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6700FR Refrigerated Sampler User Manual

1. 42 Installing 2 Bottle Kit 43 Identifying the Sampler Components 46 Running a Program 49 Reports Program Settings 59 Report Sampling Results 60 Report Combined Results 61 Report Summary 63 Taking a grab sample 65 Removing and replacing the pump tube 71 Positioning the pump tube 72 Opening the controller 13 Main circuit board connections 74 Circuit Board Wiring Connections Label 78 Refrigeration Schematic 19 Refrigerator Troubleshooting Chart 80 Sample Distribution 86 Start Time Diagram for Sampler Enable SOID ee A 89 Event Mark Timing Diagram 96 Password Protected Functions 106 6700 Menu Tree for Standard Programming 110 Standard Programming Programming DOT seed Naam OA dsd 111 Standard and Extended Programming Stari TIMER cti es ie 112 Standard Programming Quick View Programming Screens 113 Standard and Extended Programming Quick View Start Times 114 VIEW REDO 22 22 erben 115 Maintenance Screens 116 Manual Functions Screens 117 Module Setup tai 118 Quick View Module Setup 118 Extended Programming Programming SCREEN er te e Mok wae 119 Extended Programming Equipment Stili 120 Extended Pr
2. 3 6700FR Construction Materials 7 Technical Specifications for the 6700FR BAMPpler 4 cio tere 8 Connector Specifications 13 About the Keypad 84 14 15 Distributor Arm Positions and Discharge Tube Lengths for Bottle Kits 40 Selecting the Right Strainer 45 Connecting Isco Instruments to the Sampler savoir dde 48 Reports Source Error and Program EventCodes zitella nia 58 Supported YSI Calibration Methods 93 Serial Data Codes 98 6700 Telephone Commands 107 Supported YSI Parameters 108 YSI Parameter Identifiers for Serial Output 24 2464 t3266 tae en cede eeae haa 109 Hazardous Gases 158 6700FR Refrigerated Sampler 6700FR Refrigerated Sampler Chapter 1 Introduction Chapter Contents The 6700FR Refrigerated Sampler is an integral part of Isco s com About 700 Series Modules 1 prehensive sampling system The system includes the 6700FR Re frigerated Sampler the 6700 Compact Sampler and the 6700 About YSI Sondes 1 Standard Sampler e Memory to Store Data 1 The 6700FR is ideally suited for permanent installation in a wide About this Manual o variety of indoor and outdoor environments Constructed from du p Bas 5 rable corrosion resistant materials the 6700FR withstands the US eni hostile environments of industrial and municipal monitoring sites
3. Press the On Off key to turn the sampler on Press 4 Enter to clear the start up message If the words STANDARD PROGRAMMING appear on the second line of the start up message the sampler is using the standard programming screens To see the extended screens type 6 00 2 at the main menu shown in step 2 Select PROGRAM from the main menu Select PROGRAM NAME EXTENDED 1 from the quick view menu Select SELECT NEW PROGRAM to change the program You can go through QUICK VIEW screens quickly by pressing Enter at each screen You can also change settings in quick view screens see Changing Settings in a Quick View Screen on page 20 Select the name of the extended program you want to use Each program s name appears on the same line If you inadvertently give two programs identical names you can still identify them by their location on the screen To run the program immediately select YES To run the program later select NO Module Programming The module programming screens contain a branch of setup screens that let you specify the units of measure and data storage interval Some module setup screens are available to you even when no mod ule or rain gauge is attached to the sampler When you attach a 700 Series Module to the sampler the sampler adds an additional set of screens needed to program the module Because each model is differ ent the sampler adds a different set of screens The module s scre
4. 46 Installing the Sampler 47 Tips for Routing Suction Line 47 Intake Placement 47 Positioning a Sampler 47 Connecting External Instruments 47 Locking the Sampler 48 Running Programs 49 Run Time Screens 50 Module and YSI Sonde Readings 50 Error Messages 51 Fatal BrroPs ee aa 51 Warning Messages 51 Interrupting a Running Program 52 SLOD Prostani sed etiri ner 52 Resume Program 52 VIEW Data au EP ER RE 52 Grab Samples 2 22 32 rea 52 Pump Tube Alarm 52 Calibrate Volume 53 Cal Adj Parameters 53 AdjustPacind ss copiati a ge 53 Adjust Volume 53 Adjust Enable 53 Power USed d 6 dil bee eine See ee 54 Adjust Suction Head 54 Servicing the Sampler 54 Sampling Reports 54 Collecting Reports 55 Viewing the Data 55 Configuring Reports 56 Printing Reports 56 Program Settings Report 56 Sampling Results Report 57 Combined Results Report 57 Summary Report 57 Grab Samples 65 CAEN anime rie rein dune 66
5. 81 e Rinses and Retries 81 SPACO AA 82 e Distribution 84 Sampler Enable 87 Pauses Resumes 88 Start TIMES sacan rad res 89 Other Functions 91 e Manual Functions 91 e Programming Style 91 Hardware Setup 92 MEMOIV ppi ewer exes 100 e Flash Memory and Software Upgrades 101 e Pressurized Lines 101 Extended Screen for Suction Head Settings AUTO SUCTION HEAD ENTER HEAD SUCTION HEAD OF ft min max Screens for Line Rinses and Sampling Retries __ RINSE CYCLES 0 3 RETRY UP TO __ TIMES WHEN SAMPLING 0 3 6700FR Refrigerated Sampler Chapter 5 Reference Sample Event A sample event consists of a complete sampling cycle A sample event includes presample and postsample purges line rinses sampling re tries and deliveries of sample volumes Only one sample volume is placed in a given bottle during a sample event however depending on the distribution multiple bottles may receive sample volumes Sample Volume The sample volume is the discrete programmed amount of liquid delivered During a sample event the sampler may deliver a sample volume to several bottles depending on the distribution Sample volumes and samples are used interchangeably Extended programming adds a flow dependent sample volume op tion for uniform time paced programs If a fl
6. Page 69 ATTENTION Nettoyez le filtre r guli rement pour viter la sur chauffe des composants Page 69 ZAN AVERTISSEMENT Enlever les panneaux avant ou arri re entraine des risques lectriques et m caniques L appareil doit tre d branch avant son entretien Page 77 79 et 80 Enlever les panneaux avant et arriere entraine des risques lectriques et m caniques Tout entretien ou r paration doit amp tre effectues par un technicien qualifie en refrigeration Page 77 et 79 A ATTENTION Toute r paration doit tre faite par un technicien qualifi en r frig ration Purger toujours l appareil avec de l azote NE JAMAIS UTILISER d air pour purger l appareil S il fait ouvrir le syst me herm tique de la r frig ra tion pour r paration toujours capturer le r frig rant Jamais ne l cher pas le refrigerant dans latmo sph re C est interdit en la plupart de pays et peut endommager aussi l ozone de l atmosph re Pour recharger le syst me r frig rant correctement ne pas utiliser un robinet aussi qu il aura une fuite finalement ou causera la corrosion Au lieu de cela braser un tube court au tube de succion Utilisez ce tube court pour recharger Puis craser le tube court et braser son bout Utiliser toujours la soudure d argent 6700FR Refrigerated Sampler Sicurezza Il campionatore refrigerato 6700FR e un apparecchiatura per scopo specifico destinata ad essere utilizzat
7. Whenever adverse atmosphere is encoun tered forced ventilation must be used to create safe conditions After the ventilating equip ment has been operated for a few minutes the atmosphere in the manhole should be retested before anyone enters the manhole When explosive conditions are encountered the ventilating blower should be placed upwind to prevent igniting any gas that is emerging from the opening When a gasoline engine blower is used it must be located so that exhaust fumes cannot enter the manhole If testing equipment is not available the man hole should be assumed to contain an unsafe atmosphere and forced ventilation must be pro vided It should never be assumed that a man hole is safe just because there is no odor or the manhole has been entered previously 4 Entering Manholes Since the top of the manhole is usually flush with the surrounding surface there may not be anything for the per son who is entering the manhole to grab on to steady himself Persons who are entering man holes should not be permitted to carry any thing in their hands as they enter the manhole to ensure that their hands will be free to hold on or grab if they slip A good method for enter ing a manhole is to sit on the surface facing the manhole steps or ladder with the feet in the hole and the arms straddling the opening for support As the body slides forward and down ward the feet can engage a rung and the back can
8. 81 Screen Charts for Pacing Figure 25 Standard Programming Programming Screens on page 111 Figure 27 Standard Programming Quick View Programming Screens on page 113 Figure 36 Extended Programming Pacing and Distribution on page 121 Figure 40 Extended Programming Quick View Pacing and Distribution on page 125 Standard Time Pacing and Flow Pacing Screens for Samplers without Flow Modules TIME BETWEEN SAMPLE EVENTS __ HOURS __ MINUTES FLOW BETWEEN SAMPLE EVENTS PULSES 1 9999 Flow Pacing Screen for Samplers with Flow Modules FLOW BETWEEN SAMPLE EVENTS Mgal 0 001 99999 6700FR Refrigerated Sampler Pacing Sample pacing is the rate at which the sampler takes samples Depending on the type of pacing you select the rate is controlled by the sampler s internal clock or by inputs received from connect ed instruments Standard programming provides time pacing and flow pacing Ex tended programming provides additional pacing types random in terval pacing nonuniform time pacing and event pacing In time paced sampling the interval between samples is a constant time interval When you program the sampler for time pacing the sampler prompts you to enter the time between sample events in hours and minutes screen 5 The sampler always takes a sample at the start time Flow paced sampling requires a flow meter flow logger or a module A flow meter or flow logger paces
9. Overexposure by inhalation to very high concentrations may cause temporary alteration of the heart s electrical activity with irregular pulse palpitations or inadequate circulation Skin contact with the liquid may cause frostbite Individuals with preexisting diseases of the central nervous or cardiovascular system may have increased susceptibility to the toxicity of excessive exposures Carcinogenicity Information None of the components present in this material at concentrations equal to or greater than 0 1 are listed by IARC NTP OSHA or ACGIH as a carcinogen FIRST AID MEASURES First Aid INHALATION If high concentrations are inhaled immediately remove to fresh air Keep person calm If not breathing give artificial respiration If breathing is difficult give oxygen Call a physician SKIN CONTACT In case of contact immediately flush skin with plenty of water for at least 15 minutes Remove contaminated clothing and shoes Call a physician Treat for frostbite if necessary by gently warming affected area Wash contaminated clothing before reuse EYE CONTACT In case of contact immediately flush eyes with plenty of water for at least 15 minutes Call a physician INGESTION Ingestion is not considered a potential route of exposure exposure A een ia Notes to Physicians Because of possible disturbances of cardiac rhythm catecholamine drugs such as epinephrine should only be used wit
10. Getting Help 2 The 6700FR with a variety of bottle kits available is easily con 6700FR Sampler Features 3 verted both for sequential and composite sampling Like all sam 6700FR Construction Materials 7 plers in the 6700 Series it is compatible with a wide variety of Isco instruments Technical Specifications for the CORP 2222252 i About 700 Series Modules e Connector Specifications 13 The bay on the controller s right side accepts any of Isco s 700 Se ries Modules The 700 Series include e 701 pH Parameter Module for monitoring pH and temperature e 710 Ultrasonic Module for monitoring a flow stream s level and flow rate with an ultrasonic level sensor e 720 Submerged Probe Module for monitoring a flow stream s level and flow rate with a submerged probe e 730 Bubbler Module for monitoring a flow stream s level and flow rate with a bubbler system e 750 Area Velocity Module for monitoring a flow stream s level velocity and flow rate e 780 4 20mA Input Module for interfacing to non Isco devices with 4 to 20 milliampere output signals The modules are optional accessories The samplers do not require them for operation However the modules offer a number of advan tages First they are an economical way to combine flow rate or pH monitoring with sampling Second you can program the samplers and modules as a single unit Finally the samplers store the mod ule s level flow
11. OUT OF RANGE OVERRIDE YES NO REPEAT ALL pH BUFFERS __ _ mg l ___mg l o gt ENTER THE ABSOLUTE BAROMETRIC PRESSURE mm Hg CALIBRATION METHOD D O STANDARD BAROMETRIC PRESSURE ALTITUDE ENTER YOUR ALTITUDE PLACE PROBE IN CALIBRATION CUP PRESS WHEN STABLE mg l ___F ENTER THE SPECIFIC CONDUCTANCE OF YOUR KCI STANDARD _mS cm PLEASE WAIT PLACE PROBE IN mS cm STANDARD PRESS WHEN STABLE applicatie mS cm CALIBRATION READING NO OUT OF RANGE OVERRIDE YES NO PLEASE WAIT D O CALIBRATED TO If applicable CALIBRATION READING OUT OF RANGE OVERRIDE YES NO 129 6700FR Refrigerated Sampler Figure 45 Extended Programming Optional YSI Screens See Chapter 6 From Figures 42 and 43 Extended Programming Hardware Screens PLEASE WAIT Communications Failed UNABLE TO Communications COMMUNICATE Successful SETUP YSI ANYWAY YES NO If applicable DO YOU WANT TEMPERATURE DATA YES NO If applicable If applicable DO YOU WANT DO YOU WANT CONDUCTIVITY DATA LEVEL DATA YES NO YES NO If applicable If applicable DO YOU WANT DO YOU WANT SPECIFIC CONDUCTANCE AMMONIUM DATA DATA YES NO YES NO If applicable If applicable DO YOU WANT DO YOU WANT T D S DATA AMMONIA DATA YES NO YES NO If applicable If applicable DO YOU WANT DO YOU WANT SALINITY DATA NITRATE DATA YES NO YES NO If applicable If applicable DO YOU WANT DO
12. RUN PROGRAM 17 VIEW REPORT OTHER FUNCTIONS 6700FR Refrigerated Sampler Type the length of the suction line then press Enter If you change the length the sampler will display a message PLEASE WAIT GENERATING PUMP TABLES Because this example requires samples every 15 minutes select TIME PACED by pressing an arrow until the option TIME PACED blinks Then press Enter Type 0 for hours and press Enter Type 15 for minutes and press Enter Tip Move back and forth between hours and minutes by pressing an arrow key Because this program requires one sample in each bottle select SEQUENTIAL by pressing an arrow until the option SEQUENTIAL blinks Then press J Enter For this example select NO by pressing an arrow until the option blinks Then press 4 Enter Selecting YES allows the program to run indefinitely by repeating the sample distribution Continuous sampling assumes that filled bottles are replaced with empty bottles at regular service intervals Type the volume of the sample you want deposited in each bottle Then press Enter For this example select DELAYED START by pressing an arrow until the option blinks Then press Enter Type the delay period you want between the time you run the program and the time the sampler takes the first sample Then press Enter Run the program immediately by selecting YES Select NO if you want to run the program later by selecti
13. PUMPING PRESS THE RED STOP KEY WHEN DONE PUMPED COUNTS PURGING PRESS THE RED STOP KEY WHEN DONE PURGED COUNTS 6700FR Refrigerated Sampler Figure 32 Module Setup SELECT UNITS FOR LENGTH ft m SELECT UNITS FOR VELOCITY fps mps If applicable PROGRAM MODULE YES NO DATA STORAGE INTERVAL IN MINUTES 1 2 5 10 85 30 SELECT UNITS FOR SELECT UNITS FOR TEMPERATURE SELECT UNITS FOR FLOW RATE FLOW VOLUME cf gal Mgal m3 lit F C cfs gps gpm Mgd Ips m3s m3h m3d If applicable NEW MODULE SETUP STORED DATA WILL BE LOST OK YES NO Programming screens for a 700 Series module See the charts in the Module s manual If applicable INTERVAL CHANGED STORED DATA WILL PLEASE WAIT PARTITION MEMORY WILL LAST __ DAYS BE LOST OK YES NO Figure 33 Quick View Module Setup UNITS SELECTED LENGTH ft TEMP C If applicable UNITS SELECTED FLOW RATE cfs FLOW VOLUME Mgal VELOCITY fps If applicable ULTRASONIC MODULE WEIR 90 V NOTCH __ MINUTE STORAGE INTERVAL SELECT UNITS FOR LENGTH ft m If applicable SELECT UNITS FOR TEMPERATURE F C SELECT UNITS FOR FLOW RATE cfs gps gpm Mgd Ips m3s m3h m3d SELECT UNITS FOR FLOW VOLUME cf gal Mgal SELECT UNITS FOR mee tt VELOCITY fps mps If applicable NEW MODULE SETUP STORED DATA WILL BE LOST OK YES NO Programming screens for a 70
14. Press the Down Right arrow ar until DONE blinks Press Some additional tips for using the text entry menus enter e Hold an arrow key down for auto repeat e If your description uses all ten spaces in the text line the sam pler automatically moves to the next screen as soon as you add the tenth character e You can enter numbers by pressing the number keys e Erase characters by replacing them with a space character e Select the BACK UP option to move the cursor to the left 19 6700FR Refrigerated Sampler To leave the menu before completing the entry press Stop The sampler will display this menu SAVE CHANGES YES NO Quick View Screens in Standard Programming Select YES to save your entry Select NO to leave the original de scription or program name unchanged RUN PROGRAM O VIEW REPORT Quick View Screens OTHER FUNCTIONS Quick view screens are a special type of menu screen They show To see the quick view screens the current program settings and let you move quickly through the select PROGRAM program You must change the programming style to QUICK SITE DESCRIPTION VIEW CHANGE to see the quick view screens SITE 29 Paging Through Quick View Screens e Select 4 for the next quick The arrows in the corners of each quick view screen are menu op view screen If J is blinking tions that let you move from one quick view screen to another press J Enter e Select T for t
15. SECTION IX STORAGE PRECAUTIONS Store in a dry well ventilated place below 115 degrees F away from a heat source Keep in tightly closed container Protect container from physical damage Always reseal container and protective moisture barrier liner after use SECTION X HMIS Hazardous Materials Identification System for this product is as follows Health Hazard 0 Flammability 0 Reactivity 0 Personal Protection HMIS assigns choice of personal protective equipment to the customer as the raw material supplier is unfamiliar with the condition of use The information contained herein is based upon data considered true and accurate However United Desiccants makes no warranties expressed or implied as to the accuracy or dro of the information contained herein or the results to be obtained from the use thereof This information is offered solely for the user s consideration investigation and verification Since the use and conditions of use of this information and the material described herein are not within the control of United Desiccants United Desiccants assumes no responsibility for injury to the user or third persons The material described herein is sold only pursuant to United Desiccants Terms and Conditions of Sale including those limiting warranties and remedies contained therein It is the responsibility of the user to determine whether any use of the data and information is in accordance with applicable federal
16. Storage 0 to 140 F 18 to 60 C 11 6700FR Refrigerated Sampler Table 3 Technical Specifications for the 6700FR Sampler 6700FR REFRIGERATED SAMPLER PHYSICAL SPECIFICATIONS CONTINUED Electrical Power Requirements 120 Volts 60 Hz 240 Volts 50 Hz optional Running current 3 5 amp 1 75 amp Starting current 17 amp 8 5 amp Stalled Compressor current 21 amp 10 5 amp maximum Heater Capacity 60 watts Compressor Ys HP 150W Tecumseh compressor Compressor Protection Temperature safety cutout that will disengage the compressor if the compressor reaches 221 F 105 C Refrigerant R134a 7 5 ounce 0 21 kg charge Pressure High side 165 to 215 psig 1 14 to 1 48 MPa Low side 2 to 10 psig 13 8 to 69 kPa Changes or modifications to this unit not expressly approved by the party responsible for compliance could void the user s authority to operate the equipment 12 6700FR Refrigerated Sampler Table 4 Connector Specifications CONNECTOR ICON POWER SOURCE 2 PIN MALE SEALED 9 PIN FEMALE SEALED INTERROGATOR 6 PIN FEMALE SEALED FLOW METER 6 PIN MALE SEALED ul MODULE 8 PIN MALE SEALED IN MODULE BAY 13 PIN LOCATION DIAGRAM PIN FUNCTION A Ground B 12 volts DC A 12 volts DC B Ground C Programmable 1 01 pin D Rain gauge input E Switched 12 volts DC F Receive G Transmit H Programmable 1 02 pin I Programmable 1 03 pin A 12 volts DC B Ground C Pr
17. You cannot delete programs but you can modify them as often as necessary However to run a program with different settings with out losing the settings in your current program select a stored pro gram and modify its settings To understand how this works consider this example You have been running the current program named EXTENDED 1 at site A for several weeks This program contains all the settings you need for site A and you don t want to lose those settings Nevertheless you need another program because you want to move the sampler to site B so you select EXTENDED 2 and modify it for site B The settings in EXTENDED 1 are preserved automat ically When you return the sampler to site A you won t need to re program the sampler Merely select EXTENDED 1 again double check the program settings and run the program 25 6700FR Refrigerated Sampler Selecting an Extended Program To select an extended program follow the steps in Example 4 Example 4 Selecting a Stored Extended Program 6700 SAMPLER EXTENDED PROGRAMMING For HELP at any screen press key RUN EXTENDED 1 PROGRAM VIEW REPORT OTHER FUNCTIONS PROGRAM NAME EXTENDED 1 SITE DESCRIPTION SELECT NEW PROGRAM CHANGE PROGRAM NAME EXTENDED 1 EXTENDED 2 EXTENDED 3 EXTENDED 4 PROGRAMMING COMPLETE RUN THIS PROGRAM NOW YES NO RUN EXTENDED 2 PROGRAM VIEW REPORT OTHER FUNCTIONS
18. lined with polyethylene jacket STANDARD PROGRAMMING FEATURES Pacing Distribution Methods Three Flexible Start Time Settings Option for a Continuous Running Program e Uniform Time Pacing Sampling at regular time intervals e Flow Pacing Sampling at regular flow volume intervals See Pacing on page 82 eComposite Samples deposited in a single large bottle e Sequential Only one sample placed in each bottle e Samples Per Bottle Multiple samples placed in each bottle e Bottles Per Sample One sample deposited in multiple bottles See Distribution on page 84 e Start Immediately Starts the sampling program immediately e Delayed Start Starts the sampling program after a user definable delay of 1 to 999 minutes eClock Time Starts the sampling program at a user definable time on one or more days of the week See Start Times on page 89 e Continuous Sampling If the sample bottles can be properly serviced the sample distribution can restart with the first bottle set after the last bottle set 1s filled without interrupting the running program See Distribution on page 84 EXTENDED PROGRAMMING FEATURES Pacing e Uniform Time Pacing Sampling at regular time intervals e Nonuniform Time Pacing Sampling at irregular time intervals e Random Interval Pacing Sampling at unique random intervals eFlow Pacing Sampling at regular flow volume intervals eEvent Pacing Sampling each time a user definable eve
19. Includes bottle configuration kit one unlined lid 2 lids and two discharge tubes 1 Bottle Kit 9 4 liter glass bottle o 68 6700 039 Includes bottle configuration kit 2 lids and two discharge tubes 1 Bottle Kit 15 0 liter polyethylene bottle 68 6700 040 Includes bottle configuration kit 2 lids and two discharge tubes 1 Bottle Kit 18 5 liter glass bottle 68 6700 042 Includes bottle configuration kit 2 lids and two discharge tubes 1 Bottle Kit 20 5 liter polyethylene bottle 68 6700 041 Includes bottle configuration kit 2 lids and two discharge tubes 169 6700FR Refrigerated Sampler Bottle Racks Retaining Rings Discharge Tubes Distributor Arm Bottle Rack for 24 Bottle Kit 350 milliliter Glass Bottles and 8 Bottle Kits 60 2744 008 Bottle Rack for 24 Bottle Kit 1 000 milliliter Polypropylene Bottles 60 2744 007 Bottle Rack tor 12 B ttle Ritus sa I BRA ee Code DAD ek 60 9004 151 Retaining Ring for 24 Bottle Kit 350 milliliter Glass Bottles 60 2724 020 Retaining Ring for 24 Bottle Kit 1 000 milliliter Polypropylene Bottles 60 3703 058 Retaining Ring for 12 Bottle Kits israele ale 60 2903 127 S Bottle Adaptor for o bottle Rack ln der od
20. __ ft SUCTION LINE SUCTION LINE LENGTH IS ft 3 99 TIME BETWEEN SAMPLE EVENTS _ HOURS MINUTES PACING TIME EVERY TIME PACED HOURS _ FLOW PACED FLOW BETWEEN SAMPLE EVENTS _ PULSES 1 9999 SEQUENTIAL Multi Bottle BOTTLES SAMPLE SAMPLES BOTTLE __ BOTTLES PER DISTRIBUTION SAMPLE EVENT 1 max BOTTLES SAMPLE RUN CONTINUOUSLY __ SAMPLES PER BOTTLE 1 max 1 Bottle RUN CONTINUOUSLY TAKE ___ SAMPLES YES NO 1 max SAMPLE VOLUME _ ml 10 max Continued on Figure 28 Standard and Extended Programming Quick View Start Times on page 114 113 RUN CONTINUOUSLY YES NO 6700FR Refrigerated Sampler Figure 28 Standard and Extended Programming Quick View Start Times Continued from Figure 27 Standard Programming Quick View Programming Screens on page 113 FIRST SAMPLE AFTER A _ MINUTE DELAY 1 999 NO DELAY TO START NO DELAY TO START DELAYED START CLOCK TIME WAIT FOR PHONE CALL FIRST SAMPLE AT HH MM SELECT DAY S SU MO TU WE TH FR SA DONE FIRST VALID DAY IS PROGRAMMING COMPLETE RUN THIS PROGRAM NOW YES NO PROGRAM VIEW REPORT OTHER FUNCTIONS RUN See Run Time Screens on page 50 D Note A The WAIT FOR PHONE CALL option appears when using the optional Telephone Commands See Chapter 6 114 6700FR Refrigerated Sampler Figure 29 View Report RUN PROGRAM VIEW REPORT OTHER FUNCTIONS No v
21. a five minute time out will follow in which most keys are deactivated The user selected password defaults to 6700 and may be changed in the Hardware options that are available in the Extended Pro gram mode While the password may only be changed in the ex tended program mode the program lock works for both Standard and Extended programs Should you forget your password a key code can be obtained from Isco s Customer Support Department for a nominal fee 105 6700FR Refrigerated Sampler Figure 23 Password Protected Functions From Standby RUN PROGRAM VIEW REPORT OTHER FUNCTIONS While Running a Program SAMPLE 3 IN 00 03 26 On Off Key M Note The interrogator cable must be disconnected before you can use the modem Stop Key ENTER PASSWORD ENTER PASSWORD ENTER PASSWORD Programming Screens VIEW DATA SAMPLINK REPORT PRINT DATA ENTER PASSWORD FLOWLINK REPORT SYSTEM IDs SE CUSTOM REPORT CONFIGURE REPORTS ALL REPORTS MAINTENANCE ENTER PASSWORD MANUAL FUNCTIONS PROGRAMMING STYLE STOP PROGRAM RESUME PROGRAM VIEW DATA GRAB SAMPLE Switch Bottle Set at Enable When this software option is activated it allows the 6700FR to switch to a new bottle set each time a program part becomes en abled The sample interval will be reset at the enable time and a sample will be taken if programmed to SAMPLE AT ENABLE Telephone Commands Several commands are
22. screens by pressing an arrow key or enter Pressing Stop exits ei ther mode e Stop to return to the main menu 59 6700FR Refrigerated Sampler Configuring Reports Configuring Data The Configure Report option allows you to specify which of the RUN Sampling Reports will be included in any output request Each PROGRAM sampler is shipped with the option ALL REPORTS selected This peda ee provides every available report and detailed partition data from the module rain and YSI readings The SAMPLINK REPORT and FLOWLINK REPORT options al low you to tailor the output to the Isco software used to collect the e Select VIEW REPORT An Dr reports The SAMPLINK REPORT option provides the Sampling SYSTEM IDs Reports but disables the output of the detailed partition data For CONFIGURE REPORTS example if you use an RTD and Isco SAMPLINK software to collect e Select CONFIGURE the Sampling Reports the SAMPLINK REPORT option will signif REPORTS icantly reduce the data collection time and save RTD storage space The sampler withholds the partition data that cannot be read by SAMPLINK REPORT SAMPLINK EUR ON E O FLOWLINK REPORT provides the Sampling Reports and the de ALL REPORTS tailed partition data Selecting the FLOWLINK REPORT option e Select the option that matches enables the output of the detailed partition data so FLOWLINK your data collection software can add the data to the site s database file or tailor the output a
23. state or local laws and regulations No Information Available Doc 50 Updated April 4 1994 Page 4 151 6700FR Refrigerated Sampler Material Safety Data Sheet Identity Trade Name as Used on Label formerty Muttiform Desiccants Inc Address 325 Harlem Road CAS Number Buffalo NY 14224 Phone Number For information 716 824 8900 Date Prepared Aprii 19 1996 Emergency Phone Number 716 824 8900 Prepared By G E McKed Section 1 Material Identification and Information Components Chemical Name amp Common Names li O e OTHER LIMITS Hazardous Components 1 or greater Carcinogens 0 1 or greater PEL TLV RECOMMENDED Montmorillonite Clay I 86 93 NA_ __NA_ o Crystalline silica quartz 2 4 2mg m 0 1 mg m respirable respirable dust dust CA EAS Non Hazardous Ingredients Paper Vapor Density k 4 Solubility in Water Appearance Paper pouch containing tan powder and Odor i Water Not soluble but will adsorb moisture Reactive H Flash Point and Auto lgnition i Flammability Limits in i NA Methods Used Temperature Air by Volume i a Water is best extinguishing medium but dry chemical carbon dioxide and foam can be used ia i Special Fire i None The paper pouch will burn but the clay will not Fighting Procedures Unusual Fire and None Explosion Hazards Section 4 Reactivit
24. such as the 3700 Series Other types of pump tubing will not work in the 6700 pump Refer to Replacing the Pump Tube on page 70 Getting Help If you need help have any questions or think your sampler re quires repair contact Iscos Customer Service Department Isco Customer Service Department Isco Inc P O Box 82531 Lincoln NE 68501 Telephone Toll free 800 228 4373 Outside USA Canada or Mexico 402 464 0231 FAX 402 465 3022 6700FR Refrigerated Sampler Table 1 6700FR Sampler Features GENERAL FEATURES Top Cover Controller Refrigerator Adjustable Distributor Arm Discharge Tube and Support Spring Compatible Isco Products Real Time Displays Programming for Modules Programming for YSI Sondes eProtects controller e Lockable latches eContains a rechargeable desiccant to prevent moisture damage to the electronics pump and distributor systems e Control panel sloped 15 degrees for easy reading e Keys labeled with large vivid icons e80 character display 4 lines by 20 columns e Display has selectable backlight Always on or always off Timed switching off when keypad is inactive for 60 seconds e Memory for program and data storage e Flash memory for easy software upgrades e The 6700FR requires 120 volts AC 60 Hz or optional 230 volts Ac 50 Hz A built in 12 volt DC power converter powers the controller e The power supply and solid state thermostat are sealed insid
25. 30 m lengths of e 3 3 0 95 cm LD Vinyl eg 0 95 cm LD Teflon lined with polyethylene jacket e From 1 minute to 99 hours and 59 minutes in 1 minute increments between consecutive samples e Nonuniform times in minute intervals or clock time e Random time intervals between consecutive samples e From 1 to 9 999 flow pulses in single pulse intervals e Flow paced in volume with attachable flow module Inches or millimeters Module Readings pH 8 bits representing pH 0 1 pH storage resolution 16 bits representing temp 0 1 C storage resolution Ultrasonic 16 bits representing level 0 0001 m storage resolution Submerged Probe 16 bits representing level 0 0001 m storage resolution Bubbler 16 bits representing level 0 0001 m storage resolution Area Velocity 16 bits representing level 0 0001 m storage resolution 16 bits representing velocity 0 001 ft s storage resolution 4 20 mA 16 bits representing percent 0 1 storage resolution YSI 600 Sonde Readings 32 bits representing flow epH 8 bits 0 1 pH storage resolution e Temp 16 bits 0 1 C storage resolution e D O 8 bits 0 1 mg l storage resolution e Conductivity 16 bits representing Specific Conductance 0 002 mS cm storage resolution T D S 0 002 g l storage resolution Salinity 0 1 ppt storage resolution Conductivity 0 002 mS cm storage resolution 6700FR Refrigerated Sampler Table 3 Technical Specifications for the 6700FR Sampler 6700 CONTROLLER SOFTWARE SPECI
26. 313 of Title 111 of the Superfund Amendments and Reauthorization Act of 1986 and 40 CFR Part 372 OZONE DEPLETING SUBSTANCES ODS This product neither contains nor is manufactured with an ozone depleting substance subject to the labelling requiremehe Clean VOLATILE ORGANIC COMPOUNDS VOC Not Determined 145 6700FR Refrigerated Sampler ENGELHARD Page 8 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 US STATE REGULATIONS CALIFORNIA The State of California has a regulation Proposition 65 which identifies specific chemicals known to the State of California to cause cancer or birth defects Proposition 65 requires a disclosure for products sold within the State of California containing an identified chemical The following information is required by the State of California for this product This product contains chemicals known to the State of California to cause cancer VOLATILE ORGANIC COMPOUND CARB Not Determined CANADIAN REGULATIONS DSL NDSL DSL WHMIS Classification Class D Division 2 Subdivision A EUROPEAN REGULATIONS EINECS Yes OTHER REGULATIONS MITI Yes AICS Yes SECTION XVI OTHER INFORMATION REVISIONS Revision Number 10 This MSDS has been revised in the following section s SECTION II COMPOSITION INFORMATION ON INGREDIENTS SECTION VIII EXPOSURE CONTROLS PERSONAL PROTECTION SECTION IX PHYSICAL AND CHEMICAL PROPERTIES SECTION XV REGULATORY INFORMATION PREPARATION INFORMA
27. Analog Output and and includes a six pin connector to interface with external devices Dialout Screens on page 131 The analog outputs can be programmed for either 0 to 20 mA or Figure 47 Analog Output and 4 to 20 mA operation With the exception of rain any parameter 3 See View Screens on that the 6700FR sampler is currently measuring can be used to i control any or all of the analog output channels Programming the outputs requires parameter levels at each end of the analog range and then assumes a linear relationship between those points MANUAL CONTROL of each output is also available Programming the serial Serial Output output Serial ASCII data can be output through the controller s interroga PERIODIC tor port The output frequency is user selectable every 15 seconds en every minute every 5 minutes every 15 minutes or by command To receive serial data as a periodic output 1 Select YES at screen 53 PORT SETTINGS 9600N81 4800N81 2 Select the appropriate baud rate setting in screen 54 Note 2400N81 1200N81 that at all baud rates the data is sent with no parity eight data bits and one stop bit If you have difficulty with the con nection try a slower baud rate SERIAL OUTPUT EVERY 3 Select the desired output interval in screen 55 15 SEC 1 MIN 5 MIN 15 MIN 4 Connect to the 6700 controller s interrogator connector using a Serial Output interrogator cable sense line open P N 60 9004 263 Do not use a stan
28. CONTROLLER ADAPTOR ER KNOB PKG 100B 1 4 CONFIGURATION KIT FR 12 24 BTL INCLUDES ITEMS 72 73 4 75 60 60 2004 020 DIST ARM ASSY sorrow O O O o 701 60 2823 007 DiSTRISUTOR ARM NUT oS NOTE ITEM IS NOT SHOWN IN ILLUSTRATION 163 6700FR Refrigerated Sampler 35 3I OR AS PART OF 23 Va WAS X do Y VA VA SN AGI A a JODDDD y r gt QT d ASE DEP 20060 CONTROLLER MODEL 6700 INSIDE 164 6700FR Refrigerated Sampler MODEL 6700 CONTROLLER INSIDE 12 13 14 7 o IIA AAA 23 4 5 5 7 8 9 30 3 32 33 34 35 165 6700FR Refrigerated Sampler 36 37 38 40 AN Vo N AN CONTROLLER OUTSIDE 64 63 SI MODEL 6700 41 42 43 SX N LE S INEA N Y S XP Sun 44 3X A A N TZ 60 LO N 58 J Adal 027 2006 09 52 166 6700FR Refrigerated Sampler MODEL 6700 CONTROLLER OUTSIDE 40 si 42 43 44 15 46 a7 FE 49 52 53 54 75 54 NOT SHOWN 167 6700FR Refrigerated Sampler EE MODEL 6700 x PUMP GEAR CASE s ASSEMBLY Lu 65 67 68 69 70 4X O 3 na O Mm 71 3 O 72 D C DESCRIPTION WGR ASSY PMP SNSR 68 609004198 MOT MTG PL ASSY CE STDF DISTR GR CS MTG PL ASSY PMP 168 6700FR Refrigerated Sampler Appendix E Accessories List Isco Inc P O Box 82531 Lincoln NE 68501
29. Calibration Tips 66 4 Maintenance sea 67 Maintenance Screens 67 Deb Ulock us see rade rss 67 Diasnosticsk 1445 2 bed Sue ease ae 67 Maintenance Checklist 68 Cleaning Guidelines 68 Kelriserator wan trait oe pean Gee oat 68 6700FR Refrigerated Sampler Controller si Aa 68 Sample Dotes uds 68 Suction Line Pump Tube and Discharge DUDE 68 ii A a ete wok A 69 Cleaning the Air Filter 69 Cleaning the Condenser Cleaning Protocols for Priority Pollutants 69 Isco Glass Sample Bottles 69 Vinyl Suction Line 69 Isco Pump Tube 70 Replacing the Pump Tube 70 Pump Tube Alarm 70 Pump Tube Replacement Checklist 71 Opening the Controller Case 73 Recharging the Desiccant 74 How to Recharge the Desiccant 74 Replacing the Internal Battery 75 Servicing the Refrigerator TT Refrigeration System 79 Troubleshooting Guide 79 5 Reference Lea 81 Sample Eventos scappare Lose ele 81 sample Volume siete ae 81 Suction Head as uu teurere ie 81 Rinses and Retries 81 Racial Bee ie did NE de 82 Lrieser Pacino sirena ane ee a 82 Pacing in Extended Programming 83 Extended Time Pacing 83 Nonuni
30. Do this by removing the pump tubing from the bulkhead fitting See Calibrating on page 66 After the sample has been pumped you will then be asked to enter the amount actually delivered Once you have entered the deliv ered volume the sampler logs a VOLUME DELIVERED and a CALIBRATE SAMPLE event in the sampler event log Cal Adj Parameters When the sampler is configured for operation with a module or YSI Sonde this option becomes available Selecting this option will dis play the appropriate level adjustment screens and or the calibration screens If the level is adjusted an ADJUSTED LEVEL event is logged Ifa parameter is calibrated an appropriate event is logged Calibrating a parameter probe will temporarily turn off the par tition data storage and the sample enable disable functions These functions are disabled during the calibration and for five minutes after the calibration is complete During this time parameter data normally collected at the data storage interval will be logged as a 252 error message Adjust Pacing This option is available when the running program is paced by Uni form Time Flow Pulses or Flow Volume If you select this option you are asked to enter a new pacing interval The sampler logs an INTERVAL CHANGED event Ifthe sampler is running a two part program and both parts are paced by the pacing listed above you will be asked to modify both intervals The original pacing interval continues to
31. Extended mark by changing the factory settings Programming Hardware f Screens on page 127 The event mark is adjustable through the hardware setup screens Figure 43 Extended You can set up the sampler to generate an event mark for every EV Programming Hardware Quick ERY SAMPLE or for COMPLETE SAMPLES If you select COM View Screens on page 128 PLETE SAMPLES the sampler sends a three second pulse only after it successfully collects a sample The sampler will not send an event mark if an error occurs such as No Liquid Detected If you select EVERY SAMPLE the sampler will send an event mark every time a sample is initiated The event mark signal can be a e 3 second pulse at the beginning of the presample purge e 3 second pulse at the beginning of forward pumping only marking the time the sampler deposited the sample e Variable duration pulse generated during the pump cycle from the beginning of the presample purge to the end of the postsam ple purge e Variable duration pulse generated only during forward pumping Figure 22 shows event mark timing diagrams Bottle Number Concurrent with the event mark the sampler also sends a bottle number signal The bottle number signal is a series of pulses The number of pulses sent represents the bottle currently accepting a sample See Figure 22 95 6700FR Refrigerated Sampler Figure 22 Event Mark Timing Diagram Presample Purge Pulse at Beginning of urna i
32. Flow Meters Fax 402 465 3022 Email address Info isco com Website www isco com Return equipment to 4700 Superior Street Lincoln NE 68504 1398 Other correspondence P O Box 82531 Lincoln NE 68501 2531 6700FR Refrigerated Sampler SAFETY SUMMARY The Model 6700FR Refrigerated Sampler is a defi nite purpose device intended for use only with compatible Isco equipment Do not use this prod uct with any other manufacturers equipment or for any other purpose Use for any purpose not described in this manual could cause personal injury or property damage Electrical Requirements The refrigerator is available in both 120 VU and 230 V configurations The required operating voltage for the refrigerator is listed on the Identifi cation and Serial Number label placed on the inside of the sample compartment door Refrigerators configured for 120 VU operation are equipped with a North American NEMA 5 15P plug and is intended for use only with 120 VA 60 Hz The power source should be rated for 30 ampere service Refrigerators configured for 230 V operation are equipped with a Continental European CEE 7 7 plug and is intended for use only with 230 VI 50 60 Hz The power source should be rated for 16 ampere service Refrigerators in either configuration provide 12 5 V at 5 amperes for the sampler controller This output is from the two pin military type connector on the cord on top of the refrigerator This
33. Flow paced No sample at start Start Time Time Override 2 J 6 l TO 5 4 p IZ 8 7 DISTRIBUTION EXTENDED 1 BOTTLES SAMPLE PROGRAMMING SWITCH AT 13 00 ONLY THEN EVERY 1 00 y y y 86 SEQUENTIAL BOTTLES SAMPLE SAMPLES BOT TLE SAMPLES EVENT 1 24 SWITCH BOTTLES ON NUMBER OF SAMPLES TIME 1 BOTTLES PER SAMPLE EVENT 1 24 SEQUENTIAL BOTTLES SAMPLE SAMPLES BOT TLE 2 BOTTLES PER SAMPLES EVENT 1 24 SWITCH BOTTLES ON NUMBER OF SAMPLES TIME 2 BOTTLES PER gt SWITCH BOTTLES EVERY 1 SAMPLES 1 50 SWITCH BOTTLES EVERY 1 SAMPLES 1 50 SEQUENTIAL BOTTLES SAMPLE SAMPLES BOT TLE 2 SAMPLES PER BOTTLE 1 50 SWITCH BOTTLES ON NUMBER OF SAMPLES TIME 1 BOTTLES PER SAMPLE EVENT 1 24 SWITCH BOTTLES ON NUMBER OF SAMPLES TIME 2 BOTTLES PER SAMPLE EVENT 1 24 SWITCH BOTTLES ON NUMBER OF SAMPLES TIME 1 BOTTLES PER SAMPLE EVENT 1 24 2 SAMPLES PER BOTTLE 1 50 SWITCH BOTTLES EVERY 3 SAMPLES 1 50 SWITCH BOTTLES EVERY 1 HOURS 0 MINUTES FIRST SWITCH TIME AT 13 00 Internal Sampler Enable Screens Figure 37 Extended Programming Programmed Sampler Enable on page 122 Figure 41 Extended Programming Quick View Programmed Sampler Enable on page 126 6700FR Refrigerated Sampler Sampler Enable Isco flow meters flow loggers and
34. Frequent line rinses Long purge cycles such as those used with long suction 6700FR Refrigerated Sampler 5 Rinse thoroughly three times with tap water 6 Rinse thoroughly three times with distilled water 7 Rinse thoroughly with petroleum ether and dry by pulling air through the line 8 Dry overnight in a warm oven use an oven temperature of lower than 150 degrees F if possible 9 Cap ends with aluminum foil Isco Pump Tube 1 Rinse by pumping hot tap water through the pump tube for at least 2 minutes 2 Acid wash the tube by pumping at least a 20 percent solution of hydrochloric acid through the tube for at least 2 minutes 3 Rinse by pumping hot tap water through the pump tube for at least 2 minutes 4 Rinse by pumping distilled water through the pump tube for at least 2 minutes Replacing the Pump Tube Replace the pump tube only with Isco s 6700 pump tubing Other pump tubes will not work The 6700 pump tubing is easily recog nized by the blue alignment collars Improper pump tubes include those made for Isco s earlier model samplers 3700 2900 etc and tubing available from non Isco vendors Also note that the dis charge tube is not the same as the pump tube You could experience several problems if you install the wrong pump tubing e The sampler will not pump the liquid e Pump jams e Inaccurate sample volumes e Faulty liquid detection Inspect the pump tube periodically Replace the tube whe
35. If applicable REPEAT CHECK ENABLE EVERY Repeat FOR 0 5 1 2 5 SECOND 10 15 30 TYPE MINUTES SAMPLE AT DISABLE SAMPLE AT ENABLE YES NO YES NO ONCE ENABLED STAY ENABLED See Note B VES NO RESET SAMPLE SAMPLE AT ENABLE INTERVAL AT ENABLE YES NO YES NO CONTINUE COUNTDOWN START OF SAMPLING WHILE DISABLED AFTER A YES NO _ MINUTE DELAY 0 999 If applicable PAUSE RESUME PAUSE amp RESUMEs 1 HH MM DD HH MM DD MUST BE ENTERED SAMPLE AT RESUME 2 HH MM DD HH MM DD IN PAIRS YES NO CLEAR DONE A All valid enable options will be shown Enable options may include LEVEL FLOW pH TEMP PERCENT VEL RAIN I O A DONE FR TEMP Y TEMP Y COND Y SP_CO Y TDS Y SAL Y DO See Figure 26 Standard and Extended Notes Y pH Y ORP Y LEVEL Y NH4 Y NH3 Y NO3 Y TURB Y CI Programming Start Times on page 112 Y FLOW B YES Latched or Stay Enabled NO Repeatable Enable 122 6700FR Refrigerated Sampler Figure 38 Extended Programming Quick View Programming Screens RUN EXTENDED 1 PROGRAM VIEW REPORT OTHER FUNCTIONS SELECT NEW PROGRAM CHANGE PROGRAM NAME PROGRAM NAME EXTENDED 1 SITE DESCRIPTIONS FACTORY NAME ABCDEFGHIJKLMNOPQRST UVWXYZ amp 0123456789 BACK UP DONE UNITS SELECTED LENGTH ft see Figure 33 Quick View Module Setup on page 118 5 MINUTE DATA INTERVAL See Figure 39 Extended Programming Quick View Equipment Set
36. Manual 60 9004 028 6700FR Refrigerated Sampler Pocket Guide LL 60 9003 059 Bottle Kits 24 Bottle Kit 350 milliliter glass bottles 68 6700 033 Includes bottles bottle rack configuration kit and two discharge tubes 24 Bottle Kit 1 000 milliliter polypropylene bottles 68 6700 032 Includes bottles bottle rack configuration kit and two discharge tubes 12 Bottle Kit 2 5 liter polyethylene bottles 68 6700 058 Includes bottles bottle rack configuration kit and two discharge tubes 8 Bottle Kit 1 8 liter glass bottles 4444044484 i a sue ee ne 68 6700 035 Includes bottles bottle rack configuration kit and two discharge tubes 8 Bottle Kit 2 0 liter polyethylene bottles 68 6700 034 Includes bottles bottle rack configuration kit and two discharge tubes 2 Bottle Kit 7 5 liter polyethylene bottle 68 6700 036 Includes bottles configuration kit and two discharge tubes 2 Bottle Kit 9 4 liter glass bottles 68 6700 037 Includes bottles configuration kit and two discharge tubes 1 Bottle Kit 9 4 liter polyethylene bottle 68 6700 038
37. NEVER USE AIR to purge the system Always recover the refrigerant When recharging do not leave a line tap in the refriger ation system because of pos sible corrosion or leakage problems 6700FR Refrigerated Sampler Refrigeration System The refrigeration system is shown schematically in Figure 18 The charge capacity of the system is 7 5 oz of R 134a refrigerant Figure 18 Refrigeration Schematic Capillary Tube CN Condenser Coil Evaporator Plate Compressor DI Troubleshooting Guide A troubleshooting flow chart appears in Figure 19 It is a general guide and does not cover problems in detail 79 6700FR Refrigerated Sampler Figure 19 Refrigerator Troubleshooting Chart Removing the front and back panel exposes electrical and mechanical hazards Troubleshooting and repair activities should be performed by a qualified refrigeration technician Problem Refrigerator will not cool 1 Make sure the operating voltage 120 or 230 V V is present across pins 1 and 3 of circuit board connector P12 2 Is the compressor running NO a ls the compressor run LED on the circuit board lit NO Check the circuit board for a malfunction YES Continue b Is there 12 V across pins 3 and 4 of the compressor fan relay NO Check the circuit board for a malfunction YES Continue c Is there 120 or 230 VW across pins 1 and 2 of the circuit board connector P11 NO Replace the compressor fan relay YE
38. Notice that the color of the bands on the wires deter mine their source or destination The circuit board is equipped with light emitting diode LED showing the various functions of the thermostat circuitry and pow er supply Because the indicators are helpful in identifying mal functions they are described below The barrier block on the circuit board contains all the 120 volt AC circuit connections Low voltage AC comes from the transformer secondary through connectors Pll and P12 on the circuit board The power is then rectified and passes through the regulator U7 and transistor Q3 to create the 12 volt DC supply for the logic and sam pler controller The signals from the ambient air temperature sensor the internal refrigerator sensor the evaporator plate sensor and the tempera ture control potentiometer come into the circuit board on connector P10 Ifthe ambient temperature is cold the circuitry turns on three heaters Two heaters are on the evaporator plate inside the refrig erator and one heater is on the compressor The compressor cycles approximately the same amount at cold temperatures as at room temperatures The ambient temperature will vary the duty cycle of the heaters When the heaters are on the internal heat LED indi cator is on The internal temperature sensor is mounted at the top of the refrig erator s interior If the interior of the refrigerator is warmer than the temperature control potentiometer setting
39. Number 2 penis rise 95 Presample and Postsample Purge Counts 96 VO Pin Programming 96 Refrigerator Temperature 97 Anal OULDUL sociedad ant 97 Serial Output sierpien e dosi ia de 97 Dialout Alarms 99 System IDS wkend oa eh SHE as a 99 Nemorino 100 Flash Memory and Software Upgrades 101 Pressurized Lines 101 Command Driven Operation 102 Get status srias ilaria 102 Take Sample 2 mue Lu peas a 103 Ob te AN EN EN 103 Command Driven Sampler Responses 103 Command Driven Sampler Displays 104 6 Software Options 105 Program Lock isrcprorccia edad 105 Switch Bottle Set at Enable 106 Telephone Commands 106 Support for YSI 6820 and YSI 600XL Sondes 108 Appendix A Menu Charts 110 Appendix B Material Safety Data Sheets ee 133 Appendix C General Safety Procedures 155 Appendix D Replacement Parts 160 Appendix E Accessories List 169 CO N O DI m COD A CO 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 30 36 37 30 39 40 6700FR Refrigerated Sampler List of Figures Menu Tree for Standard Programming 23 Mounting the Controller 39 Installing the bottle racks 42 Installing the 24 bottle 12 bottle and 8 bottle kits
40. Order Information Prices available on request Additional items appear in Appendix D Replacement Parts Many other items are available To order Telephone Within U S A any item contact your sales representative or the factory Note Toll free 800 228 4373 that the part name listed on your order acknowledgment and Outside U S A 402 464 0231 invoice may be different than the item name listed here When Fax 402 465 3022 examining these documents use the part number for reference Samplers 6 00ER Sampler 20V 4 hows bbe en bathed bbe sd labia SIG en 68 6700 065 Includes controller top cover center section tub distributor arm manual and 2 pump tubes 6700 Rasampler 240V 351 asia dao doo Sou a a a dd ok etti 68 6700 066 Includes controller top cover center section tub distributor arm manual and 2 pump tubes Controller and Refrigerator 6700 Sampler Controller Dis ii as A e Si 68 6700 001 Includes 2 Pump Tubes 6700FR Refrigerated Sampler Platform 120 Volt 60 Hz 68 6700 004 Includes 6700FR Refrigerated Sampler Instruction Manual 6700FR Refrigerated Sampler Pocket Guide and Distributor Arm 6700FR Refrigerated Sampler Platform 220 Volt 50 Hz 68 6700 005 Includes 240 Volt 50hz Conversion Kit 6700FR Refrigerated Sampler Instruction Manual 6700FR Refrigerated Sampler Pocket Guide and Distributor Arm 6700FR Refrigerated Sampler Instruction
41. Point Calibration pH 4 7 and 10 Buffers Dissolved Oxygen D O Standard Solution Altitude Barometric Pressure Conductivity KCI potassium chloride Standard Solution No Calibration Required The 6700FR also can support the YSI 6820 and 600XL Sondes when the program option is enabled Refer to Chapter 6 for more information about the additional YSI sondes and to Figure 45 for the menu charts 93 6700FR Refrigerated Sampler Master Slave Sampling Master slave sampling lets you operate two samplers as a master slave pair The master sampler disables the slave until the master completes its sampling program The samplers then reverse roles with the second sampler becoming the master Setting Up Master Slave Sampling 1 Turn on master slave sampling in both samplers 2 Install the samplers 3 Connect the samplers with the Master Slave Interconnect Cable by attaching the cable to the sampler s flow meter con nectors If your installation includes a flow meter or flow log ger use the Master Slave to Flow Meter Cable instead 4 Decide which sampler is to be the master sampler the mas tersampler should be the sampler with the program you want to run first 5 Turn the master sampler on and run its sampling program by selecting RUN After at least 5 seconds turn the slave sampler on and select RUN from its main menu How Does It Work The master sampler sends a disable signal out its flow meter con nector The
42. Range 40 0 C to 100 C Accuracy specification 0 3 C over a range of 0 0 C to 10 0 C Reading data is 2 bytes with a storage resolution of 0 1 C 10 6700FR Refrigerated Sampler Table 3 Technical Specifications for the 6700FR Sampler 6700FR REFRIGERATED SAMPLER PHYSICAL SPECIFICATIONS Dimensions Bottle Configurations Dry Weight Height Top cover closed 49 25 in 125 cm Top cover open 59 25 in 150 5 cm Width 26 in 66 cm Depth 26 in 66 cm e 24 wedge polypropylene bottles 1 000 ml e 24 round glass bottles 350 ml e 12 wedge polyethylene bottles 2 5 liters e 8 round polyethylene bottles 2 0 liters e 8 round glass bottles 1 8 liters e 2 rectangular polyethylene bottles 7 5 liters 2 gal e 2 round glass bottles 9 4 liters 2 5 gal e 1 round polyethylene bottle 9 4 liters 2 5 gal e 1 round glass bottle 9 4 liters 2 5 gal e 1 round polyethylene bottle 15 liters 4 gal e 1 round polyethylene bottle 20 5 liters 5 5 gal e 1 round glass bottle 18 5 liters 5 0 gal 145 lbs 66 kg Refrigerator only no controller or bottle configuration 160 lbs 73 kg Includes refrigerator controller pump tube distributor shaft extension distributor arm and nut and discharge tube for the 24 plastic bottle configuration This includes the top cover center section tub controller pump tube distributor arm distributor arm nut and discharge tube for the 24 bottle configuration Dry We
43. TIME EVERY _ HOURS __ MINUTES UNIFORM TIME PACED FLOW PACED EVENT PACED NONUNIFORM TIME NONUNIFORM TIME CLOCK TIMES INTERVALS IN MINUTES RANDOM INTERVALS PROGRAM RUN TIME _ HOURS __ MINUTES FIRST SAMPLE AT TIME BETWEEN SAMPLE EVENTS _ HOURS __ MINUTES PACED BY FLOW PULSES FLOW MODULE VOLUME FLOW BETWEEN SAMPLE EVENTS _ PULSES 1 9999 TAKE SAMPLES AT 1 START TIME 2 HH MM 3 HH MM SAMPLE AT START YES NO QUANTITY AT INTERVAL START TIME 1 AT _ MIN __ BOTTLES PER SAMPLE EVENT 1 max Multi bottle DISTRIBUTION __ BOTTLES SAMPLE ___SAMPLES BOTTLE _ HOURS __ RUN CONTINUOUSLY y 1 bottle RUN CONTINUOUSLY YES NO Uniform Time Paced Only VOLUME DO YOU WANT SAMPLE VOLUMES DEPENDENT ON FLOW YES NO _ ml SAMPLES See Figure 41 Extended Programming Quick View Programmed Sampler Enable on page 126 SWITCH BOTTLES EVERY MINUTES AT 2 AT MIN 3 AT MIN SWITCH BOTTLES ON NUMBER OF SAMPLES SWITCH BOTTLES EVERY TIME ___ SAMPLES 1 max FIRST SWITCH TIME TAKE ___ SAMPLES RUN CONTINUOUSLY 1 999 YES NO SAMPLE VOLUME 10 ML FOR EVERY FLOW MODULE VOLUME ___ PULSES FLOW PULSES SAMPLE VOLUME _ ml 10 max 6700FR Refrigerated Sampler Figure 41 Extended Programming Quick View Programmed Sampler Enable Continued from Figure 40 Extended Continued from Figure 43 Extended Programming Quick View Pacin
44. This is a word which according to the dictionary is used to mean death from an atmosphere that does not support life The word has sometimes been misinterpreted as meaning suffocation which is only one kind of asphyxiation In nearly all cases of death in sewers the real killer is hydrogen sulfide It is important that this fact be recognized Many cities diligently test for explosive gases which is very impor tant and they may measure the oxygen con centration which usually is unimportant but they rarely measure H2S Death has occurred where it is unlikely that there was any measur able reduction in the oxygen concentration Waste water containing 2 mg per liter of dis solved sulfide and at a pH of 7 0 can produce in a chamber with high turbulence a concen tration of 300 PPM H25 in the air This is con sidered to be a lethal concentration Many people have died from H2S not only in sewers and industries but also from swamps and from hot springs In one resort area at least five persons died from H2S poisoning before the people were ready to admit that H2S is not a therapeutic agent Hardly a year passes in the US without a sewer fatality from H2S as well as deaths elsewhere in the world The presence of H2S in a sewer atmosphere is easily determined A bellows and ampoule type of tester is very satisfactory for the purpose even though it is only crudely quantitative When using a tester of this type do not bri
45. a sampler by sending an electronic signal to the sampler after measuring a specified volume of liquid Because each pulse represents a volume interval flow pacing rates are proportional to the volume of water flowing through the channel When you program the sampler for flow pacing and are using a flow meter or flow logger the sampler prompts you to enter the interval between sample events in pulses See screen 6 The sampler ini tiates a sample event when the set number of pulses is received Standard programs that are flow paced do not take a sample at the start time Extended programs have a SAMPLE AT START option The flow pacing screens change when you attach a flow module Be cause the sampler is more closely integrated with the modules the standard flow pacing screen prompts you for the flow volume be tween sample events instead of pulses between events screen 7 The flow volume units displayed are what you had previously pro erammed When using extended programming you are able to choose the source of the flow pacing The PACED BY screen lists both options Select FLOW PULSES for an external flow meter FLOW MODULE VOLUME for the module Trigger Pacing Isco 4200 Series Flow Meters and 4100 Series Flow Loggers send pulses for trigger pacing The flow meter or flow logger sends puls es at two different time intervals when trigger pacing a sampler Trigger pacing for example lets you sample less frequently w
46. appears in Fig ure 11 When there is no module connected the Summary report will only print the first page of Figure 11 97 6700FR Refrigerated Sampler Table 9 Reports Source Error and Program Event Codes SOURCE CODES C CALIBRATE SAMPLE D DISABLE E ENABLE Ev EVENT F FLOW G GRAB SAMPLE R RESUME S START Sw SWITCH TIME TO TIME OVERRIDE T TIME ERROR CODES DJ DISTRIBUTOR JAMMED IP SAMPLE IN PROGRESS L PUMP LATCH OPEN BOTTLE FULL ND NO DISTRIBUTOR ARM NL No LIQUID DETECTED NM No MORE LIQUID O SAMPLER SHUT OFF Ov PROBABLE OVERFLOW P POWER FAILED PJ PUMP JAMMED SK SAMPLE SKIPPED US USER STOPPED PROGRAM EVENTS A B DONE A B ENABLED DISABLED A B PAUSED RESUMED ADJUSTED LEVEL CALIBRATE SAMPLE CHANGED SUCTION HEAD ENABLE CHANGED GRAB SAMPLE INTERVAL CHANGED MANUAL PAUSE MANUAL RESUME POWER FAILED POWER RESTORED PROGRAM DONE PROGRAM ENABLED DISABLED PROGRAM PAUSED RESUMED PROGRAM STARTED PROGRAM STOPPED EXPLANATION Sample volume delivered during calibration Sample event at disable time Sample event at enable time Event paced sample event Flow paced sample event Sample volume delivered as a grab sample Sample event at resume time Sample event at start time Sample event at switch time Sample event at bottle switch time Time paced sample event The distributor jammed Sample in progress when report was printing Unable
47. area marked 30 on the paper humidity indi cator turns pink Place a sheet of brown paper on a flat metal sheet You can use a brown grocery bag and a typical cookie sheet Place only the bags on the sheet Do not stack the bags on top of each other or allow them to touch Place in a vented circulating forced air convection oven in a well ventilated room Allow two inches of air space be tween the top of the bags and the next metal tray above the bags Keep the tray a minimum of 16 inches from heating element Heat the bags at a temperature of 240 to 250 F 116 to 121 C for 12 to 16 hours At the end of the time period the bags should be imme diately removed and placed in an air tight container for cooling The desiccant will be recharged to approximately 80 to 90 of its previous capacity After repeated recharging the desiccant bag may require replacement Some bags will have the temperature and time for recharging the desiccant printed on the bag If they differ use the temperature and time printed on the bag 74 Battery Warning WARNING REPLACE INTERNAL BATTERY BEFORE 17 OCT 97 M Note Isco recommends you replace the battery every five years as soon as the battery warning appears To insure that the re placement meets Isco s speci fications use only Isco re placement batteries See Ap pendix D Replacement Parts A CAUTION The circuit boards can be dam aged from a discharge of static
48. available to control the sampler s operation from a remote location Telephone commands require the sampler to be equipped with the factory installed 2400 baud talking modem After connecting to the sampler from a touch tone telephone com mand numbers may be entered from the telephone s keypad fol lowed by the pound button The commands are listed in Table 12 To use telephone commands 1 Dial the sampler s telephone number When the sampler con nects it answers with Isco Sampler Site number If the sampler does not receive a command in five seconds it as sumes that a computer modem has called and initiates the modem connect sequence If this occurs you must hang up and try again 2 Enter the command For example to run program 1 press Il 106 6700FR Refrigerated Sampler 3 Ifthe command is valid for its current state of operation the sampler responds with command number please acknowl edge If the command is not valid the sampler responds with the command number followed by three quick beeps Enter a valid command 4 Acknowledge the valid command by pressing the number For the example press 1 If the number is incorrect the sampler responds with your entry followed by three quick beeps You must re enter the command step 2 5 After the command is confirmed the sampler replies with command number acknowledge and executes the command To enter additional commands rep
49. count down until you re turn the sampler to the running program select RESUME PRO GRAM If the new pacing interval is less than the original count remaining the new interval is used If the original count remaining is less than the new pacing interval the original count will continue to count down to the next sample event Subsequent samples are then paced by the new interval Adjust Volume Select this option to change the sample volume within the limits of the currently programmed sample distribution For two part pro grams the sampler displays a screen for changing Part A s volume and then a screen for Part B If you change a sample volume a VOLUME CHANGED event is logged Adjust Enable This option is available for extended sampling programs that have programmed enable conditions Selecting this option allows you to change the set points or ranges for the enable conditions The sam pler displays all ofthe programming screens that define the thresh olds of the programmed enables You cannot change the type of enables used or the way they are combined If rain is an enabling condition you also have the option of resetting the rain history 53 6700FR Refrigerated Sampler Power Used The 6700FR has a fuel gauge that gives an indication of power us age The controller keeps track of how much power has been con sumed since the last time it lost power If the controller is powered by an external battery this fuel ga
50. de instrucciones para m s informaci n al respecto El manual de instrucciones identifica los peligros y los pasos necesarios para evitarlos El manual presenta esta informaci n en una de las dos siguientes maneras PRECAUCION Las precauciones identifican un posible peligro que al no ser evitado puede resultar en da os menores Esta categor a puede tambi n advertirle del uso negligente o de las condiciones que pueden ocasionar da os al refrigerador Las advertencias identifican una condici n potencialmente peligrosa que al no ser evitada puede resultar en da os muy serios u ocasionar la muerte 6700FR Refrigerated Sampler Pagina 12 ADVERTENCIA Los cambios o modificaciones a esta unidad que no hayan sido expresamente aprobados por el grupo responsable para su conformidad pueden anular toda autoridad del usuario en operar el equipo Paginas 14 y 37 M Nota Lea el Resumen de seguridad que se encuentra al principio de este manual Este presenta los requisitos el ctricos y provee instrucciones para su uso seguro Pagina 69 PRECAUCION Los componentes sobrecalentados pueden ocasio nar da os si no se limpia el filtro peri dicamente Pagina 69 ADVERTENCIA Al quitar el panel frontal o posterior se exponen peligros mec nicos y el ctricos Desconecte la corriente el ctrica antes de llevar a cabo cual quier servicio de asistencia gt Pagina 77 79 y 80 Al quitar el
51. do not spill Remove the bottle rack by lifting the front edge of the rack slightly to disengage it from the two ramps Then pull it straight out of the refrigerator Be careful not to catch the distrib utor arm against the bottles Installing Composite Bottle Remove the distributor arm and discharge tube Remove the dis tributor arm stop If using the two bottle locating base remove it Slide the composite bottle discharge tube on the bulkhead fitting Composite bottle kits have two lids one with a hole drilled in the center Screw the lid with the hole in it on the bottle and place the bottle in the center of the mounting plate 43 About Suction Lines e The vinyl line contains a very low parts per million level of phenols If phenol content affects your sample analysis use the Teflon suction line Occasionally your sampling application may suggest a nonstandard line For best sampling results however use the standard suction line available from Isco When installing the sampler be sure the vertical distance between the liquid level and the pump is as small as possible Attaching Suction Line Tube Coupling Attaching the Debris Deflector 6700FR Refrigerated Sampler Thread the discharge tube through the hole in the lid Always use the lid to retain the discharge tube It prevents the sampler from spraying liquid inside the sample compartment instead of the bottle Suction Line The suction line
52. electricity Always use an anti static mat when opening the con troller to protect the circuit boards M Note Poor soldering techniques can easily damage a printed circuit board The battery should be re placed by a skilled technician 6700FR Refrigerated Sampler Replacing the Internal Battery A Lithium battery housed inside the controller maintains power to the sampler s memory when the controller is disconnected from a power source If it discharges completely the sampler win lose all program settings and all data stored in memory when the external power source is disconnected The battery requires replacement ev ery five years The sampler displays a warning within one month of its expected life to alert you to the battery s impending expira tion The warning appears each time you turn the sampler on until you reset the alarm When you reset the alarm the sampler resets the warning to a date 59 months from the current date To replace the internal battery 1 Open the controller case see Opening the Controller Case on page 73 2 Lift the desiccant box from the case Figure 15 3 Remove the EMI shield and grounding straps by loosening the five Y4 inch stop nuts 4 Disconnect the module liquid detector and pump count con nectors from the main circuit board Figure 16 5 Remove the three screws and the Y4 inch stand off attaching the main circuit board to the case 6 Detach the main circuit board from the
53. flammable or poisonous gases or the atmosphere may be deficient in oxygen Forced ventilation may be necessary Deteriorated Rungs Manhole steps may be corroded and not strong enough to support a man It may be difficult to inspect the rungs because of poor lighting Traffic Whenever manholes are located in the traveled way barricades and warning devices are essential to direct traffic away from an open manhole Falling Object Items placed near the man hole opening may fall and injure a worker in the manhole Sharp Edges Sharp edges of items in or near a manhole may cause cuts or bruises Lifting Injuries Unless proper tools are used to remove manhole covers back injuries or injuries to hands or feet may result 2 Planning Advance planning should include arrangements for test equipment tools venti lating equipment protective clothing traffic warning devices ladders safety harness and adequate number of personnel Hasty actions may result in serious injuries Time spent in the manhole should be kept to a minimum 3 Adverse Atmosphere Refer to Table 15 Hazardous Gases on page 158 at the end of this appendix Before workers enter a man hole tests should be made for explosive atmo 155 sphere presence of hydrogen sulfide and oxygen deficiency Combustible or toxic vapors may be heavier than air so the tests on the atmosphere must be run at least 3 4 of the way down the manhole
54. for the 4 20 mA module level flow rate and flow volume readings for the flow modules level velocity flow rate and positive flow vol ume readings for the area velocity module Some module screens will alternate with the sampler screens Samplers with an attached YSI Sonde will display the parameter readings selected during the YSI hardware setup The YSI screens alternate with the sampler and module screens BOTTLE 2 IN 00 14 39 150 gpm 0 82 ft 00001438200 gal Y pH 8 1 D O 4 90 mg l Y Y TDS 1 000 g l Y TEMP 292 C The Module and YSI readings are updated e Every 5 seconds when not running a program and not display ing the reading e Every 5 seconds when running a program and the backlight is on e At the programmed Data Storage interval when running a pro gram and the reading is not used for enabling the sampler e At the lesser of the Check Enable or the Data Storage intervals when running a program and the reading is used for enabling the sampler e Every second when displaying the reading during program ming An asterisk appears next to the reading if the module or YSI Sonde was unable to take a reading Ifan asterisk appears the read ing displayed is the last available reading Flow rates will be report ed as zero flow if the error persists for more than five minutes Reino If an entire reading is filled with asterisks the value exceeds the number of characters that can be displayed T
55. is the tubing from the sampling point to the pump intake The 6700FR can use Ys inch ID suction lines of lengths from 3 to 99 feet Isco offers vinyl or Teflon suction lines The Teflon has a polyethylene jacket to protect it from kinks and abrasions Guidelines for Measuring and Cutting Suction Line Cut the line to the desired length but use the shortest length feasi ble for the installation Cut the line in 1 foot increments for instance 4 feet not 3 feet Do not include the length of the strainer in the measurement Ifusing metric units of measure cut the line in increments of 0 1 meter Attaching Suction Line to the Pump Tube Attach the vinyl suction line to the pump tube with the tube cou pling Use the black clamp for the pump tube and the white clamp for the suction line Attach the line and tube to the coupling by pushing them onto each end of the coupling Then tighten the clamps by squeezing the finger pads together Loosen a clamp by twisting 1t until its teeth disengage Attach the Teflon suction line to the pump tube by inserting the line into the tube and secure with a suitable clamp Strainers Isco offers four strainers that help prevent solids from clogging the suction line e Stainless steel strainer for priority pollutant sampling e Polypropylene strainer for routine sampling conditions e CPVC strainer for acidic liquid sources e Stainless steel low flow strainer To select the right strainer for your appl
56. let you enter program settings e Quick view screens that summarize the program settings This chapter shows you how to get started and how to use the menus with a short programming example A discussion of more complicat ed menu screens follows the example Next this chapter explains the QUICK VIEW CHANGE screens the menu tree structure and the help and error messages Finally it discusses the extended program ming screens and provides several programming examples Getting Started M Note Read the Safety Summary posted at the front of this manual It out limes the electrical requirements and provides instructions for safe operation Turn the sampler on by pressing the On Off key It is labeled with this icon D The start up screen appears first 6700 SAMPLER STANDARD PROGRAMMING For HELP at any screen press key It remains on the display for about eight seconds or until you press a key It tells you the type of programming screens the sampler is us ing currently standard or extended and gives you a tip about the on line help The main menu screen a in the margin appears next If a module is attached there may be a different screen that ap pears first See the module manual for more information Using Menus and Entering Numbers A menu is a list of options The main menu has four options e RUN e PROGRAM e VIEW REPORT e OTHER FUNCTIONS The options identify the operations that can be performed fr
57. need to readjust the stops and ramps and install a different distributor arm extension Figures 4 and 5 show you how to install the bottle kits Check the kit s alignment by rotating the distributor arm with the programming steps shown in Moving the Distributor on page 91 Do not rotate the distributor manually Moving the arm manually damages the distributor drive If you see any mis alignment adjust the posts and ramps until the discharge tube at the end of the arm stops over each bottle 41 6700FR Refrigerated Sampler Figure 3 Installing the bottle racks 24 Bottle Kit 2 Bottle Kit 1000 milliliter polypropylene bottles Requires a locating base Figure 4 Installing the 24 bottle 12 bottle and 8 bottle kits Install the distributor shaft extension Use the 8 16 inch extension for the 12 and 24 bottle kits Use the 10Y2 inch ex tension for the 8 bottle kit the instruc tions on page 38 show you how to remove the controller and replace the extensions for each bottle kit Next adjust the distributor arm to position D for the 12 bottle and 24 bottle kits or to position B for the 8 bottle kit Install the arm and stop See Installing the Distribu tor Arm and Discharge Tube on page 39 Slide the rack with bottles installed onto the mounting plate Adjust the stops and ramps on the plate so that the rack is cen tered and held firmly on the plate Finally position the arm over each bottle See Moving the Distributo
58. notes w x and y that appear with the suction line length screen you can use the same tech nique to see help notes with all pro gramming screens SUCTION LINE LENGTH V IS 7 ft 3 99 e Press Help Enter the length of suction line only excluding strainer and pump tube lt more gt e Press enter or Down Left to see the next screen Press Stop to return to the programming screen See Installing Suction Line in x your manual Press enter or Down Left to see the next screen e Press Up Right to see the previous screen Press Stop to return to the programming screen Press the red STOP key to exit HELP e Press Up Right to see the previous notes Press Stop to return to the programming screen 6700FR Refrigerated Sampler The Quick View screens below shows you how to change the suction line length Begin by paging through the quick view screens until you see the quick view screen containing the suction line setting T 24 1000 ml BTLS 10 ft SUCTION LINE e Press Up Left until 10 ft SUCTION LINE blinks Then press Enter SUCTION LINE LENGTH IS 7 ft 3 99 e Type the new line length and press enter PLEASE WAIT GENERATING PUMP TABLES T 24 1000 ml BTLS 7 ft SUCTION LINE When you change a setting the sampler stores the new settings and returns to the updated quick view screen You can repeat this process until all settings shown
59. rate pH or temperature readings in memory About YSI Sondes The sampler accepts the optional YSI 600 Sonde to monitor four liq uid parameters temperature pH dissolved oxygen and conductiv 6700 Controller ity Conductivity readings can represent specific conductance total dissolved solids salinity or conductivity You program the sampler and YSI 600 Sonde as a single unit to combine parameter monitor ing with your sampling program The 6700FR also can support the YSI 6820 and YSI 600XL sondes See Chapter 6 Memory to Store Data The samplers contain enough memory to store five sampling pro grams sampling data Isco 700 Series Module readings and YSI parameter readings You can view the readings on your sampler s display or print data reports with Isco s 3770 Field Printer 6700FR Refrigerated Sampler You can also retrieve the readings and reports so that the informa tion may be processed on a personal computer Readings and re ports may be collected with a computer running Isco s Flowlink M software Flowlink can download the information through a direct connection a modem connection when the sampler is equipped with the optional dial out modem or from a 581 Rapid Transfer Device RTD The RTD is a quick and simple way to transfer the data from the field to your computer Reports are easily collected with Isco s Samplink software About this Manual This manual contains the information you ll need to
60. rest against the opposite side of the open ing If there is any doubt about the soundness of the manhole steps a portable ladder should be used A person should never enter a manhole unless he is wearing personal safety equipment including a safety harness and a hard hat Two persons should be stationed at the surface con tinuously while anyone is working inside a manhole to lift him out if he is overcome or injured One man cannot lift an unconscious man out of a manhole 6700FR Refrigerated Sampler The persons stationed at the surface should also function as guards to keep people and vehicles away from the manhole opening To avoid a serious injury a person should not be lifted out of a manhole by his arm unless it is a dire emergency When more than one person must enter a manhole the first person should reach the bot tom and step off the ladder before the next one starts down When two men climb at the same time the upper one can cause the lower one to fall by slipping or stepping on his fingers 5 Traffic Protection In addition to traffic cones markers warning signs and barricades a vehicle or a heavy piece of equipment should be placed between the working area and oncoming traffic Flashing warning signals should be used to alert drivers and pedestrians Orange safety vests should be worn by person nel stationed at the surface when the manhole 1s located in a vehicular traffic area 6 Falling Ob
61. running from the bulkhead fitting on the inside of the refrigerator through the spring and distributor arm Distributor arm and spring Sampling cycles vary somewhat according to program settings for distribution The sampler can move the distributor arm clockwise and counterclockwise making a number of distribution methods possible In this manual the words sample event refer to a full sampling cycle for any distribution Other variations include extended program settings for suction line rinses and sampling retries A sampler running a program with line rinses completes the presample purge and then rinses the line The suction line is purged after each rinse When programmed for sampling retries the sampler will attempt to pump a sample again if it fails on previous attempts Measuring Sample Volume Sample volume refers to the amount of liquid delivered into a bot tle The volume is determined by the programmed value The vol ume is dependent on the volume per revolution of the pump which is dependent on the suction head The 6700FR delivers the sample by counting the pump revolutions and automatically compensating for the suction head 46 ul Flow Meter Connector Rain Gauge Connector 6700FR Refrigerated Sampler Installing the Sampler Tips for Routing Suction Line Route the line so that it runs continuously downhill from the sam pler to the liquid source This helps drain the line during presam
62. sampler at the monitoring site e Sampling Reports 54 a Install the strainer or end of the suction line in the flow Grab Samples 65 stream and route the suction line to the sampler See In take Placement on page 47 also see Tips for Routing Suc e Calibrating 66 tion Line on page 47 b Install a module if desired Refer to the module manual for instructions on installing the module c Place the sampler in position See Positioning a Sampler on page 47 d Connect any necessary external instruments to the sam pler See Connecting External Instruments on page 47 M Note Read the Safety Summary posted at the front of this manual It out lines the electrical requirements and provides instructions for safe operation e Plug the line cord into an AC power outlet Be sure it is connected to 120 volts AC optional 230 volts AC 3 Program the Sampler Programming guidelines are in Chap ter 2 and in the module manual 4 Run the sampling program See Running Programs on page 49 5 Service the sampler a Recover the samples b Collect the sampling data See Sampling Reports on page 54 c Replace the sample bottles d Run the sampling program 37 6700FR Refrigerated Sampler Preparing the Sampler The 6700FR is shipped to you with the controller mounted on the refrigerator and a distributor shaft extension installed Use Fig ure 2 for reference when rem
63. slave sampler receiving the signal is held disabled un til the master sampler completes its program When using a flow meter or flow logger a Master Slave to Flow Meter Cable must be used This cable is constructed so that the pacing in strument receives only the event marks However when using this configuration a connected flow meter will not receive a bottle number signal and 1t cannot enable or disable the samplers Bottle Full Detect The sampler can detect a full bottle condition when collecting sam ples in a single bottle composite sampling When the sampler de tects a full bottle 1t stops the sampling routine A bottle full condition will also stop a sampling routine that is set to RUN CON TINUOUSLY The Bottle Full Detect screen allows you to enable or disable this fea ture Selecting YES enables the sampler to detect a full bottle and stop the sampling routine Selecting NO disables this feature The YES NO Bottle Full Detect setting is part of the sampling program Because it is a program setting full bottle detection can be enabled or disabled for each of the four extended programs If the Bottle Full Detect set ting is critical to your sampling program always check this Hard ware setting after you select a different Extended Program Bottle Full Detect BOTTLE FULL DETECT This feature relies on a post purge after each sample When using the Bottle Full Detect ensure that postsample purges gre
64. some thing is out of the ordinary For example the warning below ap pears when you type a number that is larger than the standard bottle volume BOTTLE VOLUME IS 3500 ml 300 30000 WARNING STANDARD BOTTLE VOLUME EXCEEDED The 6700 does accept nonstandard volumes because you might use a nonstandard container occasionally For a list of recommended volumes for Isco bottles press the Help key at the Bottle Volume Is screen or refer to the Technical Specifications The 6700 uses the bottle and sample volume settings to determine the maximum number of samples that can be deposited without overfilling the bottles Entering a volume that exceeds the stan dard volume may cause the sampler to overfill the bottle Operation Messages An operation message reports the sampler s status as it runs a pro gram See Run Time Screens on page 50 Menu Trees Selecting a menu option will take you to a number entry screen or another menu screen The screens are organized in a branching structure that resembles a tree Refer to Figure 1 for a simple chart of the menu tree for standard programming The standard programming structure is different much simpler than the ex tended programming structure Charts that show you most of the sampler s screens appear in Appendix A Menu Charts The entire structure changes a little when a module is attached be cause the sampler adds a set of screens for a module as soon as it dete
65. the sam pler must run a program with flow pacing settings and the flow instrument must run a program with trigger pacing settings e When the sampler runs an event paced program it disregards pacing pulses from a flow meter or flow logger However the sampler continues to monitor for enable signals See Sampler Enable on page 87 Rain Gauge Connector Connect the rain gauge YSI Sonde or Refrigerator Temperature Sensor connect cables to the nine pin Rain Gauge Connector Samplers with a four pin Rain Gauge Con nector can only accept a rain gauge When connecting a rain gauge and a YSI Sonde or rain gauge and a Refrigerator Temperature Sensor use the appropriate Y connect cable See the Accessories appendix at the end of this manual 47 6700FR Refrigerated Sampler M Notes e Select Extended Programming to use the YSI Sonde See Changing to and from Extended and Standard Screens on page 24 e Update the Hardware Setup whenever you add or remove a rain gauge refrigerator temperature sensor or YSI Sonde See Hardware Setup on page 92 In extended programming rain gauge and YSI Sonde readings are only available ifthey are selected in the Hardware Setup However when using standard programming rain gauge readings are auto matically stored in the sampler s memory Locking the Sampler The refrigerator is equipped with a lockable latch for the top cover and a lockable catch for the door handle To lock the refrige
66. the temper ature set on the temperature control knob The internal tempera ture indicator then goes off the compressor run indicator goes off and the compressor shuts off When the evaporator temperature warms the evaporator temper ature LED indicator goes on When the refrigerator s internal tem perature gets warm the internal temperature indicator goes on When both the evaporator temperature and the internal tempera ture indicators are on the compressor turns on the compressor run indicator The compressor runs until the internal temperature in dicator goes out If you suspect a problem with the circuitry remember that the com pressor shuts off when the internal temperature sensor reaches the setting on the temperature control knob However to turn the com pressor on both the internal temperature sensor and the evapora tor temperature sensor must be warm The compressor fan solid state relay may be replaced but do not attempt to replace any other components Replacing components will disturb the circuitry s cal ibration We suggest you replace the entire board or return the board to the factory for repair 78 Removing the front and back panel exposes electrical and mechanical hazards Trouble shooting and repair activities should be performed by a qual ified refrigeration technician All refrigeration repair work must be performed by a quali fied refrigeration technician Always purge the system with nitrogen
67. through 60 show you how to find the system IDs 60 Options List e Press STOP to return to the main menu 99 6700FR Refrigerated Sampler Memory The 6700 Sampler contains 128 kilobytes of battery backed RAM Random Access Memory that stores e Five sampling programs e The sampling results from the most recent program e The rainfall data collected from rain gauges e The data from a refrigerator temperature sensor e The data collected from a 700 Series module e Parameter data collected from a YSI Sonde e Calculated flow information from the current flow module The sampling results memory stores up to 1004 events The pro gram run and start time information is logged as four events These four entries are held for the duration of the program The remain ing 1000 are for logging sample events program events and errors from the currently running program If the running program ex ceeds 1000 events the data will roll over That is the sampler will replace the oldest stored event with the newest event When using a YSI Sonde the sampler logs two entries at each sample event This reduces the sampling results memory to 500 events Module YSI Sonde Refrigerator Temperature and rain gauge readings are stored in memory partitions The storage capacity de pends on the reading types the number of bytes per reading and the data storage interval The sampler clears the sampling results memory when the site de scrip
68. time pacing options are uniform time and nonuni Pacing and Distribution on page res Nr du TEE 121 form time Uniform time pacing is identical to time pacing in N standard programming Nonuniform time pacing uses an irregular en interval between sample events each interval is individually pro Distibulionon page 125 grammable There are three types of nonuniform time pacing e Nonuniform clock time pacing e Nonuniform interval pacing a me e Random interval pacing EVENT PACED NONUNIFORM TIME Nonuniform Clock Time Pacing For clock time pacing enter specific times for each sample event NONUNIFORM TIME See screen 10 You can enter as many as 99 clock times but the Eee interval between times cannot be greater than 24 hours Remem RANDOM INTERVALS ber to use a 24 hour clock when entering times The sampler takes a sample at the start time CLOCK TIMES Nonuniform Interval Pacing TAKE SAMPLES AT For nonuniform interval pacing enter the number of sample events 1 START TIME spaced at intervals of minutes 12 samples at 5 minute intervals 6 10 2 HH MM E 3 HH MM samples at 10 minute intervals and so on The sampler accepts as many as 99 nonuniform interval entries The sampler takes a sam ple at start time INTERVALS IN MINUTES Random Interval Pacing FIRST SAMPLE AT START TIME To program the sampler for random interval pacing enter the 11 THEN length of time you want to sample The r
69. to take sample because the pump band was opened The composite bottle is full There is no distributor arm or the stop is damaged The sampler was unable to detect liquid After the sampler detected liquid and while the sample was being taken the liquid detector stopped detecting liquid The sampler was turned off with the On Off key during the sample event The sampler was directed to take a sample that would not fit into the bottle Occurs for flow paced time override programs only The power supply failed during the sample event Note Power failures during five consecutive sample events results in a LOW BATTERY shut down The pump jammed Sample not taken You pressed the Stop key during the sample event The sampler finished program part A or B Program part A or B was enabled or disabled according to the program s settings Program part A or B reached a programmed pause or resume time The level measured by a flow module was adjusted while manually paused The sample volume was calibrated while in the Manual Paused state The suction head was changed while in the Manual Paused state Sampler enable thresholds were changed while in the Manual Paused state A grab sample was taken while in the Manual Paused state Sample pacing was changed while in the Manual Paused state Stop was pressed during the program to enter the Manual Paused state The resume program option was selected from th
70. tomacorriente accesible Nunca utilice un cord n de extensi n El tomacorriente debe estar visible y accesible La nica manera de desconectar la corriente el ctrica es desenchufando el refrigerador Para minimizar el riesgo de una descarga el ctrica el refrigerador debe estar conectado a un tomacorriente con contacto a tierra el ctrico La fuente de corriente el ctrica debe ser un circuito dedicado La linea no debe transmitir corriente el ctrica a cualquier otro dispositivo No utilice el refrigerador si se han quitado los paneles inferiores frontales o posteriores No haga funcionar el refrigerador en ambientes con sustancias explosivas No levante o mueva el refrigerador sin utilizar un dispositivo especial para transportar aparatos el ctricos Se deben reemplazar los fusibles siguiendo las especificaciones requeridas de tama o corriente voltaje y tiempo de utilidad Haga referencia a la Lista de repuestos para el n mero correcto del repuesto gt bbbobbb S mbolos de seguridad y advertencias Los iconos en el modelo 6700FR del Refrigerated Sampler y aqu llos que se encuentran en este manual de instrucciones alertan al usuario de peligros conocidos A continuaci n se describen los iconos A Este icono identifica un peligro general Haga referencia al manual de instrucciones para m s informaci n al respecto AN Este icono indica el riesgo de una descarga el ctrica Haga referencia al manual
71. two text entry Then press enter menus one for site description and another for an extended program name They work in the same way 3 Press an arrow until DONE blinks Press enter This example demonstrates both by changing the description from 2 Repeat these steps until each day you want is blinking To remove days from the list FACTORY051 to SITE 29 1 Press an arrow key until the cursor is on the day you want to remove Press enter OE E 2 When finished select DONE and press enter 1 UVWXYZ 8 0123456789 BACK UP DONE Menu Screens Site Descriptions and Program Names Screen i is a menu screen for entering a site description A site de SITE SACTORY051 scription is commonly a number address or other short note that ABCDEFGHIJKLMNOPQRST helps identify the monitoring site Extended programming has a J UVWXYZ amp 0123456789 ens BACK UP DONE similar screen that lets you enter program names for stored pro grams e Press the Down Right arrow ma until the S on line 2 blinks In screen z line 1 contains a line of text between two quotation Then press enter marks Lines 2 and 3 contain the menu options numbers letters SITE SICTORY051 and punctuation marks used to spell out the description In line ABCDEFGHIJKLMNOPQRST VR ao core 3 the space between the ampersand amp and the double quotes BACK UP DONE is a space character Line 4 contains two additional options e
72. wear Replace it if necessary 6 ABCDEFGHIJKLMNOPQRST e Clean the pump tube housing ABCDEFGHIJKLMNOPQRST cose a ABCDEFGHIJKLMNOPQRST e Change the suction line if necessary e Clean the bottles suction line strainer and pump tube ee e Check the humidity indicator e When the battery warning appears on the display replace the controller s internal battery 8 a Cleaning Guidelines Refrigerator To keep the refrigerator s exterior and interior free from corrosive so 9 ON ae y lutions grease oil and other debris clean it periodically with soapy 7 water using a sponge or nonmetallic brush Do not direct a hose spray toward the underside or into the front grille Wipe the refrigerator dry after cleaning Apply a coat of fiberglass wax to the exterior sur PURGING faces to make them easier to clean and to protect them from damage Controller When necessary clean the controller with warm soapy water To prevent moisture damage always cap the connectors at the back of 11 ON a SACE A the controller tightly Keep the controller power cable connected or replace the protective cap shipped with the sampler over the pow er source connector Make sure the pump drain hole located on the bottom right hand 12 ld side of the pump beneath the pump band is open and free of debris or buildup M Note Avoid using a high pressure hose to clean the controller especially around the control panel Extreme pressures may for
73. when using two part programming PHONE SAMPLE is valid while the program is running after the start time but not while in the Manual Pause screens 107 M Note You need to configure your sonde using PC software provid ed by YSI Only parameters out put in the units shown in Table 13 will be seen by the 6700 If the sonde is configured for a parameter other than those list ed in Table 13 the sampler may report NO SONDE PARAME TERS PLEASE RECONFIG URE If so use PC600 or a similar program to reconfigure the sonde 6700FR Refrigerated Sampler Support for YSI 6820 and YSI 600XL Sondes This software option will allow the 6700 sampler to be interfaced to a YSI 6820 sonde or a YSI 600XL sonde Before connecting the sonde its parameters and communication settings should be configured to operate with the 6700 Using YSI software such as PC600 or a similar application configure the sonde for any of the valid parameters listed in Table 13 if avail able on the sonde The serial communication settings should be set to 2400 baud 8 data bits 1 stop bit and no parity Note The 6700 will connect to the sonde at baud rates between 1200 and 19200 but after establishing communications the sampler will reconfigure the sonde s baud rate to 2400 Table 13 Supported YSI Parameters Storage Bytes Conductivity Specific Conductance Total Dissolved Solids Dissolved Oxygen Parameter Temperature Ammoniu
74. 0 Series module See the charts in the Module s manual If applicable INTERVAL CHANGED STORED DATA WILL DATA STORAGE INTERVAL IN MINUTES 1 2 5 10 15 3 0 BE LOSTI OK YES NO 118 6700FR Refrigerated Sampler Figure 34 Extended Programming Programming Screens RUN EXTENDED 1 EXTENDED 1 PROGRAM EXTENDED 2 VIEW REPORT EXTENDED 3 OTHER FUNCTIONS EXTENDED 4 If STOP key pressed PROGRAM NAME NAME ISCO 6700 SELECT NEW PROGRAM ABCDEFGHIJKLMNOPQRST CHANGE CHANGE PROGRAM NAME UVWXYZ amp 0123456789 YES NO BACK UP DONE SAVE CHANGES YES NO SITE DESCRIPTION FACTORY CHANGE If 2 ABCDEFGHIJKLMNOPQRST STOP key SAVE CHANGES UVWXYZ amp 0123456789 Inressed YES NO YES NO BACK UP DONE NO SELEGT UNITS FOR LENGTH ft m See Figure 32 Module Setup on page 118 DATA STORAGE INTERVAL IN MINUTES 28 10 15 30 See Figure 35 Extended Programming Equipment Setup on page 120 See Figure 36 Extended Programming Pacing and Distribution on page 121 ON OS See Figure 37 Extended Programming Programmed Sampler Enable on page 122 O See Figure 26 Standard and Extended Programming Start Times on page 112 EN i ws NN RUE 119 6700FR Refrigerated Sampler Figure 35 Extended Programming Equipment Setup Programming Programming Screens on Continued from Figure 34
75. 0 LOS 0 18 Le 11 le 0 18 1 1 12 1220 0 18 bp LO 11 41 0 18 leg 14 LA 0 18 Dy 15 lei 0 18 dig al 16 12 20 0 18 1 1 17 12 41 0 18 1 1 18 eo 0 18 1 1 t9 Laos Ll Ds Lo Ly 20 Lozio 0 18 Lg 21 Local 0 19 Lp 22 92206 l al by 23 12211 0 25 Lg Ll 24 14 26 020 N 61 6700FR Refrigerated Sampler Figure 10 Report Combined Results continued SAMPLER ID 0011343009 15 25 23 MAR 99 Hardware B2 Soltware 3 10 BUBBLER MODULE 638324458 Hardware AO Software 1 00 KAKKKKKKKKKK COMBINED RESULTS KRRRRRKRR RRS SITE FACTORYOO09 PROGRAM EXTENDED 1 Program Started at 08 41 TU 23 MAR 99 Nominal Sample Volume 200 ml FLOW TOTAL RATE FLOW SAMPLE BOTTLE TIME ES Mgal 1 1 1 08 41 2 495 0 000000 1 1 2 iso ES LO 0 016941 Lyt gt OS 2066 0 034698 lpt 4 09726 Zio 0 052914 lyd 09 41 Za bio 0 071707 dy dk 6 Os pao ce 2 198 080 0 el 7 20211 2198 0 109314 eg 8 10226 2 100 Oe ZL Lp 9 10 41 2 191 0 146911 gpa 0 10236 2 115 Di L09040 oe dl Ai 2 198 0 184556 Ly kt 12 11220 Ha dio 0206935 Eye LS 11 41 3 728 0 232024 1 1 14 11556 ue o 0 257108 eL deo Ia 34 128 0282171 Pee 13 12 26 Tsd To Oa SL FILO ld LI 125241 52939 l ad foo yd Ls 122 06 Se Oo il ro O LL 19 LS SE 6 651 0 441689 ple 20 1220 cuore al 0 486476 ipl Zi 13 41 Oa oo 0 531238 bal 22 12220 SEN aA ter Ist 2a 14 11 3 404 0 611500 1 1 24 14 26 SPE VAs 0 634426 N 62 6700FR Refrigerated Sampler Figure 11 Report Summary SAMPLER ID 0011343009 15 25 23 MA
76. 03 213 A EA IENA ERNIA DONE IA CEE ee NOTTI OE 60 0603 214 A a En ae Mae DER 60 0603 215 Miscellaneous for use with the YSI Sonde Calibratiow Transport Bottle Kit 24 2 2 42 ut ine re a er ad 60 0603 216 Carrying Case for YSI 600 cables accessories tools 60 0603 217 YoL600 Instruction Mandala id tee 60 0603 218 YSI 600 to Isco 4200 6700 Adapter Cable 60 0604 001 YSI 600 and Isco 674 Rain Gauge Y Connect Cable 60 0604 002 This cable allows use of the YSI 600 Sonde and the Isco 674 Rain Gauge at the same time Miscellaneous available from your YSI representative Field cable to female DB 9 PC serial connector oo oo vo ernennen Contact YSI This cable allows you to configure the Y SI Sonde from your PC using YSI PC6000 software 172 6700FR Refrigerated Sampler A Accessories 169 1101 PAL 171 1640 Liquid Level Actuator 171 4 20 mA Sampler Input Interface 171 bottle kits 169 bottle racks 170 bulk bottles 170 bulk discharge tubing 170 cables 171 controller 169 data collection accessories 171 manuals and pocket guides 169 modules 171 power sources and battery chargers 171 pump tube 170 rain gauges 171 refrigerator temperature sensor 171 refrigerators 169 retaining rings 170 samplers 169 strainers 170 suction line 170 YSI 600 172 Air filter 69 Analog output 97
77. 04 075 Refrigerator Temperature Sensor with 5 ft 1 55 m cable 68 6700 136 171 6700FR Refrigerated Sampler YSI 600 Sonde YSI 600 Sonde with pH D O conductivity temperature sensors and 25 ft cable 68 0600 111 Note Item 68 0600 111 includes a YSI to Isco 4200 6700 adapter cable calibration transport cup 1 stainless steel nose weight and YSI instruction manual Many other configurations of the YSI 600 Sonde are available without either the pH and or D O sensors or supplied with 50 100 or 200 ft cables Also available is a low ionic strength pH sensor for use in streams with very low conductivity 10 umhos cm or less Call the factory for more information YSI 600 Accessories D O Sensor Maintenance Supplies D O Probe membrane and electrolyte kit 30 membranes 30 mL KCI soln 2 O rings 60 0603 205 D O Probe reconditioning kit Instructions and sanding disks 60 0603 206 Calibration Solutions Conductivity Sensor 1 Quart LASER SE RAR ne na rene TORA NE i Ne I 60 0603 207 ss A ulisse er 60 0603 208 ION Co ads ee E a D D cle ILA 60 0603 209 Calibration Solutions Boxes of 8 1 Pint Containers A A A ee er Mains ees Be 60 0603 210 OMC parte a a Y A ESAS ANA IS 60 0603 211 o er ee ra ES ieri Mk ee fhe a roi 60 0603 212 Buffer Solutions pH Sensor Calibration Boxes of 6 1 Pint Containers Pili intentata ERI 60 06
78. 1 Disconnect power from the refrigerator 2 Remove the screws securing the refrigerator s grille See 3 Remove the grille and filter 4 Steam clean the filter or wash it in hot soapy water After washing treat the filter with a standard filter coat Cleaning the Condenser Clean the condenser and surrounding areas annually more fre quently under severe operating conditions 1 Disconnect power from the refrigerator 2 Remove refrigerator s back panel See Appendix D Replace ment Parts 3 Vacuum the fan compressor and surrounding areas 4 Check the fan for freedom of movement If the fan and fan motor do not rotate freely replace the motor You cannot oil the sealed fan motor bearings 5 Remove the front grille and filter Vacuum the condenser coil and surrounding areas 6 Clean the filter before replacing it 7 Replace the back panel and front grille Cleaning Protocols for Priority Pollutants Clean sampling equipment is essential for valid laboratory analy sis Isco recommends that you develop cleaning protocols in consul tation with a laboratory analyst when designing the monitoring program For example to clean sample bottles suction line and pump tubes Lair 1974 suggests these protocols used by USEPA Region IV Surveillance and Analysis field personnel engaged in NPDES compliance monitoring The protocols are based on US En vironmental Protection Agency Publications EPA 600 4 77 039
79. 12 24 PUMP COUNTS WARNING AT __00000 PUMP COUNTS RESET PUMP COUNTER YES NO WARNING AT 00000 PUMP COUNTS 1 99 00000 SELECT UNITS FOR LENGTH ft m SUCTION LINE LENGTH l o aaa ti 3 99 PLEASE WAIT GENERATING PUMP TABLES 6700FR Refrigerated Sampler Appendix B Material Safety Data Sheets Du Pont Chemicals 2187FR Revised 12 MAR 1994 Printed 20 MAR 1994 SUVA COLD MP CHEMICAL PRODUCT COMPANY IDENTIFICATION Material Identification Corporate MSDS Number DU000693 CAS Number 811 97 2 Formula CH2FCF3 CAS Name 1 1 1 2 TETRAFLUOROETHANE Tradenames and Synonyms SUVA 134a HFC 134a Company Identification MANUFACTURER DISTRIBUTOR DuPont 1007 Market Street Wilmington DE 19898 PHONE NUMBERS Product Information 1 800 441 7515 Transport Emergency CHEMTREC 1 800 424 9300 Medical Emergency 1 800 441 3637 COMPOSITION INFORMATION ON INGREDIENTS Components Material CAS Number 811 97 2 ETHANE 1 1 1 2 TETRAFLUORO HFC 134a 100 Continued 133 6700FR Refrigerated Sampler HAZARDS IDENTIFICATION Potential Health Effects Inhalation of high concentrations of vapor is harmful and may cause heart irregularities unconsciousness or death Intentional misuse or deliberate inhalation may cause death without warning Vapor reduces oxygen available for breathing and is heavier than air Liquid contact can cause frostbite HUMAN HEALTH EFFECTS
80. 1989 levels RESPIRATORY PROTECTION A NIOSH MSHA approved respirator is recommended if dust is generated VENTILATION General local exhaust ventilation as necessary to control any alr contaminants to within their PELs or TLVs during the use of this product PROTECTIVE EQUIPMENT Safety glasses with side shields PERSONNEL SAMPLING PROCEDURE For CRYSTALLINE SILICA Refer to NIOSH Manual of Analytical Methods 3 Edition Volume 2 Methods 7500 7601 and 7602 SECTION IX PHYSICAL AND CHEMICAL PROPERTIES Boiling Point Not Applicable Specific Gravity H 0 1 2 0 Melting Point Not Applicable Vapor Pressure mm Hg Not Applicable Vapor Density Air 1 Not Applicable Evap Solubility In Water Negli Appearance Grey to off white granules Odor Odorless pH Not Determined SECTION X STABILITY AND REACTIVITY Stability Generally considered stable Avoid None expected 143 6700FR Refrigerated Sampler ENGELHARD Page 6 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 INCOMPATIBILITY Materials to Avoid None expected HAZARDOUS DECOMPOSITION OR BY PRODUCTS None expected Polymerization Polymerization is not expected to occur Avoid Not applicable SECTION XI TOXICOLOGICAL INFORMATION CHEMICAL NAME Wt LD5SO LCSO SILICA CRYSTALLINE QUARTZ CAS NO 14808 60 7 1 3 Not Available Not Available ALUMINUM SILICATE CAS NO 12141 46 7 97 Not Available Not Available NOTE See Section
81. 56 DOT IMO Label NONNFLAMMABLE GAS Cylinders Ton Tanks 137 6700FR Refrigerated Sampler REGULATORY INFORMATION U S Federal Regulations TSCA Inventory Status Reported Included TITLE III HAZARD CLASSIFICATIONS SECTIONS 311 312 Acute Yes Chronic Yes Fire No Reactivity No Pressure Yes LISTS SARA Extremely Hazardous Substance No CERCLA Hazardous Substance No SARA Toxic Chemicals No OTHER INFORMATION NFPA NPCA HMIS NPCA HMIS Rating Health 1 Flammability O Reactivity 1 Personal Protection rating to be supplied by user depending on use conditions Additional Information CAUTION DO NOT USE IN MEDICAL APPLICATIONS INVOLVING PERMANENT IMPLANTATION IN THE HUMAN BODY JI II N ANNAN ON AP The data in this Material Safety Data Sheet relates only to the specific material designated herein and does not relate to use in combination with any other material or in any process Responsibility for MSDS DuPont Chemicals Address Engineering amp Product Safety P 0 Box 80709 Chestnut Run Wilmington DE 19880 0709 Ind cates updated section End of MSDS 138 6700FR Refrigerated Sampler Code J96001 Date 23 DEC 1993 Printed 05 JAN 1994 ENGELHARD MATERIAL SAFETY DATA SHEET Product DESICCITE 25 SECTION I CHEMICAL PRODUCT AND COMPANY IDENTIFICATION Common Name BENTONITE HEAT ACTIVATED GRANULES Chemical Name BENTONITE HEAT ACTIVATED GRANULES Formula MONTMORILL
82. 6 N Nonuniform time pacing 83 O One part programs 24 Operating grab samples 65 messages displayed during operation 50 running sampling programs 49 Other Functions see Hardware setup 91 see Maintenance 91 see Manual functions 91 see Programming Style 91 P Pacing event pacing 83 flow pacing 82 nonuniform clock time pacing 83 nonuniform time pacing 83 random interval pacing 83 PAL 1101 pH Logger 48 Pause and resume 88 Periodic serial output 97 Power sources accessories list 171 Presample purge event marks 95 Printing reports 56 Program name menu how to use 19 Program settings report see Sampling reports Program storage see Stored programs Program Style 20 Programming 14 changing program name 19 changing site description 19 clock and calendar 18 extended programming features 5 6 keys 15 menu screens 14 program name menu 19 running programs 49 site description menu 19 text entry 19 Programming modules 26 Pump Counts pump tube warning 70 Pump counts purging a nonstandard suction line 96 Pump tube accessories list 170 174 6700FR Refrigerated Sampler adjusting pump count for warning 72 replacing 70 requirements 2 warning 70 Q Quick View Screens 20 see Program Style R Rain gauge 92 Random interval pacing 83 Refrigerant 79 Refrigerator temperature sensor 97 171 Replacement parts listing 160 168 Replacing internal battery 75 Reports see Sampling reports Resume 88 Running programs 49
83. 6700FR Refrigerated Sampler Instruction Manual Part 60 9003 438 of Assembly 60 9004 028 Copyright 1996 2001 All rights reserved Isco Inc Revision K October 2001 FOREWORD This instruction manual is designed to help you gain a thorough understanding of the operation of the equipment Isco recommends that you read this manual com pletely before placing the equipment in service Although Isco designs reliability into all equipment there is always the possibility of a malfunction This manual may help in diagnosing and repairing the malfunc tion If the problem persists call or email the Isco Customer Service Department for assistance Contact information is provided below Simple difficulties can often be diagnosed over the phone If it is necessary to return the equipment to the factory for service please follow the shipping instructions provided by the Customer Ser vice Department including the use of the Return Authorization Number speci fied Be sure to include a note describing the malfunction This will aid in the prompt repair and return of the equipment Isco welcomes suggestions that would improve the information presented in this manual or enhance the operation of the equipment itself Contact Information Phone 800 228 4373 USA Canada Mexico 402 464 0231 Outside North America Repair Service 800 775 2965 Analytical and Process Monitoring Instruments 800 228 4373 Samplers and
84. 700 045 Weighted Polypropylene Strainer with 10 foot Suction Line and Coupling 60 3704 071 Weighted Polypropylene Strainer with 25 foot Suction Line and Coupling 60 3704 072 Teflon Suction Line 10 foot length 60 1683 146 Teflon Suction Line 25 foot length 60 2703 114 Bulk Vinyl Suction Line 100 foot length 68 1680 058 Bulk Vinyl Suction Line 500 foot length 68 1680 059 38 inch Vinyl Suction Line Accessory Kit includes tube coupling clamp and instructions 68 3700 007 EN A OO A 60 3704 066 Polypropylene Weighted Strainer ira Nada eee ee o da 60 1394 071 Stainless Steel Low Flow Strainer encia ds ir unie rires 60 2903 079 Stainless Steel Strainer a ID a A tee De Wat ee ba din ete ile 60 1684 110 170 6700FR Refrigerated Sampler Data Collection Devices and Cables Dol Rapid Iransier Device Ria ti iin 60 9004 027 Power Cable 581 Rapid Transfer Device RTD 60 9004 077 Flowlink 3 Software Includes Instruction Manual 60 2544 043 Flowlink 4 for Windows Software New License 60 2544 047 Flowlink 4 for Windows Software Upgrade LL 60 2544 048 SAM
85. AY TO FIRST SAMPLE RUN PROGRAM ONCE 59 6700FR Refrigerated Sampler Figure 9 Report Sampling Results SAMPLER ID 0011343009 15 25 23 MAR 99 Hardware B2 Software 3 10 KKKKKKKKKKK SAMPLING RESULTS KKKKKKKKKKK SITE FACTORYO0O9 PROGRAM EXTENDED 1 Program Started at 08 41 TU 23 MAR 99 Nominal Sample Volume 200 ml COUNT TO SAMPLE BOTTLE TIME SOURCE ERROR LIQUID 08 41 PGM ENABLED a de 1 08 41 S Tyd 7 08 56 T 1 1 3 09711 T Esa 4 0926 T iyd 5 09 41 T Ly 6 09 56 T 1 1 7 LUST T Es Ll 8 10228 ji gl 9 10241 il 1 1 10 10 56 T 1 1 11 14211 T 1 1 12 11 826 T lil 13 11 41 T 1 1 14 11 56 T Lal Js 12 11 T 1 1 16 12 26 T Ls Cy 122241 A La Lo 12256 T Lal LO i pa T 1 1 20 13 26 T 1 1 21 Pope T 1 1 22 mit T bed 23 14 11 T Ved 24 14 26 I N 14 26 PGM DONE 23 MAR SOURCE S gt STARI SOURCE T gt TIME 60 250 247 247 249 247 247 247 248 234 2 50 27 241 238 236 254 236 242 eN 0 238 Lo 201 236 230 6700FR Refrigerated Sampler Figure 10 Report Combined Results SAMPLER ID 0011343009 15 25 23 MAR 99 Hardware B2 Software 3 10 KXXKXxXXXXAkx COMBINED RESULTS KAREL KK a SITE FACTORY0O09 PROGRAM EXTENDED 1 Program Started at 08 41 TU 23 MAR 99 Nominal Sample Volume 200 ml TOTAL RAIN SAMPLE BOTTLE TIME in Led 1 08 41 0 00 El 2 03 26 0 00 el 3 UL 0 00 ld 4 0220 0 05 LE 5 09 41 IM Uy E 6 09 56 0 05 Lyd 7 10 11 0 05 1 1 8 10 26 0 05 Uy TL 9 10541 0 18 1 1 1
86. B Bottle Number Signal 95 C Cables accessories list 171 Calendar 18 setting clock and calendar 18 Calibration during a manual pause 53 sample volumes 66 Checklist installation and operation checklist Cleaning protocols 69 Clock setting clock and calendar 18 Clock start time menu 18 Combined results report see Sampling reports Command driven mode 102 Compatible Isco products 3 Condenser coil 69 Configuring reports 56 Construction compact and standard sampler 7 Continuous sampling 54 85 Controller mounting on refrigerator 38 D Data collection accessories accessories list 171 Desiccant recharging and replacing 74 Diagnostics 67 Dialout alarms 99 Discharge tube accessories list 170 installing 39 lengths for bottle kits 39 Distribution continuous sampling 85 count switched distribution 85 event pacing 83 random interval pacing 83 time switched distribution 85 Distributor arm adjusting for bottle kits 39 installing 39 moving arm 91 E Enable see Sampler enable Error messages 51 Event marks 95 3 second pulse 95 variable duration pulse 95 Event pacing 88 Extended programming extended programming features 5 6 one part and two part programs 24 showing extended screens 24 F First valid day 49 90 Flash memory 101 Flow loggers connecting 48 Flow meters connecting 48 Flow pacing 82 Flow dependent sample volumes 81 G Grab samples 52 H Hardware setup 92 rain gauge setup 92 YSI 600
87. DATE MANUAL FUNCTIONS HH MM DD MON YY PUMP COUNTS PROGRAMMING STYLE LL Lee See Note A SET GLOCK PUMP COUNTS SET PUMP TUBE ALARM RESET PUMP COUNTER INTERNAL BATTERY YES NO DIAGNOSTICS REPLACE INTERNAL BATTERY BEFORE EEE WARNING AT __00000 PUMP COUNTS 100000 9900000 DID YOU REPLACE THE PLEASE WAIT INTERNAL BATTERY TESTING RAM TES NU RAM PASSED TEST TEST PUMP YES NO PLEASE WAIT TEST DISTRIBUTOR ROM CHECK YES NO PUMPING ROM PASSED TEST FINDING ARM FLEXURE PUMPING ON OFF RATIO _ __ ABCDEFGHIJKLMNOPQRST ABCDEFGHIJKLMNOPQRST NOW AT BOTTLE __ ABCDEFGHIJKLMNOPQRST ABCDEFGHIJKLMNOPQRST PURGING DISTRIBUTOR SYSTEM ARM FLEXURE _ PURGING ON OFF RATIO _ __ RE INITIALIZE YES NO Note YES A The standard programming maintenance screen is shown YES NO Extended programming adds the HARDWARE option 116 DEFAULT SETTINGS ARE YOU SURE Figure 31 Manual Functions Screens RUN PROGRAM VIEW REPORT OTHER FUNCTIONS MAINTENANCE MANUAL FUNCTIONS PROGRAMMING STYLE GRAB SAMPLE CALIBRATE VOLUME OPERATE PUMP MOVE DISTRIBUTOR GO TO BOTTLE _ 1 max NOW AT BOTTLE __ SAMPLE VOLUME _ml 10 9990 SAMPLE VOLUME _ml 10 9990 SELECT DIRECTION PUMP FORWARD PUMP REVERSE 117 6700FR Refrigerated Sampler GRAB SAMPLE PRESS J WHEN READY CALIBRATE VOLUME PRESS 4 WHEN READY VOLUME DELIVERED ml ARE YOU SURE YES NO
88. E Enter 2500 Select NO Enter 1 34 6700FR Refrigerated Sampler Example 6 Storm Water Runoff Sampling continued 65 SWITCH BOTTLES ON NUMBER OF SAMPLES TIME SWITCH BOTTLES EVERY 1 SAMPLES 1 50 RUN CONTINUOUSLY YES NO SAMPLE VOLUME 500 ml 10 1000 ENABLE O RAIN LEVEL FLOW Y pH Y TEMP Y COND Y D O NONE ENABLE RAIN AND OR DONE ENABLE RAIN AND VO RAIN LEVEL FLOW Y pH Y TEMP Y COND Y D O NONE RAIN SET POINT 0 15 INCHES PER 15 MIN 30 MIN 1 HOUR 2 HOURS ENABLED WHEN ABOVE SET POINT BELOW SET POINT RESET RAIN HISTORY YES NO LEVEL CONDITION SET POINT RANGE LEVEL SET POINT 0 25 ft 0 100 30 000 ENABLED WHEN ABOVE SET POINT BELOW SET POINT Select NUMBER OF SAMPLES Enter 1 Select NO Enter 500 Select RAIN Select AND Select LEVEL Enter 0 15 for inches then select 30 minutes Select ABOVE SET POINT Select YES Select SET POINT Enter 0 25 Select ABOVE SET POINT 35 6700FR Refrigerated Sampler Example 6 Storm Water Runoff Sampling continued CHECK ENABLE EVERY De gt E Select 5 10 15 30 MINUTES ONCE ENABLED STAY ENABLED Select YES YES NO SAMPLE AT ENABLE Select NO YES NO START OF SAMPLING AFTER A Enter 20 20 MINUTE DELAY 1 999 PAUSE RESUME Select DONE 1 HH MM DD HH MM DD 2 HH MM DD HH MM DD Screen will say End of Part B CLEAR DONE NO DELAY TO START DE
89. EL are in effect such limits shall take precedence PHYSICAL AND CHEMICAL PROPERTIES Physical Data Boiling Point 26 5 C 15 7 F 736 mm Hg Vapor Pressure 96 psia at 25 deg C 77 deg F Vapor Density 3 60 Air 1 0 at 25 deg C 77 deg F Volatiles 100 WT l Solubility in Water 0 15 W 25 C 77 F and 14 7 psia Odor Slight ethereal Form Liquefied gas Color Colorless i Density 1 21 g cc at 25 deg C 77 deg F Liquid STABILITY AND REACTIVITY Chemical i Material is stable However avoid open flames and high temperatures Incompatibility with Other Materials Incompatible with alkali or alkaline earth metals powdered Al Zn Be etc Polymerization Polymerization will not occur Other Hazards Decomposition Decomposition products are hazardous HFC 134a can be decomposed by high temperatures open flames giowing metal surfaces etc CRUEL hydrofluoric acid and possibly carbonyl fluoride 136 6700FR Refrigerated Sampler TOXICOLOGICAL INFORMATION Animal Data Inhalation 4 hour ALC 567 000 ppm in rats A 5 or 10 second spray of vapor produced very slight eye irritation and a 24 hour occlusive application produced Slight skin irritation in rabbits The compound is not a skin sensitizer in animals No toxic effects were seen in animals from exposures by inhalation to concentrations up to 81 000 ppm Lethargy and rapid respiration were observed at a vapor concentration of 305 000 p
90. ENT MARK SENT FOR EVERY SAMPLE COMPLETE SAMPLES 4 EVENT MARK SENT WHILE PUMPING FORWARD PRE SAMPLE PURGE COUNTS 10 9999 PUMP COUNTS FOR EACH PURGE CYCLE PRE SAMPLE _ POST SAMPLE POST SAMPLE PURGE DEPENDENT ON HEAD FIXED COUNT YO1 1 0 ENABLE 1 02 PGM RUNNING 1 03 PROGRAM DONE See Note B SET 1 Ox NONE I O ENABLE FR TEMP PGM RUNNING PGM ENABLED A ENABLED B ENABLED PROGRAM DONE A DONE B DONE RUN ERROR FLOW THRU CONDITIONS gt gt gt gt gt gt gt gt gt gt See Figure 47 Analog Output and Dialout Quick View Screens on page 131 Notes USE LIQUID DETECTOR YES NO DO YOU HAVE A YES RAIN GAGE CONNECTED YES NO RAIN GAGE 0 01 inch TIP 0 imm TIP If applicable NEW HARDWARE SETUP STORED DATA WILL BE LOST OK YES NO See Figure 44 Extended Programming YSI 600 Screens on page 129 See Figure 45 Extended Programming Optional YSI Screens on page 130 See Note A BOTTLE FULL DETECT YES NO REENTER NEW PASSWORD AT THE BEGINNING OF INITIAL PURGE FORWARD PUMPING EVENT MARK DURATION 3 SECONDS WHILE PUMPING DURING ENTIRE PUMP CYCLE FORWARD PUMPING POST SAMPLE PURGE ____ COUNTS 10 9999 NEW HARDWARE SETUP STORED DATA WILL BE LOST OK YES NO RUN FLOW THRU PUMP ___ SECONDS BEFORE TAKING READINGS 0 120 See Figure 41 on page 126 A Option only
91. EVERSE functions so that the pump rollers do not over heat Continuous dry pumping may damage the pump rollers PURGED COUNTS Moving the Distributor 37 a or The sampler lets you reposition the distributor arm Use this fea ture to verify a bottle location when installing a bottle kit You can not move the distributor while the sampler runs a program Moving the Distributor Arm Always use the steps shown in the margin GRAB SAMPLE CALIBRATE VOLUME OPERATE PUMP MOVE DISTRIBUTOR AN CAUTION e Select MOVE DISTRIBUTOR DO NOT ROTATE THE DISTRIBUTOR ARM MANUALLY THIS WILL SE VERELY DAMAGE THE DISTRIBUTOR DRIVE GEARS da ta 7 MAX Programming Style The sampler has two different styles of programming screens o NORMAL and QUICK VIEW CHANGE which you want to move the distributor The NORMAL programming style steps you through each pro gramming step You simply answer each question as it is asked NOW AT BOTTLE __ The standard programming mode defaults to NORMAL 40 91 6700FR Refrigerated Sampler The QUICK VIEW CHANGE programming style includes a series of summary screens Summary screens include one or more program settings You can quickly step through the program by selecting the located in the lower right hand corner of the display You can even backstep through the program by selecting the T located in the up per left hand corner of the display Program changes are made by selecting the pro
92. Extended page 119 NUMBER OF BOTTLES 1 2 4 8 12 24 BOTTLE VOLUME IS ml 300 30000 SUCTION LINE LENGTH FS __ ft 3 99 AUTO SUCTION HEAD ENTER HEAD SUCTION HEAD OF ft min max _ RINSE CYCLES 0 3 RETRY UP TO _ TIMES WHEN SAMPLING 0 3 BOTTLES AVAILABLE ONE PART PROGRAM ASSIGN BOTTLES TWO PART PROGRAM 1 THRU __ TO PART A 1 max See Figure 36 Extended Programming Pacing and Distribution on page 121 120 6700FR Refrigerated Sampler Figure 36 Extended Programming Pacing and Distribution Continued from Figure 35 Extended Programming Equipment Setup on page 120 UNIFORM TIME PACED FLOW PACED EVENT PACED NONUNIFORM TIME See Note A NONUNIFORM TIME CLOCK TIMES INTERVALS IN MINUTES RANDOM INTERVALS PROGRAM RUN TIME _ HOURS __ MINUTES TIME BETWEEN SAMPLE EVENTS _ HOURS __ MINUTES PACED BY FLOW PULSES FLOW MODULE VOLUME FLOW BETWEEN SAMPLE EVENTS _ PULSES 1 9999 TAKE SAMPLES AT 1 START TIME 2 HH MM 3 HH MM SAMPLE AT START YES NO FIRST SAMPLE AT START TIME THEN 5 DO YOU WANT TO RUN CONTINUOUSLY YES NO QUANTITY AT INTERVAL 1 __AT___ Ca e A gt lt BOTTLES PER SAMPLE EVENT 1 max Multi bottle Fa AT oo MIN MIN MIN SWITCH BOTTLES ON NUMBER OF SAMPLES TIME SWITCH BOTTLES EVERY ___ SAMPLES 1 max SWITCH BOTTLES EVERY MINUTES gt _ HOURS __ RUN CONTINUOUSLY YES NO TAKE
93. FICATIONS CONTINUED Module Reading Conversions Level and 4 20 mA readings converted to flow rate units gallons per second gallons per minute million gallons per day cubic feet per second cubic meters per second cubic meters per hour cubic meters per day liters per second e Velocity units feet per second meters per second e Totalized flow units gallons million gallons cubic feet cubic meters liters e Devices supported in flow conversion Weirs V notch 22 5 30 45 60 90 and 120 degrees Rectangular with and without end contractions Cipoletti Flumes Parshall 1 2 3 6 9 1 5 2 3 4 5 6 8 10 12 Palmer Bowlus 4 6 8 12 15 18 21 24 27 30 48 Trapezoidal LG 60 V 2 45 WSC 12 45 SRCRC H 0 5 0 75 1 1 5 2 2 5 3 4 5 Manning Formula Round U channel Rectangular Trapezoidal Area Velocity Round U channel Rectangular Trapezoidal Data Points 50 level flow rate points 50 level area points YSI 600 Sonde Units e pH 2 0 to 14 0 e Temperature C or F e Dissolved Oxygen mg l milligrams per liter e Conductivity reported as Specific Conductance mS cm millisiemens per centimeter Salinity ppt parts per thousand Total Dissolved Solids g l grams per liter Conductivity mS cm millisiemens per centimeter Refrigerator Temperature Optional sensor and 5 ft 1 55 m cable to record temperature readings Intended Sensor for use with refrigerated samplers
94. FR Sampler s response string is the same for each of the three commands A sample response string is shown below MOG T00G ID zZ42z4741453r o O 2 0 00 SS Leow ly 30404 oo T Ey VOLO Vy Coes Xe ER gt Note that the sampler s response is a series of alphabetical and nu merical pairs The alphabetical characters are headings that de scribe the following numerical value or code A complete description of each pair is listed below MO 6700 isthe model number of the sampler ID 2424741493 is the sampler s unique identification number T1 35523 50000 is the sampler s current time STS 1 isthe sampler s current status The possible states are 1 WAITING TO SAMPLE 2 IN SETUP MENU 3 SAMPLER DISABLED pin F of external flowmeter connector 4 POWER FAILED short duration after power is re stored 5 PUMP JAMMED must be resolved before continu ing 6 DISTRIBUTOR JAMMED 9 SAMPLER OFF 12 SAMPLE IN PROGRESS 20 INVALID COMMAND This will occur for any of the following 103 6700FR Refrigerated Sampler e identifier code not supported e bottle requested is not in the current configura tion e sample volume requested is outside its range 10 9990 ml e day Set Time Command must be 5 digits and more recent than 1977 21 CHECKSUM MISMATCH STI 35523 41875 is the most recent sample time BTL 2 1s the bottle receiving the most recent sample SVO 100 is the most recent sample s vol
95. FUNCTIONS GRAB SAMPLE E iras e A new pump tube is installed Run the pump for five minutes MOVE DISTRIBUTOR before calibrating e Select CALIBRATE VOLUME e The sample source is above the sampler e Sampling from pressurized lines 15 PSI Maximum excessive wear and replace it if necessary You may want to calibrate when SAMPLE VOLUME mi 10 9990 Calibration Tips Enter the desired volume e For the best results calibrate the sampler after it s installed on CALIBRATE VOLUME site PRESS WHEN READY e Use a graduated cylinder for volume measurement e The sampler clears the previous calibration setting when you reinitialize the sampler PURGING SUCTION LINE e You cannot calibrate while the sampler is running a program e When the sampler delivers the sample it runs through a com plete sampling cycle using the current settings for volume line rinses and retries If it is a two part program the sampler uses PUMPING 200 ml the volume setting for part A To calibrate 1 Disconnect the pump tube from the bulkhead fitting PURGING LONE 2 Place the end of the tube over a collection container 3 Follow the steps in Calibrating Sample Volumes in the margin VOLUME DELIVERED 4 Reconnect the pump tube to the bulkhead fitting m e Measure the volume delivered and enter the amount here 200 ml ARE YOU SURE YES NO This screen appears when the amount you entered in step 8 was mo
96. LAYED START Select DELAYED START CLOCK TIME START STORM AFTER A Enter 1 1 MINUTE DELAY 1 999 PROGRAMMING COMPLETE RUN THIS PROGRAM Select NO NOW YES NO 36 6700FR Refrigerated Sampler Chapter 3 Operation Installation and Operation Checklist 1 Prepare the sampler a Adjust the distributor arm to fit the bottle kit Then install Chapter Contents the distributor arm and the discharge tube See Installing Installation and Operation the Distributor Arm and Discharge Tube on page 39 For Checklist 37 composite bottle kits attach the discharge tube to the Preparing the Sampler 38 bulkhead fitting and thread through the hole in the bottle Installing Bottle KIS 22 5 At lid See Installing Copos DUE on page ae Installing Composite Bottle 43 b Install the bottle kit See Installing Bottle Kits on page Suction Li 44 say SUCHON LING comida aa c Check the pump tube Replace it if necessary and reset the Strainers 44 pump tube warning See Replacing the Pump Tube on e How Does the Sampler Work 45 page 70 e Installing the Sampler 47 d Attach the suction line to the pump tube See Suction e Running Programs 49 Line on page 44 e Run Time Screens 50 e Attach a strainer to the suction line if necessary See Interrupting a Running Program 52 Strainers on page 44 Servicing the Sampler A 54 2 Install the
97. ME Enter 250 250 ml 10 1000 R le Select CLOCK TIME DELAYED START CLOCK TIME START FLOW COUNT AT NIEREN ENET O 06 00 This is the time at which the sampler will start the pacing countdown SELECT DAYS SU M TU WE TH FR SA Select MO WE and FR DONE Using the Clock Start Time Menu on page 18 shows you how to use this menu PROGRAMMING COMPLETE RUN THIS PROGRAM Select NO NOW YES NO 29 M Note To enable the Bubbler Module programming screens insert the module before turning on the sampler 6700FR Refrigerated Sampler Example 6 Storm Water Runoff Sampling Storm water runoff sampling is an ideal application for two part pro gramming Typical monitoring permits require that a series of timed samples be taken during the initial portion of the storm event fol lowed by flow paced samples during the remainder of the event This example assumes that a Rain Gauge and a Bubbler Flow Mod ule are connected to the sampler Using a 24 bottle kit 1t divides the bottles into two groups with six bottles assigned to part A and 18 to part B The sampler will begin taking samples after being en abled according to programmable enable controls that is when the rain gauge detects 0 15 inches of rainfall in 30 minutes and the module detects a flow stream level of more than 0 25 feet Because both program parts use the same enable settings the sampler will enable both parts at the same time A list of se
98. Melting Point N A Solubility in Water Insoluble Bulk Density 57 64 lbs cu ft Percent Volatile by Weight at 150 deg C lt 3 0 SECTION IV FIRE EXPLOSION DATA Fire and Explosion Hazard Negligible fire and explosion hazard when exposed to heat or flame by reaction with incompatible substances Flash Point Nonflammable Firefighting Media Dry chemical water spray or foam For larger fires use water spray fog or foam Firefighting Nonflammable solids liquids or gases Cool containers that are exposed to flames with water from the side until well after fire 1s out For massive fire in enclosed area use unmanned hose holder or monitor nozzles 1f this is impossible withdraw from area and let fire burn Withdraw immediately in case of rising sound from venting safety device or any discoloration of the tank due to fire SECTION V HEALTH HAZARD DATA This material is normally packaged and contained in a bag If the bag 1s open the resulting dust is classified a nuisance dust and may cause health hazards when inhaled ingested or in contact with the eyes and skin Prolonged inhalation may cause irritation to the upper respiratory tract and or lung damage If large amounts are ingested intestinal disorders may occur Contact with eye tissue may result in irritation Prolonged or repeated contact with the skin in the absence of proper hygiene may cause irritation DESI PAK clay may contain a small amount of crystalline
99. Mme e For the Module YSI and Rainfall Data reports it displays dai ly summaries instead of the full reports available with the field SIRO printer RTD Flowlink or SAMPLINK si Mie If you select SAMPLING REPORT or RAINFALL step 3 in View ing Data shown in the margin the sampler begins displaying the e Select VIEW DATA report data The sampler advances automatically through the re EW port items displaying each item briefly While the sampler advanc SAMPLING REPORT es automatically through the displays 3 MODULE DATA Ru RAINFALL DATA e Stop the automatic displays by pressing Stop once Then use the arrow keys to move manually through the report li DES e Return to the main menu by pressing Stop twice VIEW i DAILY SUMMARY At the end of the report the sampler leaves the last item displayed 4 CURRENT READINGS until you press e the arrow keys to move forward or backward manually through e Select Daily Summary to view the report the stored data or Current Readings to view real time data e Enter to start the automatic displays again If you select MODULE DATA or YSI DATA in step 3 the sampler displays the screen shown in step 4 Select the DAILY SUMMARY option and the sampler displays the stored data one day at a time Selecting the CURRENT READINGS option causes the sampler to display real time readings When there are multiple screens they will alternately be displayed You can quickly advance through the
100. NABLE RAIN AND VO RAIN LEVEL FLOW Y pH Y TEMP Y COND Y D O NONE RAIN SET POINT 0 15 INCHES PER 15 MIN 30 MIN 1 HOUR 2 HOURS ENABLED WHEN ABOVE SET POINT BELOW SET POINT Select UNIFORM TIME PACED Enter 0 for hours 5 for minutes Enter 1 Select NUMBER OF SAMPLES Enter 1 Select NO Select NO Enter 800 Select RAIN All valid enable options will appear here Select AND Select LEVEL Enter 0 15 for inches then select 30 minutes Select ABOVE SET POINT 33 6700FR Refrigerated Sampler Example 6 Storm Water Runoff Sampling continued 92 RESET RAIN HISTORY YES NO LEVEL CONDITION SET POINT RANGE LEVEL SET POINT 0 25 ft 0 001 30 000 ENABLED WHEN ABOVE SET POINT BELOW SET POINT CHECK ENABLE EVERY 05 1 2 5 10 15 30 MINUTES ONCE ENABLED STAY ENABLED YES NO SAMPLE AT ENABLE YES NO PAUSE RESUME 1 HH MM DD HH MM DD 2 HH MM DD HH MM DD CLEAR DONE UNIFORM TIME PACED FLOW PACED EVENT PACED NONUNIFORM TIME PACED BY FLOW PULSES FLOW MODULE VOLUME FLOW BETWEEN SAMPLE EVENTS 2500 gal 0 001 99999 SAMPLE AT START YES NO 1 BOTTLES PER SAMPLE EVENT 1 18 Select YES Select SET POINT Enter 0 25 Select ABOVE SET POINT Select 5 Select YES Select YES Select DONE Screen will say End of Part A then Beginning of Part B Select FLOW PACED Select FLOW MODULE VOLUM
101. OLLER ELECTRICAL SPECIFICATIONS Controller Internal Battery Real Time Clock Accuracy Program Memory Sampler Power Requirements 5 years minimum Maintains internal logic program settings and stored data 1 minute per month Nonvolatile programmable Flash Can be field updated via the interrogator connector Nominal 12 volts DC supplied by the refrigerator Operational 11 to 13 Volts DC Absolute Maximum 14 4 Volts DC 6700FR Refrigerated Sampler Table 3 Technical Specifications for the 6700FR Sampler 6700 CONTROLLER ELECTRICAL SPECIFICATIONS CONTINUED Sampler Standby Current Sampler Only 11 m average Sampler with pH Module 26 mA average Sampler with Ultrasonic Module 35 mA average Sampler with Submerged Probe Module 27 mA average Sampler with Bubbler Module 49 mA average Sampler with Area Velocity Module 171 mA average Sampler with 4 20 mA Module 17 mA average This is without backlight Add 220 20 mA when backlight is on Sampler Only Approximately 30 mA based on 200 ml sample every hour 10 ft 3 m suction line Operating Current and 5 ft 1 5 m suction head Flow Meter 5 to 15 volt DC pulse or isolated contact closure of at least 25 millisecond duration Signal Requirement 4 20 mAor pulse duration signal may be converted with optional interface unit 6700 CONTROLLER SOFTWARE SPECIFICATIONS Suction Line Sample Frequency Rainfall Reading Units Programmable 3 to 99 ft 1 to
102. ONITE CLAY Product CAS No 1302 78 9 Product Use Drying agent Supplier ENGELHARD CORPORATION CHEMICAL CATALYSTS GROUP Address 600 E MCDOWELL ROAD City St Zip JACKSON MS 39204 Phone 1 800 458 8650 OR 1 800 654 4039 FOR CHEMICAL EMERGENCY CALL CHEMTREC 24 HOURS 1 800 424 9300 US Canada Puerto Rico Virgin Islands 1 202 483 7616 Outside Above Area SECTION II COMPOSITION INFORMATION ON INGREDIENTS INGREDIENT CAS NO lt Wt SILICA CRYSTALLINE QUARTZ 14808 60 7 1 3 ALUMINUM SILICATE 12141 46 7 97 INGREDIENT NOTES NOTE Industrial hygiene sampling in our plant has shown the respirable fraction of crystalline silica quartz to be only 0 1 0 115 NOTE See Section VIII for Exposure Limits and Section XI for Toxicological Information 139 6700FR Refrigerated Sampler ENGELHARD Page 2 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 SECTION III HAZARDS IDENTIFICATION EMERGENCY OVERVIEW Grey to off white granules Odorless Flash Point Not Applicable SUSPECT CANCER HAZARD Risk of cancer depends on route duration and level of exposure Prolonged or repeated inhalation may cause lung damage May cause eye and respiratory tract irritation Not a fire or explosion hazard ROUTES OF ENTRY Eyes NO Skin NO Inhalation YES Ingestion NO POTENTIAL HEALTH EFFECTS EYE CONTACT may cause mechanical irritation if exposed to large amounts of dust SKIN CONTACT may cause irrita
103. PAL 1101s have a programma ble sampler enable feature that lets them enable start or disable stop a program according to certain monitored conditions For ex ample these conditions can be level flow rate pH temperature percent rainfall I O or a combination of two conditions These flow instruments enable or disable a sampler by sending a signal to pin F of the sampler s flow meter connector The instru ment can enable or disable the sampler e At a specific time and date e When the reading passes a set point e When the reading is within or outside a certain range e When the rainfall rate exceeds a set point The Model 1640 Liquid Level Actuator can also be used as well as any other instrument that can ground the input to pin F Ground ing the input disables the sampler A sampler running either a standard or extended program can rely on external input for enable or disable controls The sampler s extended programming screens let you program the sampler similar to the way devices controlling pin F are pro grammed Input from a rain gauge YSI Sonde programmable I O pin or a module may be used when programming enable condi tions Any combination of up to two conditions can be programmed Check Enable Interval If programming the sampler to use a 700 Series module or YSI Sonde parameter for enabling the sampler will request a Check Enable interval The Check Enable interval allows the sampler to compare the param
104. PAUSE 8 RESUMES PAUSE RESUME 1 HH MM DD HH MM DD SAMPLE AT RESUME 2 HH MM DD HH MM DD YES NO CLEAR DONE NO SAMPLE AT RESUME A All valid enable options will be shown Enable options may include LEVEL FLOW pH TEMP PERCENT VEL RAIN 1 0 A DONE FR TEMP Y TEMP Y COND Y SP_CO Y TDS Y SAL Y DO Notes Y pH Y ORP Y LEVEL Y NH4 Y NH3 Y NO3 Y TURB Y CI See Figure 28 Standard and Extended CORSI Programming Quick View Start Times B YES Latched or Stay Enabled on page 114 NO Repeatable Enable 126 6700FR Refrigerated Sampler Figure 42 Extended Programming Hardware Screens MAINTENANCE DO YOU HAVE A MANUAL FUNCTIONS USE LIQUID DETECTOR RAIN GAGE CONNECTED RUN EXTENDED 1 PROGRAM PROGRAMMING STYLE YES NO YES NO HARDWARE VIEW REPORT OTHER FUNCTIONS If applicable YES NEW HARDWARE SETUP RAIN GAGE STORED DATA WILL PLEASE WAIT PARTITION MEMORY 0 01 inch TIP BE LOST OK YES NO WILL LAST __ DAYS 0 1mm TIP See Figure 44 Extended Programming NO YSI SONDE YSI 600 Screens on page 129 YSI 600 OTHER YSI SONDE See Figure 45 Extended Programming Optional YSI Screens on page 130 See Note A a pag BACKLIGHT ALWAYS OFF BOTTLE FULL DETECT TIMED BACKLIGHT YES NO CONTINUOUS BACKLIGHT MASTER SLAVE YES NO See Note A ENABLE PROGRAM LOCK tes YES NO CHANGE PASSWORD TO REENTER NEW PASSWORD AT THE BEGINNING OF INITIAL PURGE FOR
105. PLE and SET TIME All commands must include the instruction set and a checksum value Get Status There is only one form of this command available TS 1269 90 1LSCER gt e STS 1 instructs the sampler to return the current status e cs 581 is the checksum value The byte by byte sum of the ASCII values in the string STS 1 CS is 581 e lt CR gt is a carriage return signifying the end of the command 102 6700FR Refrigerated Sampler Take Sample The TAKE SAMPLE command is only valid ifthe sampler is WAIT ING TO SAMPLE Format the command as follows BLE o Vor LUO CSS SS e BTL 2 instructs the sampler to place the sample in bottle 2 e SVO 100 instructs the sampler to take a 100 ml sample e CS 1039 is the checksum value The byte by byte sum of the ASCII values in the string BTL 2 SVO 100 CS is 1039 e lt CR gt is a carriage return signifying the end of the command Set Time The SET TIME command is only valid if the sampler is WAITING TO SAMPLE Format the command as follows TIL 00000 CS OSOS ERA e TT 35523 50000 sets the time The value 35523 5000 is the number of days since 00 00 00 1 Jan 1900 This example would set the sampler s clock to 12 00 00 3 Apr 1997 e CS 988 is the checksum value The byte by byte sum of the ASCII values in the string TI 35523 50000 CS is 988 Command Driven Sampler Responses The 6700
106. PLINK Software Includes Instruction Manual 60 3774 013 STD Field Printer A Lee dde et ue i 60 3774 001 Computer Connect Cable 25 pin 60 2544 040 Computer Connect Cable 9 pin sense ce ee eee eee eee tent eee eens 60 2544 044 Connector to Attach Non Isco Flow Meter to Customer Supplied Cable 68 1680 060 Serial Output connect cable for use with the periodic serial output feature 60 9004 263 Flow Meter to Two Samplers Cable 60 3004 018 Master Slave Interconnect Cables escorial edad da les 60 3704 065 Master Slave to Flow Meter Cable 222 ccm oueee ee eee nee nett een eens 60 3704 080 Non Isco Flow Meter to Sampler Cable ouoeenn eee nee eens 60 1394 077 Sampler to Flow Meter 1640 Liquid Level Actuator Y Cable 60 3004 019 Sampler to Flow Meter Cable LL 60 3004 107 Rain Gauge Refrigerator Temperature Sensor Y cable 60 9004 294 12 Volt Power Sources 913 High Capacity Power Pack 120 volt 60 1684 088 914 Battery Backed Power Pack 120 volt 60 3004 130 934 Nickel Cadmium Batteries A ADA 60 1684 040 923 High Capacity Power Pack 240 TON a
107. Presample Purge Rinse Cycle Pump Volume 1 Pump Volume 2 Pump Volume 3 Postsample Purge Event Mark Pulse at Beginning of Forward Pumping Only Variable Duration Pulse EEE During Entire Pump Cycle Bottle Number Event Mark Bottle Number Event Mark Variable Duration Pulse During Forward Pumping Only Using the Purge Count screens PRE SAMPLE PURGE COUNTS 10 9999 POST SAMPLE PURGE DEPENDENT ON HEAD 91 FIXED COUNT POST SAMPLE PURGE COUNTS 10 9999 Note The state of the I O lines is not de fined when the sampler is OFF Bottle Number Event Mark Bottle Number Presample and Postsample Purge Counts The presample purge is when the pump runs in reverse clearing the strainer of any debris before taking a sample The presample purge is set at 200 pump counts After the sample is taken a post sample purge occurs to clear the liquid from the suction line The duration of the postsample purge is determined by the length of the suction line to maximize the battery life The pre and postsample purge can also be manually set I O Pin Programming Pins C H and I on the Rain Gauge Connector are user configured as 1 01 1 02 and 1 03 Input Output pins respectively Each pin can be either an input for sampler enabling or an output for alarms such as PROGRAM DONE RUN ERROR etc The CONDITIONS VO output can report alarm conditions using the parameters the 6700 is configur
108. Press the Up Left arrow until e BACK UP an option that moves the cursor on the text line to the I blinks Press enter the left one character SITE SITTORY051 e DONE an option that tells the sampler to save the text ABCDEFGHIJKLMNOPQRST BR l UVWXYZ amp 0123456789 The cursor is the blinking rectangle It also appears in number en BACK UP DONE try screens Its position identifies the current field When screen 1 e Continue to press the arrow first appears the cursor blinks on the first character of the text keys to select the characters The matching character in lines 2 or 3 also blinks T E and space Press enter after selecting each character SITE SITE 29_ When you press enter the cursor on line 1 moves to the right one position and at the same time the sampler blinks the matching ABCDEFGHIJKLMNOPQRST character on lines 2 or 3 UVWXYZ amp _ 0123456789 BACK UP DONE To change any character in the text line e Press 29 on the keypad then 1 Press the left or right arrow until the replacement character Up Left until space blinks on lines 2 or 3 flashes Press enter 2 Press Enter The replacement character will appear on SITE SITE 29 ABCDEFGHIJKLVNOPORST the first line and the cursor will move to the next character n UVWXYZ amp _ 0123456789 Repeat steps 1 and 2 until the text in the top line is complete BACK UP DONE 3 Finish the entry by selecting DONE Then press enter
109. R 99 Hardware B2 Software 3 10 BUBBLER MODULE 638324458 Hardware AO Software 1 00 SITE FACTORYOO9 PROGRAM EXTENDED 1 Summary Report for 23 MAR 99 TU Day s Rain 0 23 in Average Rain Hour 0 01 in 08 00 Minimum Rain Hour 0 00 in 10 00 Maximum Rain Hour 0 13 in Hourly Rain Summary 00 00 01 00 NO DATA 01 00 02 00 NO DATA 02 00 03 00 NO DATA 03 00 04 00 NO DATA 04 00 05 00 NO DATA 05 00 06 00 NO DATA 06 00 07 00 NO DATA 07 00 08 00 0 00 in 08 00 09 00 0 00 in 09 00 10 00 0 05 in 10 00 11 00 0 13 in 11 00 12 00 0 00 in 12 00 13 00 0 00 in 13 00 14 00 0 05 in 14 00 15 00 0 00 in 15 00 16 00 0 00 in 16 00 17 00 0 00 in 17 00 18 00 NO DATA 18 00 19 00 NO DATA 19 00 20 00 NO DATA 20 00 21 00 NO DATA 21 00 22 00 NO DATA 22 00 23 00 NO DATA 23 00 24 00 NO DATA x 0 30 I I I I I I I I 0 20 I I I I I I I I 0 10 I I I I I tt I I tt I 0 00 dad A Hour Ending 03 16 24 Units are in 63 6700FR Refrigerated Sampler Figure 11 Report Summary continued SAMPLER ID 0011343009 15 25 23 MAR 99 Hardware B2 Software 3 10 BUBBLER MODULE 638324458 Hardware AO Software 1 00 SITE FACTORY009 PROGRMA EXTENDED 1 Summary Report for 23 MAR 99 TU Day s Flow 000000 054 Mgal Average Flow Rate 0 4437 cfs 07 20 Minimum Flow Rate 0 0237 cfs 13 25 Maximum Flow Ra
110. ROGRAM or press ing the Stop key If you do not make a selection the sampler auto matically resumes the original sampling program five minutes after the last key was pressed Stop Program This option terminates the running program and records PRO GRAM STOPPED in the sample event log The program cannot be resumed Resume Program Selecting this option will cause the sampler to exit the manual paused state and return to normal program operation A MANUAL RESUME event will be logged View Data This option allows you to view the data recorded by the sampler See Sampling Reports on page 54 for more information Grab Sample When selected you will be asked to enter the volume to be pumped A sample will then be taken as if it is to be placed into a container outside the sampler base Do this by removing the pump tubing from the bulkhead fitting See Grab Samples on page 65 A GRAB SAMPLE event will be logged Pump Tube Alarm If the pump tube is changed this option should be selected to reset the pump counts on the counter This will remove the WARNING REPLACE PUMP TUBING message that may appear while the program is running A PUMP TUBE REPLACED message is logged See Replacing the Pump Tube on page 70 52 6700FR Refrigerated Sampler Calibrate Volume When selected you will be asked to enter the volume to be pumped A sample will then be taken as if it is to be placed into a container outside the sampler base
111. RUN had been previously STOPped and no programming changes were made PROGRAMMING COMPLETE an ae Multiple Bottles ENTER START BOTTLE YES NO __ 1 MAX OR For the first run using RUN a 24 bottle base PROGRAM If applicable VIEW REPORT OTHER FUNCTIONS PLEASE WAIT TESTING FATAL ERROR DISTRIBUTOR SYSTEM NO DISTRIBUTOR ARM If applicable PROGRAM WILL START AT 06 00 MO 17 0CT OPERATION ERROR DISTRIBUTOR JAMMED Single Bottle 05 52 22 MO 17 OCT PURGING SUCTION LINE PUMPING 250 ml RUN DISPLAYS RINSING SUCTION LINE SAMPLE 2 IN 00 14 29 49 6700FR Refrigerated Sampler Run Time Screens While running a sampling program the sampler displays a variety of messages that report the program s status For example if the sampler has not yet reached the programmed start time it displays the scheduled start time as well as the current time Some com mon run time displays are shown in Figure 7 Once the program reaches the start time you can determine the time of the next sample the next bottle to receive a sample sample distribution and other information Other messages appear while the sampler runs through a sampling cycle as 1t takes a sample When the sampler needs to report multiple messages it alternates them displaying each for one to three seconds Module and YSI Sonde Readings Samplers with an attached module display the module s readings pH and temperature for the pH module percentage or flow rate
112. Refrigerated Sampler Example 6 Storm Water Runoff Sampling continued 6700 SAMPLER EXTENDED PROGRAMMING 1 For HELP at any screen press key RUN ISCO 6700 PROGRAM 2 VIEW REPORT OTHER FUNCTIONS PROGRAM NAME ISCO 6700 3 CHANGE YES NO SELECT NEW PROGRAM 4 CHANGE PROGRAM NAME NAME STORM ABCDEFGHIJKLMNOPQRST 5 UVWXYZ amp 0123456789 BACK UP DONE SITE DESCRIPTION FACTORY051 6 CHANGE YES NO SITE SITE 54 ABCDEFGHIJKLMNOPQRST 7 UVWXYZ amp 0123456789 BACK UP DONE SELECT UNITS FOR 8 LENGTH ft m SELECT UNITS FOR FLOW RATE 9 cfs gps gpm Mgd lps m3s m3h med SELECT UNITS FOR FLOW VOLUME cf gal Mgal m3 lit PROGRAM MODULE YES NO MODE OF OPERATION FLOWMETER LEVEL ONLY FLOW CONVERSION WEIR FLUME DATA POINTS MANNING FLOW INSERT Select PROGRAM Note If the start up screen displayed STANDARD PROGRAMMING type 6700 2 at this menu before selecting PROGRAM Select YES Note If the quick view screen shows up press STOP then select OTHER FUNCTIONS PROGRAMMING STYLE NORMAL Then go back to step 2 Select CHANGE PROGRAM NAME Enter the word STORM for the program name See Using the Site Description or Program Name Menus on page 19 Select YES Enter SITE 54 for the site description Select ft Select gpm Select gal Select YES Select FLOWMETER Select FLOW INSERT 31 6700FR Refrigerated Sampler Exam
113. S Safety 155 Salinity 1 Sample volume 81 calibrating 66 flow dependent 81 measuring 46 Sampler enable 87 repeatable enable 88 sample at enable 88 stay enabled 88 Samplers accessories list 169 Sampling cycle operating displays 50 Sampling programs running programs 49 Sampling reports collecting reports 55 combined reports 57 configuring 56 error codes 58 program settings report 56 sampling results report 57 source codes 58 summary report 57 viewing 55 Serial output 97 Servicing 54 see Maintenance service schedule 54 Site description menu how to use 19 Software upgrade 101 Specific conductance 1 Start times clock start time menu 18 event pacing 83 first valid day 49 90 sampler enable and nonuniform clock times 90 two part programs 90 Stored data 16 Stored programs 25 selecting a program 25 Stormwater monitoring Two part programs 24 Strainers accessories list 170 selecting 45 specifications and applications 45 Suction head maximum head for peristaltic pumps 8 44 variations in pump counts for fluctuating heads 57 Suction line accessories list 170 measuring and cutting 44 nonstandard suction line 44 T Technical specifications controller 8 10 refrigerator 11 12 Text entry numbers 15 program names 19 site descriptions 19 Times and dates entering times and dates 18 Time switched distribution 85 pause and resume 88 Total Dissolved Solids T D S 1 Two part programs 24 90 start times 90 storm water
114. S Continue d Is there 120 or 230 V across the start relay and compressor common NO Check to see ifthe thermal cutout relay is open or the start relay is defective YES Check the compressor for an open winding YES a Is the fan running NO Replace the fan YES Continue b Check the refrigerant in the refrigeration system Problem Samples freezing 1 Is the Heaters LED on the circuit board lit NO Check the circuit board for a malfunction If the board is good replace the ambient air sensor YES Continue 2 Is there 5 V across pins 3 and 4 of heater relay K2 NO Check Q4 on the circuit board for a malfunction YES Continue 3 Is there 120 or 230 VO across pins 1 and 2 of heater relay K2 NO Replace heater relay YES Continue 4 Is there 120 or 230 V across pins 2 and 3 on PCB connector P10 NO Replace heater fuse F2 Refer to the replacement parts listing for the correct part number YES Check heater wiring Problem Sampler has no power 1 Is there 12 V at the sampler connector NO Continue YES Troubleshoot the sampler controller 2 Is there 12 V between pins 1 and 8 on PCB connector P5 NO Check F1 If open replace fuse Refer to the replacement parts listing for the correct part number YES Check the power supply circuit for malfunction 80 Chapter Contents e Sample Event 81 Sample Volume 81 e Suction Head
115. SI Combined Results and daily Summary Reports Program Settings Report The printout will be the screens of the QUICK VIEW CHANGE PROGRAM sequence For nonuniform time paced programs pac ing information is also printed This report is shown in Figure 9 When in extended programming the Program Settings Report will also include the hardware settings 56 6700FR Refrigerated Sampler To print the current sampling program settings you can page through the change or view displays until you see the screen below Select YES PRINT PROGRAM YES NO This display appears only when a printer is connected Sampling Results Report As the sampler runs a program it records the program s events Program events include such items as sample events program en ables and disables power losses and so on Table 9 lists each event with a short description You can view the report by following the steps in Viewing the Data on page 55 or print the log as the Sam pling Results report The Sampling Results report includes both Figures 8 and 9 In the printed version of the report sample event entries the time of the event as well as the sample and bottle numbers The sample column contains the sample number deposited into the bottle This information reflects the distribution selected for the program The letters in the Source columns are codes for the cause of the event The letters in the Error column are codes for the causes of mis
116. SI 600 Sonde e The Module Summary report summarizing flow rate or pH temperature readings e The Rainfall Summary report listing a summary of rainfall readings Examples of the reports appear in Sampling Reports on page 54 ASCII data output from the interrogator port See Serial Output on page 97 A variety of metric and English units of measure for length flow rate flow volume and temperature Isco flow meters flow loggers and PAL 1101s have a programmable sampler enable feature that lets them send an electronic signal to a 6700 that enables starts or disables stops a running sampling program See Sampler Enable on page 87 Master slave sampling operates two samplers Note See Master Slave Sampling on page 94 Operate sampler functions using RS 232 communications See Command Driven Operation on page 102 ePump Tube Warning The 6700 displays a warning to inspect the tube See Replacing the Pump Tube on page 70 e Internal Battery Warning The 6700 displays a warning when it is time to replace the internal battery The internal battery preserves stored data when the 6700 is without external power See Replacing the Internal Battery on page 75 The 6700FR controller can be ordered with a factory installed 2400 baud dialout modem The modem requires B2 hardware With the modem you can e connect to the sampler and download data using Flowlink software e program the sampler to call a contact list when an ala
117. Sampling of Water and Wastewater by Dr Phillip E Shelley Isco Glass Sample Bottles One spectro grade acetone rinse Dishwasher cycle wash and tap water rinse no detergent Acid wash with at least 20 percent hydrochloric acid Dishwasher cycle wash and tap water rinse no detergent or WO N e Replace in covered Isco tubs Vinyl Suction Line Rinse twice with spectro grade acetone Rinse thoroughly with hot tap water using a brush if possible Rinse thoroughly three times with tap water E WC N A Acid wash with at least 20 percent hydrochloric acid 69 A CAUTION The pumps safety lock pre vents the sampler from run ning the pump when the pump band is open DO NOT tamper with the safety mechanism The pump is extremely power ful The pump rollers can in jure you severely if the sampler activates the pump while you are working on it or inside it Disconnect power from the sampler before replacing the pump tube M Note To extend the pump tube life Always use Isco pump tubes Install the tube properly align ing the blue collars correctly in the liquid detector s grooves Follow the natural curve of the tube when wrapping the tube around the pump rollers Minimize the line rinses and sampling retries in the sam pling programs Use the shortest possible suction line Conditions that shorten tube life Improper installation Abrasive materials suspended in sample liquid
118. TION Prepared By Corporate Environment Health amp Safety Group Phone Number See Section I The information in this Material Safety Data Sheet should be provided to all who will use handle store transport or otherwise be exposed to this product This information has been prepared for the guidance of plant engineering operations and management and for persons working 146 6700FR Refrigerated Sampler ENGELHARD Page 9 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 with or handling this product The information presented in the MSDS is premised upon proper handling and anticipated uses and is for the material without chemical additions alterations We believe this information to be reliable and up to date as of the date of publication but make no warranty that it is Additionally if this Material Safety Data Sheet is more than three years old please contact the supplier at the phone number listed in Section I to make certain that this sheet is current Copyright Engelhard Corporation License granted to make unlimited copies for internal use only End of MSDS 147 6700FR Refrigerated Sampler l United Catalysts Inc 101 Christine Drive UNITED DESICCANTS Desiccants Division Rio Grande industrial Park Belen NM 87002 MATERIAL SAFETY DATA SHEET Telephone 505 864 6691 ESI PAK Fax 505 864 9296 Packaged Desiccant SECTION I PRODUCT IDENTIFICATION Trade Name and Synonyms DESI PAK Chemical Fam
119. TPUT _ TO __ __ mA ANALOG OUTPUT _ 0 TO 20 mA 4 TO 20 mA DONE ANALOG OUTPUT _ 0 mA AT _ __ fps 20 mA AT _ __ fps 0 000 9999 Repeat for each channel SERIAL OUTPUT EVERY 15 SEC 1 MIN 5 MIN 15 MIN When DECIMAL POINT key is pressed SELECT CODE Analog Output and Dialout Quick View Screens Notes A Factory installed option Requires B1 hardware or newer B Requires factory installed Dialout Modem and B2 hardware or newer ANALOG OUPUT _ LEVEL VELOCITY FLOW NONE SET ANALOG OUTPUT _ TO mA ANALOG OUTPUT _ 0 TO 20 mA 4 TO 20 mA DONE ANALOG OUTPUT _ 0 mA AT _ __ fps 20 mA AT _ __ fps 0 000 9999 Repeat for each channel SERIAL OUTPUT EVERY 15 SEC 1 MIN Yes PORT SETTINGS 9600N81 4800N81 2400N81 1200N81 5 MIN 15 MIN When DECIMAL POINT key is pressed 1 Ox DIALOUT NUMBERS SELECT CODE MINUTE DELAY BETWEEN CALLS 0 99 131 6700FR Refrigerated Sampler Figure 48 Command Driven Screens RUN ISCO 6700 PROGRAM VIEW REPORT OTHER FUNCTIONS L6 7 0JLoJL 3 Displayed for 8 seconds 6700 SAMPLER COMMAND DRIVEN FATAL ERROR When Applicable NO DISTRIBUTOR ARM PLEASE WAIT TESTING DISTRIBUTOR SYSTEM OPERATOR ERROR DISTRIBUTOR JAMMED WAITING TO SAMPLE Stop Key Setup Menu ft SUCTION LINE __ BOTTLES PUMP TUBE ALARM DONE Displayed for 4 seconds 132 NUMBER OF BOTTLES 1 2 4 8
120. Up on page 124 See Figure 40 Extended Programming Quick View Pacing and Distribution on page 125 See Figure 41 Extended Programming Quick View Programmed Sampler Enable on page 126 See Figure 28 Standard and Extended Programming Quick View Start Times on page 114 C24 US a 123 EXTENDED 1 EXTENDED 2 EXTENDED 3 EXTENDED 4 NAME ABCDEFGHIJKLMNOPQRST UVWXYZ 4 0123456789 BACK UP DONE SAVE CHANGES YES NO SAVE CHANGES YES NO 6700FR Refrigerated Sampler Figure 39 Extended Programming Quick View Equipment Set Up Continued from Figure 33 Quick View Module Setup on page 118 NUMBER OF BOTTLES 1 2 4 8 12 24 SUCTION LINE LENGTH lio ft ml BOTTLES 3 99 ft SUCTION LINE BOTTLE VOLUME IS m 300 30000 AUTO SUCTION HEAD _ RINSES _RETRIES y When Liquid Detector is on _ RINSE CYCLES AUTO SUCTION HEAD SUCTION HEAD OF 0 3 ENTER HEAD fori min max RETRY UP TO _ TIMES WHEN SAMPLING 0 3 BOTTLES AVAILABLE ONE PART PROGRAM ONE PART PROGRAM ASSIGN BOTTLES TWO PART PROGRAM 1 THRU __ TO PART A 1 max See Figure 40 Extended Programming Quick View Pacing and Distribution on page 125 124 6700FR Refrigerated Sampler Figure 40 Extended Programming Quick View Pacing and Distribution Continued from Figure 39 Extended Programming Quick View Equipment Set Up on page 124 PACING
121. WARD PUMPING EVENT MARK SENT FOR EVENT MARK DURATION EVERY SAMPLE 3 SECONDS DURING COMPLETE SAMPLES WHILE PUMPING ENTIRE PUMP CYCLE FORWARD PUMPING PRE SAMPLE PURGE ____ COUNTS 10 9999 POST SAMPLE PURGE DEPENDENT ON HEAD FIXED COUNT POST SAMPLE PURGE COUNTS See Note B SET 110xX NONE lt 1 0 ENABLE lt FR TEMP PGM RUNNING PGM ENABLED A ENABLED B ENABLED PROGRAM DONE A DONE B DONE 0 120 RUN ERROR Notes FLOW THRU See Figure 37 Extended Programming in Programmed Sampler Enable on page 122 A Software option See Chapter 6 NEW HARDWARE SETUP STORED DATA WILL BE LOST OK YES NO RUN FLOW THRU PUMP SECONDS BEFORE TAKING READINGS gt gt gt gt gt 2 gt gt gt gt B lt denotes input signal gt denotes output signal See Figure 46 Analog Output and Dialout Screens on page 131 127 6700FR Refrigerated Sampler Figure 43 Extended Programming Hardware Quick View Screens RUN ISCO 6700 PROGRAM VIEW REPORT OTHER FUNGTIONS MAINTENANCE 4 LIQUID DETECTION MANUAL FUNCTIONS 0 01 inch TIP PROGRAMMING STYLE RAIN GAGE HARDWARE NO YSI SONDE YSI 600 YSI 600 Y pH Y D O Y COND OTHER YSI SONDE Y TEMP MASTER SLAVE YES NO MASTER SLAVE ON BTL FULL DETECT OFF TIMED BACKLIGHT PGM LOCK ENABLED y BACKLIGHT ALWAYS OFF TIMED BACKLIGHT CONTINUOUS BACKLIGHT CHANGE PASSWORD TO See Note A EV
122. YOU WANT D O DATA TURBIDITY DATA YES NO YES NO If applicable If applicable DO YOU WANT DO YOU WANT pH DATA CHLORIDE DATA YES NO YES NO If applicable DO YOU WANT O R P DATA YES NO 130 If applicable NEW HARDWARE SETUP STORED DATA WILL BE LOST OK YES NO If applicable PARTITION MEMORY WILL LAST __ DAYS 6700FR Refrigerated Sampler Figure 46 Analog Output and Dialout Screens See Figure 42 Extended Programming Hardware Screens on page 127 If applicable See Note A ANALOG OUTPUT HARDWARE HAS NOT SETUP BEEN INSTALLED MANUAL CONTROL SERIAL OUTPUT YES NO PORT SETTINGS 9600N81 4800N81 2400N81 1200N81 If applicable See Note B DIALOUT WHEN I Ox BECOMES TRUE DIALOUT NUMBERS YES NO 1 0x 3 __ MINUTE DELAY BETWEEN CALLS 0 99 Figure 47 See Figure 43 Extended Programming Hardware Quick View Screens on page 128 If applicable See Note ANALOG OUTPUT HARDWARE HAS NOT BEEN INSTALLED SETUP MANUAL CONTROL _ ANALOG OUTPUTS SERIAL OUTPUT EVERY __ MINUTES y PERIODIC SERIAL OUTPUT YES NO If applicable See Note B DIALOUT EACH TIME DIALOUT WHEN 1 0Ox 40 BECOMES TRUE BECOMES TRUE YES NO Notes A Factory installed option Requires B1 hardware or newer B Requires factory installed Dialout Modem and B2 hardware or newer ANALOG OUPUT _ LEVEL VELOCITY FLOW NONE SET ANALOG OU
123. ___ SAM 1 999 DO YOU WANT SAMPLE VOLUMES DEPENDENT ON FLOW YES NO Uniform Time Paced Only SAMPLE VOLUME All other pacing ml 10 max FIRST SWITCH TIME AT il PLES RUN CONTINUOUSLY YES NO SAMPLE VOLUME 19 ME FOR EVERY PULSES FLOW PULSES FLOW MODULE VOLUME See Figure 37 Extended Programming Programmed Sampler Enable on page 122 Notes A Event paced programs always use sequential distribution 121 6700FR Refrigerated Sampler Figure 37 Extended Programming Programmed Sampler Enable Continued from Figure 36 Extended Programming Continued from Figure 42 Extended Programming Pacing and Distribution on page 121 Hardware Screens on page 127 A Done and I O are not options for I O Conditions See Note A See Note A ENABLE All except ENABLE RAIN AND ENABLE RAIN AND I O RAIN LEVEL NONE I O LEVEL FLOW NONE FLOW Y pH Y TEMP AND OR DONE pH Y TEMP Y COND Y D O Y COND Y D O NONE NONE All except I O Rain and A Done RAIN SET POINT ENABLED WHEN LEVEL CONDITION __ __ INCHES PER I O ENABLE IS HIGH SET POINT 15 MIN 30 MIN I O ENABLE IS LOW RANGE 1 HOUR 2 HOURS ENABLED WHEN LEVEL RANGE LEVEL SET POINT ABOVE SET POINT LOWER _ __ft MES i BELOW SET POINT UPPER 11 0 001 30 000 0 001 30 000 ENABLED WHEN ENABLED WHEN RESET RAIN HISTORY INSIDE RANGE ABOVE SET POINT YES NO OUTSIDE RANGE BELOW SET POINT If applicable
124. a esclusivamente con apparecchiature compatibili Isco Non utilizzare il prodotto con apparecchiature di terzi n per scopi diversi da quello previsto L uso dell apparecchiatura per scopi diversi da quello previsto nel presente manuale potrebbe provocare lesioni a persone e danni a cose Alimentazione Il refrigeratore disponibile in versione a 120 VI e 230 VA La tensione d alimentazione richiesta riportata sulla targhetta d identificazione e del numero di matricola che si trova all interno dello sportello del vano portacampioni I refrigeratori in versione 120 V sono dotati di spina a norme nordamericane NEMA 5 15P e sono previsti esclusivamente per funzionare a 120 VV 60 Hz La corrente d alimentazione dev essere a 30 amp re I refrigeratori in versione 230 VU sono dotati di spina a norme europee CEE 7 7 e sono previsti esclusivamente per funzionare a 230 VU 50 60 Hz La corrente d alimentazione dev essere di 16 amp re I refrigeratori in entrambe le versioni forniscono tensione a 12 5 V 5 ampere al dispositivo di comando del campionatore L uscita utilizza il connettore di tipo militare a due contatti applicato al cavo che si trova sulla parte superiore del refrigeratore Questa uscita prevista esclusivamente per dispositivo di comando dei campionatori serie 6700 Il refrigeratore dev essere installato accanto ad un idonea presa di corrente E vietato usare prolunghe La presa d alimenta
125. a line tap in the refrigeration system because of possible corrosion or leakage problems 6700FR Refrigerated Sampler RECAPITULATIF DES MESURES DE SECURITE L chantillon r frig r mod le 6700FR est un appa reil but d fini qui doit tre utilis uniquement avec du mat riel compatible Isco Ne pas utiliser ce produit avec le mat riel d autres fabricants ou d autres fins Son usage d autres fins que celles indiqu es dans ce manuel pourrait provoquer des accidents corporels ou des d g ts mat riels Conditions lectriques requises Le r frig rateur est disponible en 120 VW et 230 Vu Le voltage n cessaire son fonctionnement est indiqu sur l tiquette d identification et de num ro de s rie qui se trouve l int rieur de la porte du compartiment de l chantillon Les r frig rateurs configur s pour du 120 VW sont quip s d une prise NEMA 5 15p am ricaine et doivent fonctionner exclusivement avec du courant de 120 VI 60 Hz L alimentation lectrique doit tre r gl e sur 30 amp res Les r frig rateurs configur s pour du 230 VA sont quip s d une prise CEE 7 7 europ enne et doivent tre utilis s exclusivement avec du courant de 230 Vu 50 60 Hz L alimentation lectrique doit tre r gl e sur 16 amp res Les r frig rateurs des deux configurations fournis sent du courant de 12 5 V 5 amp res au con tr leur de l chantillon Ce courant est aliment par le c
126. able Enable After enabling the sampler the enabling instrument or instruments continues to monitor the conditions and disables the sampler when the conditions are no longer satis M Note fied If re enabled the sampler resumes the sampling program Once enabled stay enabled is Sample at Enable or Disable You have the option of directing called sampler latching in flow the sampler to take a sample as soon as it receives the enable and meters flow loggers FLOW or disable signal If you program the sampler to stay enabled and LINK and PALs Latching a choose to take a sample at enable the sample interval will be reset sampler produces the same results as selecting YES the difference is that the external instrument controls the latching at the enable time Samples at disable do not affect the sample in tervals Standard programs do not take a sample at the enable time Delay To Start of Sampling If you have selected ONCE EN ABLED STAY ENABLED and have chosen to not sample at the en SAMPLE AT ENABLE able you have the opportunity to suspend the start of sampling YES NO This option is useful for storm programs that require a flow paced sample taken after the initial grab sample Resetting the Sample Interval at Enable You may want the START SAMPLING 3 AFTERA pacing countdown to start over each time the sampler becomes en Ta ti nd abled To accomplish this simply select YES at screen 20 The next sample event
127. alid options NO DATA TO DISPLAY SELECT DATA TO VIEW VIEW pH MODULE SAMPLING REPORT DAILY SUMMARY VIEW MODULE FR TEMP CURRENT READINGS pH DATA RAIN YSI TEMPERATURE DATA Valid Options Shown When applicable DATA TO PRINT SAMPLING REPORT MODULE FR TEMP RAIN YSI NO DATA TO PRINT VIEW DATA PRINT DATA SYSTEM IDs CONFIGURE REPORT Note B SAMPLER SOFTWARE OPTIONS 6700 1D 1234567890 HARDWARE BO NONE SOFTWARE 1 00 When applicable When applicable ULTRASONIC MODULE YSI 600 0710 1D 1234567890 HARDWARE Al SOFTWARE 1 00 SOFTWARE SAMPLINK REPORT REPORTS FOR SAMPLER FLOWLINK REPORT PROGRAM SETTINGS CUSTOM REPORT SAMPLING RESULTS ALL REPORTS BOTH NONE When applicable REPORTS FOR MODULE DAILY SUMMARY COMBINED RESULTS BOTH NONE When applicable REPORTS FOR FR TEMP DAILY SUMMARY COMBINED RESULTS BOTH NONE When applicable REPORTS FOR RAIN Note A DAILY SUMMARY Menu access can be controlled with the optional Program Lock See Chapter 6 COMBINED RESULTS BOTH NONE Note B When applicable DO YOU WANT COMBINED RESULTS FOR YSI 600 DATA YES NO 1108 Program Lock 1109 Phone Commands 1115 YSI 6820 and 600XL 1199 Switch Bottle Set at Enable INCLUDE DETAIL DATA FOR FLOWLINK AND TEXTLINK PROGRAMS YES NO 115 6700FR Refrigerated Sampler Figure 30 Maintenance Screens RUN PROGRAM VIEW REPORT OTHER FUNCTIONS MAINTENANCE ENTER TIME AND
128. ampler always takes a sample at the start time for event paced programs Nonuni form clock time programming schedules each sample event individ ually The sampler skips samples scheduled while it is disabled Although you can combine flow pacing and all time pacing types with any distribution event paced programs by definition uses only sequential distribution The sampler finishes an event paced pro gram after depositing a sample in each bottle Distribution Distribution describes how the sampler is to deposit samples A sample is the volume of liquid deposited in a bottle A sample event includes the full sampling cycle and may deposit a sample into more than one bottle You can program the sampler for five distri bution methods e Sequential e Composite e Bottles per sample e Multiple Bottle Compositing e Samples per bottle Sequential In sequential distribution the sampler deposits one sample in each bottle A sequential sample represents a snapshot of the flow stream at a point in time Bottles Per Sample In bottles per sample distribution the sampler deposits a sample in each of a set of bottles A bottle set includes at least two bottles but may include all bottles Use bottles per sample when the vol ume to be collected is larger than the amount one bottle can hold or when you need identical samples Samples Per Bottle In samples per bottle distribution the sampler deposits samples from several sample
129. appears when the program option is activated See Chapter 6 B lt denotes input signal gt denotes output signal 6700FR Refrigerated Sampler Figure 44 Extended Programming YSI 600 Screens From Figures 42 and 43 Extended Programming Hardware Screens DO YOU HAVE A YSI 600 CONNECTED YES NO TEST YSI 600 COMMUNICATIONS YES NO TEST YSI 600 COMMUNICATIONS YES NO DO YOU WANT pH DATA YES NO See Note SELECT DATA TYPE SPECIFIC CONDUCTANCE SALINITY T D S CONDUCTIVITY DONE DO YOU WANT D O DATA YES NO PLEASE WAIT DO YOU WANT CONDUCTIVITY DATA YES NO WARNING DO NOT REMOVE YSI 600 POWER ss TESTING SPECIFIC CONDUCTANCE TEMP COEFFICIENT Me LC 1 50 2 50 T D S SCALE FACTOR 0 55 0 90 PARTITION MEMORY WILL LAST __ DAYS ENTER THE D O CONTENT OF YOUR CALIBRATION STANDARD COMMUNICATIONS RATE SET AT 2400 BAUD Conductivity Units Salinity parts per thousand T D S gramslliter Specific Conductance mS cm Conductivity mS cm PLACE PROBE IN __ _ mg l STANDARD PRESSE WHEN STABLE DO YOU WANT TEMPERATURE DATA YES NO If applicable NEW HARDWARE SETUP STORED DATA WILL BE LOST OK YES NO SELECT PARAMETER TO CALIBRATE Y pH Y D O Y COND DONE pH CALIBRATION pH04 and pH07 pH07 and pH10 pH04 pH07 and pH10 RINSE PROBE THEN PLACE IN pH__BUFFER PRESS WHEN STABLE PLEASE WAIT If applicable CALIBRATION READING
130. are in Appendix B Menu Charts 23 6700FR Refrigerated Sampler Extended Programming Features Pacing Nonuniform Times See Pacing on page 82 Event Pacing See Pacing on page 82 e Sample at Start Time for Flow Paced Programs See Pacing on page 82 and Start Timeson page 89 Sampler Enable Programmable Enables See Sampler Enable on page 87 Sample at Enable See Sample at Enable or Disable on page 88 Interval Reset for Sampler Enable See Resetting the Sample Interval at Enable on page 88 e Repeatable Enable See Repeatable Enable on page 88 Distribution e Multiple bottle Compositing See Distribution on page 84 Bottle set Switching See Distribution on page 84 Suction Line e Rinses and Retries See Rinses and Retries on page 81 Manual Suction Head See Suction Headon page 81 Other e Two part Sampling Programs See One Part and Two Part Programs on page 24 Changing to and from Extended and Standard Screens The sampler is shipped so that the standard programming screens appear when you first turn the sampler on The start up screen tells you which programming screens the sampler is currently us ing After the extended programming screens are added the sam pler continues to display them even if the sampler is turned off until they are replaced by the standard programming screens e At the main menu type 6700 2 to show
131. art time screens The start Start Time Program time screens appear in Figures 26 and 28 Standard and Extended Programming Start Times Figure 21 Start Time Diagram for Sampler Enable Settings Select RUN from the Start Menu Start Delay to Start Time During the delay the sampler A sample event at the Start Time always occurs ignores disable signals from a for all time paced programs except random For flow logger flow meter a 700 flow paced programs it occurs when the program series module rain gauge or requires a sample at the Start Time I O pin Sampler Enabled at Start Time Sampler Enabled ron e I I Sampler Disabled Sampler waiting at Start Time for enable r A sample event at the Enable Time always occurs for event paced programs For other programs it occurs at the Enable Time only when the program requires a sample at enable 89 It is important to understand the difference between the time at which you run a program and the program s start time Running a program simply means selecting RUN from the sampler s start up 6700FR Refrigerated Sampler Each program contains start time settings that tell the sampler when to begin the program When programming the sampler you Delayed Start Screen can select one of three start time options NO DELAY TO START DELAYED START or CLOCK TIME NO DELAY TO START DELAYED START e Select NO DELAY TO START when you want the samp
132. ater than 100 see page 96 are used Bottle Full Detect is always disabled in the Normal Programming mode 94 6700FR Refrigerated Sampler Display Backlighting Adjusting the Display The display has a backlight that is adjustable so that the backlight Backlighting 1s always off timed or always on Enter the Hardware setup In the timed backlight mode the sampler turns the backlight off af Step through the screens until ter detecting no key strokes within 60 seconds Any keystroke ex you see cept ON OFF turns the backlighting on again In this mode the BACKLIGHT ALWAYS OFF backlight must be on before the sampler accepts a menu choice or TIMED BACKLIGHT number entry If you press a key and a screen does not respond it 1s because the keystroke turned the backlight on CONTINUOUS BACKLIGHT e Press STOP twice to return to Isco recommends you use either the setting BACKLIGHT AL the main menu WAYS OFF or TIMED BACKLIGHT when using a battery Event Marks The sampler generates an event mark at each sample event send ing it through the flow meter connector to a connected instrument a 3200 Series Flow Meter 4200 Series Flow Meter or 4100 Series Flow Logger Event Mark Screens The event mark may also control an external device a connected Charts for event marks screens ap solenoid relay for example When using the event mark for a data Be al logger or to control external devices you may need to adjust the Figure 42
133. ccording to the reports needed When you are familiar with the available Sampling Reports you may want to specify an output containing only the specific data you require The CUSTOM REPORT option will allow selection of each printed report and of detailed data Data collection time printout length and storage space may be optimized using this option Printing Reports Examples of printed reports appear in Figures 8 through 11 You can start the reports by making selections from the sampler s screens or by pressing the printer s print button Printing Data To print a report from the screens e SAN 1 Connect the field printer s cable to the sampler s interrogator VIEW REPORT connector OTHER FUCTIONS e Select VIEW REPORT Ra an 1 Connect the field printer s cable to the sampler s interrogator SYSTEM IDs connector CONFIGURE REPORTS You can collect reports with the field printer while a pro e Select PRINT DATA gram is running when the sampler is at any programming PRINT screen or even when it is turned off as long as it is connect SAMPLING REPORT ed to a power source 2 Follow the steps in the margin for Printing Data To start a report from the printer MODULE DATA RAINFALL DATA 2 Press the printer s print button once for the Program Settings e Select a report or data type report and the Sampling Results report Press the printer s print button again for a printout of the rain module and Y
134. ce department Small non fragile items can be sent by insured parcel post PLEASE BE SURE TO ENCLOSE A NOTE EXPLAINING THE DEFECT Return instruments to Isco Inc Attention Repair Service 4700 Superior Street Lincoln NE 68504 USA Mailing address Isco Inc PO Box 82531 Lincoln NE 68501 USA Phone Repair service 300 775 2965 lab instruments 300 228 4373 samplers 8 flowmeters Sales General Information 800 228 4373 USA amp Canada Fax 402 465 3001 Email service isco com November 2000 2217 Isco Inc
135. ce water past the control panel seal FINDING ARM FLEXURE Sample Bottles The sample bottles have a wide mouth to facilitate cleaning Wash them with a brush and soapy water or use a dishwasher You can autoclave the glass bottles NOW AT BOTTLE __ RE INITIALIZE Suction Line Pump Tube and Discharge Tube YES NO Clean the suction line pump tube and discharge tubes by placing the end of the suction line in a cleaning solution and pumping it through the delivery system Rinse with clean water If these items are severely contaminated replace them For critical sampling ap plications see Cleaning Protocols for Priority Pollutants on page 69 68 If the filter is not cleaned peri odically damage due to over heated components may result Removing the front or back panel exposes electrical and mechanical hazards Discon nect power before performing any service activities M Note For critical sampling applica tions consider replacing the suction line pump tube and dis charge tube Replacement elimi nates the possibility of any cross contamination from previous sampling sites 6700FR Refrigerated Sampler Strainers Clean the strainers with a brush and soapy water Cleaning the Air Filter The air filter prevents dust lint and other debris from circulating around the cooling system Clean the filter about every 3 months more frequently under severe operating conditions To remove the filter
136. cks the pacing settings and begins the pacing interval countdown e Select CLOCK TIME Sampler Enable dl en Al The sampler disregards both disable and enable signals during the delay to start time However when the sampler detects a disable signal at the start time it suspends the program until it is enabled Once enabled the sampler collects a sample only when pro Enter the time of day SELECT DAYS i i N iS SU MO TU WE TH FR SA grammed to take a sap cal the enable time The diagram in Fig ure 21 shows the sampler s response when enabled or disabled at DONE the start time Press an arrow key until the In some complex applications you may want to enable the sampler ni rSOr IS a a correct day with both a flow meter and a module If so remember that the enable ress i er conditions detected by the flow meter and the module must both be Repeat until each day you present at the same time before the sampler becomes enabled want is blinking Press an arrow until DONE Two Part Programs blinks Press Enter l Available in extended programming two part programming lets you divide a sampling program into two parts The program has a FIRST VALID DAY single start time shared by each part sampler running a two IS 20 JAN part program responds to start time settings in the same way that it responds to the start time settings for a single part program Enter the first valid day The example abo
137. corded errors by ee NENA displaying the message ERRORS HAVE OCCURRED DURING O PROGRAM See Table 9 for a description of the errors and events If five consecutive power failures occur the sampler stops the run ning program and reports a Low Battery error This error assumes that the controller is powered by a battery and therefore is not likely to occur when using the 12 VDC power supplied by the refrigerator Program Done Messages Fatal Error PROGRAM Screen k will only show up if you are using a multiple bottle config n ONE uration and the distributor system fails Failing the test can indi cate any of the following conditions Standard program e The distributor arm is not attached to the sampler completed e The stop arm on the distributor shaft extension is missing or PROGRAM EXTENDED 1 broken IS DONE e The stop inside the refrigerator is missing or broken e The distributor drive mechanism inside the controller is mal Extended program functioning completed Warning Messages Occasionally the sampler displays a warning message to alert you NM Note to a potential problem There are two warnings The first warning REPLACE PUMP TUBE reminds you to check the condition of At the completion of a multi bottle h be F inf Res he P sampling program the controller the pump tube For more in ormation see Replacing the Pump oarks the distributor towards Tube on page 70 The second
138. creens ap pear in Figure 24 6700 Menu Tree for Standard Programming on page 110 Extended characters the Comma Pound and Star also may be included in the 25 digits To enter an extended character RUN press the Decimal Point key on the 6700 keypad The 6700 displays PROGRAM a screen used to select and enter the extended characters Each VIEW REPORT E OTHER FUNCTIONS comma entered will cause the modem to pause for two seconds be Select VIEW REPORTS fore proceeding with the remaining digits VIEW DATA Dialout telephone numbers are included in the Program Settings PRINT DATA Report SYSTEM IDs CONFIGURE REPORTS Select SYSTEM IDs The sampler reports the sampler model number ID identification SAMPLER number and software version number as system identification 6700 ARE notes The sampler also reports the same information for an at SOFTWARE tached module The model and ID numbers remain unchanged through the life of the sampler The ID numbers appear on the sam pler s reports and in files created by FLOWLINK and SAMPLINK System IDs e Displayed briefly MODULE TYPE when they interrogate the sampler The software packages use the MODEL ID HARDWARE ID number to insure that data from different samplers is not com SOFTWARE __ bined in the same file Displayed briefly The software version number changes when your sampler s soft SOFTWARE OPTIONS ware is updated Screens 56
139. cts the module s presence The manuals for each module con tain menu trees for its programming screens 22 6700FR Refrigerated Sampler Figure 1 Menu Tree for Standard Programming RUN PROGRAM VIEW REPORT OTHER FUNCTIONS VIEW DATA PRINT DATA SYSTEM IDs CONFIGURE REPORTS MAINTENANCE MANUAL FUNCTIONS PROGRAMMING STYLE See Running Programs on page 49 o Ses the screen charts in Appendix A D 50 Sampling Reports on page 54 o SET CLOCK SET PUMP TUBE ALARM INTERNAL BATTERY DIAGNOSTICS See Manual Functions Screens on page L 117 PROGRAMMING STYLE NORMAL QUICK VIEW CHANGE Optional Password Security The Program Lock adds password security to the 6700 sampling pro grams See Chapter 6 Standard and Extended Programming The 6700 Sampler has two sets of programming screens The first set called standard programming screens lets you set up typical sampling programs easily and efficiently The second set extended programming screens lets you create sophisticated programs for complex sampling applications All of the sampling features available with standard programming screens are available with extended programming screens Howev er the extended screens provide several additional features which are listed in the adjacent margin and discussed in other sections of this manual The menu charts for both sets of programming screens
140. d Fitting Latches Handles Compressor Mounting Frame Refrigeration Tubing Protection Condenser Protection Evaporator Protection Refrigerant Insulation Amphenol Connectors MATERIAL Fiberglass reinforced plastic with ultraviolet resistant gel coat ABS Acrylonitrile Butadiene Styrene plastic Noryl Delrin Polyester Stainless steel Protected with polyester tubing or phenolic resin Powder coated with polyester Powder coated with food grade epoxy R134a 1 1 1 2 tetrafluoroethane CH FCF Polyurethane Cadmium Plated Aluminum 6700FR Refrigerated Sampler Table 3 Technical Specifications for the 6700FR Sampler General Notes 1 All weights may vary 1 Ib 12 kg 2 All dimensions may vary 1 4 inch 0 64 cm 3 Sample delivery specifications valid for the following conditions and ranges unless otherwise stated 75 F 24 C ambient sample liquid tap water at 50 to 80 F 10 to 27 C sample volumes from 50 ml to 1000 ml suction line lengths of 25 ft 7 6 m or less suction heads from 1 to 20 ft 0 3 to 6 1 m atmospheric pressure between 29 92 and 31 89 inHg 760 and 810 mmHg and a power source of an Isco High Capacity Power Pack at 12 5 volts DC no load output 6700 CONTROLLER PUMP AND TUBING MECHANICAL SPECIFICATIONS Weight of Controller Controller Dimensions Temperature Ranges Enclosure Typical Delivered Volume Accuracy Typical Repeatability Typical Pump Fl
141. d Sampler Chapter 6 Software Options The 6700 Sampler s software v3 0 and greater includes special ized software options that can be purchased individually from Isco Once activated the purchased option is always available even if the software is upgraded at a later time These options must be in stalled at the factory The software options include e Program Lock Secures the access to the sampler s program settings e Switch Bottle Set at Enable a sample distribution option e Telephone Commands Remotely control the sampler from a touch tone telephone e YSI 6820 and YSI 600XL Supports YSI sondes To view which software options have been activated select VIEW REPORT gt SYSTEM IDs see page 99 A software options screen will list a code for each active option Software Option 1108 Program Lock 1109 Phone Commands 1115 YSI 6820 and 600XL 1199 Switch Bottle Set at Enable Program Lock The Program Lock adds password security to the 6700 sampling pro grams With this option activated a user selected password up to five digits must be entered before any program changes or run time modifications can be made Run time modifications include access ing the Manual Pause menu options and shutting off the sampler You will still be able to run the current program view reports and interrogate the sampler without the knowledge of the password If three consecutive attempts to enter the password fail
142. d the PEL Use adequate ventilation and dust collection Practice good housekeeping Do not permit dust to collect on walls floors sills ledges machinery or equipment Maintain clean and fit test respirators in accordance with OSHA regulations Maintain and test ventilation and dust collection equipment Wash or vacuum clothing which has become dusty Product becomes slippery when wet Avoid breathing dust Avoid contact with eyes Use only with adequate ventilation SECTION VIII EXPOSURE CONTROLS PERSONAL PROTECTION EXPOSURE LIMITS INGREDIENT PEL OSHA TLV ACGIH SILICA CRYSTALLINE QUARTZ CAS NO 14808 60 7 0 1 mg m 0 1 mg m Respirable dust Respirable dust ALUMINUM SILICATE CAS NO 12141 46 7 15 mg m as Al 10 mg m as Al dust dust 5 mg m as Al respirable fraction 142 6700FR Refrigerated Sampler ENGELHARD Page 5 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 Unless otherwise noted all values are reported as 8 hour Time Weighted Averages TWAs and total dust particulates only All ACGIH TLVs refer to the 1992 93 Standards All OSHA PELs refer to 29 CFR Part 1910 Air Contaminants Final Rule January 19 1989 NOTE As a result of the July 7 1992 decision by the U S Circuit Court of Appeals AFL CIO v OSHA to vacate the 1989 PELs OSHA will no longer enforce these new limits and will return to the pre 1989 PELs Engelhard however will continue to list the more protective
143. dard interrogator cable To receive serial data by command 1 Select NO at screen 53 2 Connect your computer to the 6700 controller s interrogator connector using a standard interrogator cable sense line grounded P N 60 2544 040 25 pin or 60 2544 044 9 pin 3 Configure your communications software for a baud rate no higher than 19 200 kb 9600 recommended no parity 8 data bits and 1 stop bit 4 From the computer s keyboard type repeatedly until the 6700 controller determines the baud rate Once the baud rate 97 M Note Connecting either the serial out put or the standard interrogator cable to the 6700 disables the optional dial out modem if in stalled The interrogator cable must be disconnected before you can use the modem 6700FR Refrigerated Sampler 1s known the 6700 returns an identification banner This ban ner indicates that the connection is working properly If you have difficulty with the connection try a slower baud rate 5 Type DATA lt CR gt each time the data string is desired The serial data is in comma separated value format Only the val ues that the sampler is set up to measure will be output in the data string The string is terminated with a lt CR gt lt LF gt To read the data in the string refer to Table 11 Table 11 Serial Data Codes IDENTIFIER PARAMETER UNITS B BOTTLE NUMBER AND TIME days since 1 Jan 1900 CR CURRENT DAY S RAIN tips rolls over every 256
144. ds 68 3700 047 Set of 12 2 5 liter Polyethylene Bottles with Lined Lids 68 6700 059 Set of 100 2 5 liter Polyethylene Bottles with Lined Lids 68 6700 060 Set of 8 1 8 liter Glass Bottles with Teflon Lined Lids 68 2740 027 Set of 100 1 8 liter Glass Bottles with Teflon Lined Lids 68 3720 030 Set of 8 2 0 liter Polyethylene Bottle with Unlined Lids 68 2740 026 Set of 100 2 0 liter Polyethylene Bottle with Unlined Lids 68 3720 028 7 9 1iter Polyethylene Bottle e AI A ada 299 0013 07 9 4 liter 21 gallon Glass Bottle with Two Teflon Lined Lids 68 2930 006 9 4 liter 2 2 gallon Polyethylene Bottle with Two Unlined Lid 68 2740 009 15 0 liter 4 gallon Polyethylene Bottle with Two Unlined Lids 68 2930 004 18 5 liter 5 gallon Glass Bottle with Two Teflon lined Lids 68 6700 057 20 5 liter 5 2 gallon Polyethylene Bottle with Two Unlined Lids 68 2930 005 Pump Tubes Suction Line Strainers Pimp ube Oty Sn SN E Led se Gad one an M nn he ek 68 6700 062 Pump Dube Qty VO 4423 lhi A ato ac Dao da PRA 68 6700 044 ios A A unis tne Ge ab bete eee Are de eu ce tie du 68 6
145. e Nel manuale queste informazioni sono presentate in uno dei due modi seguenti N AVVERTENZA Avvertenza indica un pericolo potenziale che se non viene evitato pu comportare lesioni secondarie o modeste Pu inoltre servire a segnalare all operatore abitudini pericolose o condizioni che possono provocare danni a cose Attenzione indica una condizione potenzialmente pericolosa che se non evitata pu provocare gravi lesioni morte compresa 6700FR Refrigerated Sampler Page 12 ATTENZIONE Eventuali cambiamenti o modifiche senza l espressa autorizzazione del responsabile della conformit possono precludere all utilizzatore il diritto di adoperare l apparecchiatura Pages 14 and 37 M Nota Leggere le note relative alla Sicurezza sul fron tespizio del presente manuale che riportano le specifiche elettriche e le istruzioni per l uso in con dizioni di sicurezza dell apparecchiatura Page 69 AVVERTENZA La mancata pulizia periodica del filtro pu provocare danni dovuti al surriscaldamento dei componenti Page 69 ATTENZIONE Lo smontaggio del pannello anteriore o di quello posteriore espone a pericoli di natura elettrica o meccanica Prima di iniziare qualsiasi operazione di manutenzione scollegare l alimentazione gt Page 77 79 and 80 Lo smontaggio del pannello anteriore o di quello posteriore frontale espongono a pericoli di natura elettrica e meccanica Le operazioni di ricerca gua
146. e Non flam mable Not generally present in dangerous amounts unless an oxygen deficiency exists Chemical asphyxiant Colorless odorless tasteless Flammable Poisonous Heavy ethereal odor Irritant Yellow green color Choking odor detectable in very low concentrations Non flammable Colorless pungent suf focating odor Volatile solvent Colorless Odor notice able at 0 03 Flam mable Simple asphyxiant Colorless odorless tasteless Flammable Faint odor of bitter almonds Colorless gas 6700FR Refrigerated Sampler Specific Gravity or Vapor Density Air 1 2 77 5 3 Ae W 5 o Percentages shown represent volume of gas in air For concentration over 0 3 Physiological Effect Causes throat and eye irritation at 0 05 coughing at 0 17 Short exposure at 0 5 to 1 fatal Slight symptoms after several hours exposure at 0 16 to 0 32 2 rapidly fatal Very poisonous irritating vomiting convulsions psychic disturbance Cannot be endured at 10 more than a few minutes even if sub ject is at rest and oxy gen content is normal Acts on respiratory nerves Combines with hemo globin of blood Unconsciousness in 30 min at 0 2 to 0 25 Fatal in 4 hours at 0 1 Headache in few hours at 0 02 Intestinal upset loss of consciousness possi ble renal damage res piratory failure Irritates respiratory tract Kills mos
147. e 115 MAINTENANCE See Maintenance Screens on page 116 MANUAL FUNCTIONS See Figure 31 Manual Functions Screens on page 117 PROGRAMMING STYLE PROGRAMMING STYLE NORMAL QUICK VIEW CHANGE lt 2 AL 24 NS Note A Menu access can be controlled with the optional Program Lock See Chapter 6 110 6700FR Refrigerated Sampler Figure 25 Standard Programming Programming Screens RUN PROGRAM VIEW REPORT OTHER FUNCTIONS SITE DESCRIPTION SITE STOP key FACTORY ABCDEFGHIJKLMNOPQRST pressed SAVE CHANGES CHANGE UVWXYZ amp 0123456789 YES NO YES NO BACK UP DONE SELECT UNITS FOR LENGTH ft m See Figure 32 Module Setup on page 118 NUMBER OF BOTTLES BOTTLE VOLUME IS SUCTION LINE LENGTH 1 2 4 8 12 24 ml 300 30000 TIME PACED FLOW PACED TIME BETWEEN FLOW BETWEEN SAMPLE EVENTS SAMPLE EVENTS _ HOURS __ MINUTES ____ PULSES 1 9999 SEQUENTIAL BOTTLES SAMPLE SAMPLES BOTTLE ___ BOTTLES PER Multi bottle SAMPLE EVENT 1 max ___ SAMPLES PER RUN CONTINUOUSLY BOTTLE 1 max YES NO 1 bottle RUN CONTINUOUSLY TAKE ___ SAMPLES YES NO 1 999 Yes SAMPLE VOLUME mi 10 max See Figure 26 Standard and Extended Programming Start Times on page 112 111 6700FR Refrigerated Sampler Figure 26 Standard and Extended Programming Start Times Continued from Figure 25 Standard Programming Programming Screens on
148. e Manual Paused state The power source was disconnected The power source was reconnected The sampler finished the sampling program The sampler was enabled or disabled according to program settings The program reached a programmed pause or resume time The sampler started the sampling program You selected Stop from the manual paused options terminating the program 58 6700FR Refrigerated Sampler Table 9 continued Reports Source Error and Program Event Codes PUMP TUBE REPLACED SAMPLE SKIPPED SAMPLER ENABLED DISABLED VOLUME CHANGED VOLUME DELIVERED The pump tube alarm was reset while in the Manual Paused state Sampler was in Manual Paused state when a sample event was initiated The sampler was enabled or disabled by an external instrument Sample volume was changed while in the Manual Paused state The volume actually delivered entered by the user during sample volume calibration Figure 8 Reports Program Settings SAMPLER ID 0011343009 15 25 23 MAR 99 Hardware B2 Software 3 10 KEKKKKKKKKHK PROGRAM SETTINGS KAKKKKKKKKKK PROGRAM NAME EXTENDED 1 SITE DESCRIPTION FACTORYOO9 UNITS SELECTED LENGTH ft UNITS SELECTED FLOW RATE cfs FLOW VOLUME Mgal BUBBLER MODULE WEIR 90 V NOTCH 5 MINUTE DATA INTERVAL 24 1000 mL BTLS 10 ft SUCTION LINE AUTO SUCTION HEAD O RINSES 0 RETRIES PACING TIME EVERY O HOURS 15 MINUTES DISTRIBUTION SEQUENTIAL VOLUME 200 ml SAMPLES 5 MINUTE DEL
149. e YSI level reading Flowlink 4 can collect reports exceeding 40 columns A flow through chamber available from YSI which will allow a YSI sonde to be continuously wetted even in storm applications will be supported as follows e One of the I O lines can be used to control an external pump The external pump is used to refresh the liquid in the flow through chamber If selected for this purpose the signal on the VO line will be high when the sampler requires YSI sonde readings The signal will become high a user enterable time before the readings are taken and remain high until all readings have been taken e To conserve power the reading interval will always be the data storage interval The 30 second rate if a YSI reading is used in an enable condition will be ignored Readings will be taken continuously if the backlight is on For those of you who use the serial output option additional codes have been added modified to support the YSI parameters See also Table 11 on page 98 Table 14 YSI Parameter Identifiers for Serial Output emer reme CS 109 6700FR Refrigerated Sampler Appendix A Menu Charts Figure 24 6700 Menu Tree for Standard Programming See Running Programs and Run Time Screens on page 50 RUN PROGRAM VIEW REPORT OTHER FUNCTIONS Sup POWER USED CURRENT _ _ amp hr PREVIOUS _ _ amp hr nes See the charts on pages 111 through 128 See View Report on pag
150. e alarm directs the sampler to calculate a new expiration date five years in the future If you reset the alarm without replacing the battery the sampler will not be able to alert you to the battery s impending expiration MAINTENANCE MANUAL FUNCTIONS Press Stop to return to the main menu 6 PROGRAMMING STYLE HARDWARE 76 Removing the front and back panel exposes electrical and mechanical hazards Trouble shooting and repair activities should be performed by a qual ified refrigeration technician refrigeration repair work ai be performed by a quali fied refrigeration technician Always purge the system with nitrogen NEVER USE AIR to purge the system Always recover the refrigerant When recharging do not leave a line tap in the refriger ation system because of pos sible corrosion or leakage problems 6700FR Refrigerated Sampler Servicing the Refrigerator Before servicing the refrigerator disconnect it from power This precaution will protect you from the possibility of electric shock when working with the refrigerator Access the electrical and refrigeration components by removing the nine screws on the back of the refrigerator See Appendix D Re placement Parts Access the circuit board by removing the six screws securing the control box lid The wiring connections for the circuit board are printed on a label inside the temperature control box lid A copy of the label appears in Figure 17
151. e first two 6 PLS digits of the new setting The sampler accepts entries between 1 and 99 For example to increase the count to 1 500 000 enter 15 MAINTENANCE Press Stop to return to the main menu MANUAL FUNCTIONS 7 PROGRAMMING STYLE HARDWARE 12 6700FR Refrigerated Sampler Opening the Controller Case CAUTION You will need to open the controller case to gain access to The circuit boards can be dam e The desiccant bag that dries the controller s interior aged from a discharge of static electricity Always use an antistatic mat when opening the controller to To open the case protect the circuit boards e The battery that provides backup power to the controller 1 Pull the discharge tube and pump tube away from the bulk head fitting 4 2 Remove the distributor arm by unscrewing the nut that at M Note taches the arm to the distributor shaft DO NOT ROTATE The case top and bottom fit to THE DISTRIBUTOR ARM MANUALLY THIS WILL SE gether with a sealed tongue VERELY DAMAGE THE DISTRIBUTOR DRIVE GEARS and groove joint Any damage 3 Remove the controller from the sampler nicks or cuts to the tongue groove or sealing gasket pre 4 Open the case by removing the 11 screws that attach the case vent the case from sealing com bottom to the case top pletely when you close it Use Refer to Figure 15 for the location of the desiccant box To gain ac extreme care when opening the case to avoid damaging the
152. e the refrigerator s base e A forced air condensing coil and front ventilation let you place the unit close to a wall or in a corner eThe oversized wrap around evaporator plate cools the sampling compartment quickly and efficiently Heaters on the plate let the sampler continue to operate in cold temperatures The evaporator plate is self defrosting e Food srade ABS plastic interior will not support bacterial growth or leach plasticizers into the sample e A single distributor arm adjusts quickly to fit all bottle kits Easily removed for composite sampling e Routes sample liquid from pump tube through distributor arm to sample bottle e 581 Rapid Transfer Device e Refrigerator Temperature Sensor e 674 Rain Gauge e 3200 Series Flow Meters e 700 Series Modules e 4100 Series Flow Loggers e YSI 600 Sonde e 4200 Series Flow Meters e YSI 6820 Sonde e Flowlink 3 and 4 Samplink e YSI 600XL Sonde e 1640 Liquid Level Actuator e PAL 1101 e 3770 Field Printer As the sampler runs a sampling program it displays the program s status The status display may include such information as the time of the next sample the number of the next bottle or whether the sampler is disabled or stopped If the sampler encounters an error while running the program it displays a message alerting you to the problem Program the modules from the sampler s control panel The module s program settings become part of the sampling program Calibrate and pro
153. eat steps two through five The sampler will hang up after ten seconds of quiet time Table 12 6700 Telephone Commands CODE teme osseo START This command will start immediately any program that has been run and is 0 currently waiting to start This command will load program 1 as the sampler s current Extended program RUN 1 reset partition data if the storage interval has changed and run the program RUN 1 will also run the current program when in the Standard programming mode RUN 1 is valid at the Standby screen and when waiting to start RUN 2 These commands are available for Extended programming only As with RUN 1 they will load the designated program reset partition data if the storage RUN 3 interval has changed and run the program These commands are valid at the RUN 4 Standby screen and when waiting to start This command is similar in functionality to a pin F low signal a signal typically used to enable or disable the sampler from a flow meter Command 6 must ROIO GORE be used to re enable PHONE DISABLE is valid while a program is running At run time the sampler starts with the phone enable in the enabled state This command is used to re enable a phone disabled sampler PHONE 6 amp EN EN ENABLE is valid while a program is running This command causes the sampler to take a sample The sample is treated as one of the program s samples and is placed in the current bottle Part A s cur PHONE SAMPLE rent bottle
154. ed to measure Similar to the Sampler Enable you can set thresholds for one or two conditions and the CONDITIONS output can then trigger alarms when the measured parameters ex ceed the threshold Isco offers an I O module that interfaces the sampler with a large number of non Isco devices For more information about the I O module contact your sales representative 96 6700FR Refrigerated Sampler Refrigerator Temperature Isco offers a temperature sensor intended for use with the 6700FR Refrigerated Sampler The optional sensor connects to the Rain Gauge YSI port and uses 1 03 to transmit its temperature readings to the 6700 To configure an attached temperature sensor select FR TEMP as the input for 1 03 The 6700 will display the NEW HARDWARE SETUP screen Select YES and the 6700 reconfigures its memory partitions to record the temperature readings Temperature readings are updated approximately every 2 5 sec onds The readings are stored as FR TEMP readings at the data storage interval You can retrieve a history of temperature read ings through the 6700 s reports The temperature data also can be used as a sampler enable condition Analog Output Analog Output Screens Isco offers multiple analog outputs as a factory installed option Charts for analog output screens The number of isolated outputs can vary from one to three and is appear in specified at order time The option is installed inside the controller Figure 46
155. eens on page 131 sa At the transition to the true state any programmed VO output can cause the sampler to warn of the alarm condition As many as three telephone numbers can be entered The sampler tries each tele Figure 42 Extended phone number in succession until the alarm is acknowledged For Programming Hardware each alarm condition the sampler will attempt each telephone SS number entered a maximum of five times Figure 43 Extended Programming Hardware Quick When the call is answered the sampler s talking modem announc View Screens on page 128 es the alarm condition and the sampler s three digit ID number To acknowledge the call press the star key and the three digit ID number The sampler will reply with an acknowledgment when the keyed entry is correct To set up I O conditions see A record of alarms and acknowledgements is available in the Sam pling Report When the Sampler detects the alarm condition it records the type of alarm and the time it occurred Acknowledge ments are a separate Sampling Report entry recording the time and telephone number that responded to the call As mentioned previously as many as three telephone numbers may be entered Modems with serial numbers 199E00000 and greater can dial up to 25 digits Enter numbers using the numeric keys on the 6700 keypad When entering telephone numbers longer than 17 digits the display will scroll System IDs Charts showing the ID s
156. eh he In ES ia 60 2743 024 Bottle Locating Base for 6700FR 2 Bottle Kits 60 2723 102 Discharge Tube for 8 Bottle 12 Bottle and 24 Bottle Kits 60 9003 279 Discharge Tube for 2 Bottle Kits 2000 a di A ia 60 9003 283 Discharge Tube for 1 Bottle Kit 9 4 liter Polyethylene Bottle and 9400 milliliter Glass Bottle cicle urnes ra en di 60 9003 262 Discharge Tube for 1 Bottle Kit 15 0 liter Polyethylene Bottle 60 9003 264 Discharge Tube for 1 Bottle Kit 18 5 liter Glass Bottle and 20 5 liter Polyethylene Bottle ss errak 2 4 2 A de aa a ae 60 9003 266 Bulk Discharge Tube 10 foot Length 60 6700 046 Bulk Discharge Tube 50 foot Length 60 6700 047 Distributor Arm includes nut sau AA ei i 60 9004 050 Bulk Sets of Bottles with Lids Set of 24 350 milliliter Glass Bottles with Teflon Lined Lids 68 2100 001 Set of 100 350 milliliter Glass Bottles with Teflon Lined Lids 68 3700 048 Set of 24 1 000 milliliter Polypropylene Bottles with Polyethylene Foam Lined lids 68 2100 007 Set of 100 1 000 milliliter Polypropylene Bottles with Polyethylene Foam Lined lids 68 3700 046 Set of 500 1 000 milliliter Polypropylene Bottles with Polyethylene Foam Lined li
157. electrolysis of water Rarely from rock strata Insecticide and rodenticide Simplest and Cheapest Safe Method of Testing Detectable odor at low concentrations Combustible gas indicator Combustible gas indicator Oxygen deficiency indicator CO ampoules Detectable odor at low concen trations Detectable odor at low concen trations Detectable odor 1 Combustible gas indicator 2 Oxygen deficiency indicator Combustible gas indicator Detector tube 6700FR Refrigerated Sampler Hazardous Gases Continued Methane Nitrogen Nitrogen Oxides Oxygen Ozone Sludge Gas Sulfur Dioxide Toluene Turpentine Xylene Chemical Formula a DN F O E N Oo 5 T gt S O o 5 ct 8 Common Properties Irritant and poisonous volatile compound Rotten egg odor in small concentrations Exposure for 2 to 15 min at 0 01 impairs sense of smell Odor not evident at high concentrations Color less Flammable Simple asphyxiant Colorless odorless tasteless flammable Simple asphyxiant Colorless tasteless Non flammable Prin cipal constituent of air about 79 Colorless Colorless sweet odor Reddish brown Irritating odor Deadly poison Colorless odorless tasteless Supports combustion Irritant and poison ous Strong electrical odor Strong oxidizer Colorless At 1 ppm st
158. en flames Use self contained breathing apparatus SCBA if large spill or leak occurs HANDLING AND STORAGE Handling Personnel Use with sufficient ventilation to keep employee exposure below recommended limits HFC 134a should not be mixed with air for leak testing or used with air for N other purpose above atmospheric pressure See Fire and Explosion Data section Contact with chlorine or other strong oxidizing agents should also be avoided Storage Clean dry area Do not heat above 52 deg C 125 deg F 135 6700FR Refrigerated Sampler EXPOSURE CONTROLS PERSONAL PROTECTION Engineering Controls Normal ventilation for standard manufacturing procedures is generally adequate Local exhaust should be used when large amounts are released Mechanical ventilation should be used in low or enclosed places Personal Protective Equipment Impervious gloves and chemical splash goggles should be used when handling liquid Under normal manufacturing conditions no respiratory protection is required when using this product Self contained breathing apparatus SCBA is required if a large release occurs Exposure Guidelines Exposure Limits SUVA COLD MP PEL OSHA None Established TLV ACGIH None Established AEL Du Pont 1000 ppm 8 amp 12 Hr TWA WEEL AIHA 1000 ppm 8 Hr TWA AEL is Du Pont s Acceptable Exposure Limit Where governmentally imposed occupational exposure limits which are lower than the A
159. en sampling at depths exceeding the maximum ratings e All strainer dimensions are in inches e Teflon suction line is compatible only with the 1 inch diameter stainless steel strainer How Does the Sampler Work When the sampler takes a sample it draws liquid through the strainer and suction line to the pump tube The liquid flows through the pump tube past the liquid detector which senses the liquid From the detector the liquid follows the pump tube through the pump to the bulkhead fitting and then through the discharge tube to the sample bottle A typical sampling cycle consists of 1 The sampler moves the distributor arm over the bottle that 1s to receive the sample The pump reverses for the presample purge The pump direction changes filling the suction line E 0 N When the detector senses liquid the sampler begins measur ing the sample See Measuring Sample Volume on page 46 5 After depositing the sample the pump again reverses for the postsample purge 45 6700FR Refrigerated Sampler Figure 6 Identifying the Sampler Components 005000 on Controller Refrigerator Peristaltic pump Liquid Detector Strainer Suction line Coupling pump tube routed from the liquid detector s intake port through the pump out the detector s discharge port and over the side of the control ler to a bulkhead fitting at the top of the refrigerator Bulkhead fitting Discharge tube
160. ends sampling until the first resume time when it begins Figure 41 Extended Programming sampling again If the start time falls within a pause period the Quick View Programmed sampler will not begin sampling until the next resume time Pause Sampler Enable on page 126 and resumes repeat weekly Figure 37 Extended Programming Programmed Sampler Enable on page 122 88 6700FR Refrigerated Sampler You can enter up to nine pairs of pause and resume times using Ri MO Er screen suspend the program between 5 00 p m Monday and 8 00 screen 23 The pause and resume times shown as examples in this 2 17 00 TU 08 00 WE a m on Tuesday and between 5 00 p m Tuesday and 8 00 a m on CLEAR DONE 3 l RAI Del Wednesday To remove pause and resume settings from a program select CLEAR in screen 23 Wednesday If the start time is Monday at 8 00 a m the sampler takes samples between 8 00 a m and 5 00 p m Monday between 8 00 a m and 5 00 p m Tuesday and continues after 8 00 a m A sampler running a pause resume program resets the pacing in terval at each resume time You can program the sampler to take a sample at resume times See screen 24 Start Times Select RUN from the Start Menu Program s menu The start time is the time at which the sampler begins the Start Time 3 i program s first sample interval countdown The start time is con Delay to Sampling trolled by your selections from the st
161. ens work in the same way as the sampler s screens Menu charts for the modules appear in the manuals shipped with each module 26 6700FR Refrigerated Sampler YSI Sonde Programming The sampler s extended programming screens can be modified for the optional YSI 600 Sonde To use or record the YSI 600 parame ters you must first configure the sampler with the Hardware Set up See YSI 600 Sonde Setup on page 93 The 6700FR also can support YSI 6820 and YSI 600XL Sondes See Chapter 6 Once configured the sampler adds the selected YSI Sonde param eters to the Sampler Enable screens The sampler will also auto matically record the selected sonde parameter data at the programmed data storage interval Programming Examples This manual provides numerous programming examples Some demonstrating simple tasks appear in the margins Others dem onstrating more complex tasks appear as examples and include e Example 1 Program One Sample every 15 Minutes One Sam ple in Each Bottle Using Normal Programming Style on page 16 e Example 2 Setting the Clock and Calendar on page 18 e Example 3 Changing the Programming Style on page 20 e Example 4 Selecting a Stored Extended Program on page 26 e Example 5 Standard Program Flow Paced Sampling Two Bottles Per Sample on page 28 e Example 6 Storm Water Runoff Sampling on page 30 e Example 7 Resetting the Pump Tube Warning on page 72 e Example 8 Resetting the Internal Batt
162. ery Warning on page 76 27 6700FR Refrigerated Sampler Example 5 Standard Program Flow Paced Sampling Two Bottles Per Sample e Program type Standard e Site description SITE 29 e Units for Length Feet e Data Storage Interval 15 minutes Bottle kit 24 1000 milliliter bottles e Suction line length 7 feet e Pacing Flow pacing every two pulses e Distribution 2 bottles per sample e Sample Volume 250 milliliters e Start time Clock Time 6 00 a m on Monday Wednesday Fri day e Module No module installed 6700 SAMPLER STANDARD PROGRAMMING For HELP at any screen press key RUN PROGRAM Select PROGRAM VIEW REPORT OTHER FUNCTIONS SITE DESCRIPTION Select NO Ta The margin example Using the Site Description or Program Name Menus YES NO on page 19 shows you how to change the site description SELECT UNITS FOR LENGTH Select ft ft m DATA STORAGE INTERVAL IN MINUTES Select 15 1 2 5 10 15 30 NUMBER OF BOTTLES Select 24 1 2 4 8 12 24 BOTTLE VOLUME IS Enter 1000 1000 ml 300 30000 Enter 7 SUCTION LINE LENGTH IS 7ft 3 99 Select FLOW PACED TIME PACED FLOW PACED 28 6700FR Refrigerated Sampler FLOW BETWEEN SAMPLE EVENTS Enter the number of pulses between sample events 2 PULSES 1 9999 SEQUENTIAL BOTTLES SAMPLE Select BOTTLES SAMPLE SAMPLES BOTTLE 2 BOTTLES PER Enter 2 SAMPLE EVENT 1 24 RUN CONTINUOUSLY Select NO YES NO SAMPLE VOLU
163. eter to the enabling conditions at a rate faster than the Data Storage interval If the Check Enable interval is equal to or greater than the Data Storage interval the parameter will be checked at the rate of Data Storage interval Normally there are two considerations when selecting the Check Enable interval power consumption and duration of the enabling event This setting for battery powered samplers will require some degree of balance between the need to conserve power yet detect the enabling event before it has passed Sampler Enable Responses In addition to programming enable conditions extended program ming lets you control the sampler s response to its enable state You can e Stay enabled after the first enable e Set up a repeatable enable e Take a sample at enable or disable e Delay the start of sampling after the enable e Reset the sampling interval countdown each time the sampler is enabled e Control the sampling interval countdown while disabled e Enable Part B of a two part program when Part A is done 87 6700FR Refrigerated Sampler Once Enabled Stay Enabled For certain monitoring pro grams you may want the sampler to continue to sample even though the conditions that enabled the sampler no longer exist When you use the ONCE ENABLED STAY ENABLED feature af ONCE ENABLED ter becoming enabled the sampler takes samples until it reaches STAY ENABLED the end of its program YES NO Repeat
164. ettings in a Quick View SCREEN PINE REP ee 20 Niess ages 24 ok 2200ER ara ed 21 Information Messages 21 Help Notes soria ies 21 Warning Messages 22 Operation Messages 22 Menu Trees ci dd vase 22 Optional Password Security 23 Standard and Extended Programming 23 Changing to and from Extended and Standard Screens 24 One Part and Two Part Programs 24 Storage For Extended Programs 25 Selecting a Stored Program 25 Selecting an Extended Program 26 Module Programming 26 YSI Sonde Programming 27 Programming Examples 27 3 Uperation siii ai 37 Installation and Operation Checklist 37 Preparing the Sampler 38 Installing the Distributor Shaft Extension 38 Mounting the Controller 38 Installing the Distributor Arm and Discharge Tube 39 Installing Bottle Kits 41 Installing Racks 41 Removing Racks 43 Installing Composite Bottle 43 DUCLHON Bine rs helios aa 44 Guidelines for Measuring and Cutting Suction Line 44 Attaching Suction Line to the Pump Tube 44 oi AAA 44 Debris Deflector iii di 44 Alternative to Strainers 44 How Does the Sampler Work 45 Measuring Sample Volume
165. events in a single bottle before moving to the next bottle Use samples per bottle distribution to collect a series of small composite samples Composite For single bottle configurations samples per bottle distribution is known as composite sampling composite sample represents an av erage of the flow stream s characteristics during the sampling period 84 6700FR Refrigerated Sampler Multiple Bottle Compositing Multiple bottle compositing is a combination of bottles per sample and samples per bottle At each sample event the sampler depos its a sample into a set of bottles It moves to a new bottle set only after each bottle of the first set contains the programmed number of samples Use multiple bottle compositing to collect identical sets of composite samples or a composite sample that is larger than the capacity of a single bottle Multiple bottle compositing is available only in extended programming Time Switching In extended programming the sampler offers an additional distri bution feature time switching This feature determines when the sampler goes to the next bottle or bottle set and may be used with Time Switched Distribution 2 BOTTLES PER SAMPLE EVENT 1 max time paced or flow paced sample programs Time switching distri bution occurs at regular intervals as programmed in screen 16 in Enter the number of bottles the margin The switch times are relative to the programmed that should receive sam
166. factory or your sales representative for more information Flash Memory and Software Upgrades The sampler has Flash memory to store its software With Flash technology you can upgrade your sampler s software without send ing it back to the factory or replacing a chip Simply connect a com puter to the sampler and run the Flash Update program Pressurized Lines The sampler can obtain samples from pressurized lines as long as the line pressure remains below 15 PSI pounds per square inch Pres sures greater than 15 PSI may prevent the sampler from purging the suction line moreover extreme pressures can force liquid past the pump even when the pump is not running For more consistent sam ple volumes from lines under constant pressure calibrate the sam ples Isco does not recommend sampling from pressurized lines 101 6700FR Refrigerated Sampler Command Driven Operation The 6700FR controller can be placed in a mode where it is a slave to an external controller The external controller is responsible for determining when to take a sample how much volume to pump and where to put the sample The external controller directly inter faces to the sampler via an RS 232 communications port at 2400 baud 8 data bits no parity and 1 stop bit comma separated val ue protocol is used by the external controller to make requests and by the sampler to report results Use a standard computer connect cable see Appendix E to connect t
167. form Clock Time Pacing 83 Nonuniform Interval Pacing 83 Random Interval Pacing 83 Event Pacini 0 DA A oh ees 83 Distribution Vivid sd ad 84 Sequential aras des eli 84 Bottles Per Sample 84 Samples Per Bottle 84 Composite 22 mur Ea a 84 Multiple Bottle Compositing 85 Time Switching 85 Continuous Sampling 85 Sampler Enable 87 Check Enable Interval 87 Sampler Enable Responses 87 Pauses Resumes 88 Lar Lime in sue SL ns 89 How Do Start Times Work 90 Sampler Enable 90 Two Part Programs 90 Other Functions 91 Manual Functions 91 Operating the Pump 91 Moving the Distributor 91 11 Programming Style 91 Hardware Setup 4 65 biie ani 92 Liquid Detector Disable 92 Rain Gauge Setup 92 YSI 600 Sonde Setup 93 YSI 600 Sonde Communications Test 93 YSI 600 Sonde Calibration 93 Master Slave Sampling 94 Setting Up Master Slave Sampling 94 How Does It Work 94 Bottle Full Detect 94 Display Backlighting 95 Event Marks iii 2 24 0845 Gas 95 Bottle
168. g and Programming Hardware Quick View Distribution on page 125 Screens on page 128 A Done and I O are not options for I O Conditions See Note A See Note A A ENABLE ENABLE All except ENABLE RAIN AND ENABLE RAIN AND RAIN gt 0 11 12 00 I O RAIN LEVEL NONE I O LEVEL FLOW AND FLOW Y pH Y TEMP AND OR DONE pH Y TEMP Y COND Y D O 0 500 lt LEVEL lt 1 500 Y COND Y D O NONE NONE A DONE RAIN 1 0 All except I O Rain and A Done RAIN SET POINT ENABLED WHEN LEVEL CONDITION __ __ INCHES PER I O ENABLE IS HIGH SET POINT 15 MIN 30 MIN I O ENABLE IS LOW RANGE 1 HOUR 2 HOURS ENABLED WHEN LEVEL RANGE LEVEL SET POINT ABOVE SET POINT LOWER il So BELOW SET POINT UPPER ft 0 001 30 000 0 001 30 000 ENABLED WHEN ENABLED WHEN RESET RAIN HISTORY INSIDE RANGE ABOVE SET POINT YES NO OUTSIDE RANGE BELOW SET POINT ONCE ENABLED See Note B If applicable STAY ENABLED YES NO Repeatable Enable A ENABLE REPEATABLE ENABLE SAMPLE AT DISABLE SAMPLE AT DISABLE YES NO NO SAMPLE AT ENABLE SAMPLE AT ENABLE If applicable YES NO CHECK ENABLE EVERY 05 1 2 5 10 15 30 MINUTES Latched Enable A ENABLE START OF SAMPLING No Sample at Enable MINUTE DELAY TO AFTER A START OF SAMPLING MINUTE DELAY 0 999 A ENABLE RESET SAMPLE CONTINUE COUNTDOWN Repeatable Enable COUNTDOWN CONTINUES INTERVAL AT ENABLE WHILE DISABLED WHILE DISABLED YES NO YES NO A ENABLE
169. ge 24 The suction head is the vertical distance from the flow stream to the liquid detector Extended programming has two settings e Auto Suction Head The head is automatically determined e Fixed Suction Head A user definable measurement for the head Note See Suction Head on page 81 e Program setting for the number of times 0 to 3 that the 6700 rinses the suction line before drawing a sample See Rinses and Retries on page 81 e Program setting for the number of times 0 to 3 that the 6700 attempts to sample if it fails to deliver the entire sample volume See Rinses and Retries on page 81 e Run Immediately Starts the sampling program immediately e Delayed Start Starts the sampling program after a user definable delay of 1 to 999 minutes eClock Time Starts the sampling program at a user definable time on one or more days of the week See Start Times on page 89 eContinuous Sampling If the sample bottles can be properly serviced the sample distribution can restart with the first bottle set after the last bottle set 1s filled without interrupting the running program See Distribution on page 84 6700FR Refrigerated Sampler Table 2 6700FR Construction Materials ITEM Top Cover and Refrigerator Body Plastic Retaining Rings Controller Case Distributor Arm Distributor Arm Nut Pump Rollers Control Panel Connector Labels Distributor Shaft Pump Shaft Pump Paddles Pump Band Bulkhea
170. gerated Sampler Installing Bottle Kits Isco ships the refrigerator from the factory with the sample bottles in place when using the sampler for the first time you will only need to remove the bottle lids When installing cleaned bottles or a new kit keep these guidelines in mind e Do not mix glass and plastic bottles together e Install all bottles to insure that they remain in place e Align the racks correctly Ifthe racks are misaligned the sam pler may miss the bottle mouth or the sampler will deposit samples in the wrong bottle Each time you change from one size bottle to another you must ad just the length of the distributor arm install a discharge tube of the correct length and possibly install a different distributor shaft extension Each time you install a bottle kit check the program settings for the number of bottles and bottle volumes Also rotate the distribu tor arm to each bottle position to ensure the arm is correctly posi tioned over each bottle Use the controller to move the arm Do not manually rotate the distributor arm See Moving the Distrib utor on page 91 Installing Racks Install the bottle rack with bottles by sliding it into the cooling com partment until the rack drops over the two semicircular ramps which hold it in place Figure 3 The five posts and two ramps which position the rack under the dis tributor arm are adjusted at the factory When you change bottle kits you may
171. gram setting you wish to change Then make the changes as you would in the NORMAL programming mode The ex tended programming mode defaults to QUICK VIEW CHANGE Hardware Setup The hardware setup screens available with extended program Selecting Hardware Setup ming make a number of adjustments to the Sampler s hardware based features e Liquid Detector Disable RUN PROGRAM NAME PROGRAM A Rain Gauge Setup e YSI Sonde Setup Select Other Functions e Master slave sampling MAINTENANCE Full bottle detection MANUAL FUNCTIONS e Display backlighting PROGRAMMING STYLE HARDWARE e Event marks e Presample and postsample purge counts Select Hardware e I O pin programming e Analog outputs e Serial output e Dial out alarms Liquid Detector Disable Under some conditions pressurized lines sampling foam a more repeatable sample volume may be delivered by disabling the liquid detector Selecting NO at screen 43 will turn the Liquid Detector off YES NO If the Liquid Detector is off e you must enter the SUCTION HEAD e no RINSES or RETRIES will be available e you will not be able to CALIBRATE SAMPLE volumes e the RESULTS report will read a COUNT TO LIQUID of 0 e a complete purge will occur between samples when using mul Rain Gauge Setup tiple bottles per sample distribution DO YOU HAVE A g RAIN GAGE CONNECTED Rain Gauge Setup YES NO With standard programming the sampler automatically rec
172. gram the YSI 600 sonde from the sampler s control panel The YSI program settings become part of the sampling program The 6700FR can also support the YSI 6820 and 600XL sondes See Chapter 6 6700FR Refrigerated Sampler Table 1 6700FR Sampler Features GENERAL FEATURES CONTINUED Memory for Stored Programs and Readings Five Reports Available Serial Data Output Units of Measure External Sampler Enable Master Slave Sampling Command Driven Operation Warning Messages Optional Dialout Modem On Line Help Notes 128 kilobytes of battery backed RAM Random Access Memory to store e Five sampling programs e A sampling report from the most recently run program It records as many as 1000 sampling events events can be the program start time enable time sample event information etc e700 Series module readings The readings can be level flow rate velocity pH temperature or the data collected by the 4 20 mA module e Rain gauge and Refrigerator Temperature readings e YSI Sonde readings These readings include temperature pH dissolved oxygen and conductivity The 6700FR controller can be ordered with 4 megabytes of RAM as a factory installed option e The Program Settings report listing current program settings e The Sampling Results report listing the program events occurring during the program e The Combined Results report combining sampling events with readings from a rain gauge module or Y
173. h special caution in situations of emergency life support qq PP SS 134 6700FR Refrigerated Sampler FIRE FIGHTING MEASURES Flammable Properties Flash Point Will not burn Flammable limits in Air by Volume LEL Not applicable UEL Not applicable Autoignition gt 743 C gt 1369 F HFC 134a is not flammable at ambient temperatures and atmospheric pressure However HFC 134a has been shown in tests to be combustible at pressure as low as 5 5 psig at 177 deg C 351 deg F when mixed with air at concentrations of generally more than 60 volume air At lower A higher pressures are required for combustibility Experimental data have also been reported which indicate combustibility of HFC 134a in the presence of certain concentrations of chlorine Fire and Explosion Hazards Cylinders may rupture under fire conditions Decomposition may occur Extinguishing Media As appropriate for combustibles in area Fire Fighting Instructions Cool cylinders with water spray Self contained breathing apparatus SCBA may be required if cylinders rupture or release under fire conditions ACCIDENTAL RELEASE MEASURES Safeguards Personnel NOTE Review FIRE FIGHTING MEASURES and HANDLING PERSONNEL sections before proceeding with clean up Use appropriate PERSONAL PROTECTIVE EQUIPMENT during clean up Accidental Release Measures Ventilate area especially low or enclosed places where heavy vapors might collect Remove op
174. he nausea bad taste lassitude Eye irritation Head ache dizziness nau sea irritation of the kidneys Narcotic in high con centrations less toxic than benzene 50 to 100 Exposure Exposure Probably no limit provided oxygen percent age is suf ficient for life No data Would vary widely with composition 159 Explosive Range by vol in air Limits lower upper SI Lo 19 3 1 27 7 0 1 1 o Likely Location of Highest Concentration Near bottom but may be above bottom if air is heated and highly humid At top increas ing to certain depth Near top but may be found near bottom Near bottom Variable at dif ferent levels Near bottom Near top of structure At bottom can combine with water to form sulfurous acid At bottom At bottom At bottom Most Common Sources Coal gas petro leum sewer gas Fumes from blasting under some condi tions Sludge gas Natural gas sludge gas man ufactured gas sewer gas Strata of sedimentary origin In swamps or marshes Sewer gas sludge gas Also issues from some rock strata Industrial wastes Common air pollutant Oxygen deple tion from poor ventilation and absorption or chemical con sumption of oxy gen Where ozone is used for disin fection From digestion of sludge Industrial waste combustion common air pol luta
175. he previous quick e Select the reverse arrow to go to the previous screen view screen e Select the forward arrow J to go to the next screen Press Stop for the main menu e Press Stop to return to the main menu All quick view screens work Because the forward arrow is always blinking when the screen ap the same way T 24 1000 ml BTLS pears you can simply press enter to go to the next quick view screen making it easy to page through the screens 10 ft SUCTION LINE Example 3 Changing the Programming Style PACING TIME EVERY RUN Select OTHER FUNCTIONS r 0 HOURS 15 MINUTES PROGRAM y VIEW REPORT OTHER FUNCTIONS DISTRIBUTION ii SEQUENTIAL s MANUAL FUNCTIONS Select PROGRAMMING STYLE PROGRAMMING STYLE PROGRAMMING STYLE t 200 ml SAMPLES NORMAL Select QUICK VIEW CHANGE QUICK VIEW CHANGE FIRST SAMPLE 08 00 u MO TU WE TH FR I Changing Settings in a Quick View Screen Although the quick view screens offer you a quick way to see the program settings they also provide you with a way to change set tings Using quick view screens to change settings is sometimes a faster way to change a program because you can go quickly to the setting or settings that needs updating To change the program settings in a quick view screen e Press an arrow until the setting blinks Press enter The 6700 then displays the screen used to change the setting 20 Using Help Notes Although this example shows you the help
176. he sampler s interrogator port and the external controller Charts showing the Command Driv en screens appear in Figure 48 To enable the command driven mode press 6 7 0 0 J 3 at the Command Driven Screens on page main menu The sampler then displays its current command driv 132 en state normally WAITING TO SAMPLE and is ready to respond to valid commands from the external controller From the WAIT ING TO SAMPLE screen press the 9 Stop key to check the sam A SUCTION LINE pler setup screen 61 To change the setup use the arrow keys to BOTTLES select the item to modify and press enter Select DONE to save the PUMP TUBE ALARM changes and return to command driven operation DONE To return to normal sampler operation press 6 7 0 0 1 for standard programming or 6 7 0 0 J 2 for extended program ming while at the sampler setup screen screen 61 Command Driven Mode While in the command driven mode the sampler will be quite lim ited in its functionality Some of the limitations are e No modules e No partition data e No sample event log e No reports e No Flowlink communication e No programmable I O e No sample calibration e No rinses or retries e Auto suction head head based on line fill counts and line length e Purge times become a function of the line length e Event is sent during the entire pump cycle The 6700FR Sampler will respond to three commands GET STA TUS TAKE SAM
177. he sampler stores the actual reading in memory so it can be collected later gpm 5 73 ft 00001457600 gal 50 6700FR Refrigerated Sampler For those programs that have delayed or scheduled start times the readings will be displayed while waiting for the start time Keep in mind that any totalizer values will be reset at the start time Mod Error Messages ule and YSI readings are also displayed after a program is com ERRORS HAVE OCCURED plete until a key is pressed DURING PROGRAM It is not necessary to run a program to view module or YSI readings Real time data can be viewed on the display by selecting VIEW RE PORT from the main menu See Viewing the Data on page 55 Error Messages FATAL ERROR NO DISTRIBUTOR ARM If the sampler detects an error that prevents it from taking a sam ple or continuing the program it displays an error message There are messages for the following errors e Pump Jammed e No Liquid Detected e Distributor Jammed e No More Liquid e Probable Overflow e Pump Latch open e Power Failed e Sampler Shut Off e Low Battery e Bottle Full Warning Messages e User Stopped e Sample In Progress WARNING REPLACE e No Distributor Arm PUMP TUBE Since the sampler may encounter more than one error during a pro gram it does not display the messages continuously Instead it records each error and the time it occurred in the Sampling Results no and Combined Results report It alerts you to the re
178. hen the trigger condition level flow or rainfall remains below a set point The intervals are determined by the flow instrument s pro gram settings for trigger pacing When conditions change and readings pass the set point triggering the new rate you can sample more frequently Or when the trigger condition is a clock setting the instrument changes the pacing inter val according to the time of day Using a clock trigger condition for instance the flow meter or flow logger can pace the sampler slowly at night and more frequently during the day For more information about trigger pacing see your flow meter or Flowlink manual The flow meter or flow logger sends the same pulse for both flow and trigger pacing and the sampler cannot distinguish between them Therefore to program a sampler for trigger pacing simply program it for flow pacing 82 6700FR Refrigerated Sampler Pacing in Extended Programming Extended Time Pacing Both standard and extended programming provide time and flow Screens pacing but extended programming adds a feature to flow paced The screens illustrated here do not sampling programs by letting you program the sampler to take a appear in the same order that they sample at the start time Also extended programming provides appear on your sampler s display nonuniform time pacing as well as event pacing For charts of extended pacing a ee Extended Time Pacing Figure 36 Extended Programming The extended
179. hone numbers including the nearest hospital and ambulance service police precinct fire sta tion and rescue or general emergency number 10 Field Equipment The following equip ment will be available for use Blowers Gloves Breathing apparatus Hard Hats Coverall Harnesses First aid kits Manhole irons Emergency flashers Pick axes Flashlight Rain slickers Mirror Ropes Gas detectors Safety vests Gas masks Traffic cones Waders Lethal Atmospheres in Sewers The following is an article written by Dr Rich ard D Pomeroy and published in the October 1980 issue of Deeds amp Data of the WPCF Dr Pomeroy is particularly well known for his studies over a period of nearly 50 years in the field of the control of hydrogen sulfide and other odors in sewers and treatment plants He has personally worked in a great many func tioning sewers In the earlier years he did so he admits with little knowledge of the grave hazards to which he exposed himself It is gratifying that the subject of hazards to people working in sewers is receiving much more attention than in past years and good safety procedures are prescribed in various publications on this subject It is essential that people know and use correct procedures It is less important to know just what the haz ardous components of sewer atmospheres are as safety precautions should in general be broadly applicable but there should be a rea sonable understa
180. ication refer to Table 7 Debris Deflector A debris deflector prevents debris from accumulating on the hose damp that attaches the strainer to the suction line Alternative to Strainers When sampling from high velocity streams with heavy suspended solids some field investigations suggest that more representative samples are obtained without the strainer Consider attaching a short piece of thin walled aluminum tubing to the end of the suction line anchor the tubing so that the inlet opens upstream The alu minum tubing s thin wall won t disturb the flow stream and most sample analyses disregard aluminum ions Under most conditions the presample purge removes any debris over the tubing entrance 44 6700FR Refrigerated Sampler Table 7 Selecting the Right Strainer ___TT TY 9 9 32 _ 23 32 Priority Vinyl Line Stainless Steel pollutant 22 feet i Ht leo 0 0 0 00 A tr diameter sampling Teflon Line 430 4 1 8 15 feet diameter diameter Routine Vinyl Line Polypropylene applications 11 feet diameter Highly acidic Vinyl Line fe Co one n iquids 4 feet lt loco oo diameter 1 1 4 diameter 7 a ls low fl inyl Line Stainless Steel Very low flow Vinyl Line stream depths 7 feet Low Flow y liloo H on di diameter Notes e The suction lines will float when filled with air during the purge cycles and when depths exceed the listed ratings Secure the suction lines wh
181. ight With Average Thermal Resistance Factor Recovery time 24 plastic bottles rack hold down no caps 24 glass bottles rack expander ring no caps 12 plastic bottles rack hold down no caps 8 plastic bottles rack adaptor no caps 8 glass bottles rack adaptor no caps 2 plastic bottles rack no caps 2 glass bottles rack no caps 1 9 4 1 plastic bottle and cap no distributor arm or nut 1 9 4 1 glass bottle and cap no distributor arm or nut 1 15 0 1 plastic bottle and cap no distributor arm or nut 1 20 5 1 plastic bottle and cap no distributor arm or nut 1 18 5 1 glass bottle and cap no distributor arm or nut R 16 The average R value for a complete FR refrigerator not running 5 minutes 175 lbs 79 kg 195 Ibs 88 kg 175 lbs 79 kg 170 lbs 77 kg 180 Ibs 82 kg 175 lbs 79 kg 165 lbs 75 kg 165 lbs 75 kg 170 lbs 77 kg 165 lbs 75 kg 165 lbs 75 kg 170 lbs 77 kg Recovery time is the time for the internal air temperature to return to 39 F 4 C after the door has been opened for one minute The empty refrigerator is running and set at 39 F 4 C The door is opened at least 4 minutes after the compressor has turned on Ambient air temperature is 75 F 24 C Thermostat Temperature Ranges Set point range 32 to 46 F 0 to 8 C Set point accuracy 1 8 F 1 C at 39 F 4 C With an ambient air temperature of 75 F 24 C Operational 20 to 120 F 29 to 49 C
182. ily Clay Mineral Chemical Names amp Synonyms Montmorillonite Clay Mineral Smectite Clay Mineral Bentonite Calcium Aluminosilicate Formula Ca x AL xMgx Si 0 OH nH 0 NFPA HMIS HEALTH 0 FIRE 0 REACTIVITY 0 SPECIFIC HAZARD SEE SECTION X SECTION II HAZARDOUS INGREDIENTS Hazardous Components in the Solid Mixture COMPONENT CAS No 20 OSHA PEL ACGIH TLV Montmorillonite Clay Mineral 1302 78 9 gt 99 3 3 Respirable Dust 5 0 mg m 5 0 mg m Silicon dioxide 14808 60 7 lt 1 Crystalline Quartz 3 3 Respirable Dust 0 1 mg m 0 1 mg m INGREDIENT HAZARD STATEMENT Risk of cancer depends on duration and level of exposure This product contains less or equal to 1 crystalline quartz CAS 14808 60 7 The quartz contained in the material is in granular form and packed in bags for use as a desiccant Therefore no exposure to quartz dust is anticipated under normal use of this product Avoid inhaling desiccant dust Prolonged or repeated exposure may cause lung injury Unless otherwise noted all values are reported as 8 hour Time Weighted Averages TWA s and total dust particulates only All ACGIH TLV s refer to the 1989 90 Standards All OSHA PEL s refer to CFR Part 1910 Air Contaminants Final Rule January 19 1989 Updated April 4 1994 Page 1 148 6700FR Refrigerated Sampler MATERIAL SAFETY DATA SHEET DESI PAK Packaged Desiccant SECTION III PHYSICAL DATA Appearance and Odor Gray granules No odor
183. in the quick view screens have been changed When you are done select the screen s forward arrow to move to the next quick view screen or press Stop to return to the main menu Messages The sampler has four sets of messages that supplement the program ming screens The Information messages tell you about programming status Help Notes are brief comments associated with programming screens describing the setting or offering assistance Warning messag es tell you something is different than Isco s standard The Operation messages report the sampler s status as it runs a program Information Messages These are brief messages about the programming status Informa tion messages are displayed for four seconds unless terminated by pressing any key Help Notes To see the help note 1 Press the Help key 2 When the note requires several screens the word more ap pears in the lower right corner Press enter for the next note 3 Move back and forth between screens by pressing the arrow keys 4 Press Stop at any time to return to the programming screen Most help notes refer to a related section in this manual Screens 21 6700FR Refrigerated Sampler that are self explanatory or that require extensive explanation have notes that contain only references to the manual Sections men tioned in the notes appear in the index and the table of contents Warning Messages Warning messages appear when the sampler determines
184. inter Sense D Transmit E Receive F NC A 12 volts DC B Ground C Flow Pulses In D Bottle Number Out Master Slave Out Event Mark Out Inhibit In 3 q NC 12 volts DC Ground Module Sense Receive Transmit Clock Control oO O O ND HM Chapter Contents e Getting Started 14 Using Menus and Entering Numbers 14 e Stored Data Will Be Lost 16 Quick View Screens 20 e Messages 21 Warning Messages 22 Operation Messages 22 Menu Trees 22 Standard and Extended Programming 23 One Part and Two Part Programs 24 e Module Programming 26 e YSI Sonde Programming 27 e Programming Examples 27 Examples of Menu Screens RUN PROGRAM a VIEW REPORT OTHER FUNCTIONS To enter a sampling program press an arrow key until PROGRAM blinks Then press enter NUMBER OF BOTTLES 1 2 4 8 12 24 Choose the number of bottles by pressing an arrow key until the appropriate number blinks Then press enter Front Panel 6700FR Refrigerated Sampler Chapter 2 Programming Before programming the 6700 you should become familiar with its keys and how to use the programming screens A description of the keys appears in Table 5 There are three types of program ming screens e Menu screens that let you select an option from a list e Number entry screens that
185. iter polypropylene bottles e350 milliliter glass bottles Distributor Arm Position D Discharge Tube 60 9003 279 Discharge Tube Length 20 inches 50 8 cm Distributor Shaft 60 9003 273 Distributor Shaft Extension 81 16 inches 22 0 cm 12 Bottle Kits e2 5 liter polyethylene bottles Distributor Arm Position D Discharge Tube 60 9003 279 Discharge Tube Length 20 inches 50 8 cm Distributor Shaft 60 9003 273 Distributor Shaft Extension 811 16 inches 22 0 cm 8 Bottle Kits e1 8 liter glass bottles e2 0 liter polyethylene bottles Distributor Arm Position B Discharge Tube 60 9003 279 Discharge Tube Length 20 inches 50 8 cm Distributor Shaft 60 9003 274 Distributor Shaft Extension 1012 inches 26 7 cm 2 Bottle Kits e9 4 liter 212 gallon glass bottles e7 5 liter 2 gallon polyethylene bottles Distributor Arm Position A Discharge Tube 60 9003 283 Discharge Tube Length 16 inches 40 6 cm Distributor Shaft 60 9003 275 Distributor Shaft Extension 6 inches 15 2 cm Composite Bottles Discharge Tube Discharge Tube Length 9 4 liter 212 gallon glass bottle 60 9003 262 1744 in 43 8 cm e9 4 liter 212 gallon polyethylene bottle 60 9003 262 1744 in 43 8 cm 15 0 liter 4 gallon polyethylene bottle 60 9003 264 1612 in 41 9 cm 18 5 liter 5 gallon glass bottle 60 9003 266 15 4 in 40 cm e20 0 liter 51 2 gallon polyethylene bottle 60 9003 266 153 4 in 40 cm 40 6700FR Refri
186. ject All loose items should be kept away from the manhole opening This applies to hand tools as well as stones gravel and other objects 7 Removing the Covers Manhole covers should be removed with a properly designed hook Use of a pick ax screwdriver or small pry bar may result in injury A suitable tool can be made from 3 4 inch round or hex stock Two inches of one end should be bent at a right angle and the other end should be formed into a D handle wide enough to accommodate both hands Even with this tool care must be exer cised to prevent the cover from being dropped on the toes The 2 inch projection should be inserted into one of the holes in the cover the handle grasped with both hands and the cover lifted by straightening the legs which have been slightly bent at the knees 8 Other Precautions Other precautions which should be taken when entering a man hole are e Wear a hard hat e Wear coveralls or removable outer garment that can be readily removed when the work 1s completed e Wear boots or nonsparking safety shoes e Wear rubberized or waterproof gloves e Wear a safety harness with a stout rope attached e Do not smoke e Avoid touching yourself above the collar until you have cleaned your hands 156 9 Emergencies Every member of the crew should be instructed on procedures to be fol lowed in cases of an emergency It is the duty of each crew chief to have a list of emergency p
187. join cess to the main circuit board and battery remove the two distrib ing surfaces utor connectors and the EMI shield Before reassembling the case ensure the connectors shields and straps are all secured Figure 15 Opening the controller Distributor Connectors EMI Shield Desiccant Box 73 6700FR Refrigerated Sampler Figure 16 Main circuit board connections Keypad Connector Battery A CAUTION Desiccant may produce irritating fumes when heated Observe the following precautions e Use a vented oven in a well ventilated room Do not remain in the room while recharging is taking place e Use the recommended temperature There have been reports of irritating fumes coming from the desiccant during reacti vation While our attempts to duplicate the problem have been unsuccessful we still urge you to use caution Material Safety Data Sheets are provided in Appendix B Module Connector 2 27 Liquid Detector y Connector Pump Count Connector Connector Board Connector Recharging the Desiccant The 6700 samplers use a desiccant bag inside the controller case to prevent moisture damage to its electronic components Follow the instructions in Opening the Controller Case to open the controller Remove the bag from the cardboard box at the front of the case Figure 15 How to Recharge the Desiccant Do not put the cardboard box in the oven You should recharge the desiccant when the
188. keypad connector by pulling gently upward on the edges of the board next to the connector Pull the main board up until the keypad connector 1s almost even with the edge ofthe case Next detach the main circuit board from the connector board 7 Desolder the lithium battery using care to prevent damage to the circuit board Insert the replacement battery and sol der it in place 8 Reconnect the main circuit board to the connector board be fore reconnecting it to the keypad Replace the Y4 inch stand off and the three screws and reconnect the module liquid de tector and pump count connectors 9 Replace the EMI shield and grounding straps Reconnect the two distributor connectors 10 Ensure that all connections and hardware are secure Re place the desiccant and close the case 11 Reset the battery alarm 15 6700FR Refrigerated Sampler Example 8 Resetting the Internal Battery Warning RUN E ana Select OTHER FUNCTIONS 1 VIEW REPORT OTHER FUNCTIONS MAINTENANCE MANUAL FUNCTIONS Select MAINTENANCE 2 PROGRAMMING STYLE HARDWARE SET CLOCK SET PUMP ALARM Select INTERNAL BATTERY 3 INTERNAL BATTERY DIAGNOSTICS WARNING REPLACE INTERNAL 4 BATTERY BEFORE 17 OCT 97 The sampler displays this screen briefly to show you the expiration date DID YOU REPLACE THE INTERNAL BATTERY After replacing the battery select YES Select NO only if checking the 5 YES NO expiration date Resetting th
189. ler to CLOCK TIME start as soon as you select RUN e Select DELAYED START when you want the sampler to delay from 1 to 999 minutes before starting the program FIRST SAMPLE e Select CLOCK TIME when you want the sampler to begin the AFTER A __ MINUTE DELAY program at a specific time on at least one day of the week 1 999 CLOCK TIMEs also require a First Valid Day The First Valid Day setting allows you to start a program calendar date up to a year in advance e Select DELAYED START e Enter the number of minutes to delay the countdown to the first sample How Do Start Times Work START FLOW COUNT As soon as you select RUN from the start up menu the sampler AFTER A checks the program s start time settings If programmed for a DE LAYED START the sampler starts a countdown to the start time The period between the time you select RUN and the start time you ve specified in the program is called the delay to start time __ MINUTE DELAY 1 999 The sampler uses this screen for flow paced programs When you run a program with a CLOCK TIME setting the sampler waits until the programmed first valid day day of week and first Clock Start Time Menu sample time before starting the program The sampler may not collect a sample at the start time see Pacing Den on page 82 The sampler must be enabled and the pacing selected CLOCK TIME must call for a sample at start In any event the sampler che
190. ling resets the distribution when the distribution sequence is complete That is when the last bottle set is reached the next bottle set is the first bottle set All pacing modes except RANDOM are supported When running a program continuously the bottles must be serviced at regular intervals to prevent overfilling the bottles The sampler assumes that the next bottle set is empty and ready to receive sam ples If you are using this feature with two part programming keep in mind that the parts will most likely reset at different intervals 85 6700FR Refrigerated Sampler Figure 20 Sample Distribution Sequential JA 7 IA F Fu JAR Bottles per Sample JE ER FF Samples per Bottle J 7 IA JE JE JE Multiple Bottle Compositing IA JE IA JR JE 7 3 6 6 2 5 5 8 8 1 1 4 4 DISTRIBUTION SEQUENTIAL STANDARD PROGRAMMING DISTRIBUTION EXTENDED SEQUENTIAL PROGRAMMING DISTRIBUTION 2 BOTTLES SAMPLE STANDARD PROGRAMMING DISTRIBUTION EXTENDED 2 BOTTLES SAMPLE PROGRAMMING DISTRIBUTION STANDARD 2 SAMPLES BOT TLE PROGRAMMING DISTRIBUTION EXTENDED 2 SAMPLES BOTTLE PROGRAMMING DISTRIBUTION EXTENDED 2 BOTTLES SAMPLE PROGRAMMING 3 SAMPLES BOTTLE ONLY Time Switched
191. m Nitrogen Ammonia Nitrogen If the sonde is equipped with the 6026 turbidity sensor the 6700 will activate the wiper each time the sonde is powered up In the case of continuous readings the wiper is activated after 60 seconds has elapsed from the time the last wipe was completed Nitrate Nitrogen Turbidity Chloride When using the proper sensor combination the level readings from the YSI will be compensated for dissolved solids This will be espe cially helpful in coastal applications where the measurements are taken in sea water You will be able to select up to eight parameters If level is one of the measured parameters and no flow module is connected the YSI level readings will be used to calculate flow The Y FLOW values can then be used to pace the sampler or as part of an enable condi tion When generating a YSI combined report if Y FLOW is calcu lated it will show up on the chart along with the total volume since the start of the program if there is room on an 80 column chart 108 6700FR Refrigerated Sampler Flow rate takes seven columns and is put on after the selected YSI parameters Flow volume takes 15 columns and will be the last en try in the chart M Note Flowlink 3 can not handle reports longer than 40 columns If you are using Flowlink 3 to get your reports you must limit the number of YSI parameters used to three level can not be one of these three if flow rate and flow volume are calculated from th
192. mente con equipos compatibles Isco No use este producto con cualquier otro equipo de otros fabricantes o para cualquier otro prop sito El uso de este producto para cualquier otro prop sito que no sea el descrito en este manual puede ocasionar da os personales o da os al producto Requisitos el ctricos El refrigerador se encuentra disponible en las configuraciones 120 VW y 230 VI El voltaje requerido para su funcionamiento se encuentra listado en la etiqueta de Identificaci n y en el N mero de serie ubicado dentro de la puerta del compartimiento de muestra Los refrigeradores configurados para que funcionen en 120 VU est n equipados con un enchufe norteamericano NEMA 5 15P y solamente pueden ser utilizados con 120 VU 60 Hz La fuente de corriente el ctrica debe ser clasificada para un servicio de 30 amperios Los refrigeradores configurados para que funcionen en 230 VU est n equipados con un enchufe Continental europeo CEE 7 7 y solamente pueden ser utilizados con 230 VAL 60 Hz La fuente de corriente el ctrica debe ser clasificada para un servicio de 16 amperios Los refrigeradores en cualquiera de las configuraciones proporcionan 12 5 V a 5 amperios para el controlador de muestra Esta salida proviene del conector de tipo militar de dos clavijas del cable en la parte superior del refrigerador Esta salida solamente sirve para los controladores 6700 Series Sampler El refrigerador debe ser instalado cerca de un
193. monitoring 24 V Variable duration pulse 95 event marks 95 Y YSI 600 about the sonde 1 accessories 172 calibration 93 communications testing 93 displayed readings 50 hardware setup 93 175 6700FR Refrigerated Sampler 176 DECLARATION OF CONFORMITY Application of Council Directive Manufacturer s Name Manufacturer s Address Equipment Type Environment Trade Name Model No Operating Voltage Year of Issue Standards to which Conformity is Declared Standard Severity Applied Performance Criteria IEC 801 2 Electrostatic Discharge IEC 801 4 801 4 EC 1 RF Emissions Group 1 Class A Industrial Scientific EN 55011 and Medical Equipment 89 336 EEC The EMC Directive Isco Inc 4700 Superior Lincoln Nebraska 68504 USA Mailing Address P O Box 82531 Lincoln NE 68501 Laboratory Equipment for Light Industrial Commercial Environments Model FR Sampler 6700FR 3700FR 3710FR 230 VAC 50Hz 10 1996 EN 50082 1 Generic Immunity for Commercial Light Industrial Environment Limits and methods of radio disturbance characteristics EN 61010 1 Safety Requirements for Electrical Equipment for Measurement Control and Laboratory Use EN 55011 Level 3 4kV contact discharge Level 2 8kV air discharge IEC 801 3 Radiated RF Immunity 27 MHz to 500MHz Level 2 3 V m Electrical Fast Transient Level 2 1kV on ac lines PB We the undersigned hereby declare that the design of the eq
194. ms liter Requires a T D S scale factor e Conductivity in mS cm The YSI 600 setup screens are shown in Figure 44 Consult the YSI 600 manual for specific conductance temperature coefficients and T D S scale factors When connecting to the sonde the 6700 sampler will check the soft ware version of the sonde If the sampler finds an incompatible ver sion it reports INCOMPATIBLE SONDE SOFTWARE UPGRADE TO VERSION 2 11 OR NEWER Contact the factory or your repre sentative if your sonde requires a software upgrade YSI 600 Sonde Communications Test The TEST YSI 600 COMMUNICATIONS screen appears during the YSI 600 Hardware Setup if the 6700 has not successfully com municated with the Sonde Communications test TEST YSI 600 COMMUNICATIONS If you answer YES the sampler evaluates the communications link YES N with the sonde and then sets the YSI 600 data transfer protocol It is important that you allow the sampler to complete the test dam age to the YSI 600 Sonde could result if power is interrupted during the communications test WARNING DO NOT REMOVE YSI 600 POWER R x TESTING YSI 600 Sonde Calibration The YSI 600 Sonde requires initial and periodic calibration Table 10 lists the supported calibration methods Refer to the YSI 600 Sonde Manual for calibration procedures Table 10 Supported YSI Calibration Methods pH Two Point Calibration pH 4 and 7 Buffers e PH 7 and 10 Buffers Three
195. n it cracks or appears worn Inspect the tube frequently when the sample liquid contains a high percentage of suspended or abrasive solids Pump Tube Alarm The sampler tracks the pump counts in both the forward and re verse cycles with a resettable counter When the counter reaches the default count of 1 000 000 or the count you have entered the sampler displays a message WARNING REPLACE PUMP TUBE The message appears each time you turn the sampler on or run a program until you reset the counter After replacing the pump tube reset the count to zero so that the sampler can begin tallying the pump counts for the new tube Ex ample 7 shows you how to reset the pump counts Replacing the pump tube does not reset the counter Experience may suggest a significantly different pump tube life You can change the alarm count to represent the pump tube life for your application Example 7 shows how set the alarm count 70 6700FR Refrigerated Sampler Pump Tube Replacement Checklist 1 Disconnect power from the sampler 2 Loosen the liquid detector s cover by unscrewing the black knob on top of the detector Unlatch the pump band The band is the rounded metal band that holds the tube in the pump 3 Pull the tube away from the bulkhead fitting Pull it from the pump and detector 4 Clean the pump rollers and the inside of the pump band 5 Thread the new tubing through the pump so that the tube follows its natural cu
196. nding of this subject It is dis turbing to see statements in print that do not reflect true conditions One of the most common errors is the assump tion that people have died from a lack of oxy gen The human body is able to function very well with substantially reduced oxygen concen trations No one worries about going to Santa Fe New Mexico elev 2 100 meters where the partial pressure of oxygen is equal to 16 2 a normal atmosphere is about 21 oxygen 6700FR Refrigerated Sampler When first going there a person may experi ence a little shortness of breath following exercise People in good health are not afraid to drive over the high passes in the Rocky Mountains At Loveland Pass oxygen pressure is 13 2 of a normal atmosphere At the top of Mt Whit ney oxygen is equal to 12 2 Many hikers go there and to higher peaks as well After ade quate acclimation they may climb to the top of Mt Everest where oxygen is equal to only 6 7 The lowest oxygen concentrations that I have observed in a sewer atmosphere was 13 per cent It was in a sealed chamber near sea level upstream from an inverted siphon on a metro politan trunk A man would be foolish to enter the chamber Without ventilation he might die but not from lack of oxygen It seems unlikely that anyone has ever died in a sewer from suffocation that is a lack of oxy gen Deaths have often been attributed to asphyxiation
197. ne of two ways Cautions identify a potential hazard which if not avoided may result in minor or moderate injury This category can also warn you of unsafe practices or conditions that may cause property damage Warnings identify a potentially hazardous condi tion which if not avoided could result in death or serious injury 6700FR Refrigerated Sampler Page 12 WARNING Changes or modifications to this unit not expressly approved by the party responsible for compliance could void the user s authority to operate the equipment Pages 14 and 37 M Note Read the Safety Summary posted at the front of this manual It outlines the electrical requirements and provides instructions for safe operation Page 69 CAUTION If the filter is not cleaned periodically damage due to overheated components may result Page 69 AA WARNING Removing the front or back panel exposes electri cal and mechanical hazards Disconnect power before performing any service activities Page 77 79 and 80 Removing the front and back panel exposes elec trical and mechanical hazards Troubleshooting and repair activities should be performed by a qualified refrigeration technician Page 77 and 79 All refrigeration repair work must be performed by a qualified refrigeration technician Always purge the system with nitrogen NEVER USE AIR to purge the system Always recover the refrigerant When recharging do not leave
198. ng the air to the ampoule by way of a tube as this 157 may change the H2S concentration Hang the ampoule in the air to be tested with a suction tube to the bulb or bellows Lead acetate paper is very useful as a qualita tive indicator It cannot be used to estimate the amount of sulfide but it will quickly turn black in an atmosphere containing only a tenth of a lethal concentration Electrodes or other similar electrical indicat ing devices for H2S in air have been marketed Some of them are known to be unreliable and we know of none that have proved dependable Do not use one unless you check it at frequent intervals against air containing known H2S concentrations A supposed safety device that is unreliable is worse than none at all Remember that the nose fails too when it comes to sensing dangerous concentrations of HS Various other toxic gases have been mentioned in some publications It is unlikely that any person has been asphyxiated in a sewer by any of those other gases except possibly chlorine The vapor of gasoline and other hydrocarbons is sometimes present in amounts that could cause discomfort and illness but under that condition the explosion hazard would be far more serious The explosimeter tests as well as the sense of smell would warn of the danger Pipelines in chemical plants might contain any number of harmful vapors They too are sensed by smell and explosimeter tests if they ge
199. ng RUN from the main menu Press J Enter after making your choice In this example NO is selected Run the program by selecting RUN and pressing Enter 17 6700FR Refrigerated Sampler Clock and Calendar Entering Times and Dates You may have to set the internal clock or calendar The samplers ENTER TIME AND DATE are shipped with their docks set to central time If your sampler op a HH MM DEMON YY erates in a different time zone you will have to reset the clock Ex ample 2 shows you how to find the time and date screen e Move from one field to another When setting the clock and calendar use a 24 hour clock for times by pressing the arrow keys and the day month year format for dates In screen e the illustration e Change a setting in a field by shows blanks for each position that accepts an entry The positions typing a number Press enter are called fields When screen e appears on your sampler the fields to accept the new setting contain the sampler s current settings for the time and date e To move from one field to another without changing the setting press the arrow keys Use this technique when you want to change only one or two settings e Change the setting by typing a new number Press Enter to accept the new setting For example to enter 2 00 p m 2 00 p m is 14 00 on a 24 hour clock type 14 Press J Enter Next type 0 zero for the minutes and press Enter To enter a date such as Jan
200. ng program 24 About Stored Programs After selecting a stored program re view the settings with the quick view screens Each sampling program stores all the settings required by the sampler to run a program These settings include the bottle kit information number of bottles and the bottle volume the suction line length the site description start times and so on If you use the same program at two sites each requiring different bot tle configurations suction line lengths or other details always check these settings before running a program You may need to make minor changes to the program to make sure the settings match your equipment Stored Programs and Reinitializing Reinitializing the sampler restores the program settings to the factory settings shipped with the sampler Only reinitialize the sampler when you can afford to lose the program settings Note If the Bottle Full Detect setting is critical to your sampling program always check this Hardware setting after you select a different Extended Program See Bottle Full Detect on page 94 6700FR Refrigerated Sampler Storage For Extended Programs The sampler stores five sampling programs one standard and four extended Program storage eliminates the need to reprogram the sampler with frequently used settings This feature is especially useful for complex extended programs such as two part programs or programs with many nonuniform time se
201. nt Solvent Solvent used in paint Solvent Simplest and Cheapest Safe Method of Testing H S Ampoule 5 by weight lead acetate solution Combustible gas indicator Oxygen defi ciency indica tor Oxygen deficiency indicator NO detector tube Oxygen defi ciency indicator Detectable odor at 0 015 ppm See compo nents Detectable taste and odor at low concentration Combustible gas indicator 1 Detectable odor at low concentrations 2 Combustible gas indicator Combustible gas indicator 6700FR Refrigerated Sampler Appendix D Replacement Parts REFRIGERATOR ASSEMBLY MODEL 6700 160 6700FR Refrigerated Sampler MODEL 6700 REFRIGERATOR ASSEMBLY i eo 2723 088 oneen FE E E E E 7 o 2 z 3 25 HEATER FLEX CRANKCASE 115 VAC 26 HEATER FLEX CRANKCASE 230 VAC 7 28 29 WELL NUT FASTNER FOR AIR TEMP SENSOR NOTE ITEM IS NOT SHOWN IN ILLUSTRATION 161 6700FR Refrigerated Sampler SEE APPENDIX A MODEL 6700 REFRIGERATOR ASSEMBLY V Ady ce0 c006 09 162 6700FR Refrigerated Sampler MODEL 6700 REFRIGERATOR ASSEMBLY RE KE E E EI I MV J 7 eE EO OAOA Ni TOP COVER ASSY REFRIG INCLUDES ITEMS 24 43 4 44 61 60 9004 259 EVAPORATOR PLATE COP TUBING amp HTR ASSY 115 VAC EVAPORATOR PLATE COP TUBING 4 HTR ASSY 230 VAC Tes 232 1 187 02 nur VEX IA 8 8 18 OOOO Les 60 9003 017
202. nt occurs See Pacing on page 82 6700FR Refrigerated Sampler Table 1 6700FR Sampler Features EXTENDED PROGRAMMING FEATURES CONTINUED Distribution Methods e Composite Samples deposited in a single large bottle e Sequential Only one sample placed in each bottle e Samples Per Bottle Multiple samples placed in each bottle e Bottles Per Sample One sample deposited in multiple bottles e Multiple Bottle Compositing combination of samples per bottle and bottles per sample distribution methods e Time Switched Bottles or Bottle sets Control the sample distribution using clock times See Distribution on page 84 Programmable Sampler Enable A 6700 sampler can be programmed to enable or disable a running sampling Pauses and Resumes Two Part Programming Auto Suction Head or Fixed Suction Head Suction Line Rinses Sampling Retries Three Flexible Start Time Settings Option for a Continuous Running Program program when readings received from a connected rain gauge module or YSI 600 Sonde meet certain conditions See Sampler Enable on page 87 Create intermittent sampling schedules See Pauses Resumes on page 88 Two part programming lets you set up a sampling program that divides the bottles into two groups filling each group according to separate pacing distribution sampler enable and pause and resume settings Ideal for storm water run off sampling See One Part and Two Part Programs on pa
203. od Mounting Rod Distributor Shaft Extension 1 4 20 Set Screw AA Aer E l Flat Washer Flat Washer Wing Nut Stop Arm Wing Nut Distributor arm T Nut End of discharge tube below neck of bottle Installing the Distributor Arm and Discharge Tube The distributor arm is adjustable so that you can position the dis charge tube over the bottles of each kit Each bottle kit also uses a discharge tube of a specific length Table 6 lists the correct dis charge tube length for each bottle kit If using bulk tubing to cut your own tubes cut the ends of the tube square not at an angle and cut the length accurately The two piece arm has four positions marked on the underside with the letters A B C and D Adjust the arm to the correct posi tion for the bottle kit being used Table 6 shows the correct position for each kit Thread the discharge tube through the spring and arm so that the tube protrudes from the arm 416 to Ys inch Attach the arm to the distributor shaft extension Secure the arm Distributor Arm to the extension with the black plastic nut Slide the free end of the discharge tube onto the bulkhead fitting After installing the dis tributor arm and discharge tube run the distributor to each bottle position to ensure proper installation 39 6700FR Refrigerated Sampler Table 6 Distributor Arm Positions and Discharge Tube Lengths for Bottle Kits 24 Bottle Kits e1000 millil
204. ogramming Pacing and Distribution os Gs sao hed tne ES 121 Extended Programming Programmed sampler Enable eiii taa 122 Extended Programming Quick View Programming Screens 123 Extended Programming Quick View Equipment Set Up 124 Extended Programming Quick View 111 41 42 43 44 45 46 47 48 O1 WIN I O 10 11 12 13 14 15 Pacing and Distribution 125 Extended Programming Quick View Programmed Sampler Enable 126 Extended Programming Hardware POPECE Sis LOL Moi Ei 127 Extended Programming Hardware Quick View Screens 128 Extended Programming YSI 600 AS ciato 129 Extended Programming Optional YSI PCS AN rate punta daa 130 Analog Output and Dialout Screens 131 Analog Output and Dialout Quick View DERCCHSL i pittori sete 131 Command Driven Screens 132 List of Examples Program One Sample every 15 Minutes One Sample in Each Bottle Using Normal Programming Style 16 Setting the Clock and Calendar 18 Changing the Programming Style 20 Selecting a Stored Extended Program 26 Standard Program Flow Paced Sampling Two Bottles Per Sample 28 Storm Water Runoff Sampling 30 Resetting the Pump Tube Warning 72 Resetting the Internal Battery Warning 76 List of Tables 6700FR Sampler Features
205. om the menu For example to run the sampling program select RUN to modify the program select PROGRAM 14 Table 5 About the Keypad K NAME On Off Stop Enter Help Down Right Arrow Up Left Arrow Numbers Decimal Point 588 too About the Display Backlight If you press a key and the screen does not seem to re spond it is probably because the keystroke turned the backlight on instead of acting on the screen 6700FR Refrigerated Sampler FUNCTION Turns the sampler on or off Stops the pump distributor or a running sampling program In programming screens returns to a previous screen Accepts a menu choice or number entry and goes to next screen In programming screens displays a brief help message Selects the menu option right or below the current choice Selects the menu option left or above the current choice Types a number Types a decimal point Selecting Menu Options In menu screens one menu option always blinks Press Enter when the blinking option is the one you want it will accept your choice and go to the next screen The Enter key always accepts the blinking option Select a different option by pressing an arrow key until the option you want blinks Then press Enter Entering Numbers Number entry screens prompt you to enter a value An example is shown in screen c on the next page To enter a number Press the number keys to type the number Then pres
206. onnecteur de type militaire deux prises qui se trouve sur le fil au dessus du r frig rateur Cette production de courant est destin e exclusivement aux contr leurs d chantillons de la s rie 6700 Le r frig rateur doit tre install prox imit d une prise de courant murale appro pri e Ne jamais se servir de rallonge La prise de courant doit tre visible et fac ile d acc s La seule fa on d teindre le r frig rateur est de le d brancher Pour diminuer le risque de choc lec trique le r frig rateur doit tre branch dans une prise de courant quip e d une fiche de terre L alimentation lectrique doit provenir d un circuit unique Le circuit ne doit ali menter aucun autre appareil Ne jamais faire fonctionner le r frig ra teur quand les panneaux inf rieur de devant ou de derri re sont enlev s Ne jamais faire fonctionner le r frig ra teur dans un environnement explosif Ne pas soulever ou porter le r frig ra teur Utiliser un appareil pr vu pour le transport des gros appareils lectriques Les fusibles doivent tre remplac s par d autres de m mes taille courant volt age et puissance Consulter la liste des pi ces de rechange pour obtenir le bon num ro de pi ce gt e RRE pD SYMBOLES DE SECURITE ET SIGNAUX DE DANGER Les ic nes plac es sur l chantillon r frig r mod le 6700FR ainsi que celles trouv es dans ce manuel d instructions avertissent l u
207. ords the rain gauge readings However with extended programming re Select YES cording the rain gauge readings and the rain enable option can be RAIN GAGE turned on or off Enter the hardware setup and follow screens 44 0 01 inch TIP and 45 in the margin Liquid Detector Disable USE LIQUID DETECTOR 0 1 mm TIP At screen 44 select YES to record the rain gauge readings and add The rain gauge is calibrated RAIN as a sampler enable option Continue with screen 45 and the for inches or millimeters sampler will then create a rain memory partition and update the Select the calibration of your available sampler enable conditions rain gauge Select NO to disable the readings and the sampler enable option When you select NO the sampler removes the rain memory parti tion leaving the memory space available for other reading types 92 6700FR Refrigerated Sampler YSI 600 Sonde Setup When you attach a sonde to the sampler you must configure the sampler s hardware setup The YSI 600 setup and calibration screens follow the rain gauge setup screens You can configure the sampler for any or all of the YSI 600 readings pH Dissolved Oxy gen Conductivity and Temperature The conductivity readings represent one of the following e Specific Conductance in mS cm millisiemens centimeter Requires a specific conductance temperature coefficient e Salinity in parts per thousand e Total Dissolved Solids T D S in gra
208. output is intended for 6700 Series Sampler controllers only The refrigerator must be installed near a suitable power outlet Never use an extension cord The power outlet must be visible and eas ily accessible Unplugging the refrigerator 1s the only means of disconnecting power To minimize the risk of electrical shock the refrigerator must be connected to an outlet with an electrical ground contact The power source must be a dedicated circuit The line must not power any other devices Never operate the refrigerator with the lower front or rear panels removed Never operate the refrigerator in an explosive atmosphere Do not lift or carry the refrigerator Use an appliance carrying device Fuses must be replaced with the required size current voltage and blow time spec ifications Refer to the Replacement Parts Listing for the correct part number gt e e pP SAFETY SYMBOLS AND HAZARD ALERTS The icons on the Model 6700FR Refrigerated Sam pler and those found within this instruction man ual alert the user of known hazards The icons are described below AN This icon identifies a general hazard Refer to the instruction manual for more information AN This icon indicates the risk of electrical shock Refer to the instruction manual for more information The instruction manual identifies the hazardous condition and any steps necessary to correct the condition The manual presents this information in o
209. oving the controller You must remove the controller when e The internal desiccant needs recharging the internal battery needs to be replaced or when the controller needs repair e You install a different bottle kit Each bottle kit has its own extension so that the distributor arm is positioned at the right distance above the bottles You must remove the controller to replace the extension Installing the Distributor Shaft Extension 1 Install the extension before mounting the controller on the refrigerator 2 Select the extension of the correct length for the bottle kit and screw it on the distributor shaft Secure it with the set screw See Figure 2 BE SURE THE SET SCREW IS TIGHTENED INTO THE DISTRIBU TOR SHAFTS KEY YOU MAY HAVE TO LOOSEN THE EXTEN SION SLIGHTLY AND ADJUST ITS POSITION Mounting the Controller 1 Install the four mounting rods into the bosses on the bottom of the case 2 Fit the mounting rods through the four holes drilled in the top of the refrigerator 3 Slip a washer on each rod and secure the controller by tight ening the wing nuts 4 Install the distributor arm and discharge tube 5 Thread the stop arm into the hole in the side of the extension Be sure the stop arm is directly above the distributor arm 6 Connect the power cable to the controller 38 6700FR Refrigerated Sampler Figure 2 Mounting the Controller Multiple Bottle Sampling Composite Sampling Mounting R
210. ow Rate and Line Transport Velocity Maximum Suction Head Pump Tube Life Controller only 13 0 lbs 5 9 kg With pump tube 13 2 lbs 6 0 kg Length 10 3 in 26 0 cm Width 12 5 in 31 7 cm Height 10 in 25 4 cm Operational 32 F to 120 F 0 C to 49 C Storage 0 F to 140 F 18 C to 60 C NEMA 4X and 6 Pump IP17 Enclosure IP67 The ability to deliver the programmed sample volume 10 ml or 10 of programmed value whichever is greater The ability to repeat the delivered volume for a set of samples collected under the same conditions 5 ml or 5 of the average of the maximum and minimum sample volume in a sample set whichever is greater Suction Head Flow Rate Line Transport Velocity 3 feet 3 9 liters per minute 3 0 ft s 0 91 m s 5 feet 3 9 liters per minute 3 0 ft s 0 90 m s 10 feet 3 7 liters per minute 2 9 ft s 0 87 m s 15 feet 3 6 liters per minute 2 7 ft s 0 83 m s 20 feet 3 3 liters per minute 2 5 ft s 0 77 m s 23 feet 3 1 liters per minute 2 3 ft s 0 71 m s 25 feet 2 8 liters per minute 2 2 ft s 0 66 m s The maximum suction head is the vertical height at which a sample can be taken 28 ft 8 5 m at 30 inHg 762 mmHg Tube life may vary depending on the abrasiveness of the sample liquid Recommended maximum 1 000 000 pump counts This equates to 912 standard samples A standard sample is 200 ml at 5 ft 1 5 m suction head using a 10 ft 3 m vinyl suction line 6700 CONTR
211. ow module is attached the flow source may be the module s flow volume Otherwise it is the flow pulse count received at the external flow meter connector You enter the amount of flow required for each 10 ml of liquid When the sample event is initiated the sample volume will be based on the flow that has occurred since the last sample This sample volume will be at least 20 ml but not more than the bottle volume or 9990 ml whichever is smaller With flow dependent sample volumes the sampler resets the flow volume count at the start time Therefore the sampler will not take a sample at the start time Suction Head Suction head is the vertical distance between the surface of the liq uid source and the sampler s pump At each sample event the sam pler determines the suction head automatically In extended programming you can manually enter the suction head if you want Select ENTER HEAD only when the head remains stable and you can measure it accurately Rinses and Retries Rinses and retries are extended programming features You can program the sampler to rinse the suction line automatically Dur ing a line rinse cycle the sampler draws liquid through the line to the liquid detector As soon as it detects liquid the sampler revers es the pump to purge the line The sampling retries feature lets you set the number of times from 0 to 3 that the sampler tries to detect liquid in the line before skip ping the sample screen 2
212. p ischen CEE 7 7 Stecker aus ger stet und nur zur Verwendung mit 230 VO 50 60 Hz bestimmt Die Stromquelle sollte f r 16 Ampere Betrieb ausgelegt sein K hlschr nke beider Konfigurationen liefern 12 5 V bei 5 Ampere f r den Probenehmer Controller Diese Ausgabe stammt vom zweipoligen Anschlu am Kabel oben am K hlschrank Diese Ausgabe ist nur f r die Probenehmer Controller der Serie 6700 bestimmt Der K hlschrank mu in der N he einer geeigneten Steckdose aufgestellt werden Es darf kein Verl ngerungskabel verwendet werden Die Steckdose mu sichtbar und leicht zug nglich sein Der K hlschrank kann nur durch Herausziehen des Netzkabels ausgeschaltet werden Um die Gefahr von Elektroschocks zu vermindern mu der K hlschrank an einer geerdeten Steckdose angeschlossen werden Die Stromquelle mu ein dedizierter Stromkreis sein d h die Leitung darf keine anderen Ger te mit Strom versorgen Der K hlschrank darf niemals betrieben werden wenn die unteren Frontplatten vorne oder hinten entfernt sind Der K hlschrank darf nicht in einer Umgebung wo Explosionsgefahr besteht betrieben werden Der K hlschrank darf nicht angehoben oder getragen werden sondern nur mit einem Ger t zum Transport von Instrumenten oder Ger ten fortbewegt werden Bei Erneuerung der Sicherungen sind die vorgeschriebene Gr e Stromst rke Spannung und Durchbrennspezifikationen einzuhalten Die entsprechende Ersatz
213. page 111 See Note B amp C FIRST SAMPLE AFTER A NO DELAY TO START DELAYED START CLOCK TIME WAIT FOR PHONE CALL See Note A _ MINUTE DELAY 1 999 See Note D FIRST SAMPLE AT HH MM SELECT DAY S SU MO TU WE TH FR SA gt AT LEAST ONE DAY MUST BE SELECTED DONE FIRST VALID DAY Extended Programming Only PROGRAMMING COMPLETE RUN THIS PROGRAM NOW YES NO RUN See Run Time Screens on page 50 PROGRAM VIEW REPORT OTHER FUNCTIONS See Note E Notes A The WAIT FOR PHONE CALL option appears when using the optional Telephone Commands See Chapter 6 B Appears for standard START FLOW COUNT AFTER A flow paced programs MINUTE DELAY 1 999 C Appears for extended a 1 rograms prog _ MINUTE DELAY 1 999 D Appears for standard START FLOW COUNT AT flow paced programs HH MM E Main menu for RUN EXTENDED 1 extended PROGRAM j VIEW REPORT A OTHER FUNCTIONS 112 6700FR Refrigerated Sampler Figure 27 Standard Programming Quick View Programming Screens If SITE STOP key SITE DESCRIPTION ABCDEFGHIJKLMNOPQRST pressed SAVE CHANGES FACTORY UVWXYZ amp 0123456789 YES NO BACK UP DONE UNITS SELECTED LENGTH ft See Figure 33 Quick View Module Setup on page 118 5 MINUTE DATA INTERVAL NUMBER OF BOTTLES BOTTLE VOLUME IS 1 2 4 8 12 24 m 300 30000 ml BOTTLES
214. panel frontal y posterior se exponen peligros el ctricos y mec nicos Solamente los t cnicos de refrigeraci n capacitados deben encargarse de solucionar los problemas y real izar las actividades de reparaci n necesarias Pagina 77 y 79 N PRECAUCION Todos los servicios reparativos de refrigeradores deben ser realizados por t cnicos de refrigeraci n calificados Siempre limpie el sistema utilizando nitr geno NUNCA USE AIRE para limpiarlo Reponga siempre el refrigerante que sea necesario Al recargar no deje una v a lateral en el sistema de refrigeraci n porque puede ocasionar problemas de corrosi n o fugas 6700FR Refrigerated Sampler Table of Contents 1 Introduction ie 1 About 700 Series Modules 1 About YSLS0oNdeSs is ere sis russes 1 Memory to Store Data 1 About this Manual 2 Pump Requirements 2 Gettine Helpisssrssdisieeheliaba lese aa 2 2 Programming ua 14 G ttine Startel siriani aude 14 Using Menus and Entering Numbers 14 Selecting Menu Options 15 Entering Numbers 15 Stored Data Will Be Lost 16 Clock and Calendar 18 Menu Screens Clock Start Times 18 Menu Screens Site Descriptions and Program Names 19 Quick View Screens 20 Paging Through Quick View Screens 20 Changing S
215. ple and postsample purges When sampling in near freezing tempera tures thorough drainage reduces the chances of frozen liquid blocking the line Avoid loops of coiled line Intake Placement For representative samples place the intake in the main current of the flow stream not in an eddy or at the edge of the flow Placing an intake at the bottom may produce samples with excess heavy solids and no floating materials while placement at the top may produce the opposite conditions Positioning a Sampler Place the refrigerator on a relatively flat horizontal surface if pos sible The refrigerator does have leveling feet Adjust the feet to keep the refrigerator level If the refrigerator is not level the sam ple may miss the bottle mouth When installing the sampler be sure the vertical distance between the level of the liquid source and pump is as small as possible Connecting External Instruments Flow Meter Connector Connect the sampler to Isco flow meters flow loggers PAL 1101s or 1640 Liquid Level Actuators by attaching their connect cable to the Flow Meter Connector When using the sampler with an external instrument remember these guidelines e Both the sampler and the flow instrument must be on and run ning a program e Ifusing a flow meter or flow logger for flow pacing the sampler and the flow instrument must both run programs with flow pac ing settings e Ifusing a flow meter or flow logger for trigger pacing
216. ple 6 Storm Water Runoff Sampling continued 24 25 WEIR ORIFICE TYPE V NOTCH ROUND FLOW INSERT SIZE 6 8 10 12 NEW MODULE SETUP STORED DATA WILL BE LOST OK YES NO CURRENT LEVEL IS 0 5 ft ADJUST LEVEL TO 0 500 ft DATA STORAGE INTERVAL IN MINUTES 1 22 56 10 15 30 NUMBER OF BOTTLES 1 2 4 8 12 24 BOTTLE VOLUME IS 1000 ml 300 30000 SUCTION LINE LENGTH IS 5 ft 3 99 AUTO SUCTION HEAD ENTER HEAD 0 RINSE CYCLES 0 3 RETRY UP TO 0 TIMES WHEN SAMPLING 0 3 ONE PART PROGRAM TWO PART PROGRAM 24 BOTTLES AVAILABLE ASSIGN BOTTLES 1 THRU 6 TO PART A 1 23 Select ROUND Select 12 Select YES Press ENTER Press ENTER Select 24 Enter 1000 Enter 5 Select AUTO SUCTION HEAD Enter 0 Enter 0 Select TWO PART PROGRAM Enter 6 Screen will say Beginning Part A before proceeding with screen 27 32 6700FR Refrigerated Sampler Example 6 Storm Water Runoff Sampling continued 39 UNIFORM TIME PACED FLOW PACED EVENT PACED NONUNIFORM TIME TIME BETWEEN SAMPLE EVENTS O HOURS 5 MINUTES 1 BOTTLES PER SAMPLE EVENT 1 6 SWITCH BOTTLES ON NUMBER OF SAMPLES TIME SWITCH BOTTLES EVERY 1 SAMPLES 1 50 RUN CONTINUOUSLY YES NO DO YOU WANT SAMPLE VOLUMES DEPENDENT ON FLOW YES NO SAMPLE VOLUME 800 mi 10 1000 ENABLE O RAIN LEVEL FLOW Y pH Y TEMP Y COND Y D O NONE ENABLE RAIN AND OR DONE E
217. ples at FIRST SWITCH TIME screen 17 each sample event P Switch times occur regardless of the state of the sampler Be aware SWITCH BOTTLES ON NUMBER OF SAMPLES that the sampler may leave empty bottles if it becomes disabled TIME Pause and resumes are an exception the sampler will not switch bottles during a pause if the current bottle is empty Select TIME Ifthe program settings instruct the sampler to take a sample at the start time the sampler also draws a sample at the switch time SWITCH BOTTLES EVERY When this occurs the pacing will also be reset at the switch time ere MINES Time overrides can also be used with flow paced programs that do not take asample at start These programs will place a sample in the current bottle if it is empty at the switch time and then move to the next bottle set This sample is called a time override sample and en FIRST SWITCH TIME sures that at least one sample is taken into each bottle Pacing inter AT _ vals are reset at every switch time e Enter the time between bottle switches When you use the time switching feature the volume in each bottle or bottle set may vary Sample volumes that would exceed the bot tle capacity are not taken and a PROBABLE OVERFILL message 1s logged e Enter the first bottle switch time Continuous Sampling Sample programs can be run indefinitely by selecting YES at the RUN CONTINUOUSLY screen Continuous samp
218. pm and pulmonary congestion edema and central nervous system effects occurred at a vapor concentration of 750 000 ppm Cardiac sensitization occurred in dogs at 75 000 ppm from the action of exogenous epinephrine No effects in animals occurred from repeated inhalation exposures to 99 000 ppm for two weeks or to 50 000 ppm for three months Repeated exposures to higher concentations caused transient tremors incoordination and some organ weight changes Long term exposure produced increased testes weights and increased urinary fluoride levels No adverse effects were observed in male and female rats fed 300 mg kg day of HFC 134a for 52 weeks Animal testing indicates that this compound does not have carcinogenic or mutagenic effects Inhalation of 50 000 ppm for two years caused an increase in benign testicular tumors in male rats No effects were observed at lower concentrations The tumors were late occurring and were judged not to be life threatening Embryotoxic FIGA has been observed in some animal tests but only at maternally toxic dose levels DISPOSAL CONSIDERATIONS Waste Disposal Contaminated HFC 134a can be recovered by distillation or removed to a permitted waste disposal facility Comply with Federal State and local regulations TRANSPORTATION INFORMATION Shipping Information Shipping Containers Tank Cars Tank Trucks DOT IMO Proper Shipping Name LIQUIFIED GAS N 0 S TETRAFLUOROETHANE ee Class 2 2 0 19
219. program oper ate install and maintain a 6700FR refrigerated sampler There are six chapters and five appendices e Chapter 1 Introduction lists the features available with the 6700FR refrigerated sampler e Chapter 2 Programming shows how to program the sampler Np REN e Chapter 3 Operation provides installation guidelines and in You may find two sections in this structions for running a sampling program manual most helpful Chapter 2 A E l Programming shows you how to Chapter 4 Maintenance covers the basic maintenance re program the sampler and Chapter quired to keep your sampler in top operation condition 5 Reference explains the features e Chapter 5 Reference explains the advanced features and how It includes discussions on these key to use them topics e Chapter 6 Program Options explains specialized software fea Distribution tures that can be enabled for use e Pacing The appendices are Start Times Sampler Enable e Appendix A Menu Charts Piness and SIGS e Appendix B Material Safety Data Sheets e Memory e Appendix C General Safety Procedures e Appendix D Replacement Parts e Appendix E Accessories List Pump Requirements The pump requires a pump tube made specifically for the 6700 sampler These pump tubes are easily recognized by their blue alignment collars The 6700 pump tube is different from other types of tubing including the pump tubes for Isco s earlier model samplers
220. r on page 91 If the arm does not stop over each bottle re adjust the rack NEVER MANUALLY ROTATE THE DISTRIBUTOR ARM 42 6700FR Refrigerated Sampler Figure 5 Installing 2 Bottle Kit Install the distributor shaft extension Use the 5Y4 inch extension for the 2 bottle kit The instructions on page 38 show you how to remove the controller and replace the extensions for each bottle kit Next replace the controller and adjust the distributor arm to position A Install the O O O O O O arm and stop See Installing the Distribu tor Arm and Discharge Tube on page 39 Install over the mounting plate at the bot tom of the refrigerator the locating base which holds the 2Y2 gallon glass or 2 gal lon polyethylene bottles Begin by loosening the ramps Move toward the front of the compartment so that they will fit under the ridge of the lo cating base You can also remove completely Remove the two front stops and align the holes on the sides of the locating base with the holes for the stops in the mount ing plate Secure the base by replacing the stops Install the bottles and position the arm over each bottle See Moving the Distribu tor on page 91 them them Secure the base NEVER MANUALLY ROTATE Ramps located under locating base THE DISTRIBUTOR ARM Pull them to the front or remove them Removing Racks Before removing the rack place the lids on the bottles so the sam ples
221. rator use two padlocks one for the top cover and one for the door Table 8 Connecting Isco Instruments to the Sampler CONNECTOR ICON Power Source Rain Gauge Interrogator Flow Meter CONNECT THESE INSTRUMENTS E x e 12 volt power source e674 Rain Gauge 6 ae e Programmable I O Pins pins C H and I N e YSI Sonde e Refrigerator Temperature Sensor e581 RTD Rapid Transfer Device 4 e 3770 Field Printer e IBM PC or compatible computer running Flowlink or SAMPLINK ePAL 1101 e 1640 Liquid Level Actuator e 3200 Series Flow Meters Ent e4100 Series Flow Loggers e4200 Series Flow Meters e Master Slave Sampler e Pulse Duration Input Interface e 4 20 mA Input Interface 48 6700FR Refrigerated Sampler Running Programs To run a standard or extended program select RUN from the main menu You may also select YES at the RUN THIS PROGRAM NOW screen at the end of the programming screens This is illus trated in Figure 7 Extended programs scheduled to start at a clock time will not start until the programmed clock time on or after the first valid date Note that if you have recently calibrated a parameter probe the sampler may delay the start and display PLEASE WAIT until valid readings are expected from the probe The delay accounts for the time typically required to install the probe and lasts for five minutes after you complete the calibration Figure 7 Running a Program If
222. re than twice or less than half the programmed volume e Select YES when the volume delivered matches the volume displayed on this screen e Select NO to enter the volume delivered 66 Chapter Contents e Maintenance Screens 67 e Maintenance Checklist 68 e Cleaning Guidelines 68 Cleaning Protocols for Priority Pollutants ia 69 Replacing the Pump Tube 70 Opening the Controller Case 73 Recharging the Desiccant 74 Replacing the Internal Battery 75 e Servicing the Refrigerator 77 e Refrigeration System 79 e Troubleshooting Guide 79 Diagnostic Screens RUN PROGRAM 1 VIEW REPORT OTHER FUNCTIONS e Select OTHER FUNCTIONS MAINTENANCE MANUAL FUNCTIONS 2 PROGRAMMING STYLE e Select MAINTENANCE SET CLOCK SET PUMP TUBE ALARM 3 INTERNAL BATTERY DIAGNOSTICS e Select DIAGNOSTICS PLEASE WAIT 4 RAM PASSED TEST e If the RAM fails the diagnostic test the sampler reports RAM FAILED TEST Contact Isco Customer Service for as sistance 6700FR Refrigerated Sampler Chapter 4 Maintenance Maintenance Screens The maintenance screens include e Set the sampler s clock e Set the number of pump counts for the pump tube warning e Reset the battery warning for the internal battery e Run a set of diagnostic tests on the RAM ROM Read Only Memory character locations on the display pump distributor and
223. rm condition exists e use the optional Phone Commands to control the samplers operation from a remote location See Chapter 6 When programming the sampler press the Help key for a brief help note All help topics appear in the index See Help Notes on page 21 6700FR Refrigerated Sampler Table 1 6700FR Sampler Features SAMPLE DELIVERY SYSTEM FEATURES Two Programming Levels Peristaltic Pump LD90 Liquid Detector Two Line Purges in Sampling Cycle Easy Grab Samples Vinyl and Teflon Suction Lines Standard programming lets you set up typical sampling programs quickly Extended programming includes all features available in standard programming plus additional features See Standard and Extended Programming on page 28 e Benefits Liquid moves continuously under pumped flow The pump has no metering chambers or gravity fed internal tubing to trap sediment or residual liquid Sample liquid contacts only the strainer suction line tube coupling pump tube bulkhead fitting and sample bottles eNonwetted Detection Sample liquid never touches the detector The sampling cycle always includes a presample purge and postsample purge that clears the suction line of residual liquid Simply disconnect the pump tube from the bulkhead fitting on the center section and place the pump tube over your sample container See Grab Samples on page 65 8 inch ID Inside Diameter vinyl line 8 inch ID Teflon
224. rong sulfur like odor Mostly a simple asphyxiant May be practically odorless tasteless Colorless pungent odor Suffocating cor rosive poisonous non flammable Colorless benzene like odor Colorless Characteris tic odor Colorless flammable Specific Gravity or Vapor Density Air 1 Variable 3 14 4 84 3 66 Percentages shown represent volume of gas in air Mostly methane and carbon dioxide with small amounts of hydrogen nitrogen hydrogen sulfide and oxygen occasionally traces of carbon monoxide Physiological Effect Impairs sense of smell rapidly as concentra tion increases Death in few minutes at 0 2 Exposure to 0 07 to 0 1 rapidly causes acute poisoning Para lyzes respiratory cen ter Acts mechanically to deprive tissues of oxy gen Does not support life Physiologically inert 60 to 150 ppm cause irritation and coughing Asphyxiant 100 ppm dangerous 200 ppm fatal Normal air contains 20 8 of O Man can tolerate down to 12 Minimum safe 8 hour exposure 14 to 16 Below 10 dangerous to life Below 5 to 7 probably fatal Max naturally occur ring level is 0 04 ppm 0 05 ppm causes irrita tion ofeyes and nose 1 to 10 ppm causes headache nausea can cause coma Symp toms similar to radia tion damage Will not support life Inflammation of the eyes 400 to 500 ppm immediately fatal At 200 500 ppm head ac
225. rs zum Betrieb des Ger ts aufheben N D pal o gt ct D pd N Seiten 14 und 37 M HINWEIS Bitte die Zusammenfassung zu den Sicherheitsbestimmungen zu Beginn dieses Handbuchs lesen Sie fa t die elektrischen Anforderungen zusammen und gibt Anweisungen f r den sicheren Betrieb VORSICHT Der Filter mu periodisch gereinigt werden um Besch digung von Komponenten durch berhitzung zu vermeiden UN gt O pad co D co AA WARNUNG Bei Abnahme der vorderen oder hinteren Frontplatte werden elektrische und mechanische Gefahrenquellen freigelegt Vor Durchf hrung von Servicearbeiten stets das Netzkabel herausziehen Un O pad O co Seite 77 79 und 80 Beim Entfernen der vorderen und hinteren Frontplatten werden elektrische und mechanische Gefahrenquellen freigelegt Fehlersuche und Reparaturarbeiten sollten nur durch einen K hlsystemexperten durchgef hrt werden Seite 77 und 79 Alle Reparaturarbeiten am K hlsystem m ssen durch einen Spezialisten f r K hlungssysteme durchgef hrt werden Das System nur mit Stickstoff NIEMALS MIT LUFT sp len Das K ltemittel immer wiederaufbereiten Beim Wiederf llen niemals ein Abzweigventil im K hlsystem lassen da dies Korrosion oder Undichtigkeit zur Folge haben k nnte 6700FR Refrigerated Sampler Resumen de seguridad El modelo 6700FR Refrigerated Sampler es un dispositivo con un prop sito definido que se puede utilizar sola
226. running a program MODULE you must interrupt the program See Interrupting a Running HARDWARE Program on page 52 Select MANUAL FUNCTIONS To take a grab sample GRAB SAMPLE 1 Disconnect the pump tube from the bulkhead fitting CALIBRATE VOLUME 2 3 OPERATE PUMP MOVE DISTRIBUTOR 3 Follow the steps in Taking a Grab Sample in the margin 4 e Select GRAB SAMPLE Place the end of the tube over a collection container Reconnect the pump tube to the bulkhead fitting Figure 12 Taking a grab sample SAMPLE VOLUME 4 mi 10 9990 Enter the desired volume GRAB SAMPLE 5 PRESS WHEN READY PURGING SUCTION LINE PUMPING 200 ml PURGING SUCTION LINE GRAB SAMPLE CALIBRATE VOLUME 9 OPERATE PUMP MOVE DISTRIBUTOR Press stop to return to main menu 65 6700FR Refrigerated Sampler Calibrating Sample Volumes Calibrating RUN The sampler delivers accurate sample volumes without calibration 1 ent If you find that sample volumes vary significantly from the pro OTHER FUNCTIONS grammed values first check the suction line for proper installation Select OTHER FUNCTIONS Be sure it slopes continuously downhill to the liquid source and NENT drains completely after each sampling cycle Then compare the ac MANUAL FUNCTIONS tual length of the suction line to the suction line length settings in MODULE the program to see that they match Also check the pump tube for HARDWARE e Select MANUAL
227. rve around the pump rollers You may need to move the pump rollers to make the installation easi er 6 The blue collars on the tube help align the tube in the detec tor and pump Align the tube by placing the collars in the grooves inside the liquid detector 7 Close the detector s cover and tighten the black knob Close the pump band and latch it 8 Reset the pump tube counter See step 5 in Example 7 9 Take a dry manual sample to test the tube installation See Grab Samples on page 65 Figure 13 Removing and replacing the pump tube 71 6700FR Refrigerated Sampler Figure 14 Positioning the pump tube Example 7 Resetting the Pump Tube Warning RUN Select OTHER FUNCTIONS PROGRAM 1 VIEW REPORT OTHER FUNCTIONS MAINTENANCE Select MAINTENANCE MANUAL FUNCTIONS 2 PROGRAMMING STYLE HARDWARE SET CLOCK Select SET PUMP ALARM SET PUMP ALARM 3 INTERNAL BATTERY DIAGNOSTICS The sampler displays this screen briefly to give you the current pump count 4 1024000 PUMP COUNTS information The first line shows you the pump counts tallied since the WARNING AT 1000000 counter was last reset The second line shows the current alarm setting 1024000 PUMP COUNTS To reset the counter to zero select YES Always reset the counter after 5 RESET Wee co replacing a pump tube Select NO when merely checking the current count WARNING AT 1000000 If necessary change the pump count alarm setting by typing th
228. s One Sample in Each Bottle Using Normal Programming Style 6700 SAMPLER STANDARD PROGRAMMING Turn the sampler on by pressing the On Off key Press Enter 1 For HELP at any screen press key This screen disappears on its own after 8 seconds RUN NIE PROGRAM The option PROGRAM will be blinking Press 4 Enter 2 VIEW REPORT OTHER FUNCTIONS sl en The option NO will be blinking Press Enter 3 CHANGE For the purposes of this example it isn t necessary to change the description YES NO SELECT UNITS FOR LENGTH The option ft will be blinking press Enter 4 ft DATA STORAGE 4 i INTERVAL IN MINUTES The 1 option will be blinking Press J Enter 1 2 5 10 15 30 Select the number of bottles in your bottle kit by pressing either arrow key 6 de A until the correct number blinks Press Enter For this example select 24 BOTTLE VOLUME IS Type the volume for the bottles in your kit For this example 1000 is correct 7 1000 ml 300 30000 so simply press Enter 16 Example 1 Continued SUCTION LINE LENGTH IS 10 ft 3 99 TIME PACED FLOW PACED TIME BETWEEN SAMPLE EVENTS O HOURS 15 MINUTES SEQUENTIAL BOTTLES SAMPLE SAMPLES BOTTLE RUN CONTINUOUSLY YES NO SAMPLE VOLUME 200 ml 10 1000 NO DELAY TO START DELAYED START 14 CLOCK TIME FIRST SAMPLE AFTER A 15 5 MINUTE DELAY 1 999 PROGRAMMING COMPLETE RUN THIS PROGRAM 16 NOW YES NO
229. s III VIII ana XII for additional information SECTION XII ECOLOGICAL INFORMATION ECOTOXICITY No data avallable ENVIRONMENTAL FATE No data available SECTION XIII DISPOSAL CONSIDERATIONS US EPA Waste Number Not Regulated Federal state and local disposal laws and regulations will determine the proper waste disposal recycling reclamation procedures NOTE Chemical additions processing or otherwise altering this material may make the waste management information presented above incomplete inaccurate or otherwise inappropriate As local regulations may vary all waste must be disposed recycled re claimed in accordance with federal state and local environmental control regulations 144 6700FR Refrigerated Sampler ENGELHARD Page 7 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 SECTION XIV TRANSPORT INFORMATION INTERNATIONAL UN Number Not Regulated UNITED STATES EPA Waste Number Not Regulated DOT Classification Not Regulated CANADA PIN Number Not Regulated TDG Class Not Regulated EG DGL Not Regulated SECTION XV REGULATORY INFORMATION US FEDERAL REGULATIONS TSCA IN TSCA SARA 311 AND 312 HAZARD CATEGORIES IMMEDIATE Acute Health Hazard NO DELAYED Chronic Health Hazard YES FIRE Hazard NO REACTIVITY Hazard NO Sudden Release of PRESSURE NO SARA SECTION 313 NOTIFICATION This product does not contain toxic chemicals subject to the reporting requirements of Section
230. s J Enter As soon as you press Enter the sampler saves your number and moves to the next screen In some screens you use the J Decimal Point key in a number 15 6700FR Refrigerated Sampler Entering Numbers Some screens display the range of acceptable numbers between pa rentheses If you enter a number that is too low or high the control ler beeps and erases the entry Type a new number and continue SUCTION LINE LENGTH C IS__ ft 3 99 Stored Data Will Be Lost Type the length of the suction line Acceptable values are Changes to the data storage interval module setup hardware set shown between the up or selecting a new stored program make it necessary for the parentheses Press enter to sampler to reformat its memory See Memory on page 100 Refor accept the number matting the memory clears any stored data sample events and readings recorded during the last running program As a precau tion the sampler displays a message screen d If you do not need the stored data select YES The sampler will re format its memory according to your menu selection and display the new memory capacity INTERVAL CHANGED If you need to collect or view the data select NO The sampler will ala ze ignore your last menu selection s and retain the stored data Exit YES NO programming by pressing the STOP key and collect the data See Sampling Reports on page 54 Example 1 Program One Sample every 15 Minute
231. sed samples The source and error codes appear with explana tions at the end of the report A list of codes appears in Table 9 The last column in the Sampling Results report records the pump counts for the sample event Large variations in pump counts from event to event indicate fluctuating heads a relocated suction line or a temporarily clogged strainer Combined Results Report At the time of each sample event the sampler records the readings from each connected module rain gauge or YSI Sonde The Com bined Results report presents the event time sample and bottle number and the respective readings from the device For flow mod ules the readings are level and flow rate For the pH module the readings are temperature and pH For the 4 20 mA Input module the readings vary according to your programmed selections For the rain gauge and YSI Sonde the readings vary according to the selections enabled during the hardware setup When recording four or more YSI parameters the Combined Results report will exceed the standard 40 character width To read the additional columns the data must be collected with Flowlink 4 for Windows software Combined Results reports appears in Figure 10 Summary Report When a module and rain gauge are connected to the sampler the data is the same as the Combined Results report When printing the Summary report it lists the information and also graphs the rainfall data and module data A Summary report
232. setup 93 I VO pin programming 96 Installation and operation checklist 37 Installing connecting flow loggers 48 flow meters 48 PAL 1101 pH Loggers 48 distributor arm 39 173 6700FR Refrigerated Sampler locating base for 2 bottle kit 43 Internal battery battery warning 75 replacing 75 Interrupting interrupting a running program 52 manual paused operation 52 K Keys function of keys 15 L Liquid detector enable disable 92 Locating base 2 bottle kit 43 M Maintenance air filter 69 cleaning bottles 68 controller 68 delivery system 68 guidelines 68 protocols for bottles and tubing 69 refrigerator 68 strainers 68 condenser coil 69 internal battery 75 maintenance programming screens diagnostics 67 pump counts for pump tube warning 70 pump tube alarm 70 pump tube 70 refrigerant charge capacity 79 refrigerator troubleshooting guide 79 technical service information 77 80 Manual functions 91 calibrate volume 91 grab samples 91 moving distributor 91 taking grab samples 65 Manual paused operation 52 54 Manual samples 65 Materials used in sampler construction Materials Safety Data Sheets 133 153 Memory 4 100 capacity 101 creating partitions 100 data storage interval 100 partition sizes 100 roll over 101 sampling results 100 stored data will be lost 16 triggered 101 Menu screens 14 19 110 132 Module summary report see Sampling reports Modules 700 series modules 1 displayed readings 50 programming 2
233. sien 60 1684 093 924 Battery Backed Power Pack 240 volt 60 3004 160 940 Lead Acid Baley 6 015 ine as AS AS EE A A ed 60 3004 106 Isco Power Products QUIE ri AA an le e helene 60 9003 092 Modules PALs Rain Gauges amp Interfacing Instruments Note Additional accessories for modules and interfacing instruments appear in the accessories list at the back of the manual for each module or instrument 701 pH Module with Double Junction pH Sensor with Temperature Sensor 68 6700 052 701 pH Module with Single Junction pH Sensor with Temperature Sensor 68 6700 051 TAO Ultrasonic Flow Module 2 2422 A A ai He ORAS ei 68 6700 049 720 Submerged Probe Module 10 range 68 6700 068 720 Submerged Probe Module 30 range 2 hh dS A AA AA AS a 68 6700 069 130 Bubble Flow Modules rer ra re are dar den 68 6700 050 780 Analos Intertace Module 2 0 ae AA AA A 68 6700 048 PAL Parameter Actuator Logger 1101 with Single Junction Probe 68 1110 004 PAL Parameter Actuator Logger 1101 with Single Junction Probe 68 1110 005 674 Ran Gate LO Fach ID Iii er ee ai a te 60 3284 001 674 Ram Gauge 0 1 Milimeter Ip sia ee a dari 68 3280 001 1640 Liquid Level Actuators as 6 402 nee SA oil ia ia Me 60 1644 000 4 70 mA Sampler Input Interface is iaia pedala rateali 60 37
234. silica quartz Inhalation of crystalline silica in the respirable range in excess of the TLV may result in an increase in the risk of serious respiratory disease Avoid breathing the dust Use NIOSH MSHA approved respirators when the TLV for crystalline silica may be exceeded Updated April 4 1994 Page 2 149 6700FR Refrigerated Sampler MATERIAL SAFETY DATA SHEET DESI PAK Packaged Desiccant Crystalline silica is listed by the International Agency for Research on Cancer IARC as a 2A sufficient evidence in laboratory animals and limited evidence of carcinogenicity in humans CARCINOGENICITY NTP NO IARC YES OSHA NO First Aid Inhalation Remove to fresh air immediately If breathing has stopped give artificial respiration Keep affected person warm and at rest Get medical attention immediately First Aid Ingestion If large amounts have been ingested give emetics to cause vomiting Stomach siphon may be applied as well Milk and fatty acids should be avoided Get medical attention immediately First Aid Eyes Wash eyes immediately and carefully for 30 minutes with _ running water lifting upper and lower eyelids occasionally Get prompt medical attention First Aid Skin To avoid repeated or prolonged contact with this chemical use good hygienic practices Wash with soap and a large amount of water Get medical attention if irritation or inflammation develops SECTION VI REACTIVITY DATA Reacti
235. sti e riparazione devono essere affidate a tec nici frigoristi qualificati Page 77 and 79 AL AVVERTENZA Tutti i lavori di riparazione devono essere eseguiti da tecnici frigoristi qualificati Utilizzare azoto per spurgare il sistema NON UTI LIZZARE ARIA Recuperare sempre il refrigerante In fase di ricarica non lasciare i rubinetti di linea nel sistema di refrigerazione per via della possibilit di corrosione e di trafilamenti 6700FR Refrigerated Sampler Zusammenfassung Sicherheit Der gek hlte Probenehmer Refrigerated Sampler Modell 6700FR ist ein Ger t f r einen bestimmten Zweck das nur mit kompatiblen Isco Ger ten verwendet werden darf Es darf nicht mit Ger ten anderer Hersteller oder f r andere Zwecke verwendet werden Verwendung f r andere als in diesem Handbuch beschriebene Zwecke kann Verletzung von Personen oder Besch digung des Ger ts zur Folge haben Elektrische Anforderungen Der Kihlschrank ist in zwei Konfigurationen 120 Vu und 230 VA erh ltlich Die erforderliche Betriebsspannung f r den K hlschrank ist auf dem Kenn und Seriennummernetikett innen an der Probefacht r vermerkt K hlschr nke mit der 120 VU Konfiguration sind mit einem in Nordamerika blichen NEMA 5 15P Stecker ausger stet und nur zur Verwendung mit 120 VU 60 Hz bestimmt Die Stromquelle sollte f r 30 Ampere Betrieb ausgelegt sein K hlschr nke mit der 230 VU Konfiguration sind mit einem kontinental euro
236. t ani mals in a very short time at 0 1 Irritating to the nose Anesthetic effects when inhaled Rapidly fatal at 2 4 Danger ous for short exposure at 1 1 to 2 2 Acts mechanically to deprive tissues of oxy gen Does not support life Slight symptoms appear upon exposure to 0 002 to 0 004 0 3 rapidly fatal Exposure Exposure 3 000 25 to 5 000 15 5 000 50 1 000 100 to 1 500 4 1 10 4 000 1 000 to 7 000 10 158 Explosive Range by vol in air Limits lower upper 1 3 7 1 1 3 44 0 12 5 74 0 7 0 1 3 6 0 40 74 0 6 0 40 0 Likely Location of Highest Concentration Near top Concentrates in closed up per spaces At bottom At bottom At bottom when heated may stratify at points above bottom Near top espe ciallyif present with illuminat ing gas At bottom At bottom At bottom Most Common Sources Sewers chemi cal feed rooms Industrial wastes varnish sol vents An insecticide Products of combustion sewer gas sludge Also issues from car bonaceous strata Manufactured gas flue gas products of combustion motor exhausts Fires of almost any kind Industrial wastes solvent cleaning Chlorine cylin der and feed line leaks Incomplete combustion of organics Com mon air pollut ant fungicide Service stations garages storage tanks houses Manufactured gas sludge digestion tank gas
237. t displays an ON OFF ratio number After dis playing the forward pumping ratio the sampler reverses the pump to obtain a purge ratio The acceptable range is between 0 80 and 1 25 If either ratio is outside the acceptable range the pump requires re pair You do not need to pump liquid while running the test and you can run the pump test with or without a pump tube in the pump Distributor Test The distributor test is provided for factory per sonnel to verify the distributor s position as it rotates through the 24 positions screens 12 through 14 The distributor arm flexes slightly when 1t contacts the stop and the sampler measures this flexure The sampler uses this measurement to position the arm ac curately over each bottle 67 6700FR Refrigerated Sampler Diagnostic Screens Reinitialize Controller The sampler allows you to reset all pro Continued gram settings to the settings shipped with the sampler screen 15 Reinitializing also clears the memory that stores the sampler s PLEASE WAIT event log and module data Use this option cautiously 5 ROM PASSED TEST Maintenance Checklist If the ROM fails the diagnostic LL test the sampler reports e Clean the refrigerator interior and exterior periodically ROM FAILED TEST Contact e Clean the refrigerator s air filter every 3 months Isco Customer Service for assistance e Clean the condenser coil annually ABCDEFGHIJKLMNOPORST e Inspect the pump tube for
238. t into the public sewer Such occurrences are rare The attempt to instill a sense of urgency about real hazards is diluted if a man is told to give attention to a long list of things that in fact are irrelevant Be very careful to avoid high H2S concentra tions flammable atmospheres and hazards of physical injuries Remember that much H2S may be released by the stirring up of sludge in the bottom of a structure Obey your senses in respect to irritating gases such as chlorine unconsciousness comes suddenly from breath ing too much Be cautious about strange odors Do not determine percent oxygen in the air There is a danger that the result will influence a man s thinking about the seriousness of the real hazards Most important use ample venti lation and do not enter a potentially hazard ous structure except in a good safety harness with two men at the top who can lift you out Table 15 Hazardous Gases Chemical Formula Cas Benzene Carbon Bisulfide Carbon Dioxide CO Carbon Monoxide Carbon Tetra Chloride Cl Formal dehyde Gasoline CH to CoHoo Hydrogen CH 0 HCN Hydrogen Cyanide oo Common Properties Irritant and poison ous Colorless with characteristic odor Irritant colorless anesthetic Nearly odorless when pure color less anesthetic Poisonous Asphyxiant Colorless odorless When breathed in large quantities may cause acid tast
239. ta while running a sampling pro gram It uses the data to produce four reports e The Program Settings report listing the program settings e The Sampling Results report listing the program settings time of samples and other program events e The Combined Results report combining the sample event times with rainfall data module data or YSI Sonde data e The Summary report listing daily summaries of data collected The Summary report may be rainfall and or module data The sampler stores each report in memory where they remain until you select RUN Selecting RUN clears the memory so that it can store the data from the next program 54 6700FR Refrigerated Sampler Collecting Reports There are a number of ways to collect the reports e View reports on the sampler s display e Print the reports with an Isco 3770 Field Printer e Collect the reports with an Isco 581 RTD and use a computer to transfer the reports from the RTD to a file on the computer Transtar Complete CCAA e Collect the reports with a PC running Flowlink e Collect the reports with a PC running SAMPLINK 581 RTD Viewing the Data Viewing Data Because the display area is much smaller than the area available RUN with a printed report the report items displayed are a little differ PROGRAM VIEW REPORT OTHER FUCTIONS ent from the printed items e For the Sampling Report the sampler displays each program Select VIEW REPORT eveni oneal a
240. te 7 0207 cfs Hourly Average Flow Rate 00 00 01 00 NO DATA 01 00 02 00 NO DATA 02 00 03 00 NO DATA 03 00 04 00 NO DATA 04 00 05 00 NO DATA 05 00 06 00 NO DATA 06700 07700 NO DATA 07 00 05 00 NO DATA 08 00 09 00 2 812 S 09 00 10 00 2 747 cfs 10 00 11 00 2 791 cfs LLS lt O0 t2 00 3 456 cfs 12 00 13 00 5 385 cfs 13 90 14 00 6 651 cfs 14 00 15 00 2 341 CES LS 00 1L6 00 1 593 S 18 00 17 08 NO DATA 17 00 18 00 NO DATA 15 00 19300 NO DATA 19700 20300 NO DATA 20 00 21 00 NO DATA 21 00 22 00 NO DATA 22 00 23 00 NO DATA 23 00 24 00 NO DATA 00 amp oO mn oO amp HE F FF EHH HEHEH Ht HHH HH Ht HHH HH HHH HH TH HEE HH EHF HHH HEH FH HH Ht HH HH HE HHH HHH HF Hour Ending 08 16 24 Units are cfs N N o o o HHHH HHHH tHHHH HHHH HHHH HHHH tHHHH HHHH 0 00 64 6700FR Refrigerated Sampler Taking a Grab Sample Grab Samples RUN Grab samples let you take a single sample on demand collecting 1 o the sample in an external container Figure 12 It is a simple pro OTHER FUNCTIONS cedure but there are two things to keep in mind Select OTHER FUNCTIONS e When the sampler delivers a grab sample it runs through a complete sampling cycle using the current settings for line rinses or retries MAINTENANCE o MANUAL FUNCTIONS e To take a grab sample while the sampler is
241. teilnummer ist der Ersatzteilliste zu entnehmen gt ELLE Sicherheitssymbole und Gefahrenhinweise Die Symbole auf dem gek hlten Probenehmer Modell 6700FR und die in dieser Anleitung aufgef hrten Symbole machen auf bekannte Gefahren aufmerksam Diese Symbole werden nachstehend beschrieben A Dieses Symbol kennzeichnet eine allgemeine Gefahrenquelle Weiterf hrende Informationen sind im Benutzerhandbuch enthalten AN Dieses Symbol zeigt die Gefahr eines Elektroschocks an Weitere Informationen sind im Benutzerhandbuch zu finden Das Benutzerhandbuch kennzeichnet die Gefahrenbedingung und m gliche erforderliche Schritte zur Behebung dieser Bedingung In diesem Handbuch wird eine der zwei Gefahrenkategorien verwendet A VORSICHTSHINWEIS Vorsichtshinweise kennzeichnen eine potentielle Gefahr die leichte oder m ige Verletzungen zur Folge haben kann wenn sie nicht vermieden wird Diese Kategorie kann den Benutzer auch auf gef hrliche Handhabung oder Bedingungen die Besch digungen verursachen k nnen aufmerksam machen Warnungen kennzeichnen eine potentiell gef hrli che Bedingung die den Tod oder schwere Verlet zungen zur Folge haben kann wenn sie nicht vermieden wird 6700FR Refrigerated Sampler WARNUNG Umbau oder nderungen an diesem Ger t die nicht durch die Partei die f r die Einhaltung der Vorschriften verantwortlich ist ausdr cklich genehmigt wurden k nnen die Berechtigung des Benutze
242. the extended program ming screens e At the main menu type 6700 1 to show the standard program ming screens RUN PROGRAM VIEW REPORT OTHER FUNCTIONS Main Menu One Part and Two Part Programs Extended programming lets you set up a one part program or a two part program One part programs let you fill all bottles of the tub with one set of pacing distribution and enable settings Two part programs add an additional set of extended pacing distribu tion and enable screens to the sampling program Each set of screens is called a program part The program parts are simply called part A and part B Both parts share the program settings for suction line length suction head and rinses and retries They also share one start time setting Each part has its own group of bottles Because settings for each part are independent of each other the sampler when running a two part program fills each bottle group as if they were being filled by two different programs Two part programs finish when both parts are done Two part programming is ideal for sampling storm events Many storm water run off monitoring permits require a first flush grab sample within the first 30 minutes of the storm event and flow paced samples during the remainder of the event With a two part program you can set up part A for the first flush sample and part B for the remainder Example 6 on page 30 shows a storm water sampli
243. the internal tem perature LED indicator will be on The evaporator temperature sensor is mounted on the front of the evaporator plate The evaporator temperature LED indicator is on when the evaporator temperature is warm Connectors P4 and P5 are for factory calibration only They set up the correct resistances so the internal temperature and evaporator temperature indicators are on at the proper temperatures Avoid adjusting these settings The temperature control potentiometer setting the internal refrigerator temperature and the evaporator temperature together determine compressor operation and control the compressor running LED indicator 77 6700FR Refrigerated Sampler Figure 17 Circuit Board Wiring Connections Label Green Yellow Band Line Cord Green Red Band Compressor gt Brown Yellow Band Line Cord Brown Black Band Relay Pin 1 3 Blue Yellow Band Line Cord White Red Band Compressor Black Red Band Compressor Black Black Band Relay Pin 2 White White Band Transformer Red Red Band Crank Heater Transformer Brown Red Band Crank Heater From To Pa BlueBlack Band Relay Pin ps Vota Band Relay Pin Ground e m saw po sek racer voc en Redwine Band Transformer P12 Red White Band Transformer A 3 As the compressor runs the evaporator temperature falls and the evaporator temperature indicator goes out The compressor contin ues running until the internal air temperature reaches
244. tices Section 7 Precautions for Safe Handling and Use Leak Procedures Steps to be Taken if Material ls i Sweep or vacuum up the spilled material and place in a waste disposal container Avoid raising Spilled Or Released i dust Waste Disposal Dispose in an approved landfill according to federal state and local regulations Methods Precautions to be Taken i Cover promptly to avoid blowing dust Wash after handling In Handling and Storage Other Precautions and or Special Hazards i Keep in sealed container away from moisture Clay will readily adsorb moisture 153 6700FR Refrigerated Sampler 154 6700FR Refrigerated Sampler Appendix C General Safety Procedures The safety of the personnel who use the 6700 is a critical consideration The following proce dures applicable to working in and around manholes and sewers are those used by Black amp Veatch a respected consulting firm and are published here by their kind permission Field personnel must keep safety uppermost in their minds at all times When working above ground rules of common sense and safety prevail However when entering man holes strict safety procedures must be observed Failure to do so could jeopardize not only your own life but also the lives of other crew members 1 Hazards There are many hazards con nected with entering manholes Some of the most common hazards are Adverse Atmosphere The manhole may contain
245. tilisateur des dangers connus Ces ic nes sont d finies ci dessous A Cette ic ne repr sente un danger d ordre g n ral Consultez le manuel d instructions pour de plus amples infor mations AN Cette ic ne indique le risque de choc lectrique Consultez le manuel d instructions pour de plus amples infor mations Le manuel d instructions d crit chaque situation dangereuse ainsi que les mesures prendre pour la rectifier Le manuel pr sente ces renseigne ments de deux facons N ATTENTION Attention indique un danger potentiel qui s il n est pas vit pourrait provoquer des blessures plus ou moins graves Cette cat gorie sert galement a informer Putilisateur des actions ou conditions qui pourraient provoquer des d g ts mat riels Avertissement indique la pr sence de circon stances qui pourraient tre tres dangereuses pouvant si elles ne sont pas vit es provoquer des blessures graves ou m me la mort 6700FR Refrigerated Sampler Page 12 AVERTISSEMENT Tout changement ou modification fait a cet appar eil sans avoir t au pr alable approuv par la personne responsable de son fonctionnement pourrait annuler le droit de l utilisateur de s en servir M REMARQUE Lisez le R capitulatif des mesures de s curit plac au d but de ce manuel Il explique les condi tions lectriques requises et fournit les mesures de s curit d emploi au o je D un pl IN D er CO
246. tion changes It is important to collect the sampling results be fore changing the site description the data can not be retrieved afterwards Keep in mind that the description may change when selecting an extended program The partition data is cleared when the sampler automatically cre ates and sizes the memory partitions This occurs when you e Select a new program e Change the Data Storage Interval in the current program e Change the programming mode e Install a new 700 Series Module e Change 700 Series Module mode of operation e Add or remove a rain gauge with the Hardware Setup e Add or remove a YSI Sonde parameter with the Hardware Setup e Add or remove a refrigerator temperature sensor as 1 03 e Reinitialize the sampler If you need to collect sampling results and partition data do this before allowing the sampler to create and size the partitions The stored data is lost as the sampler reformats its memory As a pre caution the sampler displays the screen below INTERVAL CHANGED STORED DATA WILL BE LOST OK YES NO 100 M Note When updating the Flash mem ory power must be applied to the sampler 6700FR Refrigerated Sampler When YES is selected the sampler clears the stored data and re formats the memory partitions The sampler then displays the new capacity of the partition memory PARTITION MEMORY WILL LAST 13 DAYS If the duration is too short try changing the data storage inter
247. tion due to mechanical abrasion INHALATION causes irritation of the respiratory tract and may cause disabling progressive pulmonary fibrosis silicosis due to CRYSTALLINE SILICA QUARTZ Symptoms include cough dyspnea wheezing and impairment of pulmonary function Progression of symptoms can continue after dust exposure ceases INGESTION No adverse effects expected CARCINOGENICITY NTP YES IARC YES OSHA NO CRYSTALLINE SILICA is listed by the National Toxicology Program NTP as a confirmed animal carcinogen and by the International Agency for Research on Cancer IARC as a Group 2A sufficient evidence of carcinogenicity in laboratory animals and limited evidence in humans CHRONIC HEALTH HAZARDS Refer to Potential Health Effects and Carcinogenicity 140 6700FR Refrigerated Sampler ENGELHARD Page 3 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 MEDICAL CONDITIONS GENERALLY AGGRAVATED BY EXPOSURE May aggravate existing medical conditions such as respiratory ailments NOTE See Section VIII for Exposure Limits Section XI for Toxicological Information and Section XII for Ecological Information SECTION IV FIRST AID MEASURES EYE CONTACT Flush eyes with plenty of water If irritation develops call a physician SKIN CONTACT Procedures normally not needed If skin contact occurs flush with plenty of water If irritation develops call a physician INHALATION Remove to fresh air If breathing is diffic
248. tips cs CHECKSUM unsigned long DE DESCRIPTION 6700 Sampler FL FLOW cubic meters per second ID UNIT SPECIFIC IDENTIFIER 10 digit unsigned long LE LEVEL meters MO MODEL 6700 PE PERCENT percent of full scale PH PH none PR PREVIOUS DAY S RAIN tips rolls over every 256 tips RA RAIN tips rolls over every 256 tips RTE REFRIGERATOR TEMPERATURE degrees celsius SS SAMPLER ENABLE STATE logical TE TEMPERATURE degrees celsius TI CURRENT TIME days since 1 Jan 1900 VE VELOCITY meters per second VO VOLUME cubic meters VSI VELOCITY SIGNAL STRENGTH percent VSP VELOCITY SPECTRUM STRENGTH percent YCO YSI 600 CONDUCTIVITY milliseimens per centimeter YDO YSI 600 D O milligrams per liter YPH YSI 600 PH none YSA YSI 600 SALINITY parts per thousand YSP YSI 600 SPECIFIC CONDUCTANCE milliseimens per centimeter YTD YSI 600 TOTAL DISSOLVED SOLIDS grams per liter YTE YSI 600 TEMPERATURE degrees celsius NOTES 1 THE THREE MOST RECENT SAMPLES WILL HAVE ENTRIES AS B THE WILL BE THE FIRST BOTTLE NUMBER IN THE SET IF THE SAMPLE IS A GRAB SAMPLE IT WILL BE SHOWN AS BO 2 THE CHECKSUM DOES NOT INCLUDE THE CHECKSUM CARRIAGE RETURN AND LINEFEED 98 6700FR Refrigerated Sampler Dialout Alarms Dialout alarms require the sampler to be equipped with the facto ry installed 2400 baud talking modem The dialout alarm allows the sampler to notify a contact list when an alarm condition exists Dialout Alarm Screens is true See Dialout scr
249. to reinitialize the sampler Charts for maintenance screens appear in Figure 30 Maintenance Screens on page 116 Set Clock Isco ships the samplers from the factory with the clocks set to the correct Central Standard Time Reset the clock when installing the sampler in a different time zone for daylight savings time or when needed Setting the Clock and Calendar on page page 18 shows how to set the time and date Diagnostics The sampler has several self diagnostic tests that check the mem ory both the RAM and ROM pump and the distributor arm posi tion It also contains screens that let you reset the sampler s program settings and memory to factory settings You will not need to run the diagnostic tests routinely The diagnostic tests are a troubleshooting tool Isco s Customer Service department staff may ask you to run these tests when they work with you in diagnosing problems with your sampler Memory Tests Screen 4 and 5 show you the diagnostic tests for memory If either screen shows you a message saying that the memory failed the test contact Isco Customer Service Display tests Screen 6 shows you the display test You should see the test pattern illustrated in the screen If the pattern does not match the illustration the display or its circuitry require repair Pump Tests Screen 7 lets you start the pump test by selecting YES As the sampler runs the test it first runs the pump forward for a short period Next i
250. trument 1s the one in effect on date of shipment Warranty period begins on the shipping date unless Isco agrees in writing to a different date Excluded from this warranty are normal wear expendable items such as charts ribbon tubing and glassware and damage due to corrosion misuse accident or lack of proper maintenance This warranty does not cover Isco on line Process Analyzers and certain Isco SFE instruments which are covered under different warranty terms nor does 1t cover products not sold under the Isco trademark or for which any other warranty is specifically stated in sales literature This warranty 1s expressly in lieu of all other warranties and obligations and Isco specifically disclaims any warranty of merchantability or fitness for a particular purpose Any changes in this warranty must be in writing and signed by a corporate officer The warrantor 1s Isco Inc 4700 Superior Lincoln NE 68504 U S A This warranty applies to USA customers Customers in other countries should contact their Isco dealer for warranty service Before returning any instrument for repair please call fax or e mail the Isco service department for instructions Many problems can often be diagnosed and corrected over the phone or by e mail without returning the instrument to the factory Instruments needing factory repair should be packed carefully preferably in the original carton and shipped to the attention of the servi
251. ttings Isco ships the sampler to you with factory programs that you can modify to suit your own needs All four extended programs are identical to each other The stored programs will also save your 700 Series Module pro gram settings and any sampler enable conditions using rain gauge data or YSI 600 Sonde parameters These program settings remain as long as you do not change the type of module or change the rain gauge or YSI 600 Hardware Setup If you make any of these chang es the sampler updates the stored programs to the current sampler configuration Selecting a Stored Program The sampler shows the extended programming screens it always has one current and three noncurrent programs each occupying a permanent location in memory The first time you add the extended screens the current program is EXTENDED 1 one of the factory extended programs The name of the current extended program ap pears in quotations on the first line of the main menu See Exam ple 4 on page 26 The factory programs are named EXTENDED 1 EXTENDED 2 EXTENDED 3 and EXTENDED 4 You can rename them with more descriptive names making them easier to identify The program name is one of the extended program s settings The current program is the program you see when you select PRO GRAM from the start up menu and page through the programming screens It is the program the sampler uses when you select RUN from the start up menu
252. ttings for the pro gram follow e Program type Extended e Program name STORM e Site description SITE 54 e Units Length Ft Flow Rate gpm Flow Volume gal e Mode of Operation Flowmeter Flow Insert Round 12 e Bottle kit 24 1000 milliliter bottles e Suction line length 5 feet e Suction head Auto suction head e Line rinses None e Sampling retries None e Part A and B bottle assignments Bottles 1 6 to part A bot tles 7 24 to part P e Part A pacing Time pacing sampling every 5 minutes e Part A distribution Sequential 1 sample per bottle e Part A sample volume 800 milliliters e Part A enable At least 0 15 inches of rainfall in 30 minutes and a flow stream level of more than 0 25 feet once enabled stay enabled sample taken when the sampler is enabled e Part A pause and resumes None e Part B pacing Flow pacing sampling every 2 500 gallons e Part B distribution Sequential 1 sample per bottle e Part B sample volume 500 milliliters e Part B enable At least 0 15 inches of rainfall in 30 minutes and a flow stream level of more than 0 25 feet once enabled stay enabled no sample taken when the sampler is enabled first sample taken 20 minutes after the sampler is enabled e Part B pause and resumes None e Start time Delayed start of 1 minute e 730 Bubbler Module Installed 30 6700FR
253. uary 22 1995 Using the Clock Start Time type 22 1 Enter 01 1 Enter 95 1 Enter Menu Example 2 Setting the Clock and Calendar NO DELAY TO START DELAYED START f CLOCK TIME RUN Select OTHER FUNCTIONS i PROGRAM aa Select CLOCK TIME se FIRST SAMPLE AT MAINTENANCE 06 00 Tata Select MAINTENANCE 9 PROGRAMMING STYLE Type the time of day SELECT DAYS SET CLOCK SU MO TU WE TH FR SA SET PUMP TUBE ALARM OS 3 INTERNAL BATTERY DONE DIAGNOSTICS Press an arrow key until the cursor is on the correct day ENTER TIME AND DATE bio ile nca date Then press enter HH MM DD MON YY 4 14 00 22 JAN 95 Repeat these steps until each day you want is blinking MAINTENANCE Press Stop to return to the main Press an arrow until DONE MANUAL FUNCTIONS m nu 5 PROGRAMMING STYLE blinks Press enter Menu Screens Clock Start Times There are three start time settings you can use in a sampling pro gram This section discusses only one of these settings the clock start time A clock start time lets you set up a sampling program that starts at the same time on one or more days of the week For example you may want to begin sampling at 6 00 a m on Monday through Friday screen g in the margin 18 6700FR Refrigerated Sampler Using the Site Description or To select a day or days from the menu in h Program Name Menus 1 Press an arrow key until the cursor is on the correct day The sampler has
254. uge can help you estimate the condition of the battery Keep in mind that the sampler has no idea as to how much charge was originally stored in the battery or even if a battery is being used and therefore has no idea as to the remaining capacity of its power source Adjust Suction Head This option is available when you have chosen to enter the suction head The sampler is not calculating the suction head automatical ly Select this option to enter a new suction head value If changes are made the sampler logs a CHANGED SUCTION HEAD event Servicing the Sampler Servicing the sampler includes e Collecting the filled sample bottles and replacing them with clean bottles e Collecting the data recorded by the sampler during the pro gram See Sampling Reports on page 54 Samplers are usually serviced after they complete a sampling pro gram When working up a service schedule you will need to esti mate the program completion time You should also be familiar with the program s settings for the start time or if the sampler is programmed for continuous sampling Continuous sampling is controlled by the distribution setting en tered at the DO YOU WANT TO RUN CONTINUOUSLY screen A YES response directs the sampler to reset the distribu tion sequence and continue the countdown to the next sample event Appropriate service intervals will prevent overfilled bottles Sampling Reports The 6700 records a variety of da
255. uipment specified above conforms to the above Directive s and Standards as of April 23 1996 Bill Foster USA Representative isco Bill Foster Director of Engineering Isco Inc 4700 Superior Street Lincoln Nebraska 68504 Phone 402 464 0231 Fax 402 464 4543 60 9003 421 Rev C Michael Teutscher European Authorized Representative isco l STIP Contact Dr Dirk K ppenkastrop Gesch ftsf hrer Managing Director STIP ISCO GmbH Siemensstra e 2 64823 Gro Umstadt Telefon 06078 7 86 82 Telefax 06078 7 86 88 D ooo One Year Limited Warranty Factory Service Isco instruments covered by this warranty have a one year limited warranty covering parts and labor Any instrument that fails during the warranty period due to faulty parts or workmanship will be repaired at the factory at no charge to the customer Isco s exclusive liability is limited to repair or replacement of defective instruments Isco 1s not liable for consequential damages Isco will pay surface transportation charges both ways within the 48 contiguous United States 1f the instrument proves to be defective within 30 days of shipment Throughout the remainder of the warranty period the customer will pay to return the instrument to Isco and Isco will pay surface transportation to return the repaired instrument to the customer Isco will not pay air freight or customer s packing and crating charges The warranty for any ins
256. ult give oxygen Call a physician INGESTION Procedures normally not needed If large quantities are ingested seek medical advice SECTION V FIRE FIGHTING MEASURES Flash Point Not Applicable Auto Ignition Not Determined LEL Not Determined UEL Not Determined NFPA HAZARD CLASSIFICATION Health 0 Flammable 0 Reactivity 0 HMIS HAZARD CLASSIFICATION Health 1 Flammable 0 Reactivity O Indicates the possibility of chronic health effects See Chronic Health Hazards in Section III for more information EXTINGUISHING MEDIA Use water carbon dioxide or foam SPECIAL FIRE FIGHTING PROCEDURES Wear positive pressure self contained breathing apparatus in fire conditions 141 6700FR Refrigerated Sampler ENGELHARD Page 4 Code J96001 MATERIAL SAFETY DATA SHEET Date 23 DEC 1993 UNUSUAL FIRE AND EXPLOSION HAZARDS Not a fire or explosion hazard SECTION VI ACCIDENTAL RELEASE MEASURES Contain spillage and scoop up or vacuum Avoid dusting NOTE In the event of an accidental release of this material the above procedures should be followed Additionally proper exposure controls and personal protection equipment should be used see Section VIII Exposure Control Personal Protection and disposal of the material should be in accordance with Section XI Disposal Considerations SECTION VII HANDLING AND STORAGE Use dustless systems for handling storage and clean up so that airborne dust does not excee
257. ume SOR 0 1s the results of attempting the most recent sample The possible results are 0 SAMPLE OK 1 NO LIQUID FOUND 2 LIQUID LOST not enough liquid to satisfy require ments 3 USER STOPPED using the Stop Key 4 POWER FAILED 5 PUMP JAMMED 6 DISTRIBUTOR JAMMED 8 PUMP LATCH OPEN 9 SAMPLER SHUT OFF while sampling 11 NO DISTRIBUTOR 12 SAMPLE IN PROGRESS CS xxxx is the byte by byte sum of the entire string MO CS For commands that are not understood INVALID COMMAND or CHECKSUM MISMATCH or when no samples have been taken the most recent bottle information is left off the response string 99 Command Driven Sampler Displays The sampler LCD displays WAITING TO SAMPLE until it re ceives a TAKE SAMPLE command While sampling the display is updated throughout the sampling process and will normally include e MOVING TO BOTTLE e PURGING e PUMPING ml SAMPLE e PURGING If an error occurs during sampling an appropriate error message will be displayed When the pump tubing life threshold has been exceeded a warning message will alternate with the WAITING TO SAMPLE display If power is removed while the sampler was ON upon power resto ration the sampler will return to the ON state 104 Chapter Contents Program Lock Switch Bottle Set at Enable e Telephone Commands Support for YSI 6820 and YSI 600XL Sondes 106 6700FR Refrigerate
258. un time is the only random programming setting you ll need to enter because the sampler de rives the number of sample events required for the program up to QUANTITY AT INTERVAL 99 from the distribution settings You can combine random pacing 3 Zu Au a de with any distribution Each time you run the program the sam 3 AT__ MIN pler generates a new set of random intervals This makes each sample event unpredictable from run to run RANDOM INTERVALS In both nonuniform clock time pacing and nonuniform interval pac ing the sampler takes a sample at the start time For random pac ing however it takes the first sample at the end of the first oe ce interval not at the start time Event Pacing To program the sampler for event pacing select EVENT PACED from screen 8 When prompted for the enable setting enter the en able settings at which you want the sampler to take samples see Sampler Enable on page 90 83 Distribution Menu Charts appear in Figure 25 Standard Programming Programming Screens on page 111 Figure 35 Extended Programming Equipment Setup on page 120 6700FR Refrigerated Sampler Event pacing uses the combination of both the programmed enable conditions and the external enable pin F of the external flow meter connector to determine the enable state Each time it becomes en abled the sampler takes one sample placing it in one bottle The sampler must become disabled between events The s
259. val or eliminating unnecessary reading types in the Hardware or Mod ule Setup For example a sampler configured with a 730 Bubbler Module and a rain gauge storing data at a one minute interval cre ates level and rainfall partitions that hold 13 days of readings Changing the storage interval to two minutes extends the storage capacity to 26 days The sampler does not have to be running a program to store read ings When the sampler is on it stores readings at the selected data storage interval Once the partition is filled the readings roll over When the sampler is running a program the partitions become trig gered by the programmed start time or the first enable time which ever is later A triggered partition continues to log readings at the selected interval but will not replace any readings taken after the trigger event The sampler fills the partition and then stops record ing to preserve the data The first reading preserved in a full parti tion is one hour before the trigger event A full partition can be reset by starting another program or changing storage parameters If you require continuous readings for analysis be sure to collect the readings before the partition fills or rolls over to avoid gaps in the data Isco offers a 6 700 sampler controller with an expanded memory ca pacity Instead of the standard 128 kilobytes this controller has 4 megabytes of RAM available for program and data storage Contact the
260. ve is entered as 20 J Enter 01 Enter 90 6700FR Refrigerated Sampler Other Functions Menu Other Functions RUN PROGRAM NAME The Other Functions menu screen includes options for PROGRAM VIEW REPORT e Maintenance See Chapter 4 OTHER FUNCTIONS e Select OTHER FUNCTIONS e Manual Functions e Programming Style e Hardware See Hardware Setup The Hardware menu option MAINTENANCE appears in extended programming only MANUAL FUNCTIONS PROGRAMMING STYLE HARDWARE Manual Functions e Note that the HARDWARE op tion appears only in extended programming e Take grab samples The manual functions programming screens let you e Calibrate sample volumes e Operate the pump manually e Move the distributor Operating the Pump Grab samples and calibrate volumes are discussed in Chapter 3 GRAB SAMPLE CALIBRATE VOLUME Operating the Pump OPERATE PUMP MOVE DISTRIBUTOR You can manually operate the sampler s pump in the forward or re verse direction You can do this to test the pump draw a large sam ple or purge the suction line SELECT DIRECTION PUMP FORWARD When you run the pump manually the sampler reports the number PUMP REVERSE gt of pump counts during the pump s operation Use this feature to ob tain an estimate of the pump counts required to purge a nonstand PURGING ard suction line gt MAR a Care should be taken when using the PUMP FORWARD and PUMP R
261. vity Is stable under normal temperatures and pressures in sealed containers Hazardous polymerization will not occur SECTION VII SPILL OR LEAK PROCEDURES Notify safety personnel of spills or leaks Clean up personnel need protection against inhalation of dusts or fumes Eye protection is required Vacuuming and or wet methods of cleanup are preferred Place in appropriate containers for disposal keeping airborne particulates at a minimum Clay is slippery when wet Disposal Consult applicable local state and federal regulations to select the _ method of disposal Recover metal components by reprocessing whenever possible Updated April 4 1994 Page 3 6700FR Refrigerated Sampler MATERIAL SAFETY DATA SHEET DESI PAK Packaged Desiccant SECTION VIII SPECIAL PROTECTION INFORMATION Respiratory Protection Provide a NIOSH MSHA jointly approved respirator in the absence of proper environmental control Contact your safety equipment supplier for proper mask type Ventilation Provide general and or local exhaust ventilation to keep exposures below the TLV Ventilation used must be designed to prevent spots of dust accumulation or recycling of dusts Protective Clothing Wear protective clothing including long sleeves and gloves to prevent repeated or prolonged skin contact Eye Protection Chemical splash goggles designed in compliance with OSHA regulations are recommended Consult your safety equipment supplier
262. warning reminds you that the inter the back of the refrigerator The nal battery is near expiration and should be replaced You can find parked position allows for easier instructions for replacing the battery in Replacing the Internal access to the bottle rack Battery on page 75 51 6700FR Refrigerated Sampler Interrupting a Running Program You can interrupt a sampling program by pressing the Stop key while the sampler is waiting for the next sample event Pressing Stop places the sampler into Manual Paused operation and records a MANUAL PAUSE in the sample event log In this state the sampler allows you to access several functions You can modify the program take a grab sample etc with out ad versely affecting the running program Modifying the program is limited to adjusting the pacing intervals enable conditions sample volume and suction head The basic program structure such as the type of pacing can not be changed While in the manual paused state the sampling program continues to operate as normal with the exception of taking samples If a sample was to be taken it is skipped The sampler records SAM PLE SKIPPED in the sample event log and continues to operate as normal The manual paused state displays a scrolling menu with up to twelve options Use the Arrow keys to scroll through the manual paused options and the Enter key to make a selection Return to the running program by selecting RESUME P
263. will occur at the end of a full interval Furthermore if the sampler is enabled several times during the program it re RESET SAMPLE gt ES T ENADES sets the countdown each time YES NO Use the reset interval feature carefully For example avoid reset ting the interval when you sample with uniform time pacing and want to take samples at specific times CONTINUE COUNTDOWN WHILE Be The effects of resetting the interval can be seen in this example A YES N sampler has been programmed to sample every 15 minutes and to re set the interval when enabled It receives an enable signal at 10 03 and takes a sample After resetting the interval the sampler takes subsequent samples at 10 18 not 10 15 10 33 not 10 30 and so on Screen 22 is available only when you select NO at screen 21 You can have the sampler continue the countdown repeating it as often as necessary while the sampler is disabled or you may suspend the countdown while disabled resuming the countdown as the sampler s enabled The standard program allows the countdown to contin ue while disabled Pauses Resumes Pause and Resume Screens Screen charts containing the pause and resume screen appear in Pause and resume settings available in extended programming create an intermittent sampling schedule A program with pauses and resumes begins sampling at its programmed start time con tinuing until the first pause time and day ofthe week It then sus p
264. y Hazard Data STABILITY Conditions i Moisture clay will adsorb moisture amp Stable To Avoid i CUnstable Incompatibility Materials to Avoid Hazardous Carbon dioxide carbon monoxide water Decomposition Products i HAZARDOUS POLYMERIZATION Conditions None MMay Occur To Avoid i DI WIN Not Occur i 152 6700FR Refrigerated Sampler Page 2 Section 5 Health Hazard Data PRIMARY ROUTES inhalation Klingestion CARCINOGEN LINTP LJOSHA OF ENTRY DI Skin Absorption Not Hazardous LISTED IN DIARC Monograph 5 Not Listed HEALTH HAZARDS Acute i May cause eye skin and mucous membrane irritation Chronic Prolonged inhalation may cause lung damage Medical Conditions i Asthma Generally Aggravated by Exposure EMERGENCY FIRST AID PROCEDURES Seek medical assistance for further treatment observation and support if necessary Eye Contact i Flush with water for at least 15 minutes inhalation i Remove affected person to fresh air Ingestion No adverse effects expected Respiratory Protection i Use NIOSH approved dust respirator 3 LI tn Protective Gioves i Light cotton gloves Eye Protection Safety glasses VENTILATION L_ Local Exhaust _ Mechanical General ii AE TO BE USED i Avoid raising dust Avoid contact with skin eyes and clothing DJOther Specify None None Other Protective Clothing and Equipment Hygienic Work Prac
265. zione dev essere visi bile e facilmente accessibile Infatti l unico modo per disattivare il refrigeratore scol legarlo dalla rete Per ridurre il rischio di folgorazioni il refrigeratore dev essere collegato ad una presa dotata di messa a terra L alimentazione dev essere fornita attraverso un circuito separato che non deve alimentare altre apparecchiature Non far funzionare il refrigeratore senza i pannelli anteriore inferiore e posteriore Non utilizzare il refrigeratore in atmos fere esplosive Non sollevare n trasportare il refrigera tore Servirsi di un dispositivo per il trasporto di apparecchiature I fusibili devono essere sostituiti con altri con le stesse caratteristiche di formato corrente tensione e tempo d intervento Per il codice di ordinazione consultare l elenco ricambi gt e RRR BEBE Simboli di sicurezza ed avvertenze di pericolo I simboli riportati sul campionatore refrigerato modello 6700FR e quelli che si trovano nel presente manuale d istruzioni mettono in guardia l utilizza tore contro i pericoli conosciuti Segue la spiegazi one dei simboli N Questo simbolo rappresenta pericolo generico Per ulteriori informazioni con sultare il manuale d istruzioni A Questo simbolo rappresenta pericolo di folgorazioni Per ulteriori informazioni consultare il manuale d istruzioni Nel manuale d istruzioni sono descritte le condizioni di pericolo e le misure da adottare per evitarl

6700FR Refrigerated Sampler User Manual

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