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User Manual of AILES beamline

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1. External synchronisatiors OR F Source setting MIA Beamspltter CaF2 O0 Optical Fiter seting Open oe MA Measurement channel Front sample compartment r Background meas channel Back sample compartment ka Detector setting Bolormeter External Pos 5 Preamp gain Re scanner velocity 5k o Sample signal gain Background signal gain 1 ed Delay after device change lo ZEC Delay before measurement lo ZEC Optical bench ready OFF Save and Exit Cancel Help e In the tab Check signal you can use 3 modes previewing the interferogram previewing the spectrum previewing the ADC count displaying the amplitude useful for alignment Note After changing the beamsplitter click on Save Peak Position to save the new position of the ZPD Zero Path difference To validate this new ZPD click on another tab and wait for a bip then return to the tab Check Signal e The Display tab allows you to define the limits of display in Check Signal User Manual of AILES beamline 34 In the dialogue box Repeated measurement you can select to measure scans in series saved independently Note this mode is useful when you do long measurements Repeated Measurements 4 x a Basic a Advanced a Optic Acquisition a FT Display Background Check Signal Experiment Load _ MIRTEST AionxPM O Operator name Administrator Sample description vide cell vide spectro
2. The AILES beamline is located on the right of the main entrance in the Oreille 5 in front of an unloading area SOLEIL provides laboratories of chemistry and biology which requires an authorization prior to the users arrival There is a point of self service nitrogen in front of the main entrance and one in front of the common workshop room the manipulation of gases has to be done with appropriate glasses and gloves available there User Manual of AILES beamline 6 d AILES Laboratory SMIS amp AILES SALLE DE REUNION SALLE DE PREPARATION ATELIER LOCAL POMPAGE 2 1 IR2 2 RESOLUTION HAUTE INTERMEDIARE RESOLUTION p n AILES RESOLUTION AILES beamline shares some rooms with the other infrared beamline of SOLEIL SMIS There is a color code for the doors Yellow doors SMIS Red doors share area AILES SMIS code 1804 e a meeting room meeting relaxing coffee e a preparation room a clean room with microscopic equipments fume hood e a workshop to make assemblies to saw to cut to drill Orange doors AILES code 1803 e room CX1 middle resolution spectroscopy e room CX2 high resolution spectroscopy e the pumping room Area for noisy equipments roughing pumps systems of temperature control e room AR preparing high resolution measurements LPPM Olivier et Didier User Manual of AILES beamline 7 e Infrastructure Electrical distributions Triphased
3. User Manual of AILES beamline Summary ELAM ee e E N E EE E E E E E E 2 FOr 0 n E E E E E AE eee eee 3 T A DOUE ihe DC ANIC iis sisssssescesssseusadenisesdasssesssessdesdesseeucsdunes hdsesawssscssdesdeosssneasdensssbicacendssesesease 4 a Experiments on the beamline iy cotnscs srw seathsnedvncnanavelcioueboces sa seddbinedinewabsraishanphecntaeasentionctincys 4 I Veale Pea UU Tes orhe Derm eee aE OE 5 c AILES beamline in the Synchrotron cee cccccccccecccceeeeseeecceeeeeeaaeeseseeeeeeeeseaaeseeeeeeeeeeaaas 6 DALE EICO e A ytrr en tanen tte rer eener frre tr terre 7 ESED Issacs ests A neces esses ee ecto estou E E E E E E E 8 eey UES E O E E E E E 13 DI er A E E A E E E E 13 Db Satety Approval Sheel SAS Josssie ee E EiS 13 C Io case of meiden corse cists one capeceetycctecoeve at ustea vce erT EESE E EE ETE TE E aN Eea iiaiai 14 ys VV Se E E E A EE E A E E E E EE AEE 14 3 Umo COL GCOS i E E O T E EOE E AOE OEE O 16 a Detectors MCT and InSb wxs sccvsnsssencsdasreepassacsosanbuesenedsaveoad bo baieinessaunoaadoupeenobeesesndhouadenepeawes 16 1a W516 010 6c O MA F a ne edn Oe ee nee ee Pen ee ee eee eee 16 c Pumped Dolometrs at LOR sereine ee RE E eare arsa 18 4 Spectrometer IFS 125 room CX Z sssssscccccecccccccccsoccccccececceccecoococsecococccceccecccceccccosssossssecces 19 a Sample sets available on the spectrometer IFS 125 HR ee ecccceccceeceeeeseeeeeeeeees 20 p Detectors yi AS cs wctecertesecasesstcgecc
4. Ar P1 04mbar cell modulee 16kHz R 1 cm 1 Discharge off Auto Sample form Auto Path C Olivier ConcentrationM odulation File name OH160709 Repeat the measurement fio times Delay between measurements fioo sec Background Single Channel Yacuum Flaps Send Optical Bench Evacuated 0 00hPa Repeated Sample Single Channel Save and Exit Cancel Help Note 1 for more details refer to the OPUS manual aa Note 2 when an internal source is selected you can check this selection on Direct Control Panel in the part Source Control Please do not switch ON the three sources at the same time to avoid overheating r Source Control Ir Source Type Curent state ae wo fF MR oF jon A rR o o af oF Source Temperature OE Se User Manual of AILES beamline 35 a gt To start an acquisition click on Sample Single Channel When the acquisition is completed OPUS shows the spectrum in the active window You can select which file to display on the screen spectrum interferogram or acquisition with the 3 icons on the left of the window OPUS Operator Administrator Administrator Display MIR_R amp D ows 7 File Edit View Window Measure Manipulate Evaluate Display Print Macro Yalidation Setup Help ry Advanced Measurement i A E Repeated Measurements i E l Rapid Scan Time Resolved Measurement 4 y fi ils vey NE mecca F la A jea
5. Measure Manipulate Evaluate Display Print Macro Advanced Measurement Repeated Measurements Wa a Qs m 3 Rapid Scan Time Resolved Measurement J gt vey ANI LA daai OPUS Browser afl OH150709 8 1 o Fa astar af OH150709 9 1 e Fa HISTORY Eig OH 15070910 1 zn ia HISTORY ajf OH150709 11 1 IFG HISTORY iFa HISTORY EQ ra Tsarvs Z 2c IFG istor af OH160709 0 1 Sc IFG HISTORY af OH160709 1 1 Zo A HISTORY af OH160709 2 1 zc IFG HISTORY af OH160709 3 1 Z Ei IFG HISTORY Eig OH160709 5 1 Interleaved Time Resolved Measurement Direct Command Entry Optic Setup and Service Optics Diagnostics Temperature Control Sample Wheel Measurement O 00200 o 00000 Note It is possible to export data format TXT If you want to read your data with other software you have to click on File then Save as There are three tabs on the window Select File you have to add 0 or 1 etc in file name in order to keep the same file name Mode select Data point table as Output Data point table User Manual of AILES beamline 52 5 Backup and Data Recovery Note If the computer is shut down you must login with the account com ailes and the password utilisateur For each acquisition OPUS saves a file on the local hard disk of the PC connected to th
6. Optic Setup and Service en mint Optics Diagnostics SG FG HISTORY i Eig 0H150709 10 1 Bi Temperature Control 3 i TI Sample Wheel Measurement User Manual of AILES beamline 32 e In the tab Basic enter the sample description in the dialogue boxes sample description and sample form which is useful to identify your file The button Sample Single Channel will start acquisition with the chosen parameters Measurement x a Easic Li Advanced a Optic Acquisition a FT Display Background Check Signal Experiment __Load MIRTESTABMxPM Operator name Administrator Sample description vide cell vide spectro Ar P1 04mbar cell module 16kHz R 1 om 1 Discharge off Auto Sample form _ _ _ OT Path C Olivier ConcentrationM odulation File name OH160709 Background Single Channel Vacuum Flaps Send Optical Bench Evacuated 0 00 hPa Sample Comp Evacuated 2 00 hPa Sample Single Channel Save and Exit Cancel Help In the tab Advanced you choose the filename the path of the file the number of scans the spectral acquisition field the resolution e In the tab Optic you set up source diameter of the iris sample compartment front or back detector User Manual of AILES beamline 33 speed of acquisition beamsplitter optical filters x H Basic H Advanced a Optic Acquisition a FT Display Background Check Signal
7. Short Adjust Mode b Then clic on EVACUATE INSTRUMENT acuum Control 2 Vent instrument 3 Evacuate interferometer compartment Commands 4Evacuate sample compartment 5 Vent sample compartment User Manual of AILES beamline 46 c Check that the Primary pump CX1 is ON d Open the valve VM CX1 manual progressively the pumping should not be too noisy e Switch ON the Turbo pump CX when the pressure is at Imbar on GX on GlobalScreen or on electronic bay CH2 and wait for the pressure on GM1 on the spectrometer reaches lt 10 f When pressure is lt 10 3 bar and wait Turbo pump CX reaches max speed 53000 RPM g Open VXI using Global Screen VX has to be green Exp Hutch CX1 ESS User Manual of AILES beamline 47 4 Acquisition a Click on OPUS icon on the desktop select on the login window the user ID default and write the password OPUS OPUS 6 5 OPUS Login User IB Default Default ADMINISTRATOR Password Assigned workspaces Ic Program Files OPUS_65 default ows b Data acquisition In the menu Measure you can access the dialogue box Advanced Measurement in which you can select the parameters of your measurements I OPUS Operator Administrator Administrator Display MIR_R amp D ows T File Edit View Window Measure Manipulate Evaluate Display Print Macro Validation Setup Help L i J Advanced
8. a fire extinguisher to stop it do not take risks and then pass the alert using the red phones or 18 on a landline For a more important fire use the red phone only d Waste Waste products are of several categories Incinerable paper cardboard wood Recyclables metal Specific radioactive chemical and biological User Manual of AILES beamline 14 On the beamline different containers are prepared for different categories of waste Small boxes or yellow bins for bio waste Cans white with a color code for chemical waste red for solvents green bases acid yellow and white for specific waste Waste paper basket Cardboard and wood can be thrown directly in the containers located outside the building User Manual of AILES beamline 15 3 Using detectors a Detectors MCT and InSb On those detectors you have to fill the tank with liquid nitrogen You must refill the tank every 6hours b Bolometers at 4 2 K Generally those bolometers are already connected on a pumping bench permanently Otherwise you should pump the external compartment 48hours before the filling BE CAREFUL DO NOT PUMP THE BOLOMETERS WHEN THE FILTER WHEEL IS ON POSITION 1 SELECT POSITION 2 Say a J PE Helium tank Nitrogen tank x e Fill with liquid nitrogen the helium and the nitrogen tanks e Wait two hours then remove the nitrogen from the central tank using helium gas bott
9. anal Interleaved Time Resolved Measurement OPUS Browser ag 0H150709 8 1 Direct Command Entry _ 3 is astam Optic Setup and Service ad zeal Loo 1 Optics Diagnostics SG IFG HISTORY af OH150709 10 1 Temperature Control a il te Sample Wheel Measurement ELN IFG HISTORY 0 00200 IFG HISTORY Ss z 2c IFG HISTORY af 0H160709 0 1 ze Fa HISTORY af OH160709 1 1 zc IFG HISTORY af OH160709 2 1 S Ei IFG HISTORY Eig OH160709 3 1 Ei IFG HISTORY Eig OH160709 5 1 0 00000 Note It is possible to export data format TXT s a J E If you want to read your data with other software you have to click on File then Save file as 1 There are three parts on the window Select File you have to re type the file number O 1 1n file name in order to keep the initial name Mode select Data point table as Output Data point table User Manual of AILES beamline 36 9 Backup and Data Recovery Note If the computer is shut down you must login with the account com ailes and the password utilisateur For each acquisition OPUS saves a file on the local hard disk of the PC connected to the RCL To export data those data must be copied on the server they will then be accessible from the REL and the RS network In order to avoid loss of data you have to copy your
10. ends at the diamond window of the beamline located on the focalisation point of the mirror M6 The mirror M7 collimates the beam The M8 brings the beam at the correct height The mirror M9 permits to select the spectrometer you want to use VXI and VX2 valves isolate the two spectrometers It is important to preserve the vacuum after the diamond window to limit the risk of pollution of the machine vacuum Devices of the beamline selection mirror valves are controlled by a terminal in room CX2 with software called GlobalScreen The electronic bay which collects electronic controllers is located at the entrance of CX2 Spectrometers are controlled by PC thanks to the software OPUS b Main features of the beamline Field energy Between 1 et 400 meV 8 to 3000 cm Resolution in energy Spectrometer 1 IFS 125 MR 10 3meV 0 008 cm DE E Spectrometer 2 IFS125 HR 10 4meV 0 0008 cm Source Edge magnet Radiation 18x50mrad2 VxH Constant field Radiation 18x25mrad VxH Flow 5 10e13Phot s 0 1 bw 100cm 1 10e13Phot s 0 1 bw 10cm User Manual of AILES beamline 5 c AILES beamline in the Synchrotron SIRIUS BOOSTER 2 75 GeV Main Entrance METROLOGI Projet FEMTO Dipole Onduleur Wiggler Passerelle Vers l entt e principale User Chemistry Laboratory sv Nitrogen bottle Researcher Biology Laboratory Filling Researcher Chemistry Laboratory
11. folder on ailes SOLEIL ruche ailes So you can access to your folder from another PC of SOLEIL There is a folder dedicated to users on the server for archiving data on ailes users on CONTROLE PDC Y You can access to your folder with your SUNSet login and password 10 DATASHEET AILES A DATASHEET software allows to collect all the parameters for each measure of the acquisition file datasheet_ailes exe on the desktop The objective of this software is to facilitate future research on data acquired First you must enter your SUNSet login and password Select the menu Edition then EditProjects On the panel select the project number in the upper left Then you must create an experiment record for your session and a new line for each measurement Remember to select the spectrometer used Finally fill in all fields for each measurement User Manual of AILES beamline 37 Edition AILES Fie Edition Edit tables 3 m m m g Froject r Users Project 20060430 X Iduser 3 Last_Nane g First_rame a P73 BRUBACH ee E Title Dynamics and Structural transitions in Layered cob E ENGEDNE pint 58 Couzinel Bernard 68 DRAGO Nita 67 GAUDART Loreynie X 4 Experiments Name a Date Direclory a Spectro 8 exp 02 07 2009 tmp speclro2 babla 02 07 2009 vtutu apeco2 exp3 0270772009 D Celine Boutons monspectrc asuppimer 02 07 2009 D Celne Dou
12. in the room CX1 in the first drawer of the tool box in the right corner When in front of the local insert the card into the device and follow the instructions delivered by the device to have a new bottle e Fill this same tank with liquid helium using the transfer pipe and the bottle of liquid helium this has to be done with a beamline member e Pump very progressively with the appropriate equipment on the helium tank the pumping has to be done with a member of the beamline e Check the impedance on the BIAS point all switches OFF down using a multimeter and compare with the value written on the bolometer R gt 12Mohms During the filling you should see the resistance increase to its nominal value User Manual of AILES beamline 18 4 Spectrometer IFS 125 room CX2 S al L TA ey 5 A Ez I e Ai K A The spectrometer IFS 125 coupled with the absorption cell M ca 2000 The spectrometer IFS 125 is a high resolution FFT interferometer for the study of diluted matter User Manual of AILES beamline 19 a Sample sets available on the spectrometer IFS 125 HR e White type multi pass cell in general the optical alignment is already done by a AILES member Olivier optical path in the cell up to 200m 6 min vacuum 10 mbar Currently in the far infrared this set allows to show a transition strength of 10 km per mole with a gas pressure of 10 mbar To obtain a good quality high resoluti
13. of the iris sample compartment front or back detector speed of acquisition beamsplitter User Manual of AILES beamline 49 optical filters x H Basic H Advanced a Optic Acquistion H FT Display Background Check Signal External synchronisation oR F Source zetting MIR Beamspitter CF2 O0 OpticalFitersettng Open H Aperture setting jaan Measurement channel Front sample compartment Background meas channel Back sample compartment Detector setting Bolometer Estemal Ps5 0 Preamp gain Rep Scanner velocity Beez s S Sample signal gain 1 Background signal gain 1 Delay after device change fo ZEC Delay before measurement jo ZEC Optical bench ready OFF Save and Exit Cancel Help e In the tab Check signal you can see 3 modes previewing the interferogram previewing the spectrum previewing the ADC count displaying the amplitude useful for alignment Note After changing the beamsplitter click on Save Peak Position to save the new position of the ZPD Zero Path difference To validate this new ZPD click on another tab and wait for a bip then return to the tab Check Signal e The Display tab allows you to define the limits of display in Check Signal In the dialogue box Repeated measurement you can select to measure scans in series saved independently User Manual of AILES beamline 50 Note this mode is usefu
14. outlets Force outlets Mesure outlets o a wt b e Mesure network standard outlets 220V with a green tab Used only for sensitive equipments which needs stability and non disruptive pE e Force network used for all other equipments standard outlets 220V with a white f tab sil e Triphased network for high amperages iN The electrical cabinet where all networks control of the beamline are located is on the alley In case of disjunction you need to call the hall s coordinator 9797 Computer networks e Beamline Control Network RCL Only used for equipments which control the beamline including PCs used for data acquisition and the terminal which controls the beamline e BeamLine Network REL Network to access the Internet and Intranet of SOLEIL all other PC User Manual of AILES beamline 8 To connect a new PC on this network you have to contact the Networking system department of SOLEIL e Ruche is a server which permits to exchange data between RCL and REL e Wifi wireless SOLEIL Network is accessible in the B timent A and the guest rooms Fluid distribution in the pumping room and room CX2 e water e Industrial water Loop system used to cool down equipments e Compressed air A flow of air is available The beamline provides a flow of fry air connected permanently to the entrance of the two spectrometers e Inert Gases Evacuation Toxic
15. position STOP MODE on Direct Control Panel e Open the Michelson compartment amp 2d y l gt gt rg A _ Sh N A bd a y a M gt E X 5 y Michelson Compartiment Case and dessicator for the beamsplitters User Manual of AILES beamline 44 e Open beamsplitter flange and carefully introduce the beamsplitter corresponding to the range for the experiment it is important to put the beamsplitter in the dessicator after use Mid Infrared 8000 450 Far Infrared 6um Mylar 600 20 Far Infrared Silicium Epaisse 600 20 BEAMSPLITTERS HE NE LASER 0 6328 um WAVELENGTH 2501m Ium 10 pm i 100 um 1000 um l l T401 CaF2 NIRI v i i 7 i hs i i 4 Multilayer T222 i T602 Mylar CaF2 UV VIS NIR 25um T204 i 50um T205 a i 125um T208 D i Z A l 9 i LL mT i i I i l l i i I j l i l i 25000 13000 i 40000 i 10000 4000 1000 40 100 40 10 5 uv VIS NIR l MIR I FiR gt WAVENUMBER cm e Place flange carefully make sure that the gasket is covered to prevent leaking User Manual of AILES beamline 45 3 Evacuating the spectrometer IFS 125 MR VM CX1 A ab O 3 SPECTRO A ISF 125 MR z O O O Pompe Primaire VM PR CX CX1 a Clic on STOP MODE in Control Direct Panel 3 Slow Adjust Mode d Front Short Adjust Mode 5 Back
16. Experiments Name 4 Date 4 Direclory a Spectro 9 5 exp 02 07 2009 tmp speclro2 babla 02 07 2009 vtutu speclro2 exp3 02 07 2009 D Celne B outons monspectre asuppnmer 02 07 2009 D Celine Doutons monspectre y7 r Measures i Filename Increment Current Iris Resolution NbSsans Sample Conmenls Gain Speed BeamS plitter Fiter a tuc 10 25 61 120 12 3 esf REF 5kHz KBR OPEN a tuc W 25 51 120 12 3 est HEF 4U kHz KEH F4 a NomFichier 0 120 350 48 10 1 dfg REF 5kHz KBR OPEN a NomFichier 0 121 350 48 10 1 dfg REF 5kHz KBR OPEN a Y 4 Add a measure Gain D A na 4 a Beams plitter cn mi IL rd 4 a oo D 4 on a lt Source Filter cu 4 Pressure 4 ia ee lt Type rm Detector Filename omFichier Increment mi Current oo mm a ties Resolution HbS cans Sample Comments gi l f cL ce oo Ww User Manual of AILES beamline 54 7 Venting spectrometer IFS 125 MR a Close VX using Global Screen VX has to be white on the software b Stop the Turbo pump CX1 c When levitation is displayed on the turbo pump control box close the valve VM CX manual valve to isolate the rough pumping d Open gently the valve VM CX 3 to adjust the flow of dry air on the safety valve e Then open slowly the valve VM CX 2 manual valve to fill the spectrometer f Loosen one small cover in order to avoid high pressur
17. Gases Evacuation General SOLEIL Gases Evacuation network is not available yet so a temporary system has been installed on the line Just connect to the various exhaust on the beamline but be aware of limitations On the left water arrival On the right arrival return of industrial water compressed air and evacuation of gases in the pumping room User Manual of AILES beamline 9 Cryogenic fluids and gases e Liquid Nitrogen tank The beamline provides a tank to store near the beamline liquid nitrogen To fill this tank use the self service point of liquid nitrogen in front of the workshop or at the main entrance see picture page 6 The manipulations have to be done with appropriate glasses and gloves To transfer Nitrogen from this tank e Close the valve 1 put the valve between positions 1 and 2 e Open the valve 2 put the valve on the position 3 You should see the fluid out the transfer pipe after a few seconds IMPORTANT open the valve 1 and close the valve 2 Transfer a ae i 4 er re A i if e a f when not in use The beamline provides also small dewars for filling detectors or other equipment e Liquid Helium tank The line orders 65L or 100L bottles of liquid helium please specify your need prior to your beamtime Transfers of liquid helium have to be done with a member of the beamline in order to avoid unnecessary risks To transfer helium from this tank to the
18. Measurement P i ar Repeated Measurements Wn af i Ds Rapid Scan Time Resolved Measurement 4 y tt BEB Ta i Interleaved Time Resolved Measurement OPUS Browser af 0H150709 5 1 SC IFG HISTORY Elf OH150709 9 1 SC IFG JHISTORY af OH150709 10 1 SG IFG HISTORY Ei 0H150709 11 1 i Direct Command Entry Optic Setup and Service Optics Diagnostics Temperature Control SE AS wh e In the tab Basic enter the sample description in the dialogue boxes sample description and sample form which is important to identify your file User Manual of AILES beamline 48 The button Sample Single Channel will start acquisition with the chosen parameters Measurement x a Easic a Advanced a Optic Acquisition a FT Display Background Check Signal Experiment Load Sample description vide cell vide spectro Ar P1 04mbar cell module 16kHz R 1 cm l Discharge off Auto Sample form T Path C Olivier ConcentrationM odulation File name OH160709 Background Single Channel Yacuum Flaps Send Optical Bench Evacuated 0 00 hPa Sample Comp Evacuated 2 00 hPa Sample Single Channel Save and Exit Cancel Help e In the tab Advanced you choose the filename the path of the file the number of scans the spectral acquisition field the resolution e In the tab Optic you choose source diameter
19. Mid Infrared KBr 4800 450 Far Infrared 6um Mylar 450 80 Far Infrared 50um Mylar 55 20 Far Infrared 125um Mylar User Manual of AILES beamline 26 BEAMSPLITTERS HE NE LASER A 0 6328 um iiaii 250nm H tum l 10 pm 100 um 1000 um i l l l Mylar am T soum T205 5oumT205 T205 i iy 125um T208 25000 13000 i S 40000 i 10000 4000 1000 400 100 40 I lt vuv I VIS NIR l MIR I FiR gt WAVENUMBER cm T602 CaF2 UV VIS NIR EFFICIENCY gt e Close the cover If the beamsplitter is well introduced you will hear a beep 5 Sample compartments There are two sample compartments on the spectrometer IFS 125 Front and Back identified on their covers Do not exchange the covers 6 Evacuating spectrometer IFS 125HR User Manual of AILES beamline 27 VM PT1 CX2 SPECTRO B ISF 125 w O O Q 5 A a Click on STOP MODE on the Direct Control Panel 3 Slow Adjust Mode d Front Short Adjust Mode 5 Back Short Adjust Mode Scanner status Eror mode trying to remit b Then click on EVACUATE INSTRUMENT acuurn Control 2 Vent instrument 3 Evacuate interferometer compartment 4 Evacuate sample compartment 5 Vent sample compartment c Make sure that the Rough Pump CX2 1 in the pumping room is ON User Manual of AILES beamline 28 Primary Pump CX2 1 Control box ON OFF Control box ON OFF Primary Pump CX2 1 Roo
20. Panel Vacuum Control Location Desired state Current state Pressure IF Compartment Evacuated Evacuated 0 04 17 hPa S Mani instrument Sample Compartment Evacuated 0 0417 hPa 3 Evacuate interferometer compartment 4 Evacuate sample compartment 5 Vent sample compartment Source Control Ir Source Type Current state Commands 0 Reinit Scanner 1 Fast Adjust Mode Set scanner mode 19 Siow Adjust Mode 4 Front Short Adjust Mode 5 Back Short Adjust Mode Source Temperature 22 oC Scanner status Error mode trying to reinit Back Refresh The page is divided into 3 parts Vacuum control fro controlling valves and gauges of spectrometer Source control for selecting internal sources or synchrotron Scanner control fro selecting the scanning modes User Manual of AILES beamline 25 4 Changing the beamsplitter of the Interferometer e Before changing the beamsplitter of the Michelson check that the scanner is in position STOP MODE on Direct Control Panel e Open the Michelson compartment basgi r 5 P y ae ws n as gt s3 ya _ i Michelson Compartiment Case and dessicator for the beamsplitters e Open the cover and carefully introduce the new beamsplitter it is important to put the beamsplitter CaF2 et KBr after using in the dessicator located under the mobile mirror compartment ee Visible and UV Quartz 25000 9500 Near Infrared 14000 1850
21. REINIT SCANNER Scanner Control 3 Slow Adjust Mode 4 Front Short Adjust Mode Back Short Adjust Mode Scarner status Error mode trying to remit L Note when you have a problem with the scanner you have to click on REINIT SCANNER on Control Direct Panel Wait a few seconds you have to read IDLE in SCANNER STATUS on the software to begin measure it can take some minutes User Manual of AILES beamline 31 b Click on OPUS icon on the desktop select in the login window the user ID default and write the password OPUS PN ia Folie OPUS 6 5 OPUS Login UserID Default Default ADMINISTRATOR Password Assigned workspaces c Program Files OPUS_65 default ows Password OPUS c Data acquisition In the menu Measure you can access the dialogue box Advanced Measurement in which you can select the parameters of your measruements K OPUS Operator Administrator Administrator Display MIR_R amp D ows S file Edit view window Measure Manipulate Evaluate Display print Macro Validation Setup Help TAR Cm J J Ji Advanced Measurement i p 1 Sr Repeated Measurements Wn B Rapid Scan Time Resolved Measurement lt gt i Bb as ha i Interleaved Time Resolved Measurement OPUS Browser Ei 0H150709 8 1 HE Direct Command Entry O e fa ustory Ga
22. Screen e valves of the interferometer using the software Direct Control Panel e manual valves of rough pumping VM CX2 1 and VM CX2 2 The rough pumping is in the pumping room the ON OFF buttons are on the pumps The control of the two Turbo pumps Turbo pump I CX2 and Turbo pump 2 CxX2 connected directly to the spectrometer is realised uqsing the control boxes located under the interferometer An automatic safety disables the opening or triggers the closing of VX2 threshold pressure 10 2 mbar It prevents against venting the beamline unwillingly User Manual of AILES beamline 22 d Using the spectrometer IFS 125 HR 1 Open Global Screen this software is controlled from the terminal X Gf you have a problem with the software look at the instruction manual To open the AILES supervision software Global Screen Viewer click on the icon on the desktop called GlobalScreen or click on Application then Tango then Supervision and Global Screen Viewer Everybody A To control certain elements of the beamline enter user as identify and user as password B Machine Status button opens a panel containing all the characteristics of the machine i 14 53 m 3 4 se 20 93 h semen eee It se MELE SIRIUS LUCIA DIFFABS am zz 4 1 9 um EEEN 3 83 ni mrad 0 2046 Ez 59 7 um 340 7 um 284 pm rad Shift lignes Med Apr 16 10 22 10 20 Faisceau d di
23. Using spectrometer IFS 125 MR 1 Open Global Screen this software is controlled from the terminal X if you have a problem with the software look at the instruction manual To open the AILES supervision software Global Screen Viewer click on the icon on the desktop called GlobalScreen or click on Application then Tango then Supervision and Global Screen Viewer Everybody A To control certain elements of the beamline enter user as identify and user as password B Machine Status button opens a panel containing all the characteristics of the machine i 14 53 m 3 4 se XELEN ee a ET se Md 742 8 A h UGA DIFFABS ae 4 1 9 um EEEN 3 83 ni mrad 0 2046 Ez 59 7 um 340 7 um 284 pm rad Shift lignes Med Apr 16 10 22 10 20 Faisceau d disponible reinjection 15h00 C Help button opens the AILES GlobalScreen User Manual of AILES beamline 43 To use synchrotron radiation with the spectrometer IFS 125 MR check that e VXI is OPENED green e the mirror M9 is in position EXTRACTED green on the main synoptic e VI V2 V3 et V4 are OPENED e the diagnostic between M3 and M4 is in position EXTRACTED green e the extraction system M1 M2 is in position INSERTED E BR A vet sp cso A 2 Changing the beamsplitter of the Michelson e Before changing the beamsplitter of the Michelson check that the scanner is in
24. anseinanteenseateemacoceenbenaecednexoscisustensrssatansighesencunuesaccueescets 21 or he TINS roeiers tO Chapter is sacspeanctincsamsieninonacctnc a adoncspeaactecosudoadunenandmcorndansuenqutucesndendsens 21 c Evacuating scheme of the spectrometer IFS 125 cececccccccccssssseeeeeceeeeeeeaeeeeeeceeeeeeaaas 22 d Using the Spectrometer IFS 123 TAR oeerenesscnircirrd aoina e ir AEE 23 5 Spectrometer IFS 125 MR room CX1 cccccccooscscccssssesesseesssssovsssssscccccecccessssesssesesssesooees 40 a Sample sets available on the IFS 125 MR sssacacsntventartsinecenssuercascesieanesdvenderdetaniens suereaeenaeess 40 c Evacuating scheme of the spectrometer IFS 125 MR cccccccsssssssseesseseeeeeeeeeeeees 42 d Using spectrometer IFS 123 MR si csacpueeacaeasvasasuiesesasaasvacesaueessasduelsoeenesuledesasdudencdsauesssassucests 43 ANNEXE Manual of Global Screen and Opus User Manual of AILES beamline Foreword This document is a manual for the users of the beamline AILES Advanced Infrared Line Exploited for Spectroscopy of the synchroton SOLEIL It contains information useful to work with this beamline The objective is to facilitate the autonomy of the user Team beamline Pascale ROY Researcher AILES beamline manager 9657 Jean Blaise BRUBACH Researcher beamline scientist SOLEIL 9683 Mylene CHAPUIS Assistant Engineer SOLEIL 9661 Olivier PIRALI Researcher CNRS ISMO 9742 Laurent MANCERON D
25. bolometer e Open the valve 2 in order to evacuate the pressure e Insert slowly the transfer pipe valve2 opened e Close all valves 1 2 et 3 You should see the liquid helium white plume out of the transfer pipe after a few seconds The filling of helium in the bolometer is realised by sliding the short tube in the bolometer central entrance The operation should last less than 10 minutes When you should see a mushroom like smoke implying that the dewar is full the tank is full To finish open the valve and close the other valves Nitrogen Tank Helium Tank The manipulation of nitrogen and helium bottles represents a potential danger of high pressure in the tank So make you sure you always leave a valve open on the tank Note e The storage of gas bottle is forbidden on the line except with special authorizations e Area for gases storage point North amp South are available to users e All gases have to be notified to the security department User Manual of AILES beamline 12 2 Safety rules Every user is aware of the potential risks a Training Users internal or external of SOLEIL must follow the safety training provided by SunSet You just have to log in name password and click on Safety training in the menu on the left side of the screen b Safety Approval Sheet SAS The SAS defines the dangerousness of the experience e green without specific danger e yellow specific dan
26. e RCL To export data those data must be copied on the server they will then be accessible from the REL and the RS network In order to avoid loss of data you have to copy your folder on ailes SOLEIL ruche ailes So you can access to your folder from another PC of SOLEIL There is a folder dedicated to users on the server for archiving data on ailes users on CONTROLE PDC Y You can access to your folder with your SUNSet login and password 6 DATASHEET AILES A DATASHEET software allows to collect all the parameters for each measure of the acquisition file datasheet_ailes exe on the desktop The objective of this software is to facilitate future research on data acquired First you must enter your SUNSet login and password Select the menu Edition then EditProjects On the panel select the project number in the upper left Then you must create an experiment record for your session and a new line for each measurement Remember to select the spectrometer used Finally fill in all fields for each measurement User Manual of AILES beamline 53 Edition AILES Fie Edition _ Edit tables 0 g Froject r Users Project 20060430 X Iduser Last_Nane Qa First_rame a 73 BRUBACH Jean Blaise Title D pnamics and Struclural transitions in Layered cob ConcELST stat 58 Couzinel Berard 68 DRAGO Nita 67 GAUDART Loreyme X 4 r
27. e in the spectrometer g When the spectrometer is vented close the two valves VM CX1 2 and VM CX1 3 manual valves User Manual of AILES beamline 55 ANNEXE You can find OPUS manual on the beamline AILES It contains all details for the use of spectrometers Moreover there are instructions manual for most apparatus in the right side cabinet in room CX2 User Manual of AILES beamline 56
28. ger e rouge identified danger SAS must be signed before the start and at the end of the experiment by the main user by the Hall coordinator and in the case of a risky experiment classified yellow or red by the Security group who check for safety rules application Yellow an red Experiment cannot start outside of classic hours from Monday to Friday from 8 30 to 17 30 If your experiment is scheduled to start on a weekend you should have it approved prior to the official start The SAS is displayed during all the experiment and will be by security group afterwards User Manual of AILES beamline 13 c In case of incident Any safety incident must be reported to the Security department e Case of an injury accident At first contact someone from the list displayed next to the red phone in the alley Otherwise dial 18 on the red phone or contact a hall coordinator 9797 Victims of minor accidents can go directly to the infirmary room A2 0 21 where a rescuer can take care of them For the more serious accidents an external help will come fire fighters or EMS o Case of a fire alarm In the event of an outbreak of the fire alarm leave the place quietly leave the building by the nearest exit check on the evacuation plan displayed in the alley go to the nearest meeting point and waiting for direction of security department or the competent authorities fire fighters If you see a minor fire use
29. irector of Research CNRS LADIR 9741 Engineer to recruit Engineer CNRS ISMO 9666 e Workshop 7 9718 e Line AILES 9764 e Room AILES HR 9765 Emergency numbers e Guard house 9122 e Guard mobile phone 0677203983 e Control room 9840 e Hall Coordinator 9797 e Reception 9191 Useful numbers Helium or gas ordering e Ludovic Frenehard 01 69 35 91 68 User Manual of AILES beamline 3 1 About the beamline a Experiments on the beamline AILES is a beamline dedicated to the study of weak and intermediate strength bounds in diluted and condensed matter It uses the synchrotron radiation as a source in the range near infrared and the Tera Hertz The beamline uses the Fast Fourier Transform spectroscopy on gt a FFT spectrometer with intermediate resolution IFS 125 MR room CX1 for the study of sample of condensed matter gt a FFT spectrometer with high resolution IFS125 HR room CX2 for the study of diluted matter LEIL D CHROTRON d JLE 9 ADVANCED INFRARED LINE EXPLOITED FOR SPECTROSCORY TX DIAGNOSTIC Tz M8 t Tx vo DIAMOND VX1GX1 SPECTRO A WINDOW gt EQUINOXE 55 P EEEE EEE RE SYNCHROTRON RING SPECTRO B IFS125 The photons extraction is realized with a mirror located on a chamber of the ring A group of mirrors permit to carry the beam out of the ring through a radioprotection hutch User Manual of AILES beamline 4 The ultra high vacuum of the machine
30. l when you do long measurements xi a Basic i Advanced a Optic Acquisition a FT Display Background Check Signal Experiment Load MIRTEST APM Operator name Administrator Sample description vide cell vide spectro Ar P1 04mbar cell modulee 16kHz R 1 cm 1 Discharge off Auto Sample form Auto Path C Olivier ConcentrationModulation File name OH160709 Repeat the measurement fio times Delay between measurements f 00 sec Background Single Channel Yacuum Flaps Send Optical Bench Evacuated 0 00hPa Repeated Sample Single Channel Save and Exit Cancel Help Note 1 for more details refer to the manufacturer manual Note 2 when an internal source is selected you can check this selection on Direct Control Panel in the part Source Control Please do not switch ON the three sources at the same time aa to avoid overheating r Source Control Ivy Source Type Current state ae NR MR oF on i Ro oF ial onf oe Source Temperature OK 92 gt To start acquisition click on Sample Single Channel User Manual of AILES beamline 51 When the acquisition is completed OPUS shows the spectrum in the active window You can select which file to display on the screen spectrum interferogram or acquisition with the 3 icons on the left of the window 4 OPUS Operator Administrator Administrator Display MIR_R amp D ows 7 File Edit View Window
31. le near the meeting room special pipe in the HR cabinet for pushing User Manual of AILES beamline 16 e When the nitrogen is removed fill this central tank with liquid helium using the transfer pipe connected to the liquid helium dewar have to be done with a member of the beamline al oint BIAS TEST e Check the impedance on the BIAS point all switches OFF down using a multimeter and compare with the value written on the bolometer R During the filling you should see the resistance increase to its nominal value Note When the bolometer is ON you should wait for bolometer electronics to stabilize at least 15minutes minimum before starting measurements User Manual of AILES beamline 17 c Pumped bolometers at 1 6 K In general bolometers are already connected on a pumping bench permanently Otherwise you should pump the external compartment 48hours before the filling BE CAREFUL DO NOT PUMP THE BOLOMETERS WHEN THE FILTER WHEEL IS ON POSITION 1 SELECT POSITION 2 e Fill with liquid nitrogen both the helium on the center and the nitrogen tanks e Wait two hours then empty the central tank using helium gas bottle near the meeting room special pipe in the HR cabinet Note if the bottle of helium gas is empty there is a local outside on the right of the main entrance where you can retrieve full bottles and drop empty bottles For that you have to take the card AIR LIQUIDE located
32. ll from 65 C to 100 C acryogenic system up to 3 K under development User Manual of AILES beamline 40 b The detectors available for the filling refers to chapter3 MCT detector D313 Bolometer at 4 2 K D211 evacuated bolometer at 1 6 K D211 F Detector characteristics HE NE LASER A 0 6326 pm l logD emie 250m j 10m s gt 2 ti A a i g UV i VISI NR MIR WAVENUMBER cm User Manual of AILES beamline 41 c Evacuating scheme of the spectrometer IFS 125 MR Spectro A IFS 125 MR CX1 Sample compartment VX1 gt lt gt lt x lt x lt VM PR I CX1 Y Turbo Pump1 CX1 Dry air L gende Automatic valve VM PT gt lt control Manual valve gt a m gt lt control Software G Screen gt lt valve control Primary pump CX1 For this spectrometer the user can control e the valve VX1 which isolate the beamline using Global Screen in the room CX2 e the manual valves of rough pumping VM CX1 1 2 et 3 The rough pumping is in the pumping room Leave it ON for the duration of the experiment If you want to stop pumping turn OFF the valve t The user also controls the starting or stopping of the Turbo pump CX1 connected directly to the spectrometer To prevent accidents or manipulation errors an automatic safety triggers the closure of VX1 for pressure gt 10 2 mbar User Manual of AILES beamline 42 d
33. on spectrum you should plan for 48 hours of acquisition with synchrotron emulti pass thermostated cell for liquids and powders temperature range of 25 to 100 optical path in the gas up to 24m 2 1 max medium resolution 10 cm emulti pass cell BRUKER shorter A136 on website Bruker http www brukeroptics com fileadmin be_user Products FT_IR Product_Notes A 136 pdf optical path in the gas up to 8m emolecular supersonic jets currently under development not yet available for users User Manual of AILES beamline 20 b Detectors available for the filling refers to chapter3 e MCT detector D313 e bolometer at 4 2 K D211 e pumped bolometer at 1 6 K D211 F e FIR DTGS e InSb D413 e Diode Si D510 Detector characteristics HE NE LASER A 0 6328 um I l logD fom 250m j thn J x r 40000 i UV VSI NR i WAVENUMBER cm User Manual of AILES beamline 21 c Evacuating scheme of the spectrometer IFS 125 Spectro B IFS 125 CX2 Sample compartment gt lt gt lt D4 D4 VM PR e Turbo Turbo 7 Y Pump1 Pump2 x Dry air CX2 CX2 X j X Legend u VM PT1 VM PT2 a SAZ ee gt lt Po p pA aa n g Roots E a I Pump n CX2 gt lt c Primary Primary Primary g Pump1 Pump Pump CX2 1 CX2 2 CX2 3 For this spectrometer the user can control e valve VX2 which isolate the interferometer from the beamline using Global
34. sponible reinjection 15h00 C Help button opens the AILES GlobalScreen manual User Manual of AILES beamline 23 To use synchrotron radiation with the spectrometer IFS 125 HR e VX2 has to be OPENED green e the mirror M9 has to be in position INSERTED white on the main synoptic e VI V2 V3 and V4 have to be OPENED e the diagnostic between M3 and M4 has to be in position EXTRACTED green e the extraction system M1 M2 has to be in position INSERTED Me ves ico A 0X Main Synoptic Exp Hutch CX1 E55 p ive 3 20 Read aJ GlobalSCREEN File Browser Me com ailes 2 The He Ne laser Normally the spectrometer is ON If it is OFF follow the instruction below e Switch ON the alignment laser He Ne and put in position stabilized frequency wait about 15 minutes if it was OFF green DELs have to be ON or N y i He Ne Laser User Manual of AILES beamline 24 3 Open Direct Control Panel e Switch ON the PC HP7600E which controls the spectrometer IFS125 HR e Open Direct Control Panel by clicking on the icon Internet Explorer default address 1s http 10 10 0 1 DCNTRLO1 HTM Internet Explorer e Check that there is no error message for the vacuum the source the temperature the scanner otherwise look at Optics Diagnostics on OPUS All the windows have to be green if they are yellow you have to wait Direct Control
35. tons monspectre v r Measures he Filename Increment Current Iris Resolution NbSzans Sample Conmenls Gain Speed BeamSplitter Fiter E tuc 10 25 61 120 12 3 esf REF 5 kHz KBR OPEN a tuc WwW 25 51 12u le a est HEF 4U kHz KEH F4 a NomFichier 0 120 350 48 10 1 dfg REF 5 kHz KBR OPEN a NomFichier 0 121 350 48 10 1 dfg REF 5kHz KBR OPEN a v 4 gt Add a measure D ae Ea 4 Gain cm mi IL rd 4 Speed a oo D 4 Beams plitter on a 4 Source Filter 4 cu 4 Pressure Type Detector Filename HomFichier Increment i 5 lg 4 mi l Current Iriz Resolution MHbScans Sample Comments pa tn DJ me oc cn Tm Ci User Manual of AILES beamline 38 11 Venting spectrometer IFS 125 HR a Click on STOP MODE in Direct Control Panel b Close the valve VX2 with Global Screen the valve icon has to be white c Stop the Turbo pump CX2 wait for the displayed levitation on the control box d Close the valve VM PT CX2 1 manual e Check that the valve VM PR CX2 is closed f Check that the Roots pump CX2 is stopped g Click on VENT INSTRUMENT in Direct Control Panel 4Evacuate sample compartment 5 Vent sample compartment h When the spectrometer is vented click on STAND BY in Direct Control Panel in order to stop the flow of dry air Note 1 when you have a problem with the scanner you have to click on REINIT SCANNER on Con
36. trol Direct Panel Wait you have to read IDLE in SCANNER STATUS on the software to begin a measure it can take some minutes Note 2 after clicking on STOP MODE you have to click on REINIT SCANNER User Manual of AILES beamline 39 5 Spectrometer IFS 125 MR room CX1 The spectrometer IFS 125 MR is an intermediate resolution FFT interferometer for the study of condensed matter The max resolution with this spectrometer is 0 5cm a Sample sets available on the IFS 125 MR e ATR set Attenuated Total Reflection with a diamond crystal only the sample is under air all the optical path is under vacuum e 11 Combined transmission and specular reflection Accessory A 510 QT controlled by OPUS http www brukeroptics com fileadmin be_user Products FT_JR Product_Notes A51 0_Q T pdf When the set is connected go to Measure menu and select Direct Command Entry To place the set in transmission use the command Mot To place the set in reflection use the command Mot e Variable Angle Reflection Accessory A 513 controlled by OPUS http www brukeroptics com fileadmin be_user Products FT_IR Product_Notes A51 3 pdf When the set is connected go to Measure menu and select Direct Command Entry To adjust the reflection angle use the command Mot e athermostated transmission electrochemical cell from 65 C to 100 C e athermostated transmission ce
37. ts Pump CX2 y d Open progressively VM CX2 1 manual e z i l bolometer PT CX2 1 under the last ee compartment of the oboe gt yi t ied i i F j 137 gt l Mobile mirror compartment Pi i e Switch ON the Roots Pump CX2 control on the pump when pressure is lt 200mbar on GX2 you can read the value on GlobalScreen or on the electronic board CH3 User Manual of AILES beamline 29 Vacuum Evacuate instrument 2 Vent instrument Control 42 Vent instume i lle 3 Evacuate interferometer compartment Commands 4 Evacuate sample compartment 5 Vent sample compartment f When pressure becomes lt 107 mbar close VM CX2 manual click on STAND BY on Direct Control Panel stop Roots Pump g Make sure that the rough Pump CX2 2 is ON Primary Pump CX2 3 Primary Pump CxX2 2 Primary Pump CX2 1 WY h Open VM PTI CX2 manual User Manual of AILES beamline i Switch ON TurboPumpl CX2 green START button located under the mobile mirror compartment the TurboPump2 CX2 which is located under the detector compartment is less used as it may cause noise on the spectrometer and wait for the pump speed to reach 53000 RPM and the pressure is lt 10 mbar Control box of the Turbo pump J Open the electro pneumatic valve VX2 using GlobalScreen control when pressure is under 10 mbar 7 Acquisition a In Direct Control Panel click on

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