Actuator User s Guide Appendix Part Number Description High pressure PEEK multi position valve 494C52346 6 position 6 port with Valcon E rotor 0 016 ID ports 1 16 tubing 1 16 ZDV fittings High pressure PEEK multi position valve 494C5H2340 10 position 10 port with Valcon E rotor 0 016 ID ports 1 16 tubing 1 16 ZDV fittings High pressure stainless steel multi position valve 494C53006 6 position 6 port with Valcon H rotor 0 030 ID ports 1 16 tubing and fittings Low pressure PPS multi position valve 494C253186 6 position 6 port with Valcon E2 rotor 0 030 ID ports 1 16 tubing 1 4 28 fittings Low pressure PPS multi position valve 494C256186 6 position 6 port with Valcon E2 rotor 0 060 ID ports 1 8 tubing 1 4 28 fittings Gilson VALVEMATE II Valve Actuator User s Guide B 3 sjen zew pue swesbeig
18. error 5 Invalid command parameter 6 Homing error 7 Move while unhomed 8 Invalid setting e Clear error conditions H Clears the error and moves the valve to its home position Gilson VALVEMATE II Valve Actuator User s Guide C 3 spuewwo gt DOISD GSIOC Commands Appendix C Command Description K Reads status of input and front keys Returns abcd where a contact input HOME 0 if open 1 if closed b contact input ROTATE 0 if open 1 if closed c Counterclockwise arrow key d Clockwise arrow key Lx Locks or unlocks the front panel depending on the value assigned to x 0 unlock front panel 1 lock front panel L Reads the front panel lock state Returns x where 0 unlocked 1 locked M Reads the current motor position Returns s where P Parked R Running U Unpowered E Error Px Moves the valve to the position set by x P Returns the current valve position 1 10 T Returns s xxPs yyPt where c 4 S Valve selection switch setting XX Number of positions yy Number of ports Gilson VALVEMATE II Valve Actuator User s Guide
19. he piece of tubing Let the end of the tubing extend past the end of the ferrule When connecting the tubing to the port make sure the tubing presses against the bottom of the port before you tighten the nut Stainless steel plumbing package prep 0 030 ID x 1 16 OD tubing Part number 33035255 494C23006 LZN1 ZF1S6 i 494C53006 0 030 ID x 1 16 OD stainless steel tubing 494C23000 2 10 Gilson VALVEMATE II Valve Actuator User s Guide Installation 2 Stainless steel plumbing package analytical 0 010 ID x 1 16 OD tubing Part number 33035256 494C22006 494C52006 LZN1 ZF1S6 NN 0 010 ID x 1 16 OD stainless steel tubing 494C2H2000 494C5H2000 Gilson VALVEMATE II Valve Actuator User s Guide 2 11 suol 229UUOD Huiquinid Plumbing Connections Installation 2 PEEK plumbing package prep 0 030 ID x 1 16 OD tubing Part number 33035257 494C253186 LZN1PK ZF1PK 494C 22Z3186 0 030 ID x 1 16 OD PEEK tubing 494C22Z3180 2 12 Gilson VALVEMATE II Valve Actuator User s Guide Installation 2 PEEK plumbing package analytical 0 010 ID x 1 16 OD tubing Part number 33035258 494C52346 LZN1PK ZF1PK 0 010 ID x 1 16 OD PEEK tubing 494C52340 TFE plumbing package 0 060 ID x 1 8 OD tubing Part number 330352
20. mber Description continued 494C5H2340 High pressure PEEK multi position valve 10 position 10 port 0 016 ID ports 5000 psi liquid 50 C max 494C53006 High pressure stainless steel multi position valve 6 position 6 port 0 030 ID ports 5000 psi liquid 75 C max 494C253186 Low pressure PPS multi position valve 6 position 6 port 0 030 ID ports 100 psi gas 250 psi liquid 75 C max 494C256186 Low pressure PPS multi position valve 6 position 6 port 0 060 ID ports 100 psi gas 250 psi liquid 75 C max 494C256188 Low pressure PPS multi position valve 8 position 8 port 0 060 ID ports 100 psi gas 250 psi liquid 75 C max Control Computer control by TRILUTION Software and GSIOC RS 232 to GSIOC interface is needed Remote control by contact closure with remote cable part number 33035261 ordered separately e Manual control by front panel operation Environmental Indoor use conditions Altitude up to 2000 m Temperature range 5 40 C Air pressure 75 105 kPa Pollution degree 1 or 2 in accordance with IEC 66 Humidity Maximum relative humidity 80 for temperatures up to 31 C decreasing linearly to 50 relative humidity at 40 C 1 8 Gilson VALVEMATE II Valve Actuator User s Guide Introduction Technical Specification Front panel Definition Two arrow keys to advance valve position and two seven segment blue LED displays Liquid contact materi
21. mits Gilson VALVEMATE II Valve Actuator User s Guide Introduction Definition Technical Specification Available valves Part Number Description 494C22006 Analytical stainless steel valve 2 position 6 port 0 016 ID ports 5000 psi liquid 75 C max 494C2H2000 Analytical stainless steel valve 2 position 10 port 0 016 ID ports 5000 psi liquid 75 C max 494C23006 Preparative stainless steel valve 2 position 6 port 0 030 ID ports 5000 psi liquid 75 C max 494C23000 Preparative stainless steel valve 2 position 10 port 0 030 ID ports 3500 psi liquid 75 C max 494C22Z3186 Preparative PPS valve 2 position 6 port 0 030 ID ports 100 psi gas 250 psi liquid 75 C max 494C22Z3180 Preparative PPS valve 2 position 10 port 0 030 ID ports 100 psi gas 250 psi liquid 75 C max 494C52006 High pressure stainless steel multi position valve 6 position 6 port 0 016 ID ports 5000 psi liquid 75 C max 494C5H2000 High pressure stainless steel multi position valve 10 position 10 port 0 016 ID ports 5000 psi liquid 75 C max 494C52346 Gilson VALVEMATE II Valve Actuator User s Guide High pressure PEEK multi position valve 6 position 6 port 0 016 ID ports 5000 psi liquid 50 C max suoljerdijinads jed1uyra Technical Specifications Introduction 1 Technical Specification Definition Available valves Part Nu
22. nd conditions you were using when the problem arose e list of other devices connected to the VALVEMATE Il and a description of those connections e valve installed in the VALVEMATE II e list of other electrical connections in the room Warranty Repair Units covered under warranty will be repaired and returned to you at no charge If you have any questions about applicability please contact your local distributor Non Warranty Repair For out of warranty repairs contact your local distributor A Customer Service representative will discuss service options with you and can assist in making arrangements to return the equipment if necessary Rebuilt Exchange For some units rebuilt exchange components are available Contact your local distributor for details Gilson VALVEMATE II Valve Actuator User s Guide 5 5 Ss DIjOd U1N y pue sleday Repair and Return Policies Troubleshooting 5 5 6 Return Procedure Contact your local distributor s Customer Service Department to obtain authorization before returning any Gilson equipment To return a piece of equipment e Carefully pack the unit to prevent damage in transit Check with your distributor regarding proper method of shipment No responsibility is assumed by Gilson or your distributor for damage caused by improperly packaged instruments Indicate the authorization on the carton and on the packing slip Always insure for the replacement value of the unit Incl
23. ny carriers must receive concealed damage claims within seven days of delivery Standard Equipment Once the VALVEMATE II and accessories are unpacked you should have the following e VALVEMATE II with appropriate valve installed if the valve was ordered along with the VALVEMATE II 9 64 Allen wrench power supply 24V desktop universal e power cord 110V power cord 220V e shielded GSIOC cable 30 Keep the original container and packing assembly in case the VALVEMATE II must be returned to the factory Documentation The following documents are included with the VALVEMATE II e VALVEMATE II Documentation CD IQ procedure booklet e Unpacking the VALVEMATE II e Declaration of Conformity Gilson VALVEMATE II Valve Actuator User s Guide Introduction Accessories Valves and Plumbing Packages Based on your configuration you may also receive one of the following valves and plumbing packages ordered separately Gilson VALVEMATE II Valve Actuator User s Guide Valve Plumbing Package Part ae Part ao Number Description Number Description 494C23006 Preparative stainless steel valve 2 position 6 port 0 030 ID ports 494C23000 Preparative stainless steel valve 33035255 Stainless steel prep 2 position 10 port 0 030 ID ports 0 030 ID x 1 16 OD tubing 494C53006 High pressure stainless steel multi position valve 6 position 6 port 0 030 ID po
24. one of the arrow keys 5 Dispense additional liquid into port 2 6 Verify that the liquid exits port 1 Placing the valve in its home position Remove the valve from the instrument Using needle nosed pliers turn the valve so the pin on the back of the valve is vertical aligned with the locating hole Then re install the valve and check the flow using a syringe If the liquid is flowing out of the port opposite port 1 port 4 in a 6 port valve or port 6 in a 10 port valve turn the valve 180 degrees with the needle nosed pliers re install the valve and check the flow using the syringe Gilson VALVEMATE II Valve Actuator User s Guide Installation Plumbing Connections Before making the connections locate one of the following plumbing packages ordered separately Note All packages include surplus tubing and fittings Stainless steel plumbing package prep 0 030 ID x 1 16 OD tubing Part number 33035255 Stainless steel plumbing package analytical 0 010 ID x 1 16 OD tubing Part number 33035256 PEEK plumbing package prep 0 030 ID x 1 16 OD tubing Part number 33035257 PEEK plumbing package analytical 0 010 ID x 1 16 OD tubing Part number 33035258 TFE plumbing package 0 060 ID x 1 8 OD tubing Part number 33035259 Part Number Qty Description 499331519 2 Stainless steel tubing 0 030 ID x 0 062 1 16 OD x5 ft 494LZN1 10 1 Valco LZN1 10 stainless steel nut 0 75
25. ormation on this setting 5 Power receptacle 2 2 Gilson VALVEMATE II Valve Actuator User s Guide Installation GSIOC Gilson systems feature a two way communication interface between the computer and most Gilson modules Communication occurs along the Gilson Serial Input Output Channel GSIOC Use the GSIOC cable supplied in the accessory package to link the VALVEMATE II to other GSIOC modules Refer to the diagram below Connectto another GSIOC cable to link modules GSIOC cable Connect to another GSIOC cable to link modules SI __ ea Use the female connector located individually at one end of the cable to connect the GSIOC cable to another GSIOC cable in the system Tighten the retaining screws Connect the other female connector located on the same end as the male connector to the VALVEMATE II Tighten the retaining screws Use the male connector to join another GSIOC cable and make the necessary connection to the next Gilson module Unit ID The unit ID identifies the VALVEMATE II to Gilson software packages that can issue GSIOC commands to the VALVEMATE II At the factory Gilson set the unit ID to 35 There is no need to change this number unless it is the same as that assigned to another Gilson device that s also connected along the GSIOC If you are using more than one VALVEMATE II you will need to change the default unit ID on one of them To change the unit ID 1 Gently insert
26. rts 494C22006 Analytical stainless steel valve 2 position 6 port 0 016 ID ports 494C2H2000 Analytical stainless steel valve 2 position 10 port 0 016 ID ports ere Stainless steel analytical 494C52006 High pressure stainless steel multi position valve 0 010 ID x 1 16 OD tubing 6 position 6 port 0 016 ID ports 494C5H2000 High pressure stainless steel multi position valve 10 position 10 port 0 016 ID ports 494C22Z3186 Preparative PPS valve 2 position 6 port 0 030 ID ports 494C22Z3180 Preparative PPS valve 33035257 PEEK prep 2 position 10 port 0 030 ID ports 0 030 ID x 1 16 OD tubing 494C253186 Low pressure PPS multi position valve 6 position 6 port 0 030 ID ports 494C52346 High pressure PEEK multi position valve 6 position 6 port 0 016 ID ports ore PEEK analytical 494C5H2340 High pressure PEEK multi position valve 0 010 ID x 1 16 OD tubing 10 position 10 port 0 016 ID ports 494C256186 Low pressure PPS multi position valve 6 position 6 port 0 060 ID ports TFE 33035259 i 2 494C256188 Low pressure PPS multi position valve 0 060 ID x 1 8 OD tubing 8 position 8 port 0 060 ID ports Buppedun Unpacking Introduction Other Accessories Based on your configuration you may also receive one of the following accessories ordered separately Part Number Description 3303522 VALVEMATE II connector plate 33035261 Remote cable Gilson VALVEMATE II Valve Actuator User s Guid
27. rument and tighten the Allen screw coupler Note The locating hole on the top of i 3 Allen screw the valve should line up with the pin on the front of the collar front of the VALVEMATE II 6 Reconnect the power supply to the with no valve installed VALVEMATE II Gilson VALVEMATE II Valve Actuator User s Guide O locating hole back of valve 2 7 uo1 ejje su AJLA Valve Installation Installation 2 8 Checking Valve Position and Liquid Flow Refer to the appropriate procedures below Multi position valve 494C52006 494C5H2000 494C52346 494C5H2340 494C 53006 494C253186 494C256186 494C256188 To verify that the valve is properly installed 1 Fill a syringe 2 Connect the syringe to the center port and dispense liquid into the port 3 Verify that the liquid exits port 1 If it does not the valve may not have been homed Refer to Placing the valve in its home position below 4 Press the counterclockwise arrow key 5 Dispense additional liquid into the center port 6 Verify that the liquid exits port 2 Two position valve 494C22006 494C2H2000 494C23006 494C2H3000 494C22Z3186 494C22Z3180 To verify that the valve is properly installed 1 Fill a syringe 2 Connect the syringe to port 2 and dispense liquid into the port 3 Verify that the liquid exits port 3 If it does not the valve may not have been homed Refer to Placing the valve in its home position below 4 Press
28. tings 0 016 ID ports 494COROH Rotor Valcon H for 10 port analytical valve part number 494C2H2000 1 16 fittings 0 016 ID ports 494C230R6 Rotor Valcon H for 6 port preparative valve part number 494C23006 1 16 fittings 0 030 ID ports 494C230RO Rotor Valcon H for 10 port preparative valve part number 494C23000 1 16 fittings 0 030 ID ports 494C12316 Rotor Valcon E2 for 6 port valve part number 494C22Z3186 1 16 Valco ZDV fittings 0 030 ID ports 494C12310 Rotor Valcon E2 for 10 port valve part number 494C22Z3 180 1 16 Valco ZDV fittings 0 030 ID ports 494C520R6 Rotor Valcon H for 6 position HPLC stream selector part number 494C52006 1 16 fittings 0 016 ID ports 494C520ROH Rotor Valcon H for 10 position HPLC stream selector part number 494C5H2000 1 16 fittings 0 016 ID ports 494C523R6 Rotor Valcon E for 6 position HPLC stream selector part number 494C52346 1 16 fittings 0 016 ID ports 494C523ROH Rotor Valcon E for 10 position HPLC stream selector part number 494C5H2340 1 16 fittings 0 016 ID ports 494C530R6 Rotor Valcon H for 6 position valve part number 494C53006 1 16 fittings 0 030 ID ports 494C25316 Rotor Valcon E2 for 6 position stream selector part number 494C253186 1 4 28 fitting details for 1 16 tubing 0 030 ID ports 494C25616 Rotor Valcon E2 for 6 position stream selector part number 494C256186 1 4 28 fitting details for 1 8 tubing 0 060 ID por
29. ts 494C25618 Rotor Valcon E2 for 8 position stream selector part number 494C256188 1 4 28 fitting details for 1 8 tubing 0 060 ID ports Gilson VALVEMATE II Valve Actuator User s Guide A 3 Sal0ssad2y pue s ieg JUaWaDL day Replacement Parts and Accessories Appendix A Plumbing Packages Part Number Description 33035255 Stainless steel plumbing package prep 0 030 ID x 1 16 OD tubing 33035256 Stainless steel plumbing package analytical 0 010 ID x 1 16 OD tubing 33035257 PEEK plumbing package prep 0 030 ID x 1 16 OD tubing 33035258 PEEK plumbing package analytical 0 010 ID x 1 16 OD tubing 33035259 TFE plumbing package 0 060 ID x 1 8 OD tubing Tubing and Fittings Part Number Description 499331519 Stainless steel tubing 0 030 ID x 0 062 1 16 OD x 5 ft 499311519 Stainless steel tubing 0 010 ID x 0 062 1 16 OD x 5 ft 49953059 PEEK tubing 0 030 ID x 0 062 1 16 OD x 5 ft 49951059 PEEK tubing 0 010 ID x 0 062 1 16 OD x 5 ft 495032 TFE Tubing 1 5 mm ID x 3 0 mm OD 1 8 10 ft pkg 494LZN1 10 Valco LZN1 10 stainless steel nut 0 75 long for 1 16 OD tubing package of 10 490318021 VALCO ZF1S6 10 Type 316 stainless ferrules 1 16 package of 10 494LZN1PK 10 Valco LZN1PK 10 PEEK nut 0 87 long for 1 16 OD tubing package of 10 49031805 Valco ZF1PK 10 PEEK ferrule 1 16 package of 10 49041017P Upchurch P 301 NUT FLANGELESS 1 8 IN 1 4 28 D
30. ude a description of symptoms your name address phone number and purchase order to cover repair costs return and shipping charges if your institution requires it Unit End of Life When a unit reaches the end of its useful life refer to www gilson com for directions and information on the end of life policy This is in accordance with the European Union Directive 2002 96 EC on Waste m Electrical and Electronic Equipment WEEE Gilson VALVEMATE II Valve Actuator User s Guide Replacement Parts and Accessories A Valves Part Number Description 494C22006 Analytical stainless steel valve 2 position 6 port with Valcon H rotor 0 016 ID ports 1 16 tubing and fittings 494C2H2000 Analytical stainless steel valve 2 position 10 port with Valcon H rotor 0 016 ID ports 1 16 tubing and fittings 494C23006 Preparative stainless steel valve 2 position 6 port with Valcon H rotor 0 030 ID ports 1 16 tubing and fittings 494C23000 Preparative stainless steel valve 2 position 10 port with Valcon H rotor 0 030 ID ports 1 16 tubing and fittings 494C22Z3186 Preparative PPS valve 2 position 6 port with Valcon E2 rotor 0 030 ID ports 10 32 fittings 1 16 tubing 494C22Z3180 Preparative PPS valve 2 position 10 port with Valcon E2 rotor 0 030 ID ports 10 32 fittings 1 16 tubing 494C52006 High pressure stainless steel multi position valve 6 position 6 port with Valcon H rotor
31. uted immediately temporarily interrupting other commands in progress GSIOC Command List In the command list on the following pages the GSIOC command must be entered in the proper upper or lower case format If a buffered command requires additional information you ll see italicized text next to the command The description of the command identifies what you need to enter in place of the italicized parameter Also note that if a parameter is optional it appears within brackets Immediate B Buffered Gilson VALVEMATE II Valve Actuator User s Guide Appendix C Command Description Identifies the selected slave device Returns character string ValveMate Il vx y z where x y and z represent the firmware version Returns and resets the VALVEMATE II to the power on condition and homes the VALVEMATE II 9 Resets the information in the non volatile memory NV RAM n x Sets NV RAM address and optionally sets location n to value x Returns n x where n the current NV RAM address x the value that location contains Returns eemppabcd where ee error code m motor status pp valve position abcd CC and key input status e Returns n where n is one of the error codes listed below Refer to Error Messages on page 5 2 for details on each error 0 No error 1 Unknown command 2 Invalid NV RAM address 3 Move while busy 4 Positioning
32. y ed MOJ4 AJLA Appendix B Part Number Description Low pressure PPS multi position valve 494C256188 8 position 8 port with Valcon E2 rotor 0 060 ID ports 1 8 tubing 1 4 28 fittings Valve Flow Path Diagrams and Materials B 4 Gilson VALVEMATE II Valve Actuator User s Guide Appendix B Materials Nitronic 60 Chemical resistance is similar to Type 316 stainless but its resistance to galling and oxidation make it superior to Type 316 or 303 in the majority of applications Stainless steel Type 316 This is the standard tubing material for chromatography suitable for a wide variety of applications It is cold drawn seamless not welded with close tolerances held on both ID and OD Type 316 is most commonly used for HPLC because of its superior chloride ion resistance PAEK Polyaryletherketone is the generic name for the family of polyketone compounds PAEK includes PEK PEEK PEKK and PEKEKK which differ in physical properties and to a lesser degree in inertness A range of PAEK based composites are used for valves and fittings These composites resist all common HPLC solvents and dilute acids and bases However concentrated or prolonged use of halogenated solvents may cause the polymer to swell Avoid concentrated sulfuric or nitric acids over 10 PEEK Considered relatively inert and biocompatible polyetheretherketone tubing can withstand temperatures up to 100 C Under the right circumstances
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