Cirrus GPC Software User Guide Cirrus 软件使用手册
Contents
1. PUE Ca ee eb en rh Conditiona Batu Callertisn hovel Saises dab ler gr Pami Wede F mu ums Tujsstisn Puss w ap Jir TIJ ja Bastia HE FL Lew reug 7 x Baia Caii erii an Aa ie Lamquh H PT E E elus bua F puse EE 15 pans Ha Instruments 2 Views Method Browser 29 Select a method from the list to display a preview 3 Collection Runlist CEAR T T e Fai Iren F FA Ete eee ORERE RET ARKE 30 ESRT WERP EREMI RRA XA k fRtnUWElI2minBlnup WARN 25min rJ FER Ws IU E E C 3 5min 4 100 200k 5 Multi Offline workbook Method Browser Sample Analysis Method Use VS data only Use IW to calculateg 7 aope Apna mtercept Ts T beg H2. E GPC Online Multi Online GPC Online Multi Online PL DataStream COD 2 3 wE ENTA 4 50 DIFA AWAR C60 l ipemo Data GPC Online Workbook Summary 81 x File eR View Collection ATUM Help T H p Dae ER TEEI IK pur Views Workbook Summary Sj lt Workbook i Suhmary z CIRRUS GPC Multi Detector Software ut Method Browser Cirrus Workbook Workbook CACirrus WorkbooksW Demo Data emo Data plw Collection Title Demonstration Data for Tutorials Runlst Comments This is a Workbook containing demonstration Data Ver 1 0 Workbook Details Analysis Eluent THF Column Set 7 Flow Rate ml min 1 0000 Temperature Ambient tol Inj V ol ul 100 00 Run Time 10 00 mins at 1 Hz Results n v z FE E Ft Name Collection Device Channel Gain mv Calibratio n Browser Concentration datastream on COMI RICI 1280 H Run List Status Faral Collecting Not Connected evice Monitor Processing Samples in this Workbook Batch Name amp of Samples 10 07 2000 7 11 07 2000 3 12 07 2000 5 Help 0 0 UNE p
3. Workbook ER LUE workbook Conditions Data Collection Instruments Dptions Pump a Eluent THF RI Flow Hate 1 ml min Temperature Ambient ME j Detalls Column Set gj Total Length 0 mm Detalls Detectors Collection Device Channel Gain RI datastream on TOMI RIL 1280 Autosampler Present E Hab ss Injection Valve Loop Size Data Collection Run length Data Collection Sampling rate 12 Workbook L Automated e Manual Detale Bolection uela Time Instruments Options Method Browser Window Method Browser DISCI EA Method Method Browser Method Edit Method Method BrowsertE N A SE BV fEMethod F 3 XE PENew Method l lipemo Data GPC Online Method Browser File Edit view Colection Method Window Help Da66035 xB81 G j mmg
4. 3 5min 4 5 GPC Offline workbook Method Browser Data Processing Do Data Processing Bala phe es i reo irpo P Analysis Runlist 24 Workbook File Import Chromatograms Cirrus Calber AIA CDF ChemStation A Dene Maia phe CPT li Lu B Unknown Narrow Standard Broad Standard Method Fis Le m z be z Du ikte Sg HH AHT ya 25 Analysis Next AnalysisdZ Hl poeet paree
5. Method Browser Method Calibration Calibration Calibration Creation Modified Hame Status Date Type Date Date T view Only o 2001 5 10 14 2001 5 10 14 MUUTT 2 Review Peak 7 2001 5 10 14 2001 5 10 14 3 Manual Analy 2001 5 10 14 Narrow Stan 2001 5 10 14 2001 5 10 14 et Auto Analysi 2001 5 10 14 Narrow Stan 2001 5 10 14 2002 1 11 15 Method Browser PI Summary of Method View Only Collection This Method can be usd to View Chromatograms without performing any Processing Data Processing is Runlist Comments i switched off amp Pause time set to 1 second Column Calibration Status Analysis Last Calibrated Using yin Curve Fit No of Points DX Bp A d High Limit RT mins Flow Marker RT mins Results Low Limit RT mins K Alpha Calibration Data Processing E Perform Data Processing No E Use Flow Rate Correction No RT Window mins 1 00 Collection Karker Nane Device Monitor Column Calibrations Generate using Narrow Standard Default Curve Fit to apply Polynomial order 1 Calibrant Samples uto Detect Peaks Yes auto ssign Ws No Unknown Samples uto Detect Peaks Yes Do uto Calculations No Done f nu General Ji HH Do Data Processing Use Flow Rate Correction Results Time Between Chromatograms IX General Column Cali
6. Hide Columns Shaw All Columns Results Window Results IL TT EPE i LIT T L Fh Ed Vemm Poems Wimke Hels JD Gk medo 0 I ERI YI Diag o piuma herda hag EE EGER EF Samcie Name Injection Number v Batch Mame urik1 ELTE amples 15 1 71 TOF ALD AU ps 14 47 15 E TU Or AH Eiai uki MG imporbed 13 1 1007 2000 2001105 14 39 33 10 C 2000 0006 ri wk AQ imporbed 13 1 1007 2000 ZUO1 10 5 EA TU Du AOU rit UHEM LIE 1 TI OF EE uh ZIE TI 14 45 8 T1 Er ZODUHUDIEHI es UHEHCwH 11 07 2000 h i 200 10 5 14 47 08 11 07 2000 000 epe LUMEN 1 VU z d ZU 10 14 47 15 1 Uu Ai Engh ete saet T View Results File Pd JU O File Edit view Tools Help be as ee e E e e lL win e mm NN ux 0 Concentration mg ml 0 a i Inani nd rs dual i Calibration Browser Window Calibration Browser Demo Data GPC Offline Calibration Browser File Edit view Calibration Window Help 3 e e amp MIT 1 9 f current Calibrations LS Views Calibration Browser m Method Creation Curve Fit
7. m Demo Data GPC Online Workbook Summary TEA Workbook Summary t Method bijn Cirrus Workbook Workbook CACirrus Workbooks Demo DataiDemo Data plw L TE 8 8 ff 1E Title Demonstration Data for Tutorials Runlist Comments This is a Workbook containing demonstration Data Ver 1 0 PTT AWVorkbook Details Eluent THF Column Set Flow Rate ml min 1 0000 Temperature Ambient Inj Vol ul 100 00 Run Time 10 00 mins at 1 Hz Detectors ET Ten TARS Name Collection Device Channel Calibration Browser Concentration datastream on COMI RICI H5 Run List Status Collection i a enis d Collecting Not Connected dz fT J Y A Monitor Processing Samples in this Workbook Batch Name amp of Samples 10 07 2000 7 11 07 2000 A 12 07 2000 5 xti Workbook Details Workbook Experiment TilefllCommentsAb Ehi R Ax Kd BEAGEBIISS B Workbook Demonstration Data far Tutorials This i a Workbook containing demonstration Data Ver 1 0 11 Conditions Eluent Column Set Details Detectors Edit
8. No Injection 1000 525 E m p 5 425 D 300 1375 0 00 1 00 2 00 3 00 4 00 5 00 6 00 7 00 8 00 3 00 10 00 RT minutes Channel 1 o Channel 2 o A Channel 3 o A Channel 4 o For Help press F1 20000 EE F No Injection D gi a E Display Options A Ax Time window Y Axis Scaling Time window mins 10 fs Ajtnscale Smaath Scrolling PE A Hu W Restart Monitoring on Injection Min Apply to All Channels Set as Def
9. Calibration Browser HS Collection Device Monitor 16 Runlist Check Runlist Add Sample Add Multiple Samples Insert Sample Delete Sample Copy Down Parameters Show the Sample Details Clear Runlist Choose Column Hide Column Show AII Column Load Runlist Save Runlist EID ERREA 0000000 DARE 0000 MERE DR O O ZE H N 7v GPC Offline Multi Offline 2H GPC Offline Multi Offline fj Ej GPC Online Multi Online Fi Ed Venen Wieke Hii ale xd CIRRUS GPC Multi Detector Software Esaarit Fikar Rale rah Ta Irg V al al Derirrninrs Rum List Status Piecessimz Siamplex im ilic Varkhsak Hatch N m TO EE aU 1107 2000 12 07 2000 Done Cirrus Workbook UM mas WieekisookaM eus Dia emo Laba phr Demonstration Dala for Tutorial This is a Weskheok eentaireng demonrstraison Data Ver L0 THF Catumn St 10000 Temperabure Amber TOO EI Fun Terma 1E DO rre a E F Name Cellectiom Derice Channel Gain nn C ncentrabi n datastr em an COMI RII 1220
10. 8 of amples 7 3 E x n u GPC Offline Multi Offline Workbook Summary method Browser Analysis Runlist GPC Online Multi Online 17 Analysis Window Analysis EnoshWwaedsteaal T Done Processing Analysis FA Processing Start Analysis Processing Runlist window Help Py Start Analysis F9 i g Add Edit Calibration Comments Comments Add To Calibration f Add To Calibration F10 Calculate Results 4X Calculate Results Fii H Hold F12 Add Edit Calibration 18 Fr Analysis Analysis Window Help Lest zoom LE Autorange lcs AutoRange amp L Autorange Y Annotation A Annotate ES zoom Pe jk Detect Peak Max Delete Peaks And h Detect Peaks And Baseline Baseline A amp Delete Peak Delete Peak T Display Options Display Options Qi Display Method Display Method Choose Columns Choose Columns
11. Add to Calibration Next Analysis A UNEN T ETE 2 CE d S Cakiate Component fe Ciolan Cerent Peak Pm T T T T T T I T T T I T d 4 amp 6 amp 6 T7 B 9 iB 1 iz 12 34 1 amp 15 17 d i 20 21 27 2 234 25 28 17 2 i289 30 3d 32 I3 34 3 6 3T Fateeban Time SA Wendy A re 5 a C3 D RD oea rete ar Cp ott em Calibration Browser 34 re De Dirim Be reb Dus P g d HEI T G zee mter Aja Anak 2901 27 10 Ee 03 44 31 m i Arae a Sh iru A ag Analysis Unknown dn dc Calculate Results Peak Summary 35
12. FRM Name FRM RT mins 0 00 K 14 1000 Alpha 0 7000 Curve Fit Coefficients LogM 2325 3364 X 1 0 3277 X 0 01806 X 0 0005003 X 5 545e 006 X Curve Fit Statistics Residual Sum of Squares 0 000710653 Corrected Sum of Squares 15 8659 Details Points Calibration Unlock Selected Column Show Calibration Details HERI P 173 5 amp Calibration N RA callbration Graph Wind S Add Point K Alpha Edit Parameters change Curve Fit Undo ll Changes Je Test Calibration Show All earns Reviewer Reviewer 21 GPC RI 1 GPC Online Create a New Workbook Workbook Experiment Tile Comment Conditions RI dide he Werkbes
13. File New Workbook amp J T LIES Voc cM SN en Workbook rl Open Workbook l pou Save Workbook As Save Workbook As FETTE EA CER pid idet is NUECUR m workbook Details Close Workbook BAM m m TE EM cc HM Workbook Details LTEBES ZI RE es 0000000007 Import Chromatogram Print Ctrl F Print Preview dida 1 Demo Data 2 Ciucirrus Workbooks testO2 3 Mew Workbook Ctrl M Exit Edit TT a Dr EE Ba copy cuts esse Chev PAISEH View Toolbars d EM stus Bar Shortcut Bar Shortcut Bar FA Collection e MUTET Start Injection FE Start Injection e E Lm Stop Injection e Stop Injection zi EMAIL gt Ready Collection Device F8 Ready Collection Device Get Collection Device Version aet Gollection Device version Window eem Workbook Summar w zx Workbook Summar y Id Method Browser Ae 75Method Browser 2 Method Browser 6 Calibration Browser Calibration Browser Calibration Browser 10 TH a Workbook Summary 1E Zr Ju P TE AFN Fa Window E M rh Workbook Summary
14. Beliti ems bann CaLlertios Hostel Biati Em T Kahn 3 nimis Pee mm ses prae E Data Collection 27 Werkbesh Conditions Paha Cullevtion ES SEE dla ml er mami iai Fee S i Tejsstisn Valen A mde em la tita a E WI ba A rm 15 DE manet a Ha E 3 Instruments 2 Views Method Browser a UM UR yes edam Bei Wh bp We 4m t M eethod Browser Select a method from the list ta display a preview Do Data Processing Do Data Processing a C niss sihe LIT E T Diaries Mer met S je Y imre EH T 23 3 Collection Runlist PM 12min 25min
15. Height Approximation Use 1 data pointin Ive Hultiple Peaks Calculate Mw Ranges Detail Cancel Apply Help 15 Peak Detection Peak Detection Feak Detection Systemdetects Stnt ea 01000 a Cx m Hi Baseline Assignment Apply Horizontal Baseline Ju C Fired RT D FT imne Average in Range E to fo BT mime tr Start of First Peak Cancel Apply Help Reporting User Programs Collection Runlist Window Collection Runlist Runlist m Demo Data GPC Online Runlist I ie x File Edit View Collection Processing Runlist Window Help jn moo gi A s amp A Check Runlist 5 Add Sample Views Runlist abs r EN Add Multiple Samples j p i enar Sample Ho Bat P Insert Sample Filename Sample Type Method Cal Version 3 x Delete Sample workbook Summary Copy Down Parameters gt t ax n eja E i e X 0 ul Show Sample Details P Clear Runlist Method Choose Columns Browser Hide Columns Show All Columns iij Load Runlist Collection Save Runlist Runlist Analysis itn Were Results P
16. PL DataStream Monitor Cirrus File Channel View Help lele tel toaln For Help press F1 Channel M ili Add Channel E Add Channel A SEO RC CS PRG OK reTIImER X e er s aes esm Add Channel x Choose a Collection Device Channel datastream on COM1 Channel 4 For Help press F1 MERE m amp PL DataStream Monitor Channel 1 on DataStream on COM1 File Channel view Window Help 8 x amp er soeomu mm
17. 4 18 37 14 19 ZU 1 221 3 4 25 i8 27 20 i9 XQ X1 d 32 M o3 tation Tiri Tis PEPTT Be apr Mn m uoce Peak Summary dn dc Concentration QKE Peak MW RITE V SERJE to Detector Calibration tui heri hata baby ais E ETE pep 1 mp nl aus ree nl Gee nm 3 4 8 amp 7T B 39 1B 1 iz 12 34 1 15 47 14 t 20 z1 27 20 24 25 78 27 2M 79 20 X 37 00 34 X x 3T Repat Timer Rey Ri E Md E lida oca iaa H Cmemerts Cute i mM pr Tris mesuxd a 201 5 10 TR eri m Aca Pu merhadh pui S IO TP Geoff Mese uan Bi Prhod c 2000 35 10 TR aft Analysis Next Analysis 33 AS Ir s o Ene AS NSEN Kun 2 P5 2 J9nogoD 30300 Bateh PS Calibrants Filename ps calibrantis UU gra Type o Harrow Standard usimg marbad Universal Calibration 7 3 4 gE 7 B 9 1B 1 iz 12 34 0 15 47 14 t 20 z1 27 20 24 25 286 27 2M 79 20 X 37 00 34 X 3T Retna Time Dore Wee A MERO Hes a C3 O7 RE rng tret ar C cohorte Sjorstteeme m nante aa Ero r ie um mor mom Peak Summary F J jdn dcfH Concentration WJZ Peak MW IV Calculate Component TV
18. EE Hame Date Limits workbook Nm Manual Analy EN ECEN 2001 5 10 14 Polynomial or 15 95 26 95 CR Auto Analysi aW 1 Narrow Stan 2001 5 10 14 Polynomial or 14 35 2 a D ZD gt Method Browser 2a xi Lj CC i a Analysis Auto Analysis2001 5 10 14 46 31 Runlist Analysis E Results Calibratio n Browser CA NS Reviewer 13 135 14 145 15 155 16 165 17 175 18 185 19 195 20 205 21 215 22 225 23 235 24 245 25 255 26 265 27 3 English United States 2RTdmins Ready 15 72 Mins 6 653 logM 20 WEET Fiy3ESRR XHICalibrationfs RANAU F Calibration Window Help l Show Calibration Details m Unlock Selected calibiratian ERIE H Lock Calibration Choose Column Choose Columns Hide Column Hide Calumns Show All Columns Show AII Columns Calibration how Calibration Details Details Points JASO Calibration Details Method Auto Analysis Comments Changed to 5th Order Calibration Date 2006 6 12 11 18 57 Last Modified 2006 6 12 11 18 57 High MW Limit RT mins 14 33 Low MW Limit RT mins 25 55
19. Pa Polymer Laboratories Cirrus GPC Software User Guide Cirrus AE CH BH X JE Joe Vu Ef Ue IET D2001 010 58772 760 1 2 3 010 58772765 100029 www lumiere com cn HH gt zr ET A Hu a OO00000000000000000000000000000000000000000000000000000 r UH eeooeoeoeoooooooooooooooooooooooooocoooooooooooocooooooooooooo LE E O0O000000000000000000000000000000000000000000000000000 SI E Ma d O0O000000000000000000000000000000000000000000000000000 GPC Online Multi onlin sccoo0o00000000000000000000000000000000000 GPC Offline Multi offline soos aod oo odo oo dd v ed de herb E eru AHE SG ROMLIBEERRAEIDUREA AE ooooo0000000000000000000000000000000 1 CPU Pentium II RAM 256MB IFK 800 600 256 HEZE 1024 768 16 ME 2 Windows XP Professional Windows 2000 Professional 3t X hit Microsoft Internet Explorer 4 01 SP2 3 1 setup exe 2 USB Key Sentinel setup exe USB Key Confieurati
20. R uam D OOOD OODD D O O O DO O O D D O 4a o 4A GA 4L GA GA AD UA A i t8 n ZEReviewerZr Ifl P 3x V3 4 B e LIIGADLIN CO MH 2 f DE fee Ds gap Cake Ados Heb jhe bas BEI T 4 u Hil EIJNE E AX 7 COGDEDRDAEXI X ia pi emparied 1 PONPA FE 143 uki ET mpanad 1807 7090 F8 177108 usi 87 emere Pe 16 13718 A AL LO ing d rie GPC RI VS 1 Multi Online Create a New Workbook NEXT Multi Online File View Help ma mmm A PN rs fw DD D m oOo g Workbook Concentration Detector Type Refractive Index Light Scattering Detector E Workbook Summary ut ies Viscosity Detector Type lt None gt Collection Runlist Analysis Calibratio n Browser 28 Scattering DetectorAl iz Hr 7jNone Viscosity Detector Type Finish Workbook inei a qiiis aa Conditions Pr HIS 385 m C TEE RIS DJ M f A o m Te DPF n ae ik kkl Dalee miseHE T Viam Workbook Surmany Data Collection H
21. Use reference file Plenarme T T5 No Madel Bras ieg Repeat D rt Data Processing Do Data Processing Analysis Runlist 3 LI File Import Chromatograms Cirrus Calber AIA CDF ChemStation Workbook F LJ Unknown Narrow Standard Broad Standard 2 Method Analysis Next Analysis Chromatogram Concentration Diff Pressure 32 Eun 1 FS 1 7109000 T6800 Bateh PS Calibrants Filename ps calibrantis UOUl egrx Type Harrow Standard using marbad Universal Calibration 2 234 amp 8 7 B G3 iQ 11 iz 12 7
22. ation Manager Fille Option Help Cirus Configuration Collection Device Settings Details Canfiqured Collection Devices Dk Cancel Collection Device Settings Add Configuration Ok PL DataStream Era nfiguration Select Input Device t Miscotek TOA 301 302 C Miscotek Data Manager ce DataStream Name Ab u R55 2 4 e e Ib VALE 73 ES Je Un YEAR SCORE Channel name workbook OK Datastream Co nfiguration Datatream Name Optional Name i o E DataStream Channel Options Channel Hames Despiking ONOFF D espiking Options im B 5 3 3 E ERN Collection Device Settings Ok FHE File Update Settings IBI Cirrus Configuration Manager nl x E File ios nds Save pe Exit Contigured Collection Devices PL DataStream on COM1 OF Cancel Colection Device Settings Edit Collection Devi
23. ault Cancel Time Window Smooth Scrolling 2596 Restart Monitoring on Injection 0 000min Apply to All Channels Set as Default Y Axis Scaling Autoscale Fixed Limits Pb File Exit CHANNEL Add Channel Autorange Axes Autorange Y Plot Mode Drag amp Move Mode Zoom Mode Show Grid Lines Display Options VIEW Toolbar Status Bar Zoom Out Always on Top WINDOW Cascade Tile Horizontally Tile Vertically Always on Top Add Channel amp
24. bration Sample Analysis Peak Detection Reporting User Programs Mame view Orly Lomments MAERA atograms without performing any Processing MES switched off amp Pause time set ta 1 second Data Pracessing Da Data Processing P se Flown Hate Correction Hame Fol S irren i mire Apply Data Pretreatment Setup Report System r Eertormance Parameters pose Results Time between chromatograms secs 1 Cancel Apply Help 14 Column Calibration 91 ftColumn Calibration Generate Using Apply Calibrant Automation General Column Calibration S ample Analysis Peak Detection Reporting User Programs Column Calibration Setup alibrant Automation C Automatic Processing Manual Processing Iv Detect Peaks Automatically Cancel Apply Help Sample Analysis W Automation Peak Detection Calculation General Column Calibration Sample Analysis Peak Detection Reporting User Programs Automatian C Automatic Processing Manual Processing Iv Detect Peaks Automatically Calculation Perform GPC Calculations Ealculation Methad
25. ce Settings Remove fr Cirrus Configuration Cirrus Workbooks Folder Cirrus Templates folder Browse Ok Windows Desktop HL My Documents HD Local Disk C Ese Local Disk D DVD CD RW Drive E o BS DVD Drive F EH Shared Documents ERES B s Documents H E My Mebwark Places Details Cirrus O Cirrus Configuration Manager Tr FMRE File Save Summary txt A 001 Notepad File Edit Format View Help Eummary Installation Path EAT Files Palymer Laboratories cirrus warkBook Path c cirrus workbooks Template Path cC Program Files Polymer Laboratories cirrus Templata configured ports Col Mame PL Datastream Chl Mame RI Chl Filter off ch2 Mame DP ch2 Filter off cha Mame IP cha Filter off cCh4 Name ch4 Filter off other available ports None User name SHAOTAO company name SHMU serial Number NGAG 1717 8076 50LE Install Date Monday 29 May 2006 cirrus version 3 0 cirrus Build au Service Pack Install Type 1 End
26. oa ae De DE Wee pomo ian gie feb ine TN TIE SE E J x nm WEEK eet pa EIAk Ln Ln E ed ps ucc g BT iil te be ee te rm JOLLE EEG iE EB SUC RE wine i 743 0Au T7 Uu U 7uANGX23N3213XN 33 NE Pesten Tera ini desi ea Peak Summary Peak MW Add to Calibration 2 Next Analysis p i lerh Te DE Wes pomo ppi ndm iee imu RT J ENT Ne Tfod d Palenbon Faris Calibration Browser 26 i Die ina yia Mnaiegir 2001 5 DTP 02 48 31 i i T i 118 d 48 ii a Cb 83 df 118 18 d Cas 3 X8 X Hdi zr 0245 2 Hi Mi 0360 Hi m i di FE pues Apa 3 TEI ul Analysis Unknown Calculate Results Peak Summary F EAAS T ipi Hem f S N E gEET kkuEBE AX JEA CCE Analysis Hr x pi ra H m be m Lii An Ah Li as a W 2 ra EJ 9 z Results 27 A Ds iaia phe GPU Oriire Ae De Aea H T 2i Bania ia ie Bauen Mp 1 Toon MED TA
27. on Manager i i PL DataStream Monitor 3 y GPC Offline PL GPC Online PL Report Designer m Getting Started 9 o The Viewer b e s SPA Cirrus File Utility Elk El Cirrus Registration j Report Defect Multi Online Multi Offline Datastream Cirrus Sc ILE UI e TERT W Cirrus Cirrus Configuration Manager PL DataStream Viscotek TDA DM400 HH BOUES PESE AU EL PC Cirrus CWorkbook Template PL Configur
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