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Model 49i-PS - User Manual

1. Figure 3 1 497 Primary Standard Front Panel Display CAUTION If the LCD panel breaks do not let the liquid crystal contact your skin or clothes If the liquid crystal contacts your skin or clothes wash it off immediately using soap and water a 3 2 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Pushbuttons Pushbuttons The Pushbuttons allow the user to traverse the various screens menus Thermo Fisher Scientific Figure 3 2 Front Panel Pushbuttons Table 3 1 Front Panel Pushbuttons Soft Keys gt Run nl Menu SS SCSESBEK e jC Left Right Enter The soft keys are used to provide shortcuts that allow the user to jump to user selectable menu screens For more information on processing soft keys see Soft Keys below The is used to display the Run screen The Run screen normally displays the 03 concentration The is used to display the Main Menu when in the Run screen or back up one level in the menu system For more Information about the Main Menu see Main Menu later in this chapter The is context sensitive that is It provides additional information about the screen that is being displayed Press for a brief explanation about the Current screen or menu Help messages are displayed using lower case letters to easily distinguish them from the Operating screens To exit a help screen press Wo to return to the previous scr
2. LCD Signal 6 LFLM_5V LCD Signal 7 NC 8 IR DV LCD Signal 9 LCLK_5V LCD Signal 10 5V 11 Ground 12 25V Je LCD Bias Voltage 14 Ground KEYBOARD Jo 1 Keypad Row 1 Input Z Keypad Row 2 Input 3 Keypad Row 3 Input 4 Keypad Row 4 Input 5 Keypad Col 1 Select 6 Keypad Col 2 Select T Keypad Col 3 Select 8 Keypad Col 4 Select LCD BACKLIGHT J4 1 5V NC 3 Ground 5 14 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Troubleshooting Connector Pin Descriptions Table 5 5 IO Expansion Board Optional Connector Pin Descriptions Connector Label EXPANSION 1 0 MOTHER BD Reference Designator J J2 Pin co co N O oO FP WO N ch ech Oo one Aa O N Signal Description Analog Voltage Input 1 Analog Voltage Input 2 Analog Voltage Input 3 Ground Analog Voltage Input 4 Analog Voltage Input 5 Analog Voltage Input 6 Ground Analog Voltage Input 7 Analog Voltage Input 8 Ground NC Current Output Return Ground Current Output 1 Current Output Return Current Output 2 Current Output Return Current Output 3 Current Output Return Current Output 4 Current Output Return Current Output 5 Current Output Return Current Output 6 5V 24V 24V Ground Ground Ground Model 497 Primary Standard Instruction Manual 5 15 Troubleshooting Connector Pin Descriptions Table 5 5 O Expansion Board Optional Connector Pin Descriptions cont
3. Preventive Maintenance Leak Test and Pump Checkout 7 Note the pressure as Pyo 8 Connect the pressure transducer to the normally closed solenoid port 9 Plug the solenoid power line into the appropriate connector on the measurement interface board Make sure the solenoid is activated by choosing Pressure from the Diagnostics menu 10 Note the pressure as Pye the solenoid is faulty 11 The solenoid is faulty if either Pyo or Pyc is greater than the pressure determined in the External Leaks section described previously 4 10 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Chapter 5 Troubleshooting This instrument has been designed to achieve a high level of reliability In the event of problems or failure the troubleshooting guidelines board level connection diagrams connector pin descriptions and testing procedures presented in this chapter should be helpful in isolating and identifying problems For additional fault location information refer to the Preventive Maintenance chapter in this manual The service mode in the Operation chapter includes parameters and functions that are useful when making adjustments or diagnosing problems The Technical Support Department at Thermo Fisher Scientific can also be consulted in the event of problems See Service Locations at the end of this chapter for contact information In any correspondence with the factory please note both th
4. lrec aa bb 00 pp qq yy srec aa bb 00 pp qq yy xxxx the number of past records yy the number of records to return 1 to 10 aa hours 01 to 24 bb minutes 01 to 59 oo month 01 to 12 pp day 01 to 31 gq year These commands output long or short records The output format is determined by the set lrec format and set srec format commands The logging time is determined by the set lrec per and set srec per commands Model 497 Primary Standard Instruction Manual B 19 C Link Protocol Commands Datalogging In the following example there are 100 long records currently stored in memory When the command Irec 100 5 is sent the instrument counts back 100 records from the last record collected and then returns 5 records For details on how to decode the flag fields within these records see Figure B 1 in the flags command Send lrec 100 5 Receive lrec 100 5 19 00 8 17 05 flags 2coo0000 03 2 504e 02 cellai 100177 cellbi 99747 bncht 3 202e 01 lmpt 5 375e 01 o3lt 6767e 01 flowa 7 278e 01 flowb 7 390e 01 pres 7 557e 02 20 00 8 17 05 flags 2cooo000 03 2 514e 02 cellai 100137 cellbi 99762 bncht 3 262e 01 lmpt 5 325e 01 o3lt 6717e 01 flowa 7 248e 01 flowb 73108 01 pres 7 563e102 21 00 8 17 05 flags 2coo00000 03 2 664e 02 cellai 100115 cellbi 99756 bncht 3 168e 01 lmpt 5 255e 01 o3lt 6597e 01 flowa 7 318e 01 flowb 2406 01 pres 415e 02 22 00 8 17 05 flags c4oo000 03 2 582e 02 cellai 10
5. page 6 4 then return to the beginning of this step 2 At the Bench Lamp Setting screen use to increment decrement the Lamp Setting until Cell A Int and Cell B Int indicate approximately 100 000 Hz 3 Press to save the setting Use the following procedure to replace a sample reference solenoid valve Equipment required Solenoid Flatblade screwdriver Open end wrench 5 8 inch Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the Sample and Ref connection cables from the measurement interface board 3 Remove the plumbing from the solenoids 4 Loosen the four captive screws and lift out the solenoids and the solenoid plate 5 Remove the solenoid retaining nuts from the underside of the solenoid plate and remove the faulty solenoid Model 497 Primary Standard Instruction Manual 6 29 Servicing Detector Replacement 6 Replace the new solenoid by following the previous steps in reverse making sure that all connections are tight 7 Perform a leak test Refer to the Solenoid Leaks procedure in the Preventive Maintenance chapter Detector Use the following procedure to replace a detector Figure 6 11 Replacement Equipment Required Detector assembly Allen wrench
6. B 13 B 13 B 14 B 14 B 14 B 14 B 14 B 3 C Link Protocol Commands Commands B 4 Table B 1 C Link Protocol Commands continued Command alarm level 2 alarm level 3 alarm level 4 alarm level 5 alarm oz lamp temp max alarm oz lamp temp min alarm pressure max alarm pressure min alarm sample flow a max alarm sample flow amin alarm sample flow b max alarm sample flow b min alarm trig conc 03 analog lout range analog vin analog vout range avg time baud bench temp cal detectors cal high 03 coef cal low 03 coef cal 03 bkg cal 03 coef cell a int cell b int Model 497 Primary Standard Instruction Manual Description Reports current alarm level 2 offset from the concentration as the alarm trigger point for that level Reports current alarm level 3 offset from the concentration as the alarm trigger point for that level Reports current alarm level 4 offset from the concentration as the alarm trigger point for that level Reports current alarm level 5 offset from the concentration as the alarm trigger point for that level Reports the ozonator lamp temperature alarm maximum value Current setting Reports the ozonator lamp temperature alarm minimum value Current setting Reports the pressure alarm maximum value current setting Reports the pressure alarm minimum value current setting Reports the sample flow a alarm maximum value current setting Reports the sample flo
7. Note If seconds are omitted the seconds default to 00 Send set time 14 15 Receive set time 14 15 ok addr dns This command reports the TCP IP address for the domain name server Send addr dns Receive addr dns 192 168 1 1 set addr dns address This command sets the domain name server address where address consists cc 39 of four numbers ranging from 0 255 inclusive separated by Send set addr dns 192 168 1 1 Receive set addr dns 192 168 1 1 ok addr gw This command reports the default TCP IP gateway address Send addr gw Receive addr gw 192 168 1 1 set addr gw address This command sets the default gateway address where address consists of cc 3 four numbers ranging from 0 255 inclusive separated by Send Set addr gw 192 168 1 1 Receive set addr gw 192 168 1 1 ok addr ip This command reports the IP address of the analyzer send addr ip Receive addr ip 192 168 1 15 set addr ip address This command sets the analyzer s IP address where address consists of four cc 39 numbers ranging from 0 255 inclusive separated by B 36 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Communications Configuration Send set addr ip 192 168 1 15 Receive set addr ip 192 168 1 15 ok addr nm This command reports the TCP IP netmask address Send addr nm Receive addr nm 255 255 255 0 set
8. Temperatures The Temperatures screen read only displays the current bench temperature bench lamp temperature and O3 lamp temperature if the ozonator option is installed e Inthe Main Menu choose Diagnostics gt Temperatures Pressure The Pressure screen read only displays the current bench pressure The pressure is measured by a pressure transducer e Inthe Main Menu choose Diagnostics gt Pressure Flows The Flows screen read only displays the current flow rate through Cell A and Cell B These flows are measured by internal flow sensors For more information see Chapter 1 Operations e Inthe Main Menu choose Diagnostics gt Flows Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 53 Operation Diagnostics Menu Cell A B 0 The Cell A B O screen read only displays the current O3 concentration in each cell as well as the O3 reading displayed in the Run screen the average of the two cells e Inthe Main Menu choose Diagnostics gt Cell A B O3 Intensities The Intensities screen read only displays the current intensity in Cell A and Cell B in Hertz These intensities are read by detectors A and B respectively e Inthe Main Menu choose Diagnostics gt Intensities 3 54 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Analog Input Readings Analog Input Voltages Thermo Fisher Scientific Digital Inputs Operation Diagnos
9. This equipment generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instruction manual may cause harmful interference to radio communications Operation of this equipment in a residential area is likely to cause harmful interference in which case the user will be required to correct the interference at his own expense a WEEE Symbol The following symbol and description identify the WEEE marking used on the instrument and in the associated documentation Symbol Description Marking of electrical and electronic equipment which applies to Ki electrical and electronic equipment falling under the Directive 2002 96 EC WEEE and the equipment that has been put on the market Red after 13 August 2005 Where to Get Hel H Service is available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo com adi 1 866 282 0430 Toll Free 1 508 520 0430 International Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual xviii Thermo Fisher Scientific Chapter 1 Introduction The Model 497 Primary Standard UV Photometric Ozone Calibrator combines proven detection technology easy to use menu driven software and advanced diagnostics to offer unsurpassed flexibility and reliability The Model 497 Primary Standard has the following features 320 x 240 graphics display M
10. feature not enabled if the I O expansion board is not detected Send analog iout range 4 Receive analog iout range 4 2 set analog iout range channel range This command sets analog current output channel to the channel range where channel is between 1 and 6 inclusive and range is set according to Table B 9 The example that follows sets current output channel 4 to the 0 20 mA range This command responds with feature not enabled if the I O expansion board is not detected Send Set analog iout range 4 1 Receive set analog iout range 4 1 ok Table B 9 Analog Current Output Range Values Range Output Range 1 0 20 mA Z 4 20 mA 0 cannot be set to this but may report Undefined analog vin channel This command retrieves the analog voltage input channel data both the calculated value and the actual voltage In the example that follows the calculated value of channel 1 is 75 325 degrees E volts are 2 796 This command responds with feature not enabled if the I O expansion board is not detected Send analog vin 1 Receive analog vin 1 75 325 2 796 B 40 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands I O Configuration analog vout range channel This command reports the analog voltage output channel range where channel is between 1 and 6 inclusive according to Table B 10 Send analog vout range 2 Receive analog vout ran
11. where K molecular absorption coefficient 308 cm at 0 C and 1 atmosphere L length of cell 38 cm C ozone concentration in parts per million ppm I UV light intensity of sample with ozone sample gas I UV light intensity of sample without ozone reference gas Zero air is supplied to the Model 497 Primary Standard through the zero air bulkhead and is split into two gas streams as shown in Figure 1 1 One gas stream flows through a pressure regulator to the reference solenoid valve to become the reference gas I The second zero air stream flows through a pressure regulator ozonator and manifold to the sample solenoid valve to become the sample gas I Ozone from the manifold is delivered to the ozone bulkhead The solenoid valves alternate the reference and sample gas streams between cells A and B every 10 seconds When cell A contains reference gas cell B contains sample gas and vice versa The UV light intensities of each cell are measured by detectors A and B When the solenoid valves switch the reference and sample gas streams to opposite cells the light intensities are ignored for several seconds to allow the cells to be flushed The Model 497 Primary Standard calculates the 1 2 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Introduction Specifications ozone concentration for each cell and outputs the average concentration to the front panel display the analog outputs and
12. 03 conc 03 lamp temp 03 setting ozonator pres pres comp program no pump push range C Link Protocol Commands Table B 1 C Link Protocol Commands continued Description Reports list of digital output index numbers and variables Reports sets low average time Reports 03 concentration calculated with low range coefficients Reports sets low range 0 coefficient Reports sets current 03 low range Sets the low span concentration for autocalibration Outputs long records in the format specified in the command Outputs long records Reports sets output format for long records ASCII or binary Reports current layout of Irec data Reports maximum number of long records that can be stored Reports sets long record logging period Reports sets memory allocation for long records Reports sets memory allocation for short records Sets gas mode to sample Simulates pressing menu pushbutton Reports operating mode in local service or remote Reports sets number of long records stored in memory Reports sets number of short records stored in memory Reports current 03 concentration Reports sets current 03 background Reports sets current 03 coefficient Sets the 03 concentration to a user defined value Reports the current ozonator lamp temperature Reports what ozone concentration the calibrator is set to output Reports sets ozonator on or off Reports current reaction chamber pressure Reports sets pressure compensation on or
13. 03 lamp temp 068 7 deg C lamp This reports the current photometer lamp setting The example that follows reports that the lamp setting is 72 9 Send lamp setting Receive lamp setting 72 9 set lamp ddd d This command sets the photometer lamp setting to ddd d where ddd d is a floating point number representing a percentage of the photometer lamp setting The example that follows sets the photometer lamp to 75 5 Send set lamp 75 5 Receive set lamp 75 5 ok lamp setting This reports the current photometer lamp setting The example that follows reports that the lamp setting is 72 9 Send lamp setting Receive lamp setting 72 9 lamp temp B 10 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific C Link Protocol Commands Measurements This reports the current bench lamp temperature The example that follows reports that the current bench temperature is 55 2 C Send lamp temp Receive lamp temp 055 2 deg C lamp voltage bench This command reports the bench lamp voltage in volts Send lamp voltage bench Receive lamp voltage bench 10 3 V lamp voltage oz This command reports the ozonator lamp voltage in volts Send lamp voltage oz Receive lamp voltage oz 12 3 V pres This reports the current reaction chamber pressure The first pressure reading is the pressure reading being used in instrument calculations The second pressure is the actual pressure reading being measured If pressure c
14. 34 Register Number 40001 amp 40002 40003 amp 40004 40005 amp 40006 40007 amp 40008 40009 amp 40010 40011 amp 40012 40013 amp 40014 40015 amp 40016 40017 amp 40018 40019 amp 40020 40021 amp 40022 40023840024 40025 amp 40026 40027 amp 40028 40029 amp 40030 40031 amp 40032 40033840034 Status MODBUS Protocol MODBUS Commands Supported Table C 1 Read Coils for 497 Primary Standard continued INTENSITY B ALARM CONC ALARM NOT USED NOT USED NOT USED NOT USED NOT USED NOT USED NOT USED MOTHERBOARD STATUS ALARM MEASUREMENT INTERFACE BD STATUS ALARM I O EXP BD STATUS ALARM Table C 2 Read Registers for 497 Primary Standard Variable 03 CONC LO 03 CONC Dual Auto Range mode HI 03 CONC Dual Auto Range mode RANGE STATUS INTENSITY A INTENSITY B NOISE A NOISE B FLOW A FLOW B PRESSURE BENCH TEMP LAMP TEMP O3 LAMP TEMP ANALOG IN 1 ANALOG IN 2 ANALOG IN 3 Model 497 Primary Standard Instruction Manual C 9 MODBUS Protocol MODBUS Commands Supported Table C 2 Read Registers for 497 Primary Standard continued Register Number Variable 40035 amp 40036 ANALOG IN 4 40037 amp 40038 ANALOG IN 5 40039 amp 40040 ANALOG IN 6 40041 amp 40042 ANALOG IN 7 40043 amp 40044 ANALOG IN 8 40045 amp 40046 03 OUT CONC Table C 3 Write Coils for 497 Primary Standard Coil Number Action 101 ZERO MODE 102 SPAN MODE 103 OZONATOR LEVEL 1 104 OZONATOR LEVEL 2 105 OZONATOR LEVEL 3 106 OZONATOR LE
15. Data Query String lt STX gt DA lt CR gt D 6 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Measurements Reported in Response to DA Command for 492 and 492 PS Single Range Mode for 492 and 497 PS Dual Auto Range Mode for 492 Dual Auto Range Mode for 492 PS Thermo Fisher Scientific Geysitech Bayern Hessen Protocol Geysitech Commands Reply String lt STX gt MD03 lt SP gt 001 lt SP gt 4 2578 01 lt SP gt 03 lt SP gt 04 lt SP gt 0000000000 lt SP gt 002 lt SP gt T T T Address First Concentration E format 25 78 Address 1 5681 00 lt SP gt 03 lt SP gt 04 lt SP gt 0000000000 lt SP gt 003 lt SP gt 11754 01 lt SP gt 03 lt SP gt 04 lt SP Second Concentration 5 681 Address 2 Third Concentration 11 75 0000000000 lt SP gt lt CR gt The attached concentrations are in the selected gas units The measurements that are attached to the response if not valid in a particular mode then a value of 0 0 will be reported The following measurements reported in response to DA command are for the Model 497 and 497 Primary Standard The 1 measurement reported in single range mode for the Model 497 and 49i Primary Standard includes e O3 The 2 measurements reported in dual or auto range modes for the Model 497 include low O3 gt high O3 The 2 measurements reported in dual or auto range modes for the Model 49i Primary Standard include e O3 Actual e O3 Set point Model 497 Pri
16. Equipment Damage Some internal components can be damaged by small be worn while handling any internal component a 1 Refer to Removing the Measurement Bench and Lowering the Partition Panel in this chapter to lower the partition panel then proceed to the next step below Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 21 Servicing Front Panel Board Replacement 2 Unplug all connectors Note the locations of the connectors to facilitate reconnection 3 Remove the two retaining screws from the top of the board 4 Pop off the measurement interface board from the two mounting studs and remove the board Measurement Interface Board zonator Boar Qzonator Board Photometer Board Figure 6 9 Replacing the Measurement Interface Board 5 To install the measurement interface board follow previous steps in reverse 6 Re install the measurement bench Refer to Removing the Measurement Bench and Lowering the Partition Panel in this chapter 7 Calibrate the pressure transducer flow transducers and bench temperature sensor as described earlier in this chapter Fro nt Panel Board Use the following procedure to replace the front panel board Figure 6 10 Replacement Equipment Required 6 22 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Servicing LCD Module Replacement Front panel board amounts of static electricity A properly grounded antistatic wri
17. from OK to FAIL The number of alarms detected is displayed to indicate how many alarms have occurred If no alarms are detected the number zero is displayed To see the actual reading of an item and its minimum and maximum limits move the cursor to the item and press Items displayed are determined by the options installed The zero or span check is visible only if the zero span check or auto calibration options are enabled The O3 lamp temperature and ozonator level 1 2 3 4 and 5 checks are visible only if the ozonator option is installed The motherboard status interface board status and I O expansion board status if installed indicates that the power supplies are working and connections are successful There are no setting screens for these alarms e Inthe Main Menu choose Alarms 3 58 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific 0 Lamp Temperature Min and Max 0 Lamp Temperature Limits Thermo Fisher Scientific Operation Alarms Menu The O3 Lamp Temperature screen displays the current ozonator lamp temperature and sets the minimum and maximum alarm limits Acceptable alarm limits range from 65 to 75 C If the O3 lamp temperature reading goes beyond either the minimum or maximum alarm limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu e Inthe Main Menu choose Alarms gt O3 Lamp Temp The Minimum O3 Lamp Te
18. that is tied to the selected field item The selected item is shown by lt after it Note that at this point pressing indicates Model 497 Primary Standard Instruction Manual 3 23 Operation Instrument Controls Menu that these are proposed changes as opposed to implemented changes To change the selected record format and erase record log file data see Commit Content below e In the Main Menu choose Instrument Controls gt Datalogging Settings gt Select Content gt Select Field gt Analog Inputs Use and to move the cursor up and down e Press to select a new choice Commit Content The Commit Content screen is used to save the selected output signal that is tied to the selected field item If no changes have been made NO CHANGES TO RECORD LIST will appear For more information about selecting the analog output signal group choices see Select Content above e In the Main Menu choose Instrument Controls gt Datalogging Settings gt Commit Content e Press to commit changes to selected record format and erase record log file data e Press ER to confirm changes 3 24 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu Reset to Default Content The Reset to Default Content screen is used to reset all of the datalogging field items to default values For more information about selecting the analog output sign
19. 0 1 2 Output format see set erec Irec srec format format command B 18 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Datalogging These commands report the last long and short records stored or the dynamic data record In the example that follows the command requests a long record with no checksum in ASCII format with text For details on how to decode the flag fields within these records see Figure B 1 in the flags command Send lro Receive lro1 13 00 08 12 05 flags 1C00554A 03 0 000 hio3 0 000 cellai 0 000 cellbi 0 000 bncht 999 900 lmpt 999 900 o3lt 0 000 flowa 0 000 flowb 0 000 pres 0 000 erec This command returns a brief description of the main operating conditions at the time the command is issued i e dynamic data The example that follows shows a typical response The format is defined by the current H lt 4 KN cc KN H settings of format and erec format commands For details on how to decode the flag fields within these records see Figure B 1 in the flags command Send erec RECEIVE SE 13 05 08 12 05 flags 1C00554A 03 0 000 1 lo 03 0 000 1 lampi 0000 bencht 999 900 lampt 999 900 ozlampt 0 000 flowa 0 000 flowb 0 000 Pres 0 000 avgt 10 lo avgt 10 03bkg 0 000 03 coef 1 000 lo 03 coef 1 000 03 range 200000 000 lo 03 range 200000 000 int a 0000 int b 0000 sum 46f6 Irec srec lrec xxxx yy STEC XXXX YY
20. 2 4 Ke oer ere Reece ne rer erry errant er eee er 2 8 Operation ccccsssssesscesssessesesessesessesesaeseseeaesesaesesaeaesenaesesensesetas 3 1 tegen 3 2 KE e CONG asa creeds ds once aes tnatdeeos E AS 3 3 DB ege eg 3 4 SLO ITA CRRA i d lt x eee ee eee a Ea 3 4 eege 3 6 RUN SCE CO sissies ancien canto dacasace vane REEE EAE 3 6 Niao NV a E 3 7 tee 3 7 Raeren 3 8 KEE 3 8 oO T e P 3 11 e Ee 3 12 Calibration Factors Menu yinesesssaconcsesonencsonssamarcsaboausannunenescnsse 3212 De CU E 3 13 Eeer 3 13 Instrument Controls Menu isccsccctcsciaccensedeonbingereienvesenciorspercians 3 15 Custom eet EES 3 15 Et P E sess vente eee ne dt eter eceeseecewspeeeesd 3 16 Ee E 0 secuii een er ee een ne rer 3 16 Pressure Compensation E 3 17 IR 5 17 EE Setting Sieis koii 3 27 Model 497 Primary Standard Instruction Manual V Contents vi Model 497 Primary Standard Instruction Manual GAG EE 3 36 Screen Contrast 3 48 Service Mode 3 49 Date mee elE 3 49 EEN 3 50 POG EAT CEG OM eebe 3 51 VOA S e E E 3 51 Re 3 53 EE 3 53 ENEE 3 53 E EE 3 54 Ee 3 54 Analog Topot eebe 3 55 Analop Topar Hee 3 55 RER 3 55 age 3 56 Test Analog Eege 3 56 lnsttament Conio nrat io iernii eaan 3 57 Contact eet 3 58 Abrines eege 3 58 GER Lono en E 3 59 Camp AE ten pe Ue eege 3 60 Ben eegene 3 61 Eege 3 62 Flow Aand D casts esa sareraetctnacesseuets es ata cbvanacdetanertauaueesesies 3 63 DCIS Oy Baccara ey eei ater cies E eer oeae 3 64 ee 3
21. 3 Ee E C 3 0x01 0x02 Read Coils Read Inputs sccsisscteccesasuoreeatetsazays C 3 0x03 0x04 Read Holding Registers Read Input RegistersC 5 0x05 Force Write Single Oil vesiccececceapsacuunaptspeansecereeasees C 7 MODBUS Commands Supported orcicteveacesteeaniceestecheserners C 8 Geysitech Bayern Hessen Protocol ccscseeeeres D 1 Serial Communication Parameters cccsssescssesescceceseneeseee D 1 TCP Communication EIERE D 2 Hecno E D 2 PODESTA T ON WSCC E D 2 Basic EE D 2 Block Checksum E D 3 E EE D 3 Instrument Control Command ST D 3 Data Sampling Data Query Command UA eee D 4 Measurements Reported in Response to DA Command for 491i and 49i PS vicccsssecscscsaveucaseeseteuiovercss D 7 Operating and Error Status soaps ce ee D 8 Thermo Fisher Scientific Thermo Fisher Scientific Figures Figures Model 49i Primary Standard Flow Schematic cccscceeseee 1 3 IER E EE 2 2 Remove the Shipping ee 2 2 Model 49i Primary Standard Rear Ban 2 4 VO Terni Bora y N e E ET 2 5 D O NR RE 2 6 EE Board E 2 7 49i Primary Standard Front Panel Display ee eeeeeeeeee 3 2 Front Pandi Ps MC ee 3 3 Flowchart of Menu Driven Software scicccscsisestareiescavseuorsssreinees 3 5 Pin Out of Rear Panel Connector eebe 3 10 RE EE ees 4 6 IR EE 4 7 Board Level Connection Diagram Common Electronics 5 6 Board Level Connection Diagram Measurement System 5 7 Properly Grounded A
22. 7 Equipment Required Motherboard Philips screwdriver Nut driver 3 16 inch Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Turn instrument OFF unplug the power cord and remove the cover 6 20 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Servicing Measurement Interface Board Replacement 2 Remove the I O expansion board optional if used See the I O Expansion Board Replacement procedure in this chapter 3 Remove the digital output board See the Digital Output Board Replacement procedure in this chapter 4 Unplug all connectors from the motherboard Note connector locations to facilitate reconnection 5 Using the nut driver remove the eight standofts securing the board to the rear panel 6 Pop off the motherboard from motherboard support bracket and remove the motherboard 7 To install the motherboard follow previous steps in reverse 8 Calibrate the analog voltage outputs as described earlier in this chapter all ranges Measurement Use the following procedure to replace the measurement interface board g P p Interface Board Figure 6 9 Re p lacement Equipment Required Measurement interface board Philips screwdriver amounts of static electricity A properly grounded antistatic wrist strap must
23. Averaging Time seconds 0 10 1 20 2 30 3 60 4 90 5 120 6 180 7 240 8 300 bench temp This reports the current bench temperature The first temperature reading is the temperature being used in instrument calculations The second temperature is the actual temperature being measured If temperature compensation is ON then both temperature readings are the same If temperature compensation is OFF a temperature of 0 C is used as the default temperature even though the actual bench temperature is 32 3 C The example that follows shows that temperature compensation is on and that the bench temperature is 32 3 C Send bench temp Receive bench temp 032 3 deg C actual 032 3 03 high 03 low 03 Model 497 Primary Standard Instruction Manual B 9 C Link Protocol Commands Measurements These commands report the measured O3 concentrations when operating in single range or high and low O3 when operating in dual or auto range mode The example that follows shows that the O3 concentration is 67 2 ppb send 03 Receive 03 6720E 2 ppb flow a flow b These commands report the sample flow in Cell A and Cell B The example that follows reports that the current sample flow in Cell A is 0 608 liters minute Send flow a Receive flow a 0 608 l m o3 lamp temp This reports the current ozonator lamp temperature The example that follows reports that the current ozonator temperature is 68 7 C Send o3 lamp temp Receive
24. C Link Protocol Commands Hardware Configuration Send set date 03 19 05 Receive set date 03 19 05 ok set default params This command sets all the parameters to their default values This does not affect the factory calibrated parameters Send set default params Receive set default params ok save set save params This command stores all current parameters in FLASH memory It is important that each time instrument parameters are changed that this command be sent If changes are not saved they will be lost in the event of a power failure The example that follows saves the parameters to FLASH memoty Send Set save params Receive set save params ok ozonator This command reports the ozonator on or off The example below reports that the ozonator is on Send ozonator Receive ozonator on set ozonator onoff These commands set the ozonator on or off The example below sets the ozonator off Send set ozonator off Receive set ozonator off ok time This command reports the current time 24 hour time The example that follows reports that the internal time is 2 15 30 pm Send time Receive time 14 15 30 set time hh mm ss hh hours mm minutes ss seconds Model 497 Primary Standard Instruction Manual B 35 C Link Protocol Commands Communications Configuration Communications Configuration This command sets the internal clock 24 hour time The example that follows sets the internal time to 2 15 pm
25. Communication Settings gt RS 232 RS 485 Selection 3 32 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu e Press to leave the warning screen and move to next screen e Use ER to confirm and save the new selection change TCP IP Settings The TCP IP Settings menu is used for defining TCP IP settings Note The instrument power must be cycled after this parameter has been changed for the change to take effect e Inthe Main Menu choose Instrument Controls gt Communication Settings gt TCP IP Settings Use DHCP The Use DHCP screen is used to specify whether or not to use DHCP When DHCP is enabled the network dynamically provides an IP address for the instrument e Inthe Main Menu choose Instrument Controls gt Communication Settings gt TCP IP Settings gt Use DCHP e Press to toggle and set DHCP on or off Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 33 Operation Instrument Controls Menu IP Address The IP Address screen is used to edit the IP address The IP address can only be changed when DHCP is OFE For more information on DHCP see Use DHCP e Inthe Main Menu choose Instrument Controls gt Communication Settings gt TCP IP Settings gt IP Address e Use Tal and to move and change the value of the IP address e Press to save the new address Netmask The Netmask scr
26. Descriptions Connector Label LAMP LAMP HEATER INTF Model 497 Primary Standard Instruction Manual Reference Designator J1 J2 Pin Oo on A Ww N ch ech Signal Description Photometer Lamp Voltage Out Photometer Lamp Voltage Return Ground Photometer Lamp Thermistor 1 Photometer Lamp Heater Control Ground 24V Heater Current Sense Photometer Lamp Thermistor 2 Photometer Lamp Intensity Control Voltage Input Photometer Lamp Intensity Control Voltage Output Thermo Fisher Scientific Troubleshooting Service Locations Table 5 9 Photometer Power Supply Connector Pin Descriptions continued Connector Reference Pin Signal Label Designator Description Photometer Heater Thermistor 24V Ground Photometer Lamp On off Control Ground oOo NY O o A Ground Service Locations For additional assistance Thermo Fisher Scientific has service available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo com aqj 1 866 282 0430 Toll Free 1 508 520 0430 International Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 5 21 Troubleshooting Service Locations 5 22 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Chapter 6 Servicing This chapter explains how to replace the Model 497 Primary Standard subassemblies It assumes that a subassemb
27. Erase Log is used to erase all saved data for the selected record type not all short records and long records e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Erase Log e Press to erase all data S Press gt to confirm erasure Thermo Fisher Scientific Select Content The Select Content submenu displays a list of 32 record fields to use and a submenu list of the analog output signal group choices to choose from Choices are Concentrations Other Measurements and Analog Inputs if the I O expansion board is installed This is a temporary list of items for the selected record type that must be committed via the datalogging menu before the changes will apply Note that committing any changes to this list will erase all currently logged data as the format of the stored data is changed e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Select Content Model 497 Primary Standard Instruction Manual 3 21 Operation Instrument Controls Menu Choose Item Type The Choose Item Type submenu displays a list of data that can be logged for the current field Choices and Concentrations Other Measurements and Analog Inputs if the I O expansion board is installed In the Main Menu choose Instrument Controls gt Datalogging Settings gt Select Content gt Field 1 32 Concentrations The Concentrations screen allows the user to select the output sig
28. Fisher Scientific Model 497 Primary Standard Instruction Manual 3 81 Operation Password Menu Passwo rd Menu The Password menu allows the user to configure password protection If the calibrator is locked none of the settings may be changed via the front panel user interface The items visible under the password menu are determined by the calibrator s password status e Inthe Main Menu choose Password Set Password The Set Password screen is used to set the password to unlock the front panel The set password is shown if the calibrator is unlocked and the password not set e Inthe Main Menu choose Password gt Set Password e Press to enter password and disable instrument lock Lock Instrument The Lock Instrument screen is used to lock the calibrator s front panel so users can not change any settings from the front panel The lock instrument is shown if the calibrator is unlocked and the password set e Inthe Main Menu choose Password gt Lock Instrument e Press to enable instrument lock and returns to main menu 3 82 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Password Menu Change Password The Change Password is used to change the password used to unlock the calibrator s front panel The change password is shown if the calibrator is unlocked e Inthe Main Menu choose Password gt Change Password e Press to change password Remove Password T
29. Instruction Manual Thermo Fisher Scientific Flow Sensor Assembly Pressure Sensor Assembly Ozonator Lamp Power Supply Photometer Lamp Power Supply Digital Output Board I O Expansion Board Thermo Fisher Scientific Optional System Description Electronics The flow sensor assembly consists of a board containing an instrumentation amplifier and a flow transducer with input and output gas fittings The flow transducer output is produced by measuring the pressure difference across a precision orifice This unit is used for measuring the flow of sample gas in the measurement system The pressure sensor assembly consists of a board containing an instrumentation amplifier and a pressure transducer with a gas input fitting The pressure transducer output is produced by measuring the pressure difference between the sample gas pressure and ambient air pressure The ozonator lamp power supply board includes the circuits that generate high voltage AC to control the lamp heater A transformer outputting high voltage at approximately 15 kHz drives the lamp A resistor in series with the output limits the lamp current The voltage output is adjustable under software control for lamp intensity control The ozonator lamp can be switched on and off under software control The lamp is heated to a specific temperature to ensure reliable operation The oscillator circuit that drives the high voltage output is inhibited until this operating temp
30. Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config gt Select Channel gt Decimal Places e Use t and to increment or decrement the value e Press to save the new value Number of Table Points The Number of Table Points screen allows the user to select how many points are used in the conversion table The points range from 2 to 10 with a default of 2 3 46 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config gt Select Channel gt Table Points Use and to move the cursor up and down e Press to save the new value Table Point The Table Point submenu allows the user to set up an individual table point e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config gt Select Channel gt Point 1 10 Volts The Volts screen allows the user to set the input voltage for the selected table point in the conversion table from 0 00 to 10 50 The default table is a two point table with point 1 0 00 V 000 0 U and point 2 10 00 V 10 0 U e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config gt Select Channel gt Select Point gt Volts e Use and ER to move the cursor left or right Thermo Fisher Scientific Model 497 Primary S
31. Manual Action Replace ozonator lamp driver board or lamp bench assembly Replace lamp driver board or lamp assembly Replace fan If not operating properly Clean or replace foam filter refer to Preventive Maintenance chapter in this manual Check the pump for a tear in the diaphragm replace with pump repair kit If necessary Refer to Preventive Maintenance chapter in this manual Check that capillaries are properly installed and O rings are in good shape Replace If necessary Check flow system for leaks Check sample capillary 0 015 inch ID for blockage Replace as necessary If using sample particulate filter make sure it is not blocked Disconnect sample particulate filter from the sample bulkhead if flow increases replace the filter Check Gain adjustment Replace measurement interface board Check to insure range corresponds with expected value If not select proper range Check user defined low set point set to zero Thermo Fisher Scientific Troubleshooting Troubleshooting Guides Table 5 2 Troubleshooting Alarm Messages continued Alarm Message Possible Cause Action Alarm Motherboard Internal cables not connected Check that all internal cables Status properly are connected properly Alarm Interface Board is defective Recycle AC power to Status instrument If still alarming han rd Alarm 1 0 Exp Status change board Thermo Fisher Scientific Model 497
32. Model 497 Primary Standard Instruction Manual 4 7 Preventive Maintenance Leak Test and Pump Checkout Solenoid Leaks 4 8 Model 497 Primary Standard Instruction Manual Disconnect the OZONE out line and plug the OZONE fitting Disconnect the VENT line and plug Disconnect the zero air supply and plug the fitting Press to display the Main Menu Press A to scroll to Diagnostics and press to display the Diagnostics menu Press A to move the cursor to Flows and press to display the Flows screen The flow readings should slowly decrease to zero flow Press nl to return to the Diagnostics menu Press to move the cursor to Pressure and press to display the Pressure screen The pressure reading should drop to less than 250 mm Hg If the pump diaphragm is in good condition and the capillary is not blocked it should take less than 20 seconds from the time the inlet is plugged to the time the reading below 250 mm Hg is obtained If a leak is suspected carefully tighten each fitting until the leak is found and check to see that none of the input lines are cracked or broken Leaks across the solenoid valve can be caused by Teflon cold flowing across the valve seat or by particulates on the seat Use the following procedure to check for solenoid leaks Generate an ozone concentration of approximately 0 5 ppm 2 Press pw to display the Main Menu Thermo Fisher Scientific Solenoid Leak Test T
33. OxFFFF Number of following bytes Unit Identifier 1 Byte 0x00 to OxFF Passed back in response C 2 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Function Code Data Error Check Function Codes 0x01 0x02 Read Coils Thermo Fisher Scientific Read Inputs MODBUS Protocol Function Codes A Slave address is not required in MODBUS over TCP IP because the higher level protocols include device addressing The unit identifier is not used by the instrument The function code is a single byte in length The following function codes are supported by the instrument Read Coils 0x01 Read Inputs 0x02 Read Holding Registers i 0x03 Read Input Registers i 0x04 Force Write Single Coil 0x05 Read Exception Status l 0x07 If a function code is received that is not in this list and invalid function exception is returned The data field varies depending on the function For more description of these data fields see Function Codes below In MODBUS over Serial an error check is included in the message This is not necessary in MODBUS over TCP IP because the higher level protocols ensure error free transmission The error check is a two byte 16 bit CRC value This section describes the various function codes that are supported by the Model 497 Primary Standard Read Coils Inputs reads the status of the digital outputs relays in the instrument Issuing either of these function codes will gen
34. Primary Standard Instruction Manual 5 5 Troubleshooting Board Level Connection Diagrams Board Level Connection Diagrams Figure 5 1 and Figure 5 2 are board level connection diagrams for the common electronics and measurement system These illustrations can be used along with the connector pin descriptions in able 5 3 through Table 5 9 to troubleshoot board level faults OEXPANSICN BOARD EXPANSION I O Spal bi TOMASURMENT SYSTEM DIGTAL QUTPUT BOARD DIGITAL Jm OUTPUTS 27 Pin 11 Pin 8 Pin J2 RS232 RS485 FRONT 14 Pin LCD 9 Pin vu PANEL DISPLAY J4 Kaaner SE BOARD on i E J3 KEY PANEL 10 BASE T Set EXPANSION RS485 SEH SPARE DATA ANALOG OUTPUTS DIGITAL INPUTS 37 pin J4 3 Pin POWER GOOD 3 Pin 3 Pin QAMOC PONER SUPPLY REAR PANEL E AC 24VDC 2 Pin DE AC FRONT PANEL i POWER SW p J l l TRANSFORIVER Ps See ZE F Q0VACor 240VAC La l CPTIC S 5 6 Model 497 Primary Standard Instruction Manual Figure 5 1 Board Level Connection Diagram Common Electronics Thermo Fisher Scientific 4 Pin 4 Pin TO COMMON ELECTRONICS 5 Pin 5 Pin 8 Pin 49i MEASUREMENT INTERFACE BOARD 8 Pin DATA 4 Pin 3 Pin 2 Pin 2 Pin 2 Pin 2 Pin 24V 2 Pin 2 Pin 2 Pin AC sssoosoosooocosooosossoosossossoosoosooosoosoosossossossossoosoosooosocooosoosoosoosooso 3 Pin 3 Pin AC Troubleshooting Board Level Connection Diagrams CH A DETECTOR CH B DETECTOR FLOW A FLOW B
35. a Best results are obtained when the optical bench is cleaned prior to recalibration The cleanliness of the bench should also be checked any time the detector frequencies drop below 65 kHz since one source of low output is light attenuation due to dirt in the cell Dirt particulates are usually effective ozone removers Use the following procedure to clean the optical bench CAUTION Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component For more information about appropriate safety precautions see the Servicing chapter 1 Turn off the power and disconnect the power line 4 2 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Preventive Maintenance Lamp Replacement 2 Loosen the knurled nut around the tube and carefully slide out tube 3 Push a piece of lens paper down the tube using a 1 4 inch piece of Teflon tubing so as not to damage the tube Use a cotton swab to clean the window surfaces through the holes that the tube fits into 4 Both absorption tubes are identical so they can be replaced in either position Replacement of absorption cells is opposite to that of removal Since the Model 497 Primary Standard is a ratio instrument and cleaning the absorption tubes does not affect the calibration it is not necessary to recalibrate the instrument every time the cells are clea
36. bench Troubleshooting Troubleshooting Guides Action Remove one cell and look for blue light in hole of input block Check lamp temperature From the Diagnostics menu choose Temperatures Check 15 volts From the Diagnostics menu choose Voltages Clean cell Interchange detectors at Measurement Interface Board connectors to determine if detector is defective Clean cells Check for 1 7 volt peak to peak waveform at lamp current check point on Lamp Power Supply Board Check 15 volts From the Diagnostics menu choose Voltages Replace pressure transducer Replace or repair recorder Run instrument on stable ozone source If quiet no malfunction Clean cell Replace with known good solenoid valve Verify averaging time Is set properly Clean bench and then condition system overnight Model 497 Primary Standard Instruction Manual 5 3 Troubleshooting Troubleshooting Guides Table 5 2 Troubleshooting Alarm Messages Alarm Message Possible Cause Alarm 03 Lamp Temp Defective lamp heater Alarm Lamp Temp Defective lamp heater Alarm Bench Temp Faulty fan Dirty fan filter Alarm Pressure High pressure indication Alarm Flow A Flow low Alarm Flow B Alarm Intensity A Pre amp Gain not set properly Alarm Intensity B Defective measurement interface board Alarm Q3 Conc Concentration has exceeded range limit Concentration low 5 4 Model 497 Primary Standard Instruction
37. bulkhead When using a filter all calibrations and span checks must be performed through the filter I 0 Expansion Board The I O expansion board provides six analog current output channels 0 20 Assembly mA or 4 20 mA and eight analog voltage inputs 0 10V The DB25 connector on the rear panel provides the interface for these inputs and outputs Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 8 1 Optional Equipment Terminal Block and Cable Kits 8 2 Terminal Block and Cable Kits Cables The optional terminal block and cable kits provide a convenient way to connect devices to the instrument These kits break out the signals on the rear panel connector to individual numbered terminals Two types of terminal block and cable kits are available One kit is for the DB37 connectors and can be used for either the analog output connector or the relay output connector The other kit is for the DB25 connector and can be used for the optional I O expansion board For associated part numbers refer to External Device Connection Components in the Servicing chapter Each kit consists of e one six foot cable e one terminal block e one snap track Note Supporting all of the connections on units with the optional I O expansion board requires e two DB37 kits e one DB25 kit Table 8 1 identifies the optional individual cables that are available for the instrument and Table 8 2 provides the cable col
38. cord Pump Replacement Use the following procedure to replace the pump see Figure 6 4 To rebuild the pump see Pump Rebuilding in the Preventive Maintenance chapter Equipment Required 110V pump Philips screwdriver amounts of static electricity A properly grounded antistatic wrist strap must Equipment Damage Some internal components can be damaged by small be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect pump power line from AC PUMP connector on the measurement interface board Pump Bracket Floor Plate Pump Mounting Screws 2 Bottom Figure 6 4 Replacing the Pump 3 Remove both lines from pump 4 Loosen the four captive screws on the mounting plate and remove the pump 6 10 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Servicing Fan Replacement 5 Install the new pump by following the previous steps in reverse Fan Replacement Use the following procedure to replace the fan Figure 6 5 Equipment Required Fan Philips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the fan guard from the fan and remove the filter 3 Pull the power conne
39. cover Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 31 Servicing Pressure Transducer Calibration Pressure Transducer Calibration 2 Disconnect plumbing from the pressure transducer assembly Note the plumbing connections to facilitate reconnection 3 Disconnect the pressure transducer PRESS connector from the measurement interface board 4 Loosen the two pressure transducer retaining screws and remove the pressure transducer by sliding it towards the front of the instrument 5 Install the new pressure transducer assembly by following the previous steps in reverse 6 Calibrate the pressure transducer Refer to the Pressure Transducer Calibration procedure that follows Use the following procedure to calibrate the pressure transducer Equipment Required Vacuum pump WARNING The service procedures in this manual are restricted to qualified service representatives a If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired a Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a Note An error in the zero setting of the pressure transducer does not introduce a measurable error in the output concentration reading Therefore if only a barometer is available and not a vacuum
40. display is used to set the range To use the custom full scale range be sure to select it Custom range 1 2 or 3 in the O3 Range screen For more information about selecting ranges see O3 Range above e Inthe Main Menu choose Range gt Set Custom Ranges gt Custom range 1 2 or 3 e Use e and ER to move the cursor left or right e Use and to increment or decrement the numeric value e Press to save the new range et CHANGE VOLIE SOVE Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 11 Operation Averaging Time Ave raging Time The averaging time defines a time period 10 to 300 seconds over which O3 measurements are taken The average concentration of the readings are calculated for that time period The front panel display and analog outputs are updated every 10 seconds with the calculated averages An averaging time of 10 seconds for example means that the average concentration of the last 10 seconds will be output at each update An averaging time of 300 seconds means that the moving average concentration of the last 300 seconds will be output at each 10 second update Therefore the lower the averaging time the faster the front panel display and analog outputs respond to concentration changes Longer averaging times are typically used to smooth output data The following averaging times are available 10 20 30 60 90 120 180 240 and 300 seconds e Inthe Main Men
41. gt Custom Levels gt Custom Level 1 2 3 4 or 5 e Use and to increment or decrement the numeric value e Press to save the new level Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 15 Operation Instrument Controls Menu Pump Temperature Compensation The Pump screen allows the user to toggle the pump on and off e Inthe Main Menu choose Instrument Controls gt Pump e Press to toggle and set the pump on or off Temperature compensation provides compensation for any changes to the instrument s output signal due to variations in sample gas temperature The Model 497 Primary Standard can be operated with or without temperature compensation When temperature compensation is on the display shows the sample gas temperature measured by a thermistor on the Interface board When temperature compensation is off the display shows the standard temperature of 0 0 C e In the Main Menu choose Instrument Controls gt Temperature Compensation e Press to toggle and set the temperature compensation on or off 3 16 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu Pressure Compensation Pressure compensation provides compensation for any changes to the instrument s output signal due to variations of sample pressure The Model 497 Primary Standard can be operated with or without pressure compensation When pressure
42. gt Set Defaults e Press to warn user and enable restore with gt e Use to overwrite pressure sensor calibration parameters with factory default values when pressed after 4a Flow A and B Calibration The Flow A Calibration menu is used to calibrate the flow A sensor to zero span or restore factory default values The flow A calibration is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter The Flow B Calibration menu functions the same way Note This adjustment should only be performed by an instrument service technician a e Inthe Main Menu choose Service gt Flow Calibration A or B 3 74 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Service Menu Calibrate Flow Zero The Calibrate Flow A Zero screen calibrates the flow sensor at zero flow The Calibrate Flow B Zero screen functions the same way Note The pump must be disconnected before performing the zero calibration e Inthe Main Menu choose Service gt Select Flow Calibration A or B gt Zero e Press to save the current flow reading as the zero reading Calibrate Flow Span The Calibrate Flow A Span screen allows the user to view and set the flow sensor calibrate span point The calibrate Flow B Span screen functions the same way Note An independent flow sensor is required to read the flow then the operat
43. gt is the Instrument Address Each subsequent measurement attached to the response will have the lt address X gt where X keeps incrementing by 1 for each measurement included lt measured value gt is the concentration value in currently selected gas units represented as exponential representation with 4 characters mantissa and 2 characters exponent each with sign Mantissa sign and 4 digits The decimal point is assumed to be after the first digit and is not transmitted Exponent sign and 2 digits Example 5384000 0is represented as 5384 06 0 04567is represented as 4567 02 lt status gt is formed by lt operating status gt and lt error status gt and separated by a space i e lt operating status gt lt SP gt lt error status gt Each of the two lt operating status gt and lt error status gt are formed by two characters each representing a 2 digit hex number which is one byte 8 Bits operation status and one byte 8 Bits error status These two bytes contain the information about the main operating conditions of the instrument at that instant For details on how to interpret the status bytes refer to Table D 1 and Table D 2 lt SFKT gt is the space provided for future use for special function it currently contains a string of ten 0 s i e lt 0000000000 gt Example Geysitech Protocol with transmission of three concentrations Instrument ID is 1 Operation Status is 03 Error Status is 04
44. max 1000 Receive set alarm pressure max 1000 ok Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual B 15 C Link Protocol Commands Alarms alarm sample flow a min alarm sample flow a max alarm sample flow b min alarm sample flow b max These commands report the cell a and b sample flow alarm minimum and maximum value current settings The example that follows reports that the sample flow alarm minimum value is 0 400 LPM Send alarm sample flow min Receive alarm sample flow min 0 4 l min set alarm sample flow a min value set alarm sample flow b max value set alarm sample flow a min value set alarm sample flow b max value These commands set the cell a or b sample flow alarm minimum and maximum values to value where value is a floating point number representing sample flow alarm limits in liters per minute The example that follows sets the sample flow alarm maximum value to 1 400 LPM Send set alarm sample flow max 1 4 Receive set alarm sample flow max 1 4 ok alarm trig conc 03 This command reports the O3 concentration alarm trigger action for minimum alarm current setting to either floor or ceiling The example that follows shows the O3 concentration minimum alarm trigger to ceiling according to Table B 3 Send alarm trig conc 03 Receive alarm trig conc 03 1 set alarm trig conc 03 value These commands set the O3 concentration alarm minimum value where value is set to either floor or cei
45. may be new or refurbished at the election of Seller All replaced parts shall become the property of Seller Shipment to Buyer of repaired or replacement Products shall be made in accordance with the Delivery provisions of the Seller s Terms and Conditions of Sale Consumables including but not limited to lamps fuses batteries bulbs and other such expendable items are expressly excluded from the warranty under this warranty Notwithstanding the foregoing Products supplied by Seller that are obtained by Seller from an original manufacturer or third party supplier are not warranted by Seller but Seller agrees to assign to Buyer any warranty rights in such Product that Seller may have from the original manufacturer or third party supplier to the extent such assignment is allowed by such original manufacturer or third party supplier In no event shall Seller have any obligation to make repairs replacements or corrections required in whole or in part as the result of i normal wear and tear ii accident disaster or event of force majeure iii misuse fault or negligence of or by Buyer iv use of the Products in a manner for which they were not designed v causes external to the Products such as but not Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual A 1 Warranty limited to power failure or electrical power surges vi improper storage and handling of the Products or vii use of the Products in combi
46. minimum and maximum value current settings The example that follows reports that the alarm bench temperature minimum value is 15 0 C Send alarm bench temp min Receive alarm bench temp 15 0 set alarm bench temp min value set alarm bench temp max value These commands set the bench temperature minimum and maximum value to value where value is a floating point number representing bench temperature alarm limits in degrees C The example that follows sets the alarm bench temperature maximum value to 35 C Send set alarm bench temp max 35 Receive set alarm bench temp max 35 ok alarm conc 03 min alarm conc 03 max These commands report the conc O3 concentrations alarm minimum and maximum value current settings The example that follows reports that the O concentration minimum value is 5 2 ppb Send alarm conc 03 min Receive alarm conc 03 min 5 2 ppb set alarm conc 03 min value set alarm conc 03 max value These commands set the O3 concentration alarm minimum and maximum value to value where value is a floating point representation of the concentration alarm limits The example that follows sets the O3 concentration alarm maximum value to 150 Send set alarm conc oi max Receive set alarm conc oi max 150 ok Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual B 13 C Link Protocol Commands Alarms alarm intensity a min alarm intensity a max alarm intensity b min alarm intensity b max These
47. of points selected e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config 3 44 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu Descriptor The Descriptor screen allows the user to enter the descriptor for the selected analog input channel The descriptor is used in datalogging and streaming data to report what data is being sent out The descriptor may be from 1 to 3 characters in length and defaults to IN1 to IN8 user input channel number e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config gt Select Channel gt Descriptor e Press to save the new descriptor Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 45 Operation Instrument Controls Menu Units The Units screen allows the user to enter the units for the selected analog input channel The units are displayed on the diagnostic screen and in datalogging and streaming data The units may be from 1 to 3 characters in length and defaults to V volts e In the Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config gt Select Channel gt Units e Press to save the new value Decimal Places The Decimal Places screen allows the user to select how many digits are displayed to the right of the decimal from 0 to 6 with a default of 2 e Inthe
48. of the data response and interpreted as a string 03 18sBd ddd set no coef Ban This is a line which also appears slightly indented The next field is also 03 but the value is taken from the eighteenth element of the data response again interpreted as a string A button appears on this line which when pressed pops up an input dialog which will state Please enter a new value for 03 using a d ddd format The string entered by the user is used to construct the output command If the user enters for example 1 234 the constructed command will be set no coef 1 234 03 21f Code 0 Code 1 Code 2 Code 3 Code 4 Code 5 Code 6 Code 7 Code 8 Code 9 Code 10 Code 11 Lset range no d n This is a line which appears slightly indented the title is again 03 and the value the twenty first element of the data response interpreted as a floating point number There is a no translation button which creates a selection list of twelve Code nn options The number of the user selection is used to create the output command Mode 6 12 13x local remote service service 0 1 Tset mode s n This is a line which has a title of Model and value taken from the sixth field of the data response There is a bitfield extraction of bits 12 through 13 from the source the value type is not important here because the value is being translated to an output string Once the bits have been extracted they are shifted down to the bit zero position Thus the
49. off Reports analyzer program number Sets the pump on or off Simulates pressing a key on the front panel Reports sets current 03 range Commands Page B 43 B 8 B 9 B 25 B 29 B 27 B 18 B 19 B 20 B 21 B 21 B 22 B 22 B 22 B 32 B 28 B 39 B 22 B 22 B 9 B 27 B 25 B 26 B 10 B 26 B 35 B 11 B 32 B 39 B 33 B 28 B 29 Model 497 Primary Standard Instruction Manual B 7 C Link Protocol Commands Measurements B 8 Measurements Table B 1 C Link Protocol Commands continued Command range mode relay relay stat resp coef ri right ru run sample save save params sc screen sp conc sp field span Sr srec srec format srec layout srec mem size srec per stream per stream time temp comp time up Zero avg time high avg time low avg time Description Reports sets current range mode Reports sets relay logic status of designated relay s Reports sets relay logic status of designated relay s Reports sets the current 03 response coefficient Simulates pressing right pushbutton Simulates pressing run pushbutton Sets zero span valves to sample mode Stores parameters in FLASH Stores parameters in FLASH C series legacy command that reports a generic response Use iscreen instead Reports sets the span concentration for autocalibration Reports sets item number and name in scratch pad list Sets zero span valves to span mode Reports last short record stored Reports
50. press A to select Span The Calibrate Pressure Span screen appears Model 497 Primary Standard Instruction Manual 6 33 Servicing Flow Transducer Replacement 9 Wait at least 10 seconds for the ambient reading to stabilize use C a and t to enter the known barometric pressure and press to save the pressure value 10 Reconnect the instrument tubing to the pressure transducer 11 Install the cover Flow Tra nsducer Use the following procedure to replace the flow transducer Replacement Equipment Required Flow transducer Philips screwdriver Wrench 5 16 inch Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect plumbing from the flow transducer 3 Disconnect the flow transducer cable FLOW A or FLOW B from the measurement interface board 4 Loosen the retaining nuts 2 and remove the faulty flow transducer from the mounting bracket 5 Install the new flow transducer by following the previous steps in reverse 6 Calibrate the flow transducer Refer to the Flow Transducer Calibration procedure that follows 6 34 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Flow Transducer Thermo Fisher Scientific Calibration Servicing Flow Transduce
51. standard cycle or every four seconds fast cycle The analog output ranges are user selectable via software The analog outputs are defaulted based on the measurement range The defaults are calculated by dividing the data values by the full scale range for each of the three parameters and then multiplying each result by the user selected output range Negative concentrations can be represented as long as they are within 5 of full scale The zero and span values may be set by the user to any desired value All electronics operate from a universal switching supply which is capable of auto sensing the input voltage and working over the entire operating range Internal pumps and heaters all operate on 110VAC An optional transformer is required if operating on the 210 250VAC or 90 110VAC ranges An on off switch controls all power to the instrument and is accessible on the front panel The motherboard contains the main processor power supplies a sub processor and serves as the communication hub for the instrument The motherboard receives operator inputs from the front panel mounted function key panel and or over I O connections on the rear panel and sends commands to the other boards to control the functions of the instrument and to collect measurement and diagnostic information The motherboard outputs instrument status and measurement data to the front panel mounted graphics display and to the rear panel I O The motherboard also co
52. the MODBUS Protocol Interface and is supported both over RS 232 485 RTU protocol as well as TCP IP over Ethernet The MODBUS Commands that are implemented are explained in detail in this document The MODBUS protocol support for the Series enables the user to perform the functions of reading the various concentrations and other analog values or variables read the status of the digital outputs of the analyzer and to trigger or simulate the activation of a digital input to the instrument This is achieved by using the supported MODBUS commands listed below For details of the Model 497 Primary Standard MODBUS Protocol specification see the following topics e Serial Communication Parameters on page C 2 describes the parameters used to support MODBUS RTU protocol e TCP Communication Parameters on page C 2 describes the parameters used for TCP connection e Application Data Unit Definition on page C 2 describes the formats used over serial and TCP IP e Function Codes on page C 3 describes the various function codes supported by the instrument e MODBUS Commands Supported on page C 8 lists the MODBUS commands supported in Table C 1 through Table C 3 Additional information on the MODBUS protocol can be obtained at http www modbus org References are from MODBUS Application Protocol Specification V1 la MODBUS IDA June 4 2004 Thermo Fisher Scientific Model 497 Primary Standard Instruction
53. the Main Menu choose Service gt O3 Response Coefficient e Use the t and to increment or decrement the numeric value e Press to save the new coefficient Manual 0 Lamp Setting The Manual O3 Lamp Setting screen is used to manually control the O3 output concentration by adjusting the ozonator lamp intensity In this mode the automatic feedback control of the ozonator is defeated This is Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 71 Operation Service Menu useful to determine how much ozone is produced at a certain percentage of lamp intensity The pressure calibration is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in this chapter Note This adjustment should only be performed by an instrument service technician e Inthe Main Menu choose Service gt Manual O3 Lamp Setting Pressure Calibration The Pressure Calibration menu is used to calibrate the pressure sensor to zero span or restore factory default values The pressure calibration is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in this chapter The pressure sensor s zero counts and span slope are displayed on the menu Note This adjustment should only be performed by an instrument service technician a e In the Main Menu choose Service gt Pressure C
54. the current O3 response coefficient The example that follows reports that the O3 response coefficient is 1 000 Model 497 Primary Standard Instruction Manual B 25 C Link Protocol Commands Calibration Send resp coef Receive resp coef 1 000 set resp coef value This command sets the O3 response coefficient to user defined values to value where value is a floating point representation of the coefficient The example that follows sets the O3 response coefficient to 1 500 Send set resp coef 1 500 Receive set resp coef 1 500 ok set 03 conc This command sets the O3 concentation to a user defined value The following example sets the O3 concentation to 500 ppb Send set 03 conc 500 Receive set oi conc 500 ok o3 setting This command reports what the O concentation the calibrator is set to output The following example reports that the calibrator is set to output 500 ppb Send 03 setting Receive 03 setting 0500 o3 gas high 03 gas low 03 gas These commands report the low O3 span gas concentrations used to auto calibrate low O3 coefficients The high and low commands are only available in dual and auto range mode If the mode is incorrect the instrument responds with can t wrong settings The example that follows shows that the O3 low span gas concentration is 240 0 ppm Send low 03 gas Receive low 03 gas 2400E 1 ppm set 03 gas value set high 03 gas value set low 03 gas value These commands se
55. the locations to facilitate reconnection 6 26 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Servicing Photometer Lamp Replacement 3 Remove the two screws from the top of the board 4 Pop off the board from the bottom mounting studs and remove the board 5 To install the new photometer board follow previous steps in reverse Photometer Lam H Equipment required Replacement Photometer lamp Allen wrench 7 64 inch and 3 32 inch Screwdriver flat medium size Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component Use the following procedure to replace the photometer lamp 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the photometer lamp cable from the LAMP connector on the photometer board 3 Remove the two retaining screws from the rear panel access hole cover on the rear panel and remove the cover 4 Slide the insulation off the end of the lamp 5 Loosen Allen screw on lamp clamp 6 Loosen two screws holding the clamp to the optical bench Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 27 Servicing Photometer Lamp Voltage Adjustment 7 Carefully slide lamp out of bench and instrument case through access hole 8 Carefully slide new lamp into place until it bottoms Loosely
56. tighten the Allen screw on clamp Tighten two screws holding the clamp to the optical bench Pull the lamp out approximately 1 32 inch to 1 16 inch to allow for expansion when the lamp warms up tighten Allen screw on the clamp 9 Plug new photometer lamp cable into the LAMP connector on the photometer board 10 Slide the insulation back on the end of the lamp 11 Replace access hole cover and secure with the two retaining screws 12 Re install the instrument cover 13 Reconnect power and turn instrument ON 14 After lamp has stabilized approximately 15 minutes adjust the lamp voltage in the Service Mode menu until the output from each detector is about 100 kHz Photometer Lamp Use the following procedure to adjust the photometer lamp voltage until the Voltage Adj ustment output from each detector is approximately 100 kHz Note After turning power ON wait for the lamp to stabilize approximately 15 minutes before beginning the following lamp voltage adjustment procedure 1 From the Main Menu press to scroll to Service gt press zi gt p to scroll to Lamp Setting gt and press Ce The Bench Lamp Setting screen appears 6 28 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Sample Reference Replacement Thermo Fisher Scientific Solenoid A Servicing Sample Reference Solenoid Replacement Note If Service is not displayed refer to Accessing the Service Mode on
57. 0173 cellbi 99780 bncht 3 258e 01 lmpt 5 366e 01 o3lt 6672e 01 flowa 7 318e 01 flowb 7 301e 01 pres 7 515e 02 23 00 8 17 05 flags c4o0000 03 2 567e 02 cellai 100205 cellbi 99653 bncht 3 291e 01 lmpt 5 372e 01 o3lt 6714e 01 flowa 7 351e 01 flowb 7 302e 01 pres 7 493e 02 where cellai Cell A Intensity cellbi Cell B Intensity bncht Bench Temperature Impt Lamp Temperature 03lt Ozonator Lamp Temperature flowa Cell A Flow flowb Cell B Flow press Pressure erec format srec format Irec format These commands report the output format for long and short records and dynamic data in various formats such as ASCII without text ASCII with text or binary The example that follows shows the output format for long records is ASCII with text according to Table B 4 Send lrec format Receive lrec format 1 B 20 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific C Link Protocol Commands Datalogging set erec format format set lrec format format set srec format format These commands set the output format for long and short records and dynamic data according to able B 4 The example that follows sets the long record output format to ASCII with text Send set lrec format 1 Receive set lrec format 1 ok Table B 4 Record Output Formats Format Output Format 0 ASCII no text 1 ASCII with text 2 binary data erec layout Irec layout srec layout These commands reports the layout st
58. 03 coef set cal low 03 coef These commands will auto calibrate the O3 coefficient based on the O3 span gas concentrations The high and low commands are only available in dual and auto range mode If the mode is incorrect the instrument responds with can t wrong settings The example that follows shows a successful auto calibration of the low O3 coefficient Send set cal low 03 coef Receive set cal low 03 coef ok set cal 03 bkg These commands will auto calibrate the O3 background If the instrument is set to manual O3 mode the response to set O3 bkg will be can t wrong settings The example that follows shows a successful auto calibration of the O3 background Send set cal 03 bkg Receive set cal 03 bkg ok 03 coef high 03 coef low 03 coef These commands report the O3 coefficient in single range mode or the high and low range coefficients in dual or auto range mode If the mode is incorrect the instrument responds with cant wrong settings The example that follows reports that the O3 coefficient is 1 000 Send 03 coef Receive 03 coef 1 000 set 03 coef value set high 03 coef value set low 03 coef value These commands set the O3 coefficient to user defined values to value where value is a floating point representation of the coefficient The example that follows sets the O3 coefficient to 1 005 Send set 03 coef 1 005 Receive set oi coef 1 005 ok resp coef This command reports
59. 1 range to 55 5 ppm Send set custom 1 range 55 5 Receive set custom 1 range 55 5 ok range mode This command reports the current range mode Send range mode Receive range mode single set range mode mode This command sets the current range mode to single dual or auto The example that follows sets the range mode to single Send set range mode single Receive set range mode single ok gas mode This command reports the current mode of sample zero or span The example that follows reports that the gas mode is sample Send gas mode Receive gas mode sample set sample set zero set span Model 497 Primary Standard Instruction Manual B 31 C Link Protocol Commands Measurement Configuration These commands set the current gas mode to sample zero or span The example that follows sets the instrument to span mode that is the instrument is sampling span gas Send set span Receive set span ok set manual This command sets the current gas mode to sample The example that follows sets the instrument to sample mode Send set manual Receive set manual ok gas unit This command reports the current gas units ppm or mg vm The example reports that the gas unit is set to ppb Send gas unit Receive gas unit ppb set gas unit unit ppb ppm g m mg m This command sets the gas units to ppb ppm g m or mg m The example that follows sets the gas units to mg m Send set gas unit mg m
60. 3 Receive set gas unit mg m3 ok pres comp This command reports whether pressure compensation is on or off The example that follows shows that pressure compensation is on Send pres comp Receive pres comp on set pres comp onoff These commands turn the pressure compensation on or off The example that follows turns pressure compensation off Send set pres comp off Receive set pres comp off ok set pump onoff This command turns the pump on or off The example that follows turns the pump off B 32 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Measurement Configuration Send set pump off Receive set pump off ok temp comp This command reports whether temperature compensation is on or off The example that follows shows the temperature compensation is off Send temp comp Receive temp comp off set temp comp onoff These commands turn the temperature compensation on or off The example that follows turns temperature compensation off Send set temp comp off Receive set temp comp off ok l1 conc D conc 13 conc 14 conc These commands report the concentration setting of each of the four custom levels The example that follows reports that custom level 1 is 125 ppb Send 11 conc Receive 11 conc 0125 ppb set 11 conc value set 12 conc value set 13 conc value set 14 conc value set 15 conc value These commands set the con
61. 65 Service Moni EE 3 66 PHS SS C Reck cryno uT EEUNA EIEEE 3 67 enee 3 69 Detector E O airian inanir T EiT 3 69 i e E E E E qseeeeenes 3 70 Oe Repone Coc E a 3 7 1 Manual Os Lamp SUUE eserine e Fl Pressure Mi lO apart os tesco canes NE E 3 72 Flow A and B Calibration sscscsosssonweoesenaaesonssanencoanennsanncnersees 3 74 Tempera E 3 76 Analog Output Ee 3 77 Analog Input Cal Drato sieisen ie 3 79 Dipo NW KE 3 81 Restore User IDS ail tS sen egene 3 81 Thermo Fisher Scientific Thermo Fisher Scientific Chapter 4 Chapter 5 Chapter 6 Contents Password ett 3 82 Set ASSOC WEE 3 82 Lock Instrument E 3 82 DE ON E 3 83 Remove 17 AGS Oi E 3 83 Unlock Teen gege 3 84 Preventive Maintenance cccccssseesseeeeseeseseeeeseeeeeeaes 4 1 Say EE 4 2 eelere eege 4 2 EE Case E 4 2 Opu eege 4 2 kanp Rop AC EE 4 3 Monitoring Detector Frequencies and Notse 4 4 IFE io E 4 4 Monitoring Lamp E 4 5 EE 4 5 Porp FR DCA A pcs eccee qovieeeeys nnen anieri eian iieri 4 6 Leak Test and Pump Checkoutasscarianicoisareraominniiis 4 7 Pecna eebe 4 7 Solen id Leaks as scsrscne ves iceecnsveane veteaaeomsanetoserdusaaniaaheaneoeswiasss 4 8 Soleno d Leak WeSC EEN 4 9 Troubleshooting ee 5 1 E P S a E E E E 5 1 deeg eege eeii n a A 5 2 Board Level Connection Diagrams ssssssesesesssseressresssrsssressees 5 6 Connector Pin Descriptions peer eer errr ENEE nI 5 8 EY e E EE 5 21 SEENEN 6 1 DA EE 6 3 Berri Ae Cett
62. 9 64 inch and 1 16 inch amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a Equipment Damage Some internal components can be damaged by small 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the detector electrical connections CHA and CHB from the measurement interface board 3 Loosen the two screws securing the detector clamping block to the optical bench and remove the clamping block and detectors Figure 6 12 6 30 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Servicing Pressure Transducer Replacement Clamping Block Screws 2 Detector Screws 2 Detectors Figure 6 12 Replacing the Detectors 4 Loosen the Allen screw s securing the detector s in detector block and remove the detector s 5 Install the new detector s by following the above steps in reverse 6 Calibrate the instrument Refer to the Calibration chapter in this manual Pressu re Tra nsducer Use the following procedure to replace the pressure transducer Replacement Equipment Required Pressure transducer assembly Philips screwdriver amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a Equipment Damage Some internal components can be damaged by small 1 Turn instrument OFF unplug the power cord and remove the
63. Analog Output Configuration menu displays a list of the analog output channels available for configuration Channel choices include all voltage channels all current channels voltage channels 1 6 and current channels 3 40 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Select Output Range Thermo Fisher Scientific Operation Instrument Controls Menu 1 6 if the I O expansion board option is installed Configuration choices include selecting range setting minimum maximum values and choosing signal to output e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Output Config e Use and to scroll through a list of choices e Press to select a choice The Select Output Range screen is used to select the hardware range for the selected analog output channel Possible ranges for the voltage outputs are 0 100 mV 0 1 0 5 0 10 V e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Output Config gt Select Channel gt Select Range e Use and to scroll through a list of choices e Press to save the new range Model 497 Primary Standard Instruction Manual 3 41 Operation Instrument Controls Menu ep CHANGE VOLIE Minimum and Maximum Value The MinimumValue screen is used to edit the zero 0 to full scale 100 value in percentages for the selected analog output channel See Table 3 6 for a list
64. Binary Responses Format Specifier for Front Panel Layout Thermo Fisher Scientific C Link Protocol Commands Record Layout Definition The first line of the Layout response is the scanf like parameter list for parsing the fields from an ASCII ERec response Parameters are separated by spaces and the line is terminated by a n the normal line separator character Valid fields are Ae parse yd parse ld parse yf parse string decimal number long 32 bit decimal number floating point number x parse a hexadecimal number 41x parse a long 32 bit hex number AT ignore the field d d d d d d Note Signed versus unsigned for the integer values does not matter it is handled automatically a The second line of the Layout response is the binary parameter list for parsing the fields from a binary response Parameters MUST be separated by spaces and the line is terminated by a n Valid fields are parse a time specifier 2 bytes parse a date specifier 3 bytes ignore one 8 bit character 1 byte parse a 24 bit floating point number 3 bytes n x parse a 24 bit floating point number 3 bytes N x parse a 32 bit floating point number 4 bytes parse an 8 bit signed number 1 byte parse an 8 bit unsigned number 1 byte parse a 16 bit signed number 2 bytes parse a 16 bit unsigned number 2 bytes parse a 24 bit signed number 3 bytes parse a 24 bit unsigned number 3
65. Board PCB Assemblies in the Installation chapter for information on attaching the cable to the connector board For associated part numbers refer to External Device Connection Components in the Servicing chapter The analyzer can be installed in the configurations described in Table 8 3 and shown in Figure 8 1 through Figure 8 4 Table 8 3 Mounting Options Mounting Type Description Bench Positioned on bench includes mounting feet and front panel side trim ears Model 497 Primary Standard Instruction Manual 8 3 Optional Equipment Mounting Options Table 8 3 Mounting Options Mounting Type Description EIA rack Mounted in an EIA style rack includes mounting slides and front panel ElA rack mounting ears Retrofit rack Mounted in a Thermo non ElA rack includes mounting slides and retrofit front panel rack mounting ears F Le ke Le rP ka Le Le Lei Let Figure 8 1 Rack Mount Option Assembly 8 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific G 3 jenuey UONINASU PIEPURIS Aewnd 267 I3PON DIMUBIIS JOUSI4 OWY Buljunoj youag 2 8 ni DIJMUBIIS 1 yS14 OWBU jenuey uoNanAsu psepuels MEW 16y IPON 9 8 Buunoy J324 up E 8 aan ae O6L s igi AH L 8 jenuey UONINASU PIEPURIS AIS 267 I3PON DIMUBIIS JOUSI4 OWY Buljunoy yOeY 71401734 p g an Optional Equipment Mounting Options 8 8 Model 497 Primary Standard Instruct
66. C PUMP connector on the measurement interface board Connect a calibrated flow sensor at the SAMPLE bulkhead on the rear panel Press nl to return to the Flow A Sensor Cal screen At the Flow A Sensor Cal screen press to select Span The Calibrate Flow A Span screen appears Wait at least 10 seconds for the reading to stabilize use gt and to enter the flow sensor reading and press to save the value Install the cover Use the following procedure to replace the ozonator lamp Equipment Required Ozonator lamp Allen wrench 7 64 inch Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component be 6 36 Model 497 Primary Standard Instruction Manual Turn instrument OFF unplug the power cord and remove the cover Thermo Fisher Scientific Ozonator Lamp Heater Replacement Thermo Fisher Scientific Servicing Ozonator Lamp Heater Replacement 2 Unplug the ozonator lamp cable from the LAMP connector on ozonator board Figure 6 13 g Kei ZON ER Ozonator Board Figure 6 13 Ozonator Board Location 3 Slide insulation off the lamp handle onto the lamp cord Loosen both lamp clamp screws Carefully slide lamp out of ozonator housing Slide insulation off of old lamp and slide onto new lamp Carefully slide new lamp into ozonator ho
67. CD polarizing plate is very fragile handle it carefully Do not wipe the LCD polarizing plate with a dry cloth it may easily scratch the plate Do not use alcohol acetone MEK or other Ketone based or aromatic solvents to clean the module use a soft cloth moistened with a naphtha cleaning solvent a Do not place the LCD module near organic solvents or corrosive gases a Do not shake or jolt the LCD module a 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the ribbon cable and the two wire connector from the front panel board 3 Remove the four screws at the corners of the LCD module 4 Slide the LCD module out towards the right and rear of the instrument 5 Replace the LCD module by following previous steps in reverse 6 24 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Servicing Optical Bench Replacement Optical Bench Use the following procedure to replace the optical bench Figure 6 11 Replacement Equipment required Optical bench Screwdriver flatblade amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a Equipment Damage Some internal components can be damaged by small Use the following procedure to replace the optical bench 1 Turn instrument OFF unplug the power cord and remove the cover 2 Disconnect the plumbing and electrical connections 3 Remove t
68. Configuration gt Output Relay Settings gt Select Relay gt Instrument State Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 37 Operation Instrument Controls Menu Alarms The Alarms status screen allows the user to select the alarm status for the selected relay output The selected item is shown by lt after it The I O board status alarm is present only if the I O expansion board is installed The zero and span check calibration alarms are present only if the zero span valve option is installed and the instrument is operating in manual mode e In the Main Menu choose Instrument Controls gt I O Configuration gt Output Relay Settings gt Select Relay gt Instrument State gt Alarms e Use t and to scroll through a list of choices e Press to save the new selection for the relay Non Alarm The Non Alarm status screen allows the user to select the non alarm status for the selected relay output The selected item is shown by lt after it e In the Main Menu choose Instrument Controls gt I O Configuration gt Output Relay Settings gt Select Relay gt Instrument State gt Non Alarm e Use and to scroll through a list of choices e Press to save the new selection for the relay 3 38 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu Digital Input Settings The Digital Input Settings men
69. EF OZ SOL Reference Designator J7 J11 J3 JI J17 J2 site J14 J15 J16 Pin N N Signal Description Ground Measurement Frequency B sample Flow A Sensor Input Ground 15V 15V Ground Bench Temperature Thermistor Ground 24V Ground AC HOT AC NEUT AC Ground 24V Ground AC HOT AC NEUT Switched AC Ground 24V Zero Span Solenoid Control 24V Sample Solenoid Control 24V Reference Solenoid Control 24V Ozone Solenoid Control Table 5 8 Ozonator Power Supply Connector Pin Descriptions Connector Label LAMP Thermo Fisher Scientific Reference Designator JI Pin Signal Description Ozonator Lamp Voltage Out Model 497 Primary Standard Instruction Manual 5 19 Troubleshooting Connector Pin Descriptions 5 20 Table 5 8 Ozonator Power Supply Connector Pin Descriptions continued Connector Label LAMP HEATER INTF Reference Designator J2 Pin Oo Oo A Ww N gt ch CO NY O o A Ww Signal Description Ozonator Lamp Voltage Return Ground Ozonator Lamp Thermistor 1 Ozonator Lamp Heater Control Ground 24V Heater Current Sense Ozonator Lamp Thermistor 2 Ozonator Lamp Intensity Control Voltage Input Ozonator Lamp Intensity Control Voltage Output Ozonator Heater Thermistor 24V Ground Ozonator Lamp On off Control Ground Ground Table 5 9 Photometer Power Supply Connector Pin
70. Manual C 1 MODBUS Protocol Serial Communication Parameters Serial Commun i cat on The following are the communication parameters that are used to configure Parameters the serial port of the Series to support MODBUS RTU protocol Number of Data bits 8 Number of Stop bits 1 Parity None Data rate from 1200 115200 Baud 9600 is default TCP Communication iSeries Instruments support the MODBUS TCP protocol The register Parameters definition is the same as for the serial interface TCP connection port bor MODBUS 502 Appl ication Data Unit Here are the MODBUS ADU Application Data Unit formats over serial Definition and TCP IP Serial Slave Address Error Check Slave Address The MODBUS slave address is a single byte in length This is the same as the instrument ID used for C Link commands and can be between 1 and 127 decimal i e 0x01 hex to 0x7F hex This address is only used for MODBUS RTU over serial connections Note Device ID 0 used for broadcast MODBUS commands is not supported Device IDs 128 through 247 i e 0x80 hex to OxF7 hex are not supported because of limitations imposed by C Link a MBAP Header In MODBUS over TCP IP a MODBUS Application Protocol Header MBAP is used to identify the message This header consists of the following components Transaction Identifier 2 Bytes 0x0000 to OxFFFF Passed back in response Protocol Identifier 2 Bytes 0x00 MODBUS protocol Length 2 Bytes 0x0000 to
71. Measurement Interface Board Replacement on page 6 21 Front Panel Board Replacement on page 6 22 LCD Module Replacement on page 6 23 Optical Bench Replacement on page 6 25 Photometer Board Replacement on page 6 26 Photometer Lamp Replacement on page 6 27 Photometer Lamp Voltage Adjustment on page 6 28 Sample Reference Solenoid Replacement on page 6 29 Detector Replacement on page 6 30 Pressure Transducer Replacement on page 6 31 Pressure Transducer Calibration on page 6 32 Flow Transducer Replacement on page 6 34 Flow Transducer Calibration on page 6 35 Ozonator Lamp Replacement on page 6 36 Ozonator Lamp Heater Replacement on page 6 37 Ozonator Replacement on page 6 39 Ozonator Board Replacement on page 6 39 6 2 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Safety Precautions Thermo Fisher Scientific A A Servicing Safety Precautions Service Locations on page 6 40 Read the safety precautions before beginning any procedures in this chapter WARNING The service procedures in this manual are restricted to qualified service representatives If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired a The Model 497 Primary Standard is supplied with a three wire grounding cord Under no circumstances should this gro
72. Model 49 Primary Standard Instruction Manual UV Photometric 0 Calibrator Part number 102474 00 11Jan2008 SCIENTIFIC 2007 Thermo Fisher Scientific Inc All rights reserved Specifications terms and pricing are subject to change Not all products are available in all countries Please consult your local sales representative for details Thermo Fisher Scientific Air Quality Instruments 27 Forge Parkway Franklin MA 02038 1 508 520 0430 www thermo com aqi Thermo Fisher Scientific WEEE Compliance This product is required to comply with the European Union s Waste Electrical amp Electronic Equipment WEEE Directive 2002 96 EC It is marked with the following symbol Thermo Fisher Scientific has contracted with one or more recycling disposal companies in each EU Member State and this product should be disposed of or recycled through them Further information on Thermo Fisher Scientific s compliance with these Directives the recyclers in your country and information on Thermo Fisher Scientific products which may assist the detection of substances subject to the RoHS Directive are available at www thermo com WEEERoHS WEEE Compliance Thermo Fisher Scientific Chapter 1 Chapter 2 Chapter 3 Contents Introduction ee 1 1 eelere eege 1 2 SE 1 3 Installation E 2 1 ee 2 1 Etgen 2 1 SFU EE 2 3 EN DEVICES cases dere eee eee 2 4 Terminal Board PCB Assembblies 0cccccccssssncessseneecers
73. Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Ozonator Replacement A Ozonator Board Replacement A Thermo Fisher Scientific Servicing Ozonator Replacement Use the following procedure to replace the ozonator Equipment Required Philips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover 2 Unplug heater cable from the LAMP HEATER and LAMP connectors on the ozonator board Figure 6 13 3 Disconnect plumbing from the ozonator 4 Remove the ozonator by removing the two screws securing the ozonator to the floor plate and lifting the ozonator straight up 5 Install new ozonator by following the above procedure in reverse 6 Re install the instrument cover Use the following procedure to replace the ozonator board Figure 6 13 Equipment Required Ozonator board Philips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component 1 Turn instrument OFF unplug the power cord and remove the cover Model 497 Primary Standard Instruction Manual 6 39 Servicing Service Locations 2 Remove the connection cables from
74. OZONATOR LAMP POWER SUPPLY 2 Pin LAMP 6 Pin HEATER PHOTOMETER _ LAMP 2 Pin POWER SUPPLY LAMP 6 Pin HEATER PRESSURE BENCH TEMP THERM ZERO SPAN SOL 7 SAMPLE SOL REF SOL 7 OZ SOL 1 FAN PUMP AC Figure 5 2 Board Level Connection Diagram Measurement System Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 5 7 Troubleshooting Connector Pin Descriptions Connector Pin The connector pin descriptions in Table 5 3 through Table 5 9 can be used Descri ptions along with the board level connection diagrams to troubleshoot board level faults Table 5 3 Motherboard Connector Pin Descriptions Connector Label INTF DATA 10 BASE T EXPANSION BD SPARE DATA LU 5 8 Model 497 Primary Standard Instruction Manual Reference Designator J1 J2 J3 J4 Ji Pin CO N O oO A OQO N gt O N O OI A O N gt O N O OI A O N gt O BR Gl ech Signal Description Ground RS485 to Interface Board RS485 to Interface Board Ethernet Output Ethernet Output Ethernet Input NC NC Ethernet Input NC NC 5V 24V 24V Ground Ground Ground RS485 to Expansion Board RS485 to Expansion Board 5V 24V 24V Ground Ground Ground RS485 to Spare Board RS485 to Spare Board Power Fail Relay N C Contact Ground TIL Input 1 Thermo Fisher Scientific Thermo Fisher Scientific Trou
75. Panel Board Connector Pin Diagram ssesssesseseerseeressresserrseresserese 5 13 I O Expansion Board Optional Connector Pin Descriptions 5 15 Digital Output Board Connector Pin Descriptions drsg egzeeen d ses 5 16 Measurement Interface Board Connector Pin Descriptions 06 5 17 Ozonator Power Supply Connector Pin Descriptions lt sisiscecssasctessscteoeioes 5 19 Photometer Power Supply Connector Pin Descriptions eee 5 20 Model 49i Primary Standard Replacement Parts saicesssscoiecsnascrivanascneusiensnse 6 4 Model49i Primary e EE 6 6 External Device Connection E 6 6 Analog Output Channels and Rear Panel Pin Connections 6 13 Analog Input Channels and Rear Panel Pin Connections ee eee 6 14 RS 232 DB Connector Pin Com AOS Seege 7 11 RS 485 DB Connector E 7 11 Oe EE 8 2 Color Codes for 25 Pin and 37 Pin Cables scsisicanteveceumsseennslctinsieess 8 3 Nion e 8 3 OE E EE B 3 PE E E E E B 9 Plaids Ee N S Ee B 16 Recort Ou ORE PONAS serrer eap EEE E E E B 21 SE T N S aa a ER E N EE EEE B 24 eebe B 30 EE eet B 34 ICs oJ euer B 38 Analog Current Outpat MER speed eege B 40 Analog Voltage Output Range Values cic ictesstireemnicteissteqeditaee B 41 IR B 42 Read Coils for 49i Primary Standard eebe C 8 Read Registers for 491 Primary SiC eege C 9 Write Coils for 49i Primary Standard s ssisssssiiressirsiisoiionnaserssrsnirissuena C 10 Thermo Fisher Scientific Model 497 Primary Standard Instruc
76. Receptacle Assembly Measurement Interface Board to Photometer Board Measurement Interface Board to Ozonator Board Fan Power Cable Table 6 3 lists the standard and optional cables and components used for connecting external devices such as PCs and data loggers to an iSeries Table 6 3 External Device Connection Components Cable List Cable List External Device Connection Components 6 6 Model 497 Primary Standard Instruction Manual Part Number 102562 00 102556 00 102645 00 102646 00 102659 00 6219 102888 00 102891 00 103084 00 Description Terminal Block and Cable Kit DB25 optional Terminal Block and Cable Kit DB37 optional Cable DB37M to Open End Cable Six Feet optional Cable DB37F to Open End Six Feet optional Cable DB25M to Open End Six Feet optional Cable RS 232 optional Terminal Board PCB Assembly DB37F standard with all instruments Terminal Board PCB Assembly DB37M standard with all instruments Terminal Board PCB Assembly DB25M included with optional I O Expansion Board in all instruments Thermo Fisher Scientific I O Expansion Board Optional Fan solenoid Assembly sample Valve Reference Valve Photometer Lamp Thermo Fisher Scientific Servicing External Device Connection Components Motherboard Beete Ozonator Pump a Ge Ce Digital Output Boa
77. Scale procedure that follows Calibrating the Input Use the following procedure to calibrate the input channels to full scale by Channels to Full Scale applying a known voltage to the channels Equipment Required Model 497 Primary Standard Instruction Manual DC voltage source greater than 0 volts and less than 10 volts Connect the known DC voltage source to the input channel 1 8 to be calibrated Figure 6 6 shows the analog input pins and Table 6 5 identifies the associated channels From the Main Menu press to scroll to Service press gt to scroll to Analog Input Calibration and press e The Analog Input Cal screen displays input channels 1 8 At the Analog Input Cal screen press to scroll to the channel selected in Step 1 and press a Press A to scroll to Calibrate Full Scale and press The screen displays the current input voltage for the selected channel Use and to enter the source voltage and press to calibrate the input voltage for the selected channel to the source voltage Thermo Fisher Scientific Servicing Optical Bench Temperature Calibration 6 Press gt to return to the input channels display and repeat Steps 3 5 to calibrate other input channels to the source voltage as necessary Optical Bench Use the following procedure to calibrate the optical bench temperature Temperature Ca libration Equipment Required Calibrated thermometer or 10K 1 Resisto
78. VEL 4 107 OZONATOR LEVEL 5 108 SET BACKGROUND um CALTO LOW SPAN Dual Auto Range mode mn CAL TO HIGH SPAN Dual Auto Range mode Mo OZONATOR SOLENOID ss S 112 AOUTS TO ZERO DS AOUTS TOFS C 10 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Serial Communication Thermo Fisher Scientific Parameters Appendix D Geysitech Bayern Hessen Protocol This appendix provides a description of the Geysitech Bayern Hessen or BH Protocol Interface and is supported both over RS 232 485 as well as TCP IP over Ethernet The Geysitech Commands that are implemented are explained in detail in this document The Geysitech protocol support for the iSeries enables the user to perform the functions of reading the various concentrations and to trigger the instrument to be in sample zero span mode if valid for that instrument This is achieved by using the supported Geysitech commands listed below For details of the Model 497 Primary Standard Geysitech Protocol specification see the following topics Serial Communication Parameters on page D 1 TCP Communication Parameters on page D 2 Instrument Address on page D 2 Abbreviations Used on page D 2 Basic Command Structure on page D 2 Block Checksum lt BCC gt on page D 3 Geysitech Commands on page D 3 The following are the communication parameters that are used to configure the serial port of the Series to support Geysitec
79. addr nm address This command sets the netmask address where address consists of four cc 9D numbers ranging from 0 255 inclusive separated by Send set addr nm 255 255 255 0 Receive set addr nm 255 255 255 0 ok baud This command reports the current baud rate for the serial port RS232 RS485 The example that follows reports that the current baud rate is 9600 Send baud Receive baud 9600 set baud rate rate 1200 2400 4800 9600 19200 38400 57600 115200 This command sets the instrument baud zate The example that follows sets the instrument s baud rate to 115200 Note After the command is sent the baud rate of the sending device must be changed to agree with the instrument Send set baud 115200 Receive set baud 115200 ok dhcp This command reports the current state of use of DHCP on or off DHCP is used to assign an IP address to the analyzer automatically The example that follows shows that DHCP is on Send dhcp Receive dhcp on set dhcp onoff Model 497 Primary Standard Instruction Manual B 37 C Link Protocol Commands Communications Configuration These commands enables and disables the DHCP service by either on or off Changes to this parameter will only take effect when the analyzer is powered up The example that follows sets the DHCP service on Note When DHCP is set to on the user supplied addr gw addr dns addr ip and addr nm parameters are not used a Send
80. aeunese 6 32 Flow Transducer Replacement ease green 6 34 Fow Transducer EE 6 35 Ozonator Tain pe place mie tb ascs tesa sseescacctustenesteutieceraiaces 6 36 7onator Lamp lleater Replacement acisini 6 37 Eed 6 39 Ozonator Board Replace tine We serorpenssaniien kenient rike 6 39 a eege 6 40 Chapter7 System Description ccsssseesssseeseseeeessseeeseeeneeseeen 7 1 Eege 7 1 Optical Bench with Photometer Lamp asicecnsssanicisiesssntesaieced Les IR 7 2 lee eege 7 2 Pressure RE 7 2 KEE ee 7 3 Ozonator Lamp Eeer 7 3 Eegeregie 7 3 Optical Bench Temperature Thermistor ss escceveccestassscesasactes 7 3 Eege 7 3 Sample Reference WEE 7 3 DC ELS EEEN E EE 7 3 ET a e E E te eee 7 4 Monitorning SP E 7 4 Measurement E 7 4 Oupa TEE 7 5 viii Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Chapter 8 Appendix A Appendix B Contents E EEE E E E EE 7 5 Motherboard EE 7 5 Measurement Interface Board 7 6 Dipal ee 7 7 I O Expansion Board Optional cscnsscrccavavinevaneranancrasaacncnss 7 7 Front Panel Connector Board occas cscancavadseassasasancisedtenvaaes iar 7 8 KO ONDON E 7 8 Analog Voltado E 7 8 Analog Current Outputs Optional EE 7 9 Analog Voltage Inputs Optional E 7 9 E ET 7 9 Dicta Tapat aser ne E A E E 7 9 SI NEE 7 10 RS 232 Connection EE 7 11 RS 485 Connection E 7 11 Ethernet erhuele GH tele Connector ueeggese ee r 7 12 Optional SZ UE 8 1 E 8 1 Teflon Part
81. age 4 2 e Outside Case Cleaning on page 4 2 e Optical Bench Cleaning on page 4 2 e Lamp Replacement on page 4 3 e Monitoring Detector Frequencies and Noise on page 4 4 e Capillary Service on page 4 5 e Pump Rebuilding on page 4 6 e Leak Test and Pump Checkout on page 4 7 Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 4 1 Preventive Maintenance Safety Precautions Safety Precautions A A Replacement Parts Outside Case Cleaning A Optical Bench Cleaning A Read the safety precautions before beginning any procedures in this chapter WARNING If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired The Model 497 Primary Standard is supplied with a three wire grounding cord Under no circumstances should this grounding system be defeated Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component For more information about appropriate safety precautions see the Servicing chapter See the Servicing chapter for a list of replacement parts Clean the outside case using a damp cloth being careful not to damage the labels on the case Equipment Damage Do Not use solvents or other cleaning products to clean the outside case
82. al group choices see Select Content above e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Reset to Default Content e Press to reset selected record format and erase record log file data e Press ER to confirm reset Configure Datalogging The Configure Datalogging menu deals with datalogging configuration for the currently selected record type e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Configure Datalogging Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 25 Operation Instrument Controls Menu 3 26 Logging Period Min Memory Allocation Percent The Logging Period Min screen is used to select the logging period in minutes for the record format srec or lrec List of choices include off 1 5 15 30 and 60 minutes default e In the Main Menu choose Instrument Controls gt Datalogging Settings gt Configure Datalogging gt Logging Period Min e Use and to scroll through a list of choices e Press to set the logging period The Memory Allocation Percent screen is used to select the percentage of each record type for both short records and long records Percentages between 0 and 100 are available in increments of 10 Changing this value results in log erasure for both short records and long records e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Configure D
83. alibration 3 72 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Service Menu Calibrate Pressure Zero The Calibrate Pressure Zero screen calibrates the pressure sensor at zero pressure Note A vacuum pump must be connected to the pressure sensor before performing the zero calibration e Inthe Main Menu choose Service gt Pressure Calibration gt Zero e Press to save the current pressure reading as the zero reading Calibrate Pressure Span The Calibrate Pressure Span screen allows the user to view and set the p pressure sensor calibration span point Note The plumbing going to the pressure sensor should be disconnected so the sensor is reading ambient pressure before performing the span calibration The operator should use an independent barometer to measure the ambient pressure and enter the value on this screen before calibrating a e Inthe Main Menu choose Service gt Pressure Calibration gt Span e Use el gt t and to move and change the value e Press to save set to value as actual value rt CHANGE VALUE o SAY Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 73 Operation Service Menu Restore Default Pressure The Restore Default Calibration screen allows the user to reset the pressure Calibration calibration configuration values to factory defaults e Inthe Main Menu choose Service gt Pressure Calibration
84. also makes the data available over the serial or ethernet connection Specifications Thermo Fisher Scientific JUMP ICNS Photometer Preset ranges Custom ranges Zero roise Lower detectable limit Response time Lag time Linearity Flow rate Operating temperature Power requirements Physical dimensions Figure 1 1 Model 497 Primary Standard Flow Schematic Table 1 1 Model 497 Primary Standard Specifications 50 100 200 500 1000 2000 5000 ppb 100 200 500 1000 2000 5000 10000 uginn 50 to 5000 ppb 100 to 10000 g m 0 25 ppb RMS 60 second averaging time 1 ppb 20 seconds 0 95 10 seconds 1 of full scale 1 3 LPM 0 45 C 100 VAC 50 60 Hz 115 VAC 50 60 Hz 220 240 VAC 50 60 Hz 150 watts 16 75 W X 8 62 H X 23 D Model 497 Primary Standard Instruction Manual 1 3 Introduction specifications Photometer Weight Approximately 35 Ibs Analog outputs 6 voltage outputs 0 100 mV 1 5 10 V user selectable 5 of full scale over under range 12 bit resolution user selectable for measurement input alarm output relay logic 100 mA 200 VDC Digital inputs 16 digital inputs user select programmable TTL level pulled high Serial Ports 1 RS 232 or RS 485 with two connectors baud rate 1200 115200 data bits parity and stop bits protocols C Link MODBUS and streaming data all user selectable Ether
85. and gives examples of the communication commands Model 497 Primary Standard Instruction Manual B 1 C Link Protocol Commands Instrument Identification Number Instrument Identification Number Entering Units in PPB Accessing Streaming Data Commands e I O Configuration on page B 40 describes and gives examples of the I O commands e Record Layout Definition on page B 44 describes and gives examples of the record layouts Each command sent to the analyzer must begin with the American Standard Code for Information Interchange ASCII symbol or byte value equivalent of the instrument s identification number plus 128 For example if the instrument ID is set to 25 then each command must begin with the ACSI character code 153 decimal The analyzer ignores any command that does not begin with its instrument identification number If the instrument ID is set to 0 then this byte is not required For more information on changing Instrument ID see Chapter 3 Operation When interfacing to an instrument via C link commands always enter the concentration values in ppb or pg m units For example to set a background value to 20 ppm enter 20000 ppb as the value for the set background command Streaming data is sent out the serial port or the Ethernet port on a user defined periodic basis Streaming data over Ethernet is only generated when a connection is made on TCP port 9881 The analyzer must be in the rem
86. ands Alarms Send set alarm level 1 20 5 Receive set alarm level 1 20 5 ok alarm oz lamp temp min alarm oz lamp temp max These commands report the ozonator lamp temperature minimum and maximum value current settings The example that follows reports that the alarm ozonator lamp temperature minimum value is 52 C Send alarm ozonator lamp temp min Receive alarm ozonator lamp temp 52 0 deg C set alarm oz lamp temp min value set alarm oz lamp temp max value These commands set the ozonator lamp temperature minimum and maximum value to value where value is a floating point number representing bench lamp temperature alarm limits in degrees C The example that follows sets the alarm ozonator lamp temperature maximum value to 58 C Send set alarm ozonator lamp temp max 58 0 Receive set alarm ozonator lamp temp max 58 0 ok alarm pressure min alarm pressure max These commands report the pressure alarm minimum and maximum value current settings The example that follows reports that the pressure alarm minimum value is 200 mmHg Send alarm pressure min Receive alarm pressure min 200 mmHg set alarm pressure min value set alarm pressure max value These commands set the pressure alarm minimum and maximum values to value where value is a floating point number representing pressure alarm limits in millimeters of mercury The example that follows sets the pressure alarm maximum value to 1000 mmHg Send Set alarm pressure
87. atalogging gt Memory Allocation e Use and to scroll through a list of choices e Press to set the percentage for both record types and proceed to the erasure warning screen Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu e Press ER to confirm change Data Treatment The Data Treatment screen is used to select the data type for the selected record whether the data should be averaged over the interval the minimum or maximum used or the current value logged Data treatment doesn t apply to all data just to the concentration measurement All other data points log the current value at the end of the interval e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Configure Datalogging gt Data Treatment e Use t and to scroll through a list of choices e Press to save the data type t CHAHGE VALUE a Communication Settings The Communication Settings menu is used with communications control and configuration e Inthe Main Menu choose Instrument Controls gt Communication Settings Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 27 Operation Instrument Controls Menu Baud Rate The Baud Rate screen is used to set the RS 232 RS 485 interface baud rate Baud rates of 1200 2400 4800 and 9600 19200 38400 57600 and 115200 are available e Inthe Main Menu choose Inst
88. ation reading in the Analog Output Testing procedure differed by more than one percent or after replacing the optional I O expansion board Equipment Required Multimeter 1 Connect a meter to the channel to be adjusted and set to voltage or current as appropriate Figure 6 6 shows the analog output pins and Table 6 4 identifies the associated channels From the Main Menu press to scroll to Service press gt A to scroll to Analog Out Calibration and press ol The Analog Output Cal screen displays Note If Service is not displayed refer to Accessing the Service Mode on page 6 4 then return to the beginning of this step a Model 497 Primary Standard Instruction Manual At the Analog Output Cal screen press to scroll to the voltage channel or current channel corresponding to the rear panel terminal pins where the meter is connected then press With the cursor at Calibrate Zero press a Thermo Fisher Scientific Analog Input Calibration Calibrating the Input Channels to Zero Volts Thermo Fisher Scientific Servicing Analog Input Calibration The Analog Output Cal line displays Zero Note When calibrating the analog output always calibrate zero first and then calibrate full scale 5 Use until the meter reads the value shown in the Set Output To line then press to save the value 6 Press nl to return to the previous screen 7 Press to select Calibrate F
89. ation menu is used to allow for configuration of the 8 streaming data output items streaming interval current data format and current timestamp setting The Choose Item Signal submenu displays a list of the analog output signal group choices to choose from Choices are Concentrations Other Measurements and Analog Inputs if the I O expansion board option is installed e Inthe Main Menu choose Instrument Controls gt Communication Settings gt Streaming Data Config Model 497 Primary Standard Instruction Manual 3 29 Operation Instrument Controls Menu Streaming Data Interval The Streaming Data Interval screen is used to adjust the streaming data interval The following interval times are available 1 2 5 10 20 30 60 90 120 180 240 and 300 seconds e Inthe Main Menu choose Instrument Controls gt Communication Settings gt Streaming Data Config gt Streaming Data Interval e Use and to scroll through a list of choices e Press to save the new streaming data period 3 30 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Concentrations Other Measurements Thermo Fisher Scientific Operation Instrument Controls Menu The Concentrations screen allows the user to select the output signal that is tied to the selected streaming data item The selected item is shown by lt after it e Inthe Main Menu choose Instrument Controls gt Communication Setti
90. ble 3 3 for channels and pin connections For more information about custom ranges see Set Custom Ranges below Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 9 Operation Range Menu 33 ANALOG VOLTAGE OUTPUTS Figure 3 4 Pin Qut of Rear Panel Connector Table 3 3 Default Analog Outputs Channel 1 Oo Oil Sy Wy N Ground Pin 14 33 15 34 17 36 1 0 Terminal Pin 1 O NI OJ 11 2 4 6 8 10 12 Description O3 Analog Output O3 Analog Output None None None None 16 10 19 35 37 Signal Ground Note All channels are user definable If any customization has been made to the analog output configuration the default selections may not apply 3 10 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Range Menu Set Custom Ranges The Set Custom Ranges menu lists three custom ranges Cl C2 and C3 Custom ranges are user defined ranges In the standard range mode any value between 50 ppb 0 05 ppm and 5 000 ppb 5 ppm can be specified as a range In the ug m mg m mode any value between 100 ug m 0 1 mg m and 10 000 ug m 10 mg m can be specified as a range e Inthe Main Menu choose Range gt Set Custom Ranges Custom Ranges The Custom Ranges screen is used to define the custom ranges The display shows the current custom range The next line of the
91. bleshooting Connector Pin Descriptions Table 5 3 Motherboard Connector Pin Descriptions continued Connector Label Reference Designator Pin co co N oo on B Signal Description TTL Input 2 Ground TTL Input 5 TTL Input 7 TTL Input 8 TTL Input 10 Ground TTL Input 13 TTL Input 15 Ground Analog Voltage Output 1 Analog Voltage Output 3 Ground Analog Voltage Output 5 Ground Ground Power Fail Relay COM Power Fail Relay N O Contact Ground TTL Input 3 TTL Input 4 TTL Input 6 Ground TTL Input 9 TTL Input 11 TTL Input 12 TTL Input 14 TTL Input 16 Ground Analog Voltage Output 2 Analog Voltage Output 4 Ground Analog Voltage Output 6 Model 497 Primary Standard Instruction Manual 5 9 Troubleshooting Connector Pin Descriptions Table 5 3 Motherboard Connector Pin Descriptions continued Connector Label SER EN 24V IN DIGITAL 1 0 EXT RS485 24V MONITOR 5 10 Model 497 Primary Standard Instruction Manual Reference Designator J7 J10 J14 J15 J17 Pin 3 co co N O on FP WO N gt oO ech O co co N O0 oO A WW N Signal Description Ground Serial Enable Jumper 3 3V 24V Ground 5V 24V 24V Ground Ground Ground SPI Reset SPI Input SPI Output SPI Board Select SPI Clock RS485 to Rear Panel RS485 to Rear Panel 5V 5V 5V Ground Ground Ground NC NC 24V 24V 24V 24V 24V 24V Po
92. by a The string up to the first will be read and inserted in the text field of the line Value String This is followed by a possible string enclosed in quotes This is used to place a string into the value field Value Source The value source which is the item or word number in the DATA ERec response appears next This is followed by an optional bitfield designator The datum identified by the value source can be printed as a string s hexadecimal x decimal d or floating point f or binary bh number Typically bitfield extractions are only done for decimal or hexadecimal numbers Floating point numbers can be followed with an optional precision specifier which will be used as an argument to printf s f format e g a field of A would be translated into the printf command of 3f Alternately the special character can precede the precision specifier this causes an indirection on the precision specifier which now becomes a field number This is useful when formatting for example numbers which have varying precision depending on the mode of the instrument Binary numbers can also have an optional precision specifier which is used to determine how many bits to print For example the specifier b4 will print the lowest four bits of the parsed number There are serious restrictions on where an s field may appear currently sources and 2 must be s and no others may be e Alarm Information The value sour
93. bytes parse a 32 bit signed number 4 bytes parse a 32 bit unsigned number 4 bytes T e SS Z 5 OQ en PTT EE e St ek l d d d d d d There is an optional single digit d which may follow any of the numeric fields which indicates that after the field has been parsed out the resulting value is to be divided by 104d Thus the 16 bit field 0xFFC6 would be interpreted with the format specifier n3 as the number 0 058 The subsequent lines in the ERec Layout response describe the appearance of the full panel The full instrument panel as it appears on the screen has two columns of lines Each line is composed of three major components 1 a text field 2 a value field and 3 a button None of these three components is required The text field contains statically displayed text Model 497 Primary Standard Instruction Manual B 45 C Link Protocol Commands Record Layout Definition The value field displays values which are parsed out of the response to a DATA ERec command It also displays though background changes alarm status The button when pressed triggers input from either a dialog box or a selection list There are five kinds of buttons B I L T and N Each line in the layout string corresponds to one line on the display The layout string describes each of the three major fields as well as translation mechanisms and corresponding commands Text The first field in the layout string is the text It is delimited
94. ce is followed by optional alarm information indicated by a commercial at sign with a source indicator and a starting bit indicator All alarm information is presumed to be two bits long low and high The bitfield extraction is performed on the integer part of the source Typical alarm information would appear as 6 4 B 46 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Translation Table Selection Table Button Designator Thermo Fisher Scientific Examples C Link Protocol Commands Record Layout Definition Then there appears an optional translation table within braces This is a string of words separated by spaces An example translation table would be Code_0 Code_1 Code_2 Code_3 The value once extracted is used as a zero based index into the translation table to determine the string to display Then there appears an optional selection table within parentheses This is a string of numbers separated by spaces 0 1 The selection table lists the translation table entries which the user may select from when setting the parameter This is not necessarily the same as the entries which may be displayed Then there appears an optional button designator This will be one of B T L T or NI B Indicates a button which pops up an input dialog prompting the user for a new value using the designated input format The input format is specified from the B through the s
95. centration for each of the five custom levels The example that follows sets custom level 1 to 325 ppb Send set 14 conc 325 Receive set 14 conc 325 ok level d This command sets the instrument to level d where d represents custom levels 1 2 3 4 or 5 The example that follows sets the custom level 1 Send set level 1 Receive set level 1 ok Model 497 Primary Standard Instruction Manual B 33 C Link Protocol Commands Hardware Configuration Hardware contrast Configuration This command reports the screen s level of contrast The example that follows shows the screen contrast is 50 according to Table B 7 Send contrast Receive contrast 5 50 set contrast evel This command sets the screen s evel of contrast according to able B 7 The example that follows sets the contrast level to 50 Send set contrast 5 Receive set contrast 5 ok Table B 7 Contrast Levels Level Contrast Level 0 0 10 20 30 40 50 60 70 80 90 100 j co NI Oy ojl By wy NI on date This command reports the current date The example that follows reports the date as December 1 2004 Send date Receive date 12 01 04 set date mm dd yy mm month dd day yy year This command sets the date of the analyzer s internal clock The example that follows sets the date to March 19 2005 B 34 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific
96. col e Instrument Control Command ST e Data Sampling Data Query Command DA There are three control commands supported by the Geysitech protocol This lt control command gt is a single letter which triggers an action in the instrument These commands are active only when service mode is inactive and the zero span option is present Command N switches the instrument gas mode to Zero For the 497 PS command K switches the instrument gas mode to g Level 1 For the 497 command K is not used unless the Sample Cal option is present When the Sample Cal option is present e Ifthe ozonator is present command K switches the instrument gas mode to Level 1 Model 497 Primary Standard Instruction Manual D 3 Geysitech Bayern Hessen Protocol Geysitech Commands Data Sampling Data Query Command DA e If the the ozonator is not present command K switches the instrument gas mode to Span Command M switches the instrument gas mode to Sample for the 497 and Manual for the 492 PS The following are the different acceptable formats of the ST command lt STX gt ST lt address gt lt control command gt lt ETX gt lt BCC gt OR lt STX gt ST lt address gt lt control command gt lt CR gt OR lt STX gt ST lt address gt lt SP gt lt control command gt lt CR gt OR lt STX gt ST lt address gt lt SP gt lt control command gt lt ETX gt lt BCC gt The lt address gt is optional which means it can b
97. commands report the cell a or b intensity alarm minimum and maximum value current settings The example that follows reports that the cell a minimum value is 45000 Hz Send alarm intensity a min Receive alarm intensity a min 45000 Hz set alarm intensity a min value set alarm intensity a max value set alarm intensity b min value set alarm intensity b max value These commands set the cell a or b intensity alarm minimum and maximum value to value where value is a representation of the intensity alarm limits The example that follows sets the cell a intensity alarm maximum value to 150000 Hz Send set alarm intensity a max 150000 Receive set alarm intensity a max 150000 ok alarm level 1 alarm level 2 alarm level 3 alarm level 4 alarm level 5 These commands report the offset value in ppb from the concentration stored at ozonator level 1 5 as the alarm trigger point for that level The example that follows reports that the alarm level 1 offset is 20 5 Send alarm level 1 Receive alarm level 1 20 5 set alarm level 1 value set alarm level 2 value set alarm level 3 value set alarm level 4 value set alarm level 5 value These commands set the offset value in ppb from the concentration stored at ozonator level 1 5 as the alarm trigger point for that level The example that follows sets the alarm level 1 offset to 20 5 B 14 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific C Link Protocol Comm
98. compensation is on the first line of the display represents the current sample pressure When pressure compensation is off the first line of the display shows the standard pressure of 760 mmHg e Inthe Main Menu choose Instrument Controls gt Pressure Compensation e Press to toggle and set the pressure compensation on or off Datalogging Settings The Datalogging Settings menu deals with datalogging e Inthe Main Menu choose Instrument Controls gt Datalogging Settings Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 17 Operation Instrument Controls Menu Select SREC LREC View Logged Data The Select SREC LREC is used to select short record or long record format for other operations in this menu e In the Main Menu choose Instrument Controls gt Datalogging Settings gt Select SREC LREC e Press to toggle and set to either short record or long record format The View Logged Data screen is used to select the start point to view the logged data by number of records or date and time e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Select SREC or LREC gt View Logged Data e Use and to toggle between number of records or date and time e Press to accept 3 18 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu TR CHHMiGe V Number of Records The Number of Reco
99. ctor board interfaces between the motherboard and Board the front panel mounted function key panel and Graphics display It serves as central location to tie the three connectors required for the function key panel the graphics display control lines and the graphics display backlight to a single ribbon cable extending back to the motherboard This board also includes signal buffers for the graphics display control signals and a high voltage power supply for the graphics display backlight UO Components External UO is driven from a generic bus that is capable of controlling the following devices e Analog output voltage and current e Analog input voltage e Digital output TTL levels e Digital input TTL levels Note The instrument has spare solenoid valve drivers and I O support for future expansion a Analog Voltage Outputs The instrument provides six analog voltage outputs Each may be software configured for any one of the following ranges while maintaining a minimum resolution of 12 bits e 0 100mV e 0 1V 0 5V e 0 10V The user can calibrate each analog output zero and span point through firmware At least 5 of full scale over and under range are also supported 7 8 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific System Description 1 0 Components The analog outputs may be assigned to any measurement or diagnostic channel with a user defined range in the units of the selected parameter Th
100. ctor off the fan 4 Remove the four fan mounting screws and remove the fan 5 Install a new fan following the previous steps in reverse Mounting Screws 4 Filter Fan Guard Figure 6 5 Replacing a Fan Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 11 Servicing Analog Output Testing Analog Outp ut Testi DU The analog outputs should be tested if the concentration value on the front panel display disagrees with the analog outputs To check the analog outputs you connect a meter to an analog output channel voltage or current and compare the meter reading with the output value displayed on the Test Analog Outputs screen Equipment Required Multimeter Use the following procedure to test the analog outputs l 6 12 Model 497 Primary Standard Instruction Manual Connect a meter to the channel to be tested Figure 6 6 shows the analog output pins and Table 6 4 identifies the associated channels From the Main Menu press 4 to scroll to Diagnostics press gt E to scroll to Test Analog Outputs and press The Test Analog Outputs screen displays Press to scroll to the channel corresponding to the rear panel terminal pins where the meter is connected and press The Set Analog Outputs screen displays Press A to set the output to zero The Output Set To line displays Zero Check that the meter is displaying a zero value If the meter reading di
101. d Description Clears away all logging records that have been saved Clears away only short records that have been saved Reports sets current screen contrast Sets copies current Irec selection into the scratch pad Sets copies current selections in scratch pad into Irec list Sets copies current selections in scratch pad into srec list Sets copies current selections in scratch pad into stream list Sets copies current srec selection into the scratch pad Sets copies current streaming data selection into the scratch pad Reports sets defined custom range concentration Reports sets current date Sets parameters to default values Reports sets state of use of DHCP Reports diagnostic voltage level for I O expansion board Reports diagnostic voltage level for motherboard Reports diagnostic voltage level for measurement interface board Reports status of the digital inputs Reports sets digital input channel and active state Simulates pressing down pushbutton Reports sets digital output channel and active state Reports outputs of the digital to analog converters per channel Simulates pressing enter pushbutton Returns a brief description of the main operating conditions in the format specified in the commands Returns a brief description of the main operating conditions in the format specified in the command Reports sets erec format ASCII or binary Reports current layout of erec data Reports 8 hexadecimal digits or flags that repres
102. d noise reading of each detector to be determined with either reference or sample gas flow Selecting any of these menu items will disturb the analog outputs e In the Main Menu choose Service gt Intensity Check Intensity A B Check The Intensity A Reference Gas screen read only switches the solenoid valves so that reference gas is flowing through Cell A The intensity and noise reading are displayed The Intensity B Reference Gas screen functions the same way Also the Intensity A and Intensity B Sample Gas screens function the same way only with sample gas instead of reference gas e In the Main Menu choose Service gt Intensity Check gt Int A or B Ref or Sample 3 70 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Service Menu 0 Response Coefficient The O Response Coefficient screen is used to change the response of the ozonator lamp feedback circuit The larger the number the more rapid the response and the higher the noise Smaller numbers have slower response times and less noise Normally this coefficient should be set to 1 0 Valid coefficients range from 0 5 to 1 5 The O3 response coefficient is visible only when the calibrator is in service mode and if the ozonator option is installed For more information on the service mode see Service Mode earlier in this chapter Note This adjustment should only be performed by an instrument service technician e In
103. d short record or streaming data lists using the set copy sp to lrec set copy sp to srec or set copy sp to stream commands Send Set Sp field 5 11 Receive set sp field 5 11 ok stream per This command reports the currently set time interval in seconds for streaming data Send stream per Receive stream per 10 set stream per number value number value 1 2 5 10 20 30 60 90 120 180 240 300 This command sets the time interval between two consecutive streaming data strings to number value in seconds The example that follows sets the number value to 10 seconds Send set stream per 10 Receive set stream per 10 ok stream time This command reports if the streaming data string will have a time stamp attached to it or not according to Table B 5 Send stream time Receive stream time 1 set stream time value This command enables value where value is to attach or disable time stamp to streaming data string according to able B 5 The example that follows attaches a time stamp to streaming data Send set stream time O Receive set stream time O ok Table B 5 Stream Time Values Value Stream Time 0 Attaches time stamp to streaming data string 1 Disables time stamp to streaming data string B 24 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Calibration C Link Protocol Commands Calibration set cal 03 coef set cal high
104. decrement the numeric value e Press to save set to value as actual value 3 62 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Alarms Menu Flow AandB The Flow A screen displays the current sample flow reading in cell A and sets the minimum and maximum alarm limits Acceptable alarm limits range from 0 4 to 1 6 LPM If the pressure reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu The Flow B screen functions the same way e Inthe Main Menu choose Alarms gt Flow A or Flow B Min and Max Flow Limits The Minimum Flow A alarm limit screen is used to change the minimum flow A alarm limit The minimum and maximum flow A and flow B screens function the same way e Inthe Main Menu choose Alarms gt Select Flow gt Min or Max e Use and to increment or decrement the numeric value e Press to save set to value as actual value Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 63 Operation Alarms Menu Intensity A and B The Intensity A screen displays the current lamp intensity reading in Cell A and sets the minimum and maximum alarm limits Acceptable alarm limits range from 45 000 to 150 000 Hertz If the intensity A reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in th
105. default to 5 ppm Therefore whenever you change units you should also check the range settings e In the Main Menu choose Range gt Gas Units e Use and to scroll through a list of choices e Press to save the new units Note If the units change from ppb ppm to ug m mg m or vice versa the instrument should be re calibrated particularly if the user s standard temperature is different from 20 C A display warning will appear that ranges will be defaulted and calibration parameters reset et CHAHGE VALUE SAVE 0 Range The O Range screen defines the concentration range of the analog outputs For example an O3 range of 0 500 ppb restricts the analog output to concentrations between 0 and 500 ppb The display shows the current O3 range The next line of the display is used to change the range Table 3 2 lists the standard ranges 3 8 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Range Menu e Inthe Main Menu choose Range gt O Range e Use and to scroll through a list of choices e Press to save the new range Table 3 2 Standard Ranges ppb ppm ug m mg m 50 0 05 100 0 1 100 0 10 200 0 2 200 0 20 400 0 4 500 0 50 1 000 1 1 000 1 2 000 2 2 000 2 5 000 5 5 000 5 10 000 10 C1 C1 C1 C1 C2 C2 C2 C2 C3 C3 E C3 C1 C2 and C3 are custom ranges The analog outputs are arranged on the rear panel connector as shown in Figure 3 4 See Ta
106. des parameters and functions that are useful when making adjustments or diagnosing the Model 49 Primary Standard For more information about the service mode see Service Menu later in this chapter Note The service mode should be turned off when finished as it prevents remote operation e Inthe Main Menu choose Instrument Controls gt Service Mode e Press to toggle and set the service mode on or off Date Time The Date Time screen allows the user to view and change the system date and time 24 hour format The internal clock is powered by its own battery when instrument power is off Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 49 Operation Diagnostics Menu e Inthe Main Menu choose Instrument Controls gt Date Time e Use al and to move and change the value of the date and time e Press to edit and save the new date and time Diagnostics Menu The Diagnostics menu provides access to diagnostic information and functions This menu is useful when troubleshooting the instrument The analog input readings and analog input voltages are only displayed if the I O expansion board option is installed e Inthe Main Menu choose Diagnostics 3 50 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Diagnostics Menu Program Version The Program Version screen read only shows the version number of the program installed Prior t
107. dure If the Service is not displayed on the Main Menu use the following procedure to display it a At the Main Menu press to scroll to Instrument Controls gt press gt to scroll to Service Mode gt and press 4 a The Service Mode screen appears b Press to toggle the Service Mode to ON c Press nl gt nl to return to the Main Menu d Return to the procedure Table 6 1 lists the replacement parts for the Model 497 Primary Standard major subassemblies Refer to Figure 6 2 to identify the component location Table 6 1 Model 497 Primary Standard Replacement Parts Part Number Description 100480 00 Front Panel Pushbutton Board 101491 16 Processor Board 100533 00 Motherboard 100539 00 Digital Output Board 6 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Part Number 100542 00 102340 00 102496 00 101399 00 101863 00 100874 00 102554 00 102458 00 8645 100895 00 101023 00 102055 00 102441 00 102443 00 102455 00 102439 00 8992 102472 01 8940 100554 00 101426 00 102464 01 102464 02 101055 00 100907 00 8630 4510 14007 4124 102701 00 14697 4291 Servicing Replacement Parts List Table 6 1 Model 497 Primary Standard Replacement Parts continued Description LO Expansion Board Optional Front Panel Connector Board Front Panel Display Transformer 220 240VAC Optional Transformer 100VAC Optional Measurement Int
108. e Analog Input Calibrate Full Scale The Analog Input Calibration Full Scale screen allows the user to calibrate the full scale state of the selected analog input e Inthe Main Menu choose Service gt Analog Input Calibration gt Select Channel gt Calibrate Full Scale Hook up a voltage source of 10 V to the analog input channel e Use the t and to increment or decrement the numeric value e Press to save the value 3 80 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Service Menu Display Pixel Test The Display Pixel Test is used to test the LCD display The display pixel test is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter e In the Main Menu choose Service gt Display Pixel Test e Press to begin test by turning all pixels on then toggle between on or oft Restore User Defaults The Restore User Defaults screen is used to reset the user calibration and configuration values to factory defaults The restore default user is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter e Inthe Main Menu choose Service gt Restore User Defaults e Press to warn and enable restore with al e Press a to overwrite all user settings with factory default values Thermo
109. e Eege 6 4 Accessing the Savice ModE eiris a 6 4 Replhcement E E 6 4 EEN E E 6 6 External Device Connection Components ccesseeeeeseeeeees 6 6 Removing the Measurement Bench and Lowering the Partition ae ele Renee et emerr rarer armen ret een ert errr eres 6 8 eege 6 9 Pamp atc 6 RCE ae reste nner et eee ert ne et enaere ye 6 10 ee ebe 6 11 Ao EE e E 6 12 Model 497 Primary Standard Instruction Manual vil Contents ee 6 14 Analog need 6 15 Calibrating the Input Channels to Zero Volts eee 6 15 Calibrating the Input Channels to Full Scale 6 16 Optical Bench Temperature Calibration 0 ee eeeeeeeeeeeeee 6 17 I O Expansion Board Optional Replacement ss ssssssenen 6 18 Digital Output Board Rep lacente nt ssc catecesiescacncettiepessencects 6 19 tert Rebeet eebe ege 6 20 Measurement Interface Board Replacement icccissi seicsvevsieie 6 21 Front Panel Board ep ace iiem isc scneces cote cosaetaeeiedeanecnteterers 6 22 ECD Module Replace ico sal eae ey terre pre reren E ner 6 23 Optical Bench eenegen 6 25 Photometer Board Replacement sorscccaceiccenvsonstnsassntceraacnaes 6 26 Photometer Lamp Replacement ensani 6 27 Photometer Lamp Voltage Adjustment scceitssccesecerscceaetesccenes 6 28 Sample Reference Solenoid Replacement sisssirsvisisiisssrarssri 6 29 Detector EE 6 30 Pressure Transducer Replacement srisesasiiisrosiieinaa 6 31 Piessure Transducer Calibration ys deceasascsavinccvavaccavigaxtne
110. e Main Menu e Inthe Main Menu choose Alarms gt Intensity A or Intensity B Min and Max Intensity Limits The Minimum Intensity A alarm limit screen is used to change the minimum intensity A alarm limit The minimum and maximum intensity A and intensity B screens function the same way e Inthe Main Menu choose Alarms gt Select Intensity gt Min or Max e Use and to increment or decrement the numeric value e Press to save set to value as actual value 3 64 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific 0 Concentration Min and Max 03 Concentration Thermo Fisher Scientific Limits Operation Alarms Menu The O3 Concentration screen displays the current O3 concentration and sets the minimum and maximum alarm limits Acceptable alarm limits range from 0 to 5 000 ppb The minimum alarm may be programmed as a floor trigger alarm is triggered when the concentration falls below the minimum value or a ceiling trigger alarm is triggered when the concentration goes above the minimum value If the O3 concentration goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu Inthe Main Menu choose Alarms gt O3 Concentration The Minimum O3 Concentration alarm limit screen is used to change the minimum O concentration alarm limit The minimum and maximum O3 concentration alarm limit scree
111. e Overview on page 3 4 describes the menu driven software and submenus e Range Menu on page 3 7 describes the gas units O3 range and custom ranges e Averaging Time on page 3 12 describes the averaging period applied to O3 measurements e Calibration Factors Menu on page 3 12 describes the calibration factors used to make minor corrections to the Oz measurement readings s Instrument Controls Menu on page 3 15 describes the items that control the calibrator e Diagnostics Menu on page 3 50 describes the diagnostic information and functions e Alarms Menu on page 3 58 describes a list of items that are monitored by the calibrator e Service Menu on page 3 66 describes service related menu items e Password Menu on page 3 82 describes how to enter change a password lock and unlock the calibrator Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 1 Operation Display Display The 320 x 240 graphics liquid crystal display LCD shows the sample concentrations instrument parameters instrument controls help and error messages Some menus contain more items than can be displayed at one time For these menus use and to move the cursor up and down to each item gt KR 4 Ki J B cl Y J N J Y J j ly N D re DN CG lt 2 SC
112. e S A OW A Temp Not Used ow B Compensatior ntensity A a e ntensity B off Ozone Concentration Alarm d off N j EH W elelaa U NEE Gas Mode Status S 1 SS 01 1 on Not Used i 10 mg m O00 zero 11 yg m yh alarm JO1 oz level 1 10 oz level 2 J11 oz level 3 Hex to Binary Conversion Table 100 oz level 4 Cal BO sch X j ch a C 00 LU UU ei CH Se II 2 U J E 4 1 a C 40 Eh H U E U 111 Vd F Figure B 1 Flag Status Alarms alarm bench lamp temp min alarm bench lamp temp max These commands report the bench lamp temperature minimum and maximum value current settings The example that follows reports that the alarm bench lamp temperature minimum value is 52 C Send alarm bench lamp temp min Receive alarm bench lamp temp 52 0 deg C set alarm bench lamp temp min value set alarm bench lamp temp max value These commands set the bench lamp temperature minimum and maximum value to value where value is a floating point number representing bench lamp temperature alarm limits in degrees C The example that follows sets the alarm bench lamp temperature maximum value to 58 C B 12 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific C Link Protocol Commands Alarms Send set alarm bench lamp temp max 58 0 Receive set alarm bench lamp temp max 58 0 ok alarm bench temp min alarm bench temp max These commands report the bench temperature
113. e active state assigned to output channel The example that follows reports the input 4 to be assigned an index number 11 corresponding to general alarm with the active state being open Send dout 4 Receive dout 4 11 GEN ALARM open set dout channel index state This command assigns digital output channel to be assigned to the action associated with index and assigns it an active state of state open or closed Send set dout 4 11 open Receive set dout 4 11 open ok dtoa channel This reports the outputs of the 6 or 12 digital to analog converters according to Table B 11 The example that follows shows that the DAC 1 is 97 7 full scale Send dtoa 1 Receive doa 1 97 7 Note All channel ranges are user definable If any customization has been made to the analog output configuration the default selections may not apply Table B 11 Default Output Assignment DtoA Function 1 Voltage Output Voltage Output Voltage Output Voltage Output Voltage Output Voltage Output N OM Oil A Wy N Current Output B 42 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific C Link Protocol Commands I O Configuration Table B 11 Default Outout Assignment continued DtoA Function 8 Current Output 9 CurrentOutput 10 Current Output mi Current Output 12 Current Output list var aout list var dout list var din These commands report the list of index numbers and the variables associated with t
114. e left out completely The lt address gt if present must match the Instrument Address Additional space can be present after the lt address gt If the received command does not satisfy the above formats or if the lt address gt does not match the Instrument Address the command is ignored This is a sample command to switch the instrument to zero mode instrument id 5 lt STX gt ST005 lt SP gt N lt CR gt s This command DA initiates a data transfer from the instrument The instrument responds with measurement data which depends on the range mode and is listed in Measurements Reported in Response to DA Command for 49i and 49i PS on page D 7 The command structure for a data query command is as follows lt STX gt DA lt address gt lt ETX gt lt BCC gt D 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Geysitech Bayern Hessen Protocol Geysitech Commands The lt address gt is optional which means it can be left out completely The lt address gt if present must match the Instrument Address Additional space can be present after the lt address gt If the lt address gt is left out then no space is allowed in the query string A command with no address is also a valid command The following are the different acceptable formats of the DA command with Instrument Address 5 lt STX gt DA lt CR gt lt STX gt DA005 lt CR gt lt S TX gt DA lt SP gt lt SP gt 5 l
115. e mode Send Sp conc Receive sp conc 1000 set sp conc value set high sp conc value set low sp conc value These commands set the span concentrations to user defined values to value where value is a floating point representation of the span concentration in current selected units The example below sets the span concentration to 1000 ppb in the single range mode Model 497 Primary Standard Instruction Manual B 27 C Link Protocol Commands Keys Display Keys Display Send set sp conc 1000 Receive set sp conc 1000 ok push button do down en enter he help le left me menu ri right ru run button do down en enter he help le left me menu ri right ru run up 1 2 3 4 These commands simulates pressing the front panel pushbuttons The numbers represent the front panel soft keys from left to right Send push enter Receive push enter ok isc iscreen This command retrieves the framebuffer data used for the display on the iSeries instrument It is 19200 bytes in size 2 bits per pixel 4 pixels per byte arranged as 320 by 240 characters The data is sent in RLE encoded form to save time in transmission It is sent as a type 3 binary c_link response with no checksum B 28 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific C Link Protocol Commands Measurement Configuration The RLE encoding consists of a 0 followed by an 8 bit count of consecutive OxFF bytes T
116. e serial number and program number of the instrument This chapter provides the following troubleshooting and service support information e Safety Precautions on page 5 1 e Troubleshooting Guides on page 5 2 e Board Level Connection Diagrams on page 5 6 e Connector Pin Descriptions on page 5 8 e Service Locations on page 5 21 Safety Precautions Read the safety precautions in the Preface and the Servicing chapter before performing any actions listed in this chapter Thermo Fisher Scientific Model 497 Primary Standard Primary Standard Instruction Manual 5 1 Troubleshooting Troubleshooting Guides Troubleshooti ng The troubleshooting guides presented in this chapter are designed to help Guides isolate and identify instrument problems Table 5 1 provides general troubleshooting information and indicates the checks that you should perform if you experience an instrument problem Table 5 2 lists all the alarm messages you may see on the graphics display and provides recommendations about how to resolve the alarm condition Table 5 1 Troubleshooting General Guide Malfunction Does not start up Cell Aor B frequency high Cell A and B frequency high Cell A or B frequency low or zero Cell A and B frequency low or zero 5 2 Model 497 Primary Standard Instruction Manual Possible Cause No power Power supply Light adjustment Defective detector Lamp supply Light adjus
117. e voltage outputs are independent of the current outputs Analog Current Outputs The optional I O Expansion board includes six isolated current outputs Option al These are software configured for any one of the following ranges while maintaining a minimum resolution of 11 bits e 0 20 mA e 4 20 mA The user can calibrate each analog output zero and span point through firmware At least 5 of full scale over and under range are also supported The analog outputs may be assigned to any measurement or diagnostic channel with a user defined range in the units of the selected parameter The current outputs are independent of the voltage outputs The current outputs are isolated from the instrument power and ground but they share a common return line Isolated GND Analog Voltage Inputs The optional I O expansion board includes eight analog voltage inputs Optional These inputs are used to gather measurement data from third party devices such as meteorological equipment The user may assign a label unit and a voltage to user defined unit conversion table up to 16 points All voltage inputs have a resolution of 12 bits over the range of 0 to 10 volts Digital Relay Outputs The instrument includes one power fail relay on motherboard and ten digital output relays on the digital output board These are reed relays rated for at least 500 mA 200VDC The power fail relay is Form C both normally opened and normally closed contacts All oth
118. ed set relay open set relay open value set relay closed set relay closed value These commands set the relay logic to normally open or closed for relay number value where value is the relay between 1 and 16 The example that follows sets the relay no 1 logic to normally open Note If the command is sent without an appended relay number then all the relays are assigned the set logic of normally open closed a Send set relay open 1 Receive set relay open 1 ok The Erec Lrec and Srec Layouts contain the following e A format specifier for parsing ASCII responses e A format specifier for parsing binary responses In addition to these the Erec Layout contains e A format specifier for producing the front panel displays In operation values are read in using either the ASCII or binary format specifiers and converted to uniform internal representations 32 bit floats or 32 bit integers These values are converted into text for display on the screen using the format specifier for the front panel display Normally the specifier used to parse a particular datum from the input stream will be strongly related to the specifier used to display it e g all of the floating point inputs will be displayed with an f output specifier and all of the integer inputs will be displayed with a d specifier B 44 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Format Specifier for ASCII Responses Format Specifier for
119. ed concentration is not a valid span value either higher than the selected range or 0 or lower a Model 497 Primary Standard Instruction Manual 3 13 Operation Calibration Factors Menu s Inthe Main Menu choose Calibration Factors gt O3 Coef e Use and to increment or decrement the coefficient value e Press to save the new coefficient Reset User Calibration Default The Reset User Calibration Default screen allows the user to reset the calibration configuration values to factory defaults e Inthe Main Menu choose Service gt Calibration Factors gt Reset User Cal Defaults e Press to warn user and enable restore with EW e Usel e to reset the calibration pressure reference value when pressed after e 3 14 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu Instrument Controls The Instrument Controls menu contains items that control the calibrator Menu e Inthe Main Menu choose Instrument Controls Custom Levels The Custom Levels menu contains four custom levels 1 2 3 4 and 5 In the Run screen use to scroll through Zero Level 1 Level 2 Level 3 Level 4 Level 5 Press enter to select a custom level zero e Inthe Main Menu choose Instrument Controls gt Custom Levels Custom Levels The Custom Levels screen is used for setting user defined concentration levels e Inthe Main Menu choose Instrument Controls
120. een or to return to the Run screen The four arrow pushbuttons l l and move the cursor up down left and right or change values and states in specific screens The is used to select a menu item accept set save a change and or toggle on off functions Model 497 Primary Standard Instruction Manual 3 3 Operation Software Overview Soft Keys The Soft Keys are multi functional keys that use part of the display to identify their function at any moment The function of the soft keys allow immediate access to the menu structure and most often used menus and screens They are located directly underneath the display and as the keys functions change this is indicated by user defined labels in the lower part of the display so that the user knows what the keys are to be used for To change a soft key place the menu cursor gt on the item of the selected menu or screen you wish to set Press followed by the selected soft key within 1 second of pressing the right arrow key The edit soft key prompt will be displayed for configuration for the new label Note Not all menu items may be assigned to soft keys If a particular menu or screen item cannot be assigned the key assignment screen will not come up upon entering right arrow soft key combinations All items under the Service menu including the menu itself cannot be assigned soft keys a Software Overview The Model 49 Primary Standard utilizes the menu driv
121. een is used to edit the netmask The netmask is used to determine the subnet the instrument uses to directly communicate with other devices The netmask can only be changed when DHCP is OFE For more information on DHCP see Use DHCP e Inthe Main Menu choose Instrument Controls gt Communication Settings gt TCP IP Settings gt Netmask e Use al and to move and change the value of the netmask 3 34 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Operation Instrument Controls Menu e Press to save the new netmask Defalt Gateway The Default Gateway screen is used to edit the gateway address Any traffic to addresses that are not on the local subnet will be routed through this address The default gateway can only be changed when DHCP is OFF For more information on DHCP see Use DHCP e Inthe Main Menu choose Instrument Controls gt Communication Settings gt TCP IP Settings gt Gateway e Use EC gt t and to move and change the value of the gateway address e Press to save the new address Host Name The host name screen is used to edit the host name When DHCP is enabled this name is reported to the DHCP server e Inthe Main Menu choose Instrument Controls gt Communication Settings gt TCP IP Settings gt Host Name e Use e gt and to move the cursor or change between the edit
122. en software illustrated by the flowchart in Figure 3 3 The Power Up screen shown at the top of the flowchart is displayed each time the instrument is turned on This screen is displayed while the instrument is warming up and performing self checks After the warm up period the Run screen is automatically displayed The Run screen is the normal operating screen It displays the O3 concentration depending on operating mode From the Run screen the Main Menu can be displayed by pressing _m The Main Menu contains a list of submenus Each submenu contains related parameters and or functions This chapter describes each submenu and screen in detail Refer to the appropriate sections for more information 3 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific bt jenuey UONINASU PIEPURIS Aewnd 267 I3PON sjjnejeg Joen 310 S Y4 S L eXIq Aejdsiq les ndu Boyeuy snjeis pg don sn amp s pg 1 aJEMIJOS UBALG Nus JO WeyIMo g e aniy Oju OEIUO Duo JUSWINIA SU sindjno Bojeuy seL DIMUBIIS JOUSI4 OWWJBU ieo indjno Hojyeuy snjejs gN sajeis Aejoy ieo duet 2u09 O sinduy jeu6ig wu L 94eq Ieo g mold g su Ul s eyog Indu Bojeuy SPO 3211S Ieo V WO v sue s6uipeay 1mdu Bojeuy SB1 U0D UB219S Je gifSSald g Mol 4 SdI ISUS U Byuod O I D
123. ent the Status of the ozonator gas mode and alarms Reports current measured flow in cell a Reports current measured flow in cell b Reports sets current reply termination format Commands Page B 17 B 17 B 34 B 23 B 23 B 23 B 23 B 23 B 23 B 30 B 34 B 35 B 37 B 17 B 17 B 17 B 41 B 41 B 28 B 42 B 42 B 28 B 18 B 19 B 20 B 21 B 11 B 10 B 10 B 38 Model 497 Primary Standard Instruction Manual B 5 C Link Protocol Commands Commands Table B 1 C Link Protocol Commands continued Command Description Page gas mode Reports current mode of sample zero or span B 31 gas unit Reports sets current gas units B 32 he help Simulates pressing help pushbutton B 28 high avg time Reports sets high range averaging time B 8 high 03 Reports 03 concentration calculated with high range B 9 coefficients high 03 coef Reports sets high range 03 coefficient B 25 high range Reports selects current 04 high range B 29 high sp conc Sets the high span concentration for autocalibration B 27 host name Reports sets host name string B 38 instr name Reports instrument name B 39 instrument id Reports sets instrument id B 39 isc iscreen Retrieves framebutfer data used for the display B 28 conc _Reports sets the current custom level 1 concentration B Denn Reports sets the current custom level 2 concentration B 3conc _Reports sets the current custom level 3 concentration B l4conc _Report
124. enu driven software Multiple user defined analog outputs Analog input options Fast internal ozonator Fast response time Short lag time Automatic temperature and pressure compensation User selectable digital input output capabilities Standard communications features include RS232 485 and Ethernet C Link MODBUS Geysitech Bayern Hessen protocol and streaming data protocols For details of the calibrator s principle of operation and product specifications see the following topics Principle of Operation on page 1 2 describes the principles by which your calibrator operates Specifications on page 1 3 is a list of the calibrator s performance specifications Model 497 Primary Standard Instruction Manual 1 1 Introduction Principle of Operation Thermo Fisher Scientific is pleased to supply this UV photometric ozone calibrator We are committed to the manufacture of instruments exhibiting high standards of quality performance and workmanship Service personnel are available for assistance with any questions or problems that may arise in the use of this calibrator For more information on servicing see Chapter 7 Servicing Principle of Operation The Model 497 Primary Standard operates on the principle that ozone O3 molecules absorb UV light at a wavelength of 254 nm The degree to which the UV light is absorbed is directly related to the ozone concentration as described by the Beer Lambert Law
125. eption code 1 Byte 0x05 2 Bytes 0x0000 to maximum allowed by instrument 2 Bytes 0x0000 or OxFFOO 1 Byte 0x05 2 Bytes 0x0000 to maximum allowed by instrument 2 Bytes 0x0000 or OxFFOO 1 Byte Function code 0x80 1 Byte 01 IIlegal Function 02 IIlegal Address 03 IIlegal Data 04 Slave Device Failure Here is an example of a request to write Coil 5 ON Request Field Name Function Output Address Hi Output Address Lo Output Value Hi Output Value Lo Thermo Fisher Scientific Hex 05 00 05 Fr 00 Model 497 Primary Standard Instruction Manual C 7 MODBUS Protocol MODBUS Commands Supported Response Field Name Function Output Address Hi Output Address Lo Output Value Hi Output Value Lo Hex 05 00 05 FF 00 MODBUS Commands Table c 1 through table C 3 list the MODBUS commands supported for Supported the Model 497 Primary Standard Table C 1 Read Coils for 497 Primary Standard C 8 Model 497 Primary Standard Instruction Manual Coil Number 1 j Cc NI Om oj By Wy N Status NOT USED SERVICE GAS UNITS ZERO MODE SPAN MODE SAMPLE MODE 0 LEVEL 1 Ox LEVEL 2 0 LEVEL 3 0 LEVEL 4 Oz LEVEL 5 PURGE MODE GEN ALARM CONC MAX ALARM CONC MIN ALARM BENCH TEMP ALARM BENCH LAMP TEMP ALARM O3 LAMP TEMP ALARM PRESSURE ALARM FLOW A ALARM FLOW B ALARM INTENSITY A ALARM Thermo Fisher Scientific Thermo Fisher Scientific Coil Number 23 24 25 26 27 28 29 30 31 32 ce
126. er relays are Form A normally opened contacts and are used to provide alarm status and mode information from the analyzer as well as remote control to other devices such as for controlling valves during calibration The user may select what information is sent out each relay and whether the active state is opened or closed Digital Inputs Sixteen digital inputs are available which may be programmed to signal instrument modes and special conditions including e Zero Gas Mode Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 7 9 System Description 1 0 Components e Span Gas Mode e Set Background e QOvzonator Level 1 5 e Cal to Lo Span e Cal to High Span e Ovzonator Solenoid e Aouts to Zero e Aouts to FS The actual use of these inputs will vary based on analyzer configuration The digital inputs are TTL level compatible and are pulled up within the analyzer The active state can be user defined in firmware Serial Ports Two serial ports allow daisy chaining so that multiple analyzers may be linked using one PC serial port The standard bi directional serial interface can be configured for either RS 232 or RS 485 The serial baud rate is user selectable in firmware for standard speeds from 1200 to 19 200 baud The user can also set the data bits parity and stop bits The following protocols are supported e C Link e Streaming Data e Modbus Slave e Geysitech Bayern Hessen The Streaming Data protocol transmi
127. erate the same response These requests specify the starting address i e the address of the first output specified and the number of outputs The outputs are addressed starting at zero Therefore outputs numbered 1 16 are addressed as 0 15 Model 497 Primary Standard Instruction Manual C 3 MODBUS Protocol Function Codes The outputs in the response message are packed as one per bit of the data field Status is indicated as 1 Active on and 0 Inactive off The LSB of the first data byte contains the output addressed in the query The other outputs follow toward the high order end of this byte and from low order to high order in subsequent bytes If the returned output quantity is not a multiple of eight the remaining bits in the final data byte will be padded with zeros toward the high order end of the byte The Byte Count field specifies the quantity of complete bytes of data Note The values reported may not reflect the state of the actual relays in the instrument as the user may program these outputs for either active closed or open Request Function code 1 Byte 0x01 or 0x02 Starting Address 2 Bytes 0x0000 to maximum allowed by instrument Quantity of outputs 2 Bytes 1 to maximum allowed by instrument Unit Identifier 1 Byte 0x00 to OxFF Passed back in response Response Function code 1 Byte 0x01 or 0x02 Byte count 1 Byte N Output Status n Byte n NorN l N Quantity of Outputs 8 if the remainder not equal t
128. erature is reached A power transistor is used to heat the lamp housing Thermistors sense the housing temperature for heater control and for status information The photometer lamp power supply is similar to the ozonator power supply except for the operating temperature set point and the value of the resistor in series with the output The photometer is always on when the operating temperature is reached Software on off control is not required The digital output board connects to the motherboard and provides solenoid driver outputs and relay contact outputs to a connector located on the rear panel of the instrument Ten relay contacts normally open with power off are provided which are electrically isolated from each other Eight solenoid driver outputs open collector are provided along with a corresponding 24VDC supply pin on the connector The I O expansion board connects to the motherboard and adds the capability to input external analog voltage inputs and to output analog currents via a connector located on the rear panel of the instrument It contains local power supplies a DC DC isolator supply a sub processor Model 497 Primary Standard Instruction Manual 7 7 System Description 1 0 Components and analog circuits Eight analog voltage inputs are provided with an input voltage range of OV to 1OVDC Six current outputs are provided with a normal operating range of 0 to 20 mA Front Panel Connector The front panel conne
129. erface Board Photometer Board Ozonator Assembly Ozonator Lamp Ozonator Power Supply Board Pressure Transducer Assembly Flow Transducer sample Reference Solenoid Assembly Sample Reference Solenoid Valve Air Regulator Assembly Optional Optical Bench Assembly Detector Assembly Lamp Heater Assembly Photometer Lamp Photometer Board Pump 110VAC w Plate and Fittings Pump Zero Air Supply 110V Optional Pump Zero Air Supply 220V Option AC Receptacle Assembly Fan 24VDC Fan Filter Fuse 250VAC 3 0 Amp SloBlow for 100VAC and 110VAC models Fuse 250VAC 1 60 Amp SloBlow for 220 240VAC models Capillary Purple 0 015 ID 2 Teflon Particulate Filter Scrubber Ozone Charcoal Scrubber Assembly Model 497 Primary Standard Instruction Manual 6 5 Servicing Table 6 2 describes the Model 497 Primary Standard cables See the Troubleshooting chapter for associated connection diagrams and board connector pin descriptions Table 6 2 Model 497 Primary Standard Cables Part Number 101036 00 101037 00 101048 00 101038 00 101364 00 101054 00 101035 00 101033 00 101377 00 101055 00 101706 00 102446 00 101267 00 instrument Description DC Power Supply 24V Output 115VAC Supply to Measurement Interface Board RS 485 Data AC Power Switch to Motherboard DC Power Supply Status Monitor Motherboard to Front Panel Board DC Power Supply AC Input AC from Receptacle AC to Power Switch Main AC
130. ets the long record logging period to 15 minutes Send set Irec per 15 Receive set Irec per 15 ok no of lrec no of srec These commands report the number of long and short records stored in the long and short records memory The example that follows shows that 50 long records have been stored in the memory Send no of lrec Receive no of lrec 50 recs malloc lrec malloc srec These commands report the currently set memory allocation for long and short records in percent of total memory Send malloc lrec Receive malloc lrec 10 set malloc lrec value set malloc srec value value 0 to 100 These commands set the percent of memory space allocated for long and short records to value where value is a floating point number representing percent The example that follows sets the memory allocation for long records to 10 B 22 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Datalogging Note Issuing these commands will clear all the logging data memory All the existing records should be retrieved using appropriate commands if required a Send set malloc lrec 10 Receive set malloc lrec 10 ok set copy sp to lrec set copy sp to srec set copy sp to stream These commands copy the current selections in scratch pad sp into the long record short record or streaming data list The example that follows copies the current list in scratch pad i
131. eysitech command lt STX gt Command text lt ETX gt lt BCC gt OR lt STX gt Command text lt CR gt Each Command is framed by control characters lt STX gt at the start and terminated with either lt ETX gt or lt CR gt Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Block Checksum lt BCC gt Geysitech Commands Instrument Control Command ST Thermo Fisher Scientific Geysitech Bayern Hessen Protocol Block Checksum lt BCC gt If a command is terminated with lt ETX gt then additional two characters lt BCC gt is attached after lt ETX gt this is the block checksum The block checksum is calculated beginning with a seed value of 00000000 binary 0x00 and bitwise exclusive ORing with each of the characters of the command string or response including the framing characters lt STX gt and lt ETX gt The checksum works as an error check The command terminator determines the presence or absence of lt BCC gt If a command is terminated by lt ETX gt then the next two characters are the checksum if the command is terminated with lt CR gt no checksum is attached The block checksum is represented by two characters which represent a 2 digit hex number 1byte e g 1 byte OxAB hex checksum will be represented by the two characters A amp BI The checksum is referred to as lt BCC gt throughout this document The following commands are supported by the Geysitech proto
132. face Board Connector Pin Descriptions Connector Reference Pin Signal Label Designator Description PHOTOMETER J6 1 Photometer Lamp Intensity Control Voltage Output 2 Photometer Lamp Intensity Control Voltage Input J Photometer Heater Thermistor Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 5 17 Troubleshooting Connector Pin Descriptions Table 5 7 Measurement Interface Board Connector Pin Descriptions continued Connector Label DATA PRES FLOW B OZONATOR CHA CHB 5 18 Model 497 Primary Standard Instruction Manual Reference Designator J4 J12 J8 Jo J9 J10 Pin Aa O N _ WO N O N O o A on Aa wo N a O N gt O N OO o A WwW ech Signal Description 24V Ground Ground Ground Ground Ground RS485 from Motherboard RS485 from Motherboard Pressure Sensor Input Ground 15V 15V sample Flow B Sensor Input Ground 15V 15V Ground Ozonator Lamp Intensity Control Voltage Output Ozonator Lamp Intensity Control Voltage Input Ozonator Heater Thermistor 24V Ground Ozonator Lamp On off Control Ground Ground 15V 15V Ground Measurement Frequency A 15V 15V Thermo Fisher Scientific Troubleshooting Connector Pin Descriptions Table 5 7 Measurement Interface Board Connector Pin Descriptions continued Connector Label FLOW A TEMP 24V IN AC IN FAN AC PUMP ZIS SOL SAMPLE SOL R
133. ffers by more than one percent the analog outputs should be adjusted Refer to the Analog Output Calibration procedure that follows Press to set the output to full scale The Output Set To line displays Full Scale Check that the meter is displaying the full scale value If the meter reading differs by more than one percent the analog outputs should be Thermo Fisher Scientific Thermo Fisher Scientific Servicing Analog Output Testing adjusted Refer to the Analog Output Calibration procedure that follows 8 Press e to reset the analog outputs to normal Analog Voltage _ _ gt Outputs dE O O O O O O o O O O O 0 O0O00000000000 z G Current Outputs Analog lt q _4 Voltage Inputs Figure 6 6 Rear Panel Analog Input and Output Pins Table 6 4 Analog Output Channels and Rear Panel Pin Connections Voltage Channel 1 Oo on A Ww N Ground Pin 14 33 19 34 17 36 1618 19 35 37 Current Pin Channel 1 15 2 17 J 19 4 21 5 23 6 25 Current Output Return 13 16 18 20 22 24 Model 497 Primary Standard Instruction Manual 6 13 Servicing Analog Output Calibration 6 14 Table 6 5 Analog Input Channels and Rear Panel Pin Connections Input Channel Pin 1 1 2 2 3 3 4 5 5 6 6 7 i 9 8 10 Ground 4 8 11 14 Analog Outp Ut Use the following procedure to calibrate the analog outputs if a meter Calibr
134. field and the alpha page Model 497 Primary Standard Instruction Manual 3 35 Operation Instrument Controls Menu e Press to save the new letter in the alpha table or save the new alpha page I O Configuration The I O Configuration menu deals with configuration of the calibrator s I O system The analog input configuration is displayed only if the I O expansion board option is installed e Inthe Main Menu choose Instrument Controls gt I O Configuration Output Relay Settings The Output Relay Settings menu displays a list of the 10 analog output relays available and allows the user to select the logic state or instrument parameter for the relay selected Note The digital outputs may take up to one second after the assigned state occurs to show up on the outputs a e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Output Relay Settings 3 36 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu Logic State The Logic State screen is used to change the I O relay to either normally open or normally closed e Press to toggle and set the logic state open or closed Instrument State The Instrument State submenu allows the user to select the instrument state that is tied to the selected relay output A submenu lists signal types of either alarm and non alarm to choose from e Inthe Main Menu choose Instrument Controls gt I O
135. g should be less than 10 feet 2 Connect the EXHAUST bulkhead to a suitable vent The exhaust line should be 1 4 inch OD with a minimum ID of 1 8 inch The length of the exhaust line should be less than 10 feet Verify that there is no restriction in this line 3 Connect a suitable recording device to the rear panel connector See the Operation chapter for more information about the rear panel pin outs 4 Plug the instrument into an outlet of the appropriate voltage and frequency grounding cord Under no circumstances should this grounding system be WARNING The Model 497 Primary Standard is supplied with a three wire A defeated 5 Connect the instrument to be calibrated to the OZONE bulkhead The total flow though the ozonator should be set to at least 1 LPM Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 2 3 Installation Connecting External Devices EXTERNAL ACCESSORY 1 0 EXPANSION RS 252 485 Gs ooo000000000 oo0o00000000000 ei 000000000000000000 OOOO000000000000000 O Se oO oO oO oO oO oO oO oO oO oO oO oO oO oO 38 Co Connecting External Devices Terminal Board PCB Assemblies VENT OZONE Ga au Xe Xe YI YP Rei GEO AIR ON Figure 2 3 Model 497 Primary Standard Rear Panel Several components are available for connecting external devices to Series instruments These connection options include e Individual term
136. ge 2 3 set analog vout range channel range This command sets analog voltage output channel to the range where channel is between 1 and 6 inclusive and range is set according to Table B 10 The example that follows sets channel 2 to the 0 10 V range Send set analog vout range 2 3 Receive set analog vout range 2 3 ok Table B 10 Analog Voltage Output Range Values Range Output Range 1 0 1 V Ro AN BV SEU dig in This command reports the status of the digital inputs as a 4 digit hexadecimal string with the most significant bit MSB being input 16 Send dig in Receive dig in Oxft7f din channel This command reports the action assigned to input channel and the corresponding active state The example that follows reports the input 5 to be assigned an index number 9 corresponding to action of analog outputs to zero with the active state being high Send din 5 Receive din 5 9 AOUTS TO ZERO high set din channel index state This command assigns digital input channel 1 16 to activate the action indicated by index 1 35 when the input transitions to the designated state high or low Use list din var command to obtain the list of supported index values and corresponding actions Model 497 Primary Standard Instruction Manual B 41 C Link Protocol Commands I O Configuration Send set din 1 3 high Receive set din 1 3 high ok dout channel This command reports the index number and output variable and th
137. h protocol Number of Data bits 8 Number of Stop bits 1 Parity None Model 497 Primary Standard Instruction Manual D 1 Geysitech Bayern Hessen Protocol TCP Communication Parameters D 2 TCP Communication Parameters Instrument Address Abbreviations Used Basic Command Structure Data rate from 1200 115200 Baud 9600 is default iSeries Instruments support the Geysitech TCP protocol over TCP IP The register definition is the same as for the serial interface TCP connection port for Geysitech 9882 The Geysitech instrument address has a value between 0 and 127 and is represented by 3 digit ASCII number with leading zeros or leading spaces if required e g Instrument address of 1 is represented as 001 or lt SP gt lt SP gt 1 The instrument Address is the same as the Instrument ID used for C Link and MODBUS commands This can be set via the front panel The Instrument Address is represented by lt address gt in the examples throughout this document Note Device IDs 128 through 247 are not supported because of limitations imposed by the C Link protocol a The following is a list of abbreviations used in this document lt CR gt is abbreviation for Carriage Return ASCII code 0x0D lt STX gt is abbreviation for Start of Text ASCII code 0x02 lt ETX gt is abbreviation for End of Text ASCII code 0x03 lt SP gt is abbreviation for space ASCII code 0x20 The following is the basic structure of a G
138. hat index number available for selection in the current mode determined by single dual auto gas mode no no or no no for analog output digital output and digital inputs The index number is used to insert the variable in a field location in a list using set sp field index The example that follows reports the list of analog output index numbers and variables Send list var aout Receive list var aout index variable none 03 no2 cellai cellbi noisa noisb 9 flowa 10 flowb 11 pres 12 bncht 13 lmpt CON DUN FP CH relay relay stat This command reports the current relay logic normally open or normally closed if all the relays are set to same state that is all open or all closed The example that follows shows that the status when all the relays logic is set to normally open Send relay stat Receive relay stat open Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual B 43 C Link Protocol Commands Record Layout Definition Record Layout Definition Note If individual relays have been assigned different logic the response would be a 4 digit hexadecimal string with the least significant byte LSB being relay no 1 For example Receive relay stat 0x0001 indicates relay no 1 is set to normally open logic all others are normally closed Receive relay stat 0x0005 indicates relay no 1 and 3 are set to be normally open logic all others are normally clos
139. he Remove Password screen is used to erase the current password and disable password protection The remove password is shown if the calibrator is unlocked and the password set e Inthe Main Menu choose Password gt Remove Password e Press to remove password and returns to main menu Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 83 Operation Password Menu Unlock Instrument The Unlock Instrument screen is used to enter the password to unlock the front panel The Unlock Instrument is shown if the calibrator is locked e Inthe Main Menu choose Password gt Unlock Instrument e Press to disable instrument lock and returns to main menu 3 84 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Chapter 4 Preventive Maintenance This chapter describes the periodic maintenance procedures that should be performed on the instrument to ensure proper operation Since usage and environmental conditions vary greatly you should inspect the components frequently until an appropriate maintenance schedule is determined This includes the sample pump and solenoid valves which have a limited life Other operations such as cleaning the optics and checking the calibration of the pressure should be performed on a regular basis This chapter includes the following maintenance information and replacement procedures e Safety Precautions on page 4 2 e Replacement Parts on p
140. he following c code will expand the incoming data Void unpackDisplay void far tdib unsigned char far rlescreen Lic agg unsigned char far sc4bpp sc2bpp screen ptr ptr screen unsigned char far malloc 19200 RLE decode the screen for i 0 i lt 19200 amp amp ptr screen lt 19200 i otr rlescreen i if rlescreen i 0 unsigned char rlecount unsigned char rlescreen i while rlecount ptr 0 rlecount j else if rlescreen i Oxff unsigned char rlecount unsigned char rlescreen i while rlecount ptr Oxff rlecount i j To convert this data into a BMP for use with windows it needs to be turned into a 4BPP as that is the smallest windows can display Also note that BMP files are upside down relative to this data i e the top display line is the last line in the BMP SC screen This command is meant for backward compatibility on the C series Screen information is reported using the iScreen command above Send screen Receive screen This is an I series Instrument Screen Information not available Measurement range Configuration high range Thermo Fisher Scientific low range Model 497 Primary Standard Instruction Manual B 29 C Link Protocol Commands Measurement Configuration These commands report the O3 range in single range mode or the high and low ranges in dual or auto range mode acco
141. he two screws from the photometer lamp access hole cover on the rear panel and remove the cover 4 Loosen the captive screws 4 securing the optical bench to the floor plate Figure 6 11 and remove the bench by first moving the photometer slightly towards the rear through the lamp access hole and then lifting up and towards the front 5 Perform the previous steps in reverse to install the new optical bench 6 Calibrate the instrument Refer to the Calibration chapter in this manual Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 25 Servicing Photometer Board Replacement Photometer Lamp Lamp Heater Access Port Cell B IN Absorption Cell B Access Port Cell A IN pC L Input Block gt Access Port Cell B OUT Captive Screws 4 Absorption Cell AS Detector B Access Port Cell A OUT Detector A Figure 6 11 Replacing the Optical Bench Photometer Board Use the following procedure to replace the photometer board Figure 6 9 Replacement Equipment required Photometer board Philips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a Use the following procedure to replace the photometer board 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the connection cables from the board Note
142. hermo Fisher Scientific Preventive Maintenance Capillary Service Monitoring Lamp Noise To monitor the lamp noise display Intensity Check from the Service mode menu 1 Press to display the Main Menu 2 Use t to scroll to Service press gt to scroll to Intensity Check and press 4a The Intensity Check screen appears The noise value displayed after 20 seconds should be below 4 0 Hz for a fully warmed up lamp see the Troubleshooting chapter if the noise is excessive Lan lary Service The capillaries normally only require inspection when performance indicates there may be a flow problem Use the following procedure to service the capillary Figure 4 1 Equipment Required Capillary Wire less than 0 015 inch OD amounts of static electricity A properly grounded antistatic wrist strap must Equipment Damage Some internal components can be damaged by small be worn while handling any internal component a 1 Turn instrument OFF unplug the power cord and remove the cover Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 4 5 Preventive Maintenance Pump Rebuilding 2 Remove capillary check for particulate deposits clear any blockage with a wire less than 0 015 inch OD or replace the capillary by following the above steps in reverse Capillary Capillary Figure 4 1 Capillary Location Pump Rebuildi NG Use the following procedure to reb
143. hermo Fisher Scientific Preventive Maintenance Leak Test and Pump Checkout 3 Press A to scroll to Diagnostics and press to display the Diagnostics menu 4 Use rt to move the cursor to Cell A B O3 and press to display the O3 PPB screen This display presents the concentration for each cell Once the instrument stabilizes the average of 10 successive simultaneous readings should agree within 3 percent A balanced measurement of better than 3 percent indicates that there are no leaks across the solenoid A constant low reading from one cell indicates an imbalance The imbalance can be caused by a dirty cell dirty lines to that cell or by a leaky valve Refer to the Solenoid Leak Test procedure that follows to check for a leaky solenoid To check if the imbalance is caused by an absorption cell interchange the cells If the imbalanced side switches the imbalance is caused by the cell Use the following procedure to test the solenoid valve for leaks 1 Remove the solenoid valve that appears to be faulty 2 Connect the pump directly to the common solenoid port 3 Connect the pressure transducer to the normally open solenoid port 4 Press to display the Main Menu 5 Dress to scroll to Diagnostics and press to display the Diagnostics menu 6 Use to scroll to Pressure and press to display the Pressure screen Model 497 Primary Standard Instruction Manual 4 9
144. iculate EE 8 1 SR E NERT eens 8 1 Terminal Blockand Cable Kits acca cranes ona sasapapsnsaesenteeaanntenecanns 8 2 EEN 8 2 25 Pin Terminal Board Assen Dy cccssesexecassasnansanesccazentsenesanvence 8 3 DV AE TD EE 8 3 Warranty E A 1 C Link Protocol Command cccsssssssssssssssseeseseeeees B 1 Instrument Identification Number ccccccccceseeecssseseees B 2 Fete EE RN D E B 2 CCE SSNS SCA Eegenen B 2 ere EE B 2 TV VCAG USING TES Sinn atevoninacunscans obocecnetuieeados ntat sadeeeterasoaauesnns oloceonedie B 8 EE B 12 Eege B 17 Bie leet aera nt rere eee E ee ee B 17 Ee EE B 25 eebe B 28 eene B 29 Hardware Eeer B 34 EEN eege B 36 EE B 40 Model 497 Primary Standard Instruction Manual IX Contents X Appendix C Appendix D Model 497 Primary Standard Instruction Manual Record Layout RE B 44 Format Specifier for ASCH Responses sicsecandesanvesszaceeeatoiers B 45 Format Specifier for Binary Responses ssssssessssessssesress B 45 Format Specifier for Front Panel Layout ejcsccstsecaicseccdesvans B 45 MODBUS PlOtOG ON sisiciescscccvorsecavstuestasieesetiverstituroeenianneiuieediiens C 1 Serial Communication Parameters cccccsssscssesesccecesenseseee C 2 TCP Communication Parameters esi covesdensessaiateeeeasiandeasieceaes C 2 Application Data Unit EE ege eeegebederegegehebtegeen steet C 2 SE C2 INDE Header sepiro e E TE C 2 EEE E N E E A E N C 3 RE C 3 Ee E E er ener C
145. ield Name Function Byte Count Register value Hi 10 Register value Lo 10 Register value Hi 11 Register value Lo 11 Register value Hi 12 Register value Lo 12 Register value Hi 13 Register value Lo 13 Hex 0x03 0x00 0x09 0x00 0x04 Hex 0x03 0x06 0x02 0x2B 0x00 0x00 0x00 0x64 0x00 0x64 The contents of register 10 are shown as the two byte values of 0x02 0x2B The contents of registers 11 13 are 0x00 0x00 0x00 0x64 and 0x00 0x64 respectively Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific MODBUS Protocol Function Codes 0x05 Force Write Single The force write single coil function simulates the activation of the digital Gol inputs in the instrument which triggers the respective action This function code is used to set a single action to either ON or OFF The request specifies the address of the action to be forced Actions are addressed starting at zero Therefore action number is addressed as 0 The requested ON OFF state is specified by a constant in the request data field A value of OxFF00 requests the action to be ON A value of 0x0000 requests it to be OPE All other values are illegal and will not affect the output The normal response is an echo of the request returned after the state has been written Request Function code Output Address Output Value Response Function code Output Address Output Value Error Response Function code Exc
146. inal board PCB assemblies e Terminal block and cable kits optional e Individual cables optional For detailed information on the optional connection components refer to the Optional Equipment chapter For associated part numbers refer to External Device Connection Components in the Servicing chapter The following terminal board PCB assemblies are available for iSeries instruments e I O terminal board PCB assembly 37 pin standard 2 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Installation Connecting External Devices e D O terminal board PCB assembly 37 pin standard e 25 pin terminal board PCB assembly included with optional I O Expansion Board UU Terminal Board Figure 2 4 shows the recommended method for attaching the cable to the terminal board using the included tie down and spacer able 2 1 identifies the connector pins and associated signals Note Not all of the available I O for the instrument are brought out on this terminal If more I O is desired you must use an alternative connection method See Detail A See Detail B Detail A Detail B Assembled Connector Figure 2 4 O Terminal Board Views Table 2 1 UU Terminal Board Pin Descriptions Pin Signal Description Pin Signal Description 1 Analog 13 Power_Fail_NC Z Analog ground 14 Power_Fail_COM Thermo Fisher Scientific Model 497 Primary Standard Instruction Man
147. inued Connector Reference Pin Signal Label Designator Description 7 RS485 to Motherboard 8 RS485 to Motherboard Table 5 6 Digital Qutput Board Connector Pin Descriptions Connector Reference Pin Signal Label Designator Description MOTHER BD di 5V 24V 24V Ground Ground Ground SPI Reset SPI Input SPI Output SPI Board Select SPI Clock Relay 1 Contact a co co N O oO A W N E ech DIGITAL J2 OUTPUTS ech Relay 2 Contact a Relay 3 Contact a Relay 4 Contact a Relay 5 Contact a Relay 6 Contact a Relay 7 Contact a Relay 8 Contact a co co N O oO A W N Relay 9 Contact a Relay 10 Contact a 11 NC 12 Solenoid Drive Output 1 13 Solenoid Drive Output 2 14 Solenoid Drive Output 3 5 16 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Troubleshooting Connector Pin Descriptions Table 5 6 Digital Output Board Connector Pin Descriptions continued Connector Reference Pin Signal Label Designator Description 15 solenoid Drive Output 4 16 solenoid Drive Output 5 17 Solenoid Drive Output 6 18 solenoid Drive Output 7 19 solenoid Drive Output 8 20 Relay 1 Contact b 21 Relay 2 Contact b 22 Relay 3 Contact b Se Relay 4 Contact b 24 Relay 5 Contact b 25 Relay 6 Contact b 26 Relay 7 Contact b 2I Relay 8 Contact b 28 Relay 9 Contact b 29 Relay 10 Contact b 30 24V 31 24V 32 24V 33 24V 34 24V 25 24V 36 24V di 24V Table 5 7 Measurement Inter
148. ion Service Menu e Use el gt and to move and change the value e Press to save set to value as actual value et CHANGE VOLLE SOY Analog Output Calibration The Analog Output Calibration menu is a selection of 6 voltage channels and 6 current channels if I O expansion board option is installed to calibrate and allows the user to select the calibration action zero or span The analog output calibration is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician a e Inthe Main Menu choose Service gt Analog Out Calibration Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 77 Operation Service Menu 3 78 Analog Output Calibrate Zero Analog Output Calibrate Full Scale The Analog Output Calibrate Zero screen allows the user to calibrate the zero state of the selected analog output The operator must connect a meter to the output and adjust the output until it reads 0 0 V on the meter e Inthe Main Menu choose Service gt Analog Out Calibration gt Select Channel gt Calibrate Zero e Use the and to increment or decrement the numeric value e Press to save the value The Analog Output Calibrate Full Scale screen allows the user to calibrate the full scale state of the
149. ion Manual Thermo Fisher Scientific Appendix A Warranty Seller warrants that the Products will operate or perform substantially in conformance with Seller s published specifications and be free from defects in material and workmanship when subjected to normal proper and intended usage by properly trained personnel for the period of time set forth in the product documentation published specifications or package inserts If a period of time is not specified in Sellers product documentation published specifications or package inserts the warranty period shall be one 1 year from the date of shipment to Buyer for equipment and ninety 90 days for all other products the Warranty Period Seller agrees during the Warranty Period to repair or replace at Seller s option defective Products so as to cause the same to operate in substantial conformance with said published specifications provided that a Buyer shall promptly notify Seller in writing upon the discovery of any defect which notice shall include the product model and serial number if applicable and details of the warranty claim b after Seller s review Seller will provide Buyer with service data and or a Return Material Authorization RMA which may include biohazard decontamination procedures and other product specific handling instructions and c then if applicable Buyer may return the defective Products to Seller with all costs prepaid by Buyer Replacement parts
150. ion board option is installed This allows the user to select the output signal to the selected output channel The Concentrations screen is shown below See Table 3 7 below for a list of items for each signal group choice The Choose Signal Type To Output screen displays a submenu list of the analog output signal group choices Group choices are Concentrations e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Output Config gt Select Channel gt Choose Signal To Output Use and to move the cursor up and down e Press to select a choice Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 43 Operation Instrument Controls Menu Table 3 5 Signal Type Group Choices Concentrations None Other Measurements None Intensity A Analog Inputs None Analog Input 1 03 Intensity B Analog Input 2 Noise A Analog Input 3 Noise B Analog Input 4 Flow A Analog Input 5 Flow B Analog Input 6 Pressure Analog Input 7 Bench Temp Analog Input 8 Lamp Temp 03 Lamp Temp Analog Input Configuration The Analog Input Configuration menu displays a list of the 8 analog input channels available for configuration This screen is only displayed if the I O expansion board option is installed Configuration includes entering descriptor units decimal places choice of 1 10 points in the table and corresponding number
151. is chapter Motherboard Support Bracket A 1 OR sl i pen e Li N A E A Mounting Studs Motherboard Digital Output Board O Expansion Board Opt Figure 6 7 Replacing the 1 0 Expansion Board Optional O Expansion Board Digital Output Board on Figure 6 8 Rear Panel Board Connectors Dig ital Outp ut Board Use the following procedure to replace the digital output board Replacement igure 6 7 Equipment Required Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 19 Servicing Motherboard Replacement Motherboard Replacement A Digital output board Nut driver 3 16 inch Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the I O expansion board optional if used See the I O Expansion Board Replacement procedure in this chapter 3 Disconnect the digital output board ribbon cable from the motherboard 4 Using the nut driver remove the two standoffs securing the board to the rear panel Figure 6 8 5 Pop off the digital output board from the mounting studs and remove the board 6 To install the digital output board follow previous steps in reverse Use the following procedure to replace the motherboard Figure 6
152. l 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Range Menu Main Menu The Main Menu contains a number of submenus Parameters and features are divided into these submenus according to their function The concentration appears above the main menu and submenus in every screen The Service menu is visible only when the calibrator is in service mode For more information on the service mode see Service Mode later in this chapter e Use and to move the cursor up and down p e Press to select a choice e Press nl to return to the Main Menu or gt to return to the Run screen Range Menu The Range menu allows the operator to select the gas units O3 range and to set the custom ranges e Inthe Main Menu choose Range Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 7 Operation Range Menu Gas Units The Gas Units screen defines how the O3 concentration reading is expressed Gas units of parts per billion ppb parts per million ppm micrograms per cubic meter ug m or milligrams per cubic meter mg m are available The g m and mg m gas concentration modes are calculated using a standard pressure of 760 mmHg and a standard temperature of 20 C When switching the selected units from ppb or ppm to ug m or mg m the analog ranges all default to the highest range in that mode For example when switching from mg mi to ppm all the ranges
153. limits Acceptable alarm limits range from 5 to 50 C If the bench temperature reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu e Inthe Main Menu choose Alarms gt Bench Temp Min and Max Bench Temperature The Minimum Bench Temperature alarm limit screen is used to change the Limits minimum bench temperature alarm limit The minimum and maximum bench temperature screens function the same way e Inthe Main Menu choose Alarms gt Bench Temp gt Min or Max e Use and to increment or decrement the numeric value e Press to save set to value as actual value Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 61 Operation Alarms Menu Pressure The Pressure screen displays the current pressure and sets the minimum and maximum alarm limits Acceptable alarm limits range from 200 to 1 000 mmHg If the pressure reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu e Inthe Main Menu choose Alarms gt Pressure Min and Max Pressure Limits The Minimum Pressure alarm limit screen is used to change the minimum pressure alarm limit The minimum and maximum pressure screens function the same way e Inthe Main Menu choose Alarms gt Pressure gt Min or Max e Use and to increment or
154. ling according to able B 3 The example that follows sets the O3 concentration minimum alarm trigger to ceiling Send set alarm trig conc no 1 Receive set alarm trig conc no 1 ok Table B 3 Alarm Trigger Values Value Alarm Trigger 0 Floor 1 Ceiling B 16 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Diagnostics Datalogging Thermo Fisher Scientific C Link Protocol Commands Diagnostics cell a int cell b int The example that follows reports that the lamp intensity in cell A is 98 425 Hz Send cell a int Receive cell a int 98425 Hz diag volt mb This command reports the diagnostic voltage measurements on the motherboard The sequence of voltages is Positive 24 positive 15 positive 5 positive 3 3 and negative 3 3 Each voltage value is separated by a space Send diag volt mb Receive diag volt mb 24 1 14 9 4 9 3 2 3 2 diag volt mib This command reports the diagnostic voltage measurements on the measurement interface board The sequence of voltages is Positive 24 positive 15 negative 15 positive 5 positive 3 3 and positive 15 Each voltage value is separated by a space Send diag volt mib Receive diag volt mib 24 1 14 9 14 9 4 9 3 2 14 9 diag volt iob This command reports the diagnostic voltage measurements on the I O expansion board The sequence of voltages is Positive 24 positive 5 positive 3 3 and negative 3 3 Each voltage value is separated by a space Se
155. list It also includes contact information for product support and technical information e Chapter 7 System Description describes the function and location of the system components provides an overview of the software structure and includes a description of the system electronics and input output connections e Chapter 8 Optional Equipment describes the optional equipment that can be used with this analyzer e Appendix A Warranty is a copy of the warranty statement e Appendix B C Link Protocol Commands provides a description of the C Link protocol commands that can be used to remotely control an analyzer using a host device such as a PC or a datalogger Model 497 Primary Standard Instruction Manual XV Preface e Appendix C MODBUS Protocol provides a description of the MODBUS Protocol Interface and is supported both over RS 232 485 RTU protocol as well as TCP IP over Ethernet e Appendix D Geysitech Bayern Hessen Protocol provides a description of the Geysitech Bayern Hessen Protocol Interface and is supported over RS 232 485 and TCP IP over Ethernet Safety Review the following safety information carefully before using the analyzer This manual provides specific information on how to operate the analyzer however if the analyzer is used in a manner not specified by the manufacturer the protection provided by the equipment may be impaired Safety and Equipment This manual contains impor
156. lue is a decimal number between 0 and 127 inclusive Note Sending this command via RS 232 or RS 485 will require the host to use the new id for subsequent commands Send set instrument id 50 Receive set instrument id 50 ok mode This command reports what operating mode the instrument is in local service or remote The example that follows shows that the instrument is in the remote mode Send mode Receive mode remote set mode local set mode remote These commands set the instrument to local or remote mode The example that follows sets the instrument to the local mode Send set mode local Receive set mode local ok program no This command reports the analyzer s model information and program version number which will be dependant on the current version Model 497 Primary Standard Instruction Manual B 39 C Link Protocol Commands I O Configuration I O Configuration Send program no Receive program no iSeries 491 01 00 01 074 set layout ack This command disables the stale layout layout change indicator that is attached to each response if the layout has changed Send set layout ack Receive set layout ack ok analog iout range channel This command reports the analog current output range setting for channels where channel must be between 1 and 6 inclusive The example that follows reports current output channel 4 to the 4 20 mA range according to Table B 9 This command responds with
157. ly has been identified as defective and needs to be replaced For fault location information refer to the Preventive Maintenance chapter and the Troubleshooting chapter in this manual The service mode in the Operation chapter also includes parameters and functions that are useful when making adjustments or diagnosing problems For additional service assistance see Service Locations at the end of this chapter This chapter includes the following parts information testing adjustment and calibration procedures and component replacement procedures Safety Precautions on page 6 3 Replacement Parts List on page 6 4 Firmware Updates on page 6 4 Replacement Parts List on page 6 4 Cable List on page 6 6 External Device Connection Components on page 6 6 Removing the Measurement Bench and Lowering the Partition Panel on page 6 8 Fuse Replacement on page 6 9 Pump Replacement on page 6 10 Fan Replacement on page 6 11 Analog Output Testing on page 6 12 Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 1 Servicing Analog Output Calibration on page 6 14 Analog Input Calibration on page 6 15 Optical Bench Temperature Calibration on page 6 17 I O Expansion Board Optional Replacement on page 6 18 Digital Output Board Replacement on page 6 19 Motherboard Replacement on page 6 20
158. mary Standard Instruction Manual D 7 Geysitech Bayern Hessen Protocol Geysitech Commands Operating and Error Status See Table D 1 for operating status and Table D 2 for error status for the Model 497 and the Model 497 Primary Standard Table D 1 Operating Status for Model 497 and 497 Primary Standard po LH UR LR D4 DB D2 DI DO ETE j6 5 ja f3 2 1 eege A DEA ee on se LSB Operating status J Service Mode On fo jo fo fo f o o o 1 Maintenance Local jo o fo o fo jo 1 0 Zerogas On JO o fo jo 1 o 0 Spangas On Jo o fo jo jo o 0 Notused ft jo o 0 Gas Unit Indication ppb OR ppm 0 0 1 0 o 0 o 0 Notused Tf jo o 0 Not used tt ll do ddo o o Jo Table D 2 Error Status for Model 497 and 497 Primary Standard Dip D5 D4 D3 2 D1 DO gt Bit 8 7 e 5 a 3 2 1 2 Hexvalue 80 40 20 10 08 04 02 01 ease MSB E LSB LI ft tt S T To o 0 Lamp Temperature Alarm BEE tof Tf a Internal Temperature Alarm O o III 1 0 a ea a a a fo Pressure Alarm o jo o jo 1 o jo Jo FowAAlam Ir fo 1 fo jo o 0 FowBAlam III o 0 IntensityAAlarm II fo jo JO jo o 0 Intensity B Alarm tt 0 o o Jo o o o D 8 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific
159. maximum number of short records Reports sets output format for short records ASCII or binary Reports current layout of short record data Reports maximum number of short records Reports sets short record logging period Reports sets current set time interval for streaming data Reports sets a time stamp to streaming data or not Reports sets temperature compensation on or off Reports sets current time 24 hour time Simulates pressing up pushbutton Sets zero span valves to zero mode Page B 31 B 43 B 43 B 25 B 28 B 28 B 31 B 35 B 35 B 29 B 27 B 23 B 31 B 18 B 19 B 20 B 21 B 21 B 22 B 24 B 24 B 33 B 35 B 28 B 31 These commands report the averaging time in seconds when operating in single range or averaging time used with the high and low ranges when operating in dual or auto range mode The example that follows shows that the averaging time is 300 seconds according to Table B 2 Send avg time Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Measurements Receive avg time 11 300 sec set avg time selection set high avg time selection set low avg time selection These commands set the averaging time high and low averaging times according to able B 2 The example that follows sets the low range averaging time to 120 seconds Send set low avg time 8 Receive set low avg time 8 ok Table B 2 Averaging limes Selection
160. mmediately and hold for inspection The carrier is responsible for any damage incurred during shipment Use the following procedure to unpack and inspect the instrument 1 Remove the instrument from the shipping container and set it on a table or bench that allows easy access to both the front and rear 2 Remove the cover to expose the internal components Model 497 Primary Standard Instruction Manual 2 1 Installation Unpacking and Inspection 3 Remove the packing material Figure 2 1 Ges E TI set WI Remove Packing 2 pieces Remove Packing 2 pieces G Z i Units without Optional 0 Board Units with Optional I O Board Figure 2 1 Remove the Packing Material 4 Remove the three shipping screws Figure 2 2 Figure 2 2 Remove the Shipping Screws 5 Check for possible damage during shipment 6 Check that all connectors and circuit boards are firmly attached 2 2 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Installation Setup Procedure 7 Re install the cover 8 Remove any protective plastic material from the case exterior Setup Procedure Use the following procedure to setup the instrument 1 Connect the zero air supply to the ZERO AIR bulkhead on the rear panel Figure 2 3 All tubing should be constructed of FEP Teflon 316 stainless steel borosilicate glass or similar tubing with an OD of 1 4 inch and a minimum ID of 1 8 inch The length of the tubin
161. mperature alarm limit screen is used to change the minimum O3 Lamp temperature alarm limit The minimum and maximum O Lamp temperature screens function the same way e Inthe Main Menu choose Alarms gt O3 Lamp Temp gt Min or Max e Use t and to increment or decrement the numeric value e Press to save set to value as actual value Model 497 Primary Standard Instruction Manual 3 59 Operation Alarms Menu Lamp Temperature The Lamp Temperature screen displays the current lamp temperature and sets the minimum and maximum alarm limits Acceptable alarm limits range from 50 to 60 C If the lamp temperature reading goes beyond either the minimum or maximum limit an alarm is activated The word ALARM appears in the Run screen and in the Main Menu e Inthe Main Menu choose Alarms gt Lamp Temp Min and Max Lamp Temperature The Minimum Lamp Temperature alarm limit screen is used to change the Limits minimum lamp temperature alarm limit The minimum and maximum lamp temperature screens function the same way e In the Main Menu choose Alarms gt Lamp Temp gt Min or Max e Use and to increment or decrement the numeric value e Press to save set to value as actual value 3 60 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Alarms Menu Bench Temperature The Bench Temperature screen displays the current bench temperature and sets the minimum and maximum alarm
162. nal that is tied to the selected field item The selected item is shown by lt after it Note that at this point pressing indicates that these are proposed changes as opposed to implemented changes To change the selected record format and erase record log file data see Commit Content below In the Main Menu choose Instrument Controls gt Datalogging Settings gt Select Content gt Select Field gt Concentrations Use and to move the cursor up and down p Press to select a new choice 3 22 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Other Measurements Thermo Fisher Scientific Analog Inputs Operation Instrument Controls Menu The Other Measurements screen allows the user to select the output signal that is tied to the selected field item The selected item is shown by lt after it Items displayed are determined by the options installed Note that at this point pressing indicates that these are proposed changes as opposed to implemented changes To change the selected record format and erase record log file data see Commit Content below e Inthe Main Menu choose Instrument Controls gt Datalogging Settings gt Select Content gt Select Field gt Other Measurements e Use and to move the cursor up and down e Press to select a new choice The Analog Inputs screen allows the user to select the output signal none or analog inputs 1 8
163. nation with equipment or software not supplied by Seller If Seller determines that Products for which Buyer has requested warranty services are not covered by the warranty hereunder Buyer shall pay or reimburse Seller for all costs of investigating and responding to such request at Seller s then prevailing time and materials rates If Seller provides repair services or replacement parts that are not covered by the warranty provided in this warranty Buyer shall pay Seller therefor at Seller s then prevailing time and materials rates ANY INSTALLATION MAINTENANCE REPAIR SERVICE RELOCATION OR ALTERATION TO OR OF OR OTHER TAMPERING WITH THE PRODUCTS PERFORMED BY ANY PERSON OR ENTITY OTHER THAN SELLER WITHOUT SELLER S PRIOR WRITTEN APPROVAL OR ANY USE OF REPLACEMENT PARTS NOT SUPPLIED BY SELLER SHALL IMMEDIATELY VOID AND CANCEL ALL WARRANTIES WITH RESPECT TO THE AFFECTED PRODUCTS THE OBLIGATIONS CREATED BY THIS WARRANTY STATEMENT TO REPAIR OR REPLACE A DEFECTIVE PRODUCT SHALL BE THE SOLE REMEDY OF BUYER IN THE EVENT OF A DEFECTIVE PRODUCT EXCEPT AS EXPRESSLY PROVIDED IN THIS WARRANTY STATEMENT SELLER DISCLAIMS ALL OTHER WARRANTIES WHETHER EXPRESS OR IMPLIED ORAL OR WRITTEN WITH RESPECT TO THE PRODUCTS INCLUDING WITHOUT LIMITATION ALL IMPLIED WARRANTIES OF MERCHANTABILITY OR FITNESS FOR ANY PARTICULAR PURPOSE SELLER DOES NOT WARRANT THAT THE PRODUCTS ARE ERROR FREE OR WILL ACCOMPLISH ANY PARTICULAR RESULT A 2 Model 497 Primary Sta
164. nd diag volt iob Receive diag volt iob 24 1 4 9 3 2 3 2 clr records This command will clear all long and short records that have been saved Send clear records Receive clear records ok set clr lrecs set clr srecs These commands will clear only the long records or only the short records that have been saved The example that follows clears short records Send set clr srecs Receive set clr srecs ok Model 497 Primary Standard Instruction Manual B 17 C Link Protocol Commands Datalogging list din list dout These commands report the current selection for the digital outputs in the format Output no Index number variable name active state The active state for digital outputs is open or closed The active state for digital inputs is high or low Send list dout Receive list dout output index variable state 1 23 CONC ALARM open 3 3 UNITS open 4 12 GEN ALARM open list lrec list srec list stream list sp These commands report the list of current selections for long record logging data short record logging data streaming data output or the scratch pad sp list The example that follows shows the list for streaming data output Send list stream Receive list stream field index variable x xX time 1 03 cellai cellbi noisa noisb 9 flowa 10 flowb 11 pres oo N On UI 1 2 3 4 5 6 7 8 er xy Ir xy st xy EREM Reply termination format see set format format command y
165. ndard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Appendix B C Link Protocol Commands This appendix provides a description of the C Link protocol commands that can be used to remotely control a Model 497 Primary Standard analyzer using a host device such as a PC or a datalogger C Link protocol may be used over RS 232 RS 485 or Ethernet C Link functions can be accessed over Ethernet using TCP IP port 9880 s Instrument Identification Number on page B 2 describes the C Link command format e Commands on page B 2 lists all the 492 Primary Standard C Link commands in Table B 1 e Measurements on page B 8 describes and gives examples of the measurement commands e Alarms on page B 12 describes and gives examples of the alarm commands e Diagnostics on page B 17 describes and gives examples of the diagnostic commands e Datalogging on page B 17 describes and gives examples of the datalogging commands e Calibration on page B 25 describes and gives examples of the calibration commands e Keys Display on page B 28 describes and gives examples of the keys and display commands e Measurement Configuration on page B 29 describes and gives examples of the measurement configuration commands e Hardware Configuration on page B 34 describes and gives examples of the hardware commands e Communications Configuration on page B 36 describes
166. ned 5 Re install the instrument cover If windows are severely contaminated they are best cleaned by removing the windows from the bench The windows on the detector side can be removed by removing the detector block and carefully removing the windows The windows on the source side can be removed by removing the source block to gain access to the windows It is recommended that the Model 497 Primary Standard be recalibrated if the optical bench has been completely disassembled Always leak check the system after any component removal Lamp Replacement The lamp control system of the Model 497 Primary Standard has been designed to operate the lamp conservatively to increase its life However the lamp should be replaced when any one of the following conditions occur e No light output e Inability to adjust lamp position to obtain an output detection frequency of 65 kHz e Noisy output signal which has been traced to an unstable lamp see the Troubleshooting chapter It is not necessary to recalibrate the Model 497 Primary Standard since it is a ratio instrument and replacing the lamp does not affect the calibration Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 4 3 Preventive Maintenance Monitoring Detector Frequencies and Noise 4 4 Monitoring Detector Frequencies and Noise Increasing Lamp Output The Model 497 Primary Standard measures intensity ratios and not absolute values Theref
167. net connection RJ45 connector for 10Mbs Ethernet connection static or dynamic TCP IP addressing Ozonator Output 0 025 1 000 ppm at 3 4 LPM Response to 98 or 5 1 minute ppb of final value whichever is greater Stability 4 ppb or 1 of reading whichever is greater In non condensing environments 1 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Lifting A Unpacking and Thermo Fisher Scientific Inspection Chapter 2 installation Installing the Model 49i Primary Standard includes the following recommendations and procedures e Lifting on page 2 1 e Unpacking and Inspection on page 2 1 e Setup Procedure on page 2 3 e Connecting External Devices on page 2 4 e Startup on page 2 8 When lifting the instrument use procedure appropriate to lifting a heavy object such as bending at the knees while keeping your back straight and upright Grasp the instrument at the bottom in the front and at the rear of the unit Although one person can lift the unit it is desirable to have two persons lifting one by grasping the bottom in the front and the other by grasping the bottom in the rear Equipment Damage Do not attempt to lift the instrument by the cover or other external fittings a The Model 497 Primary Standard is shipped complete in one container If there is obvious damage to the shipping container when you receive the instrument notify the carrier i
168. ngs gt Streaming Data Config gt Select Item gt Concentrations Use J and to move the cursor up and down e Press to select a new choice The Other Measurements screen allows the user to select the output signal that is tied to the selected streaming data item The selected item is shown by lt after it e Inthe Main Menu choose Instrument Controls gt Communication Settings gt Streaming Data Config gt Select Item gt Other Measurements Use and to move the cursor up and down e Press to select a new choice Model 497 Primary Standard Instruction Manual 3 31 Operation Instrument Controls Menu Analog Inputs The Analog Inputs screen allows the user to select the analog input signal none or analog inputs 1 8 that is tied to the selected streaming data item The selected item is shown by lt after it e Inthe Main Menu choose Instrument Controls gt Communication Settings gt Streaming Data Config gt Select Item gt Analog Inputs Use and to move the cursor up and down e Press to select a new choice RS 232 RS 485 Selection The RS 232 RS 485 Selection screen allows the user to choose between the RS 232 or RS 485 specification for serial communication Note Disconnect the serial cable before changing RS 232 and RS 485 selection to prevent damage to the connected equipment e Inthe Main Menu choose Instrument Controls gt
169. ns function the same way e Inthe Main Menu choose Alarms gt O3 Concentration gt Min or Max e Use e and ER to move the cursor left or right e Use and to increment or decrement the numeric value e Press to save set to value as actual value Model 497 Primary Standard Instruction Manual 3 65 Operation Service Menu Min Trigger The Minimum Trigger screen allows the user to view and set the O3 concentration alarm trigger type to either floor or ceiling The minimum alarm may be programmed as a floor trigger alarm is triggered when the concentration falls below the minimum value or a ceiling trigger alarm is triggered when the concentration goes above the minimum value e Inthe Main Menu choose Alarms gt O3 Concentration gt MinTrigger e Press to toggle and set the minimum trigger to floor or ceiling Service Menu The Service menu appears only when the calibrator is in the service mode To put the calibrator into service mode e Inthe Main Menu choose Instrument Controls gt Service Mode Advanced diagnostic functions are included in the service mode Meaningful data should not be collected when the calibrator is in the service mode e Inthe Main Menu choose Service 3 66 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Service Menu Pressure Check The Pressure Check menu is used to manually control the flow of reference or sample gas through Cell B Thi
170. ntains I O circuitry and the associated connector to monitor external digital status lines and to output analog voltages that represent the measurement data Connectors located on the motherboard include External connectors include e External Accessory e RS 232 485 Communications two connectors e Ethernet Communications Model 497 Primary Standard Instruction Manual 7 5 System Description Electronics e I O connector with Power Fail Relay 16 Digital Inputs and 6 Analog Voltage Outputs Internal Connectors Internal connectors include e Function key panel and Display e Measurement Interface Board Data s I O Expansion Board Data e Digital Output Board e AC distribution Measurement Interface The measurement interface board serves as a central connection area for all Board measurement electronics in the instrument It contains power supplies and interface circuitry for sensors and control devices in the measurement system It sends status data to the motherboard and receives control signals from the motherboard Measurement Interface Board Connectors located on the measurement interface board include Connectors e Data communication with the motherboard e 24V and 120VAC power supply inputs e Fan and solenoid outputs e 120VAC outputs for the pump e Flow and pressure sensors inputs e Detector board inputs CH A and CH B e Optical bench temperature thermistor e Photometer lamp power supply 7 6 Model 497 Primary Standard
171. ntistatic Wrist Strap eeeeseseeeceseseeeeseees 6 4 Cormier Une see 6 7 Removing the Measurement Bench and TE the Partition Panch ME 6 8 Re EE 6 10 FRG AGING E e E E 6 11 Rear Panel Analog Input and Output Pins acess cecsscsetessersesenss 6 13 Replacing the I O Expansion Board Optional 0 6 19 Redt Panel Board CONOCIO Eeer 6 19 Replacing the Measurement Interface Board 0 eee eeeeeeee 6 22 Replacing the Front Panel Board and the LCD Module 6 23 Replacing th Optical E 6 26 Peep AG tne the RE 6 31 Ozonacor Dord E 6 37 Hardware COON GOS seseorenisisrip aee 7 2 Rack Mount Opon Assembly nririsineioseiie Runna 8 4 The a e 8 5 ee VB a E E E E A 8 6 Retrofit Rack Mounting sicssicsconstiioenosin iii 8 7 EE a E E E E S B 12 Model 497 Primary Standard Instruction Manual xi Figures xii Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Tables Tables Model 49i Primary Standard Specifications ccceesscceeseeeeeteeeeeneeeeeaeeeees 1 3 VO Terminal Board Pin Descriptions tee 2 5 D O Terminal Board Pin Descriptions ee Ier 25 Pin Terminal Board Pin Descriptions gege eegener 2 8 Prone eege 3 3 Eet E 3 9 Pert Aao O UN ce nmr a te ree ne E eee 3 10 Analog Output Zero to KT cscceczsnexeaaseinascessaanecsys iaanecenessecce 3 42 Sonal Lype Group CHOICES age 3 44 Troubleshooting General Guide E 5 2 Troubleshooting Alarm Messages A 5 4 Motherboard Connector Pin Descriptions sessionaris 5 8 Front
172. nto the long records list Send set copy sp to lrec Receive set copy sp to lrec ok set copy lrec to sp set copy srec to sp set copy stream to sp These commands copy the current contents of the long record short record or streaming data list into the scratch pad sp These commands are useful in easy modification of current long record short record or streaming data lists The example that follows copies the current list of long records into the scratch pad Send set copy lrec to sp Receive set copy lrec to sp ok sp field number This command reports the variable number and name stored at index in the scratch pad list The example that follows shows that the field 5 in the scratch pad is set to index number 11 which is for the variable pres Send sp field 5 Receive sp field 5 11 pres set sp field number value number 1 32 is the maximum number of fields in long and short record lists number 18 is for streaming data lists This command sets the scratch pad field number item number in scratch pad list to value where value is the index number of a variable in the analog out variable list Available variables and their corresponding index numbers may be obtained using the command list var aout The set sp field Model 497 Primary Standard Instruction Manual B 23 C Link Protocol Commands Datalogging command is used to create a list of variables which can then be transferred into the long recor
173. o contacting the factory with any questions regarding the instrument please note the program version number e Inthe Main Menu choose Diagnostics gt Program Version Voltages The Voltages menu displays the current diagnostic voltage readings This screen enables the power supply to be quickly read for low or fluctuating voltages without having to use a voltage meter The I O board is only displayed if the I O expansion board option is installed e Inthe Main Menu choose Diagnostics gt Voltages Motherboard Voltages The Motherboard screen read only is used to display the current voltage readings on the motherboard e Inthe Main Menu choose Diagnostics gt Voltages gt Motherboard Voltages Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 51 Operation Diagnostics Menu Interface Board Voltages The Interface Board screen read only is used to display the current voltage readings on the interface board e Inthe Main Menu choose Diagnostics gt Voltages gt Interface Board Voltages UU Board Voltages The I O Board screen read only is used to display the current voltage readings on the I O expansion board This menu is only displayed if the I O expansion board option is installed e Inthe Main Menu choose Diagnostics gt Voltages gt I O Board Voltages 3 52 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Diagnostics Menu
174. o zero then N N 1 Error Response Function code 1 Byte Function code 0x80 Exception code 1 Byte 01 IIlegal Function 02 IIlegal Address 03 lllegal Data 04 Slave Device Failure Here is an example of a request and response to read outputs 2 15 Request Field Name Hex Function 0x01 Starting Address Hi 0x00 Starting Address Lo 0x02 Quantity of Outputs Hi 0x00 Quantity of Outputs Lo 0x0D C 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific MODBUS Protocol Function Codes Response Field Name Hex Function 0x01 Byte Count 0x03 Outputs status 2 10 OxCD Outputs status 11 15 0x0A The status of outputs 2 10 is shown as the byte value 0xCD or binary 1100 1101 Output 10 is the MSB of this byte and output 2 is the LSB By convention bits within a byte are shown with the MSB to the left and the LSB to the right Thus the outputs in the first byte are 10 through 2 from left to right In the last data byte the status of outputs 15 11 is shown as the byte value 0x0A or binary 0000 1010 Output 15 is in the fifth bit position from the left and output 11 is the LSB of this byte The four remaining high order bits are zero filled 0x03 0x04 Read Holding Read holding input registers reads the measurement data from the Registe rs Read Input instrument Issuing either of these function codes will generate the same Registers SPO These functions read the contents of one or more contiguous g
175. ode on page 6 4 then return to the beginning of this step a 4 Wait at least 10 seconds for the reading to stabilize use gt and to enter the known temperature and press to save the temperature value 5 Install the cover Use the following procedure to replace the optional I O expansion board Figure 6 7 Note After replacing the optional I O expansion board calibrate the current outputs and the analog voltage inputs See the Analog Output Calibration procedure and the Analog Input Calibration procedure in this chapter Equipment Required I O expansion board Nut driver 3 16 inch Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Turn instrument OFF unplug the power cord and remove the cover 2 Unplug the I O expansion board cable from the EXPANSION BD connector on the motherboard 3 Remove the two standoffs holding the I O expansion board connector to the rear panel Figure 6 8 4 Pop off the board from the mounting studs and remove the board 5 To install the I O expansion board follow previous steps in reverse 6 18 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Servicing Digital Output Board Replacement 6 Calibrate the analog current outputs and the analog voltage inputs as described earlier in th
176. of choices The minimum and maximum output value screens function the same way The example below shows the set minimum value screen e Inthe Main Menu choose Instrument Controls gt IO Configuration gt Analog Output Config gt Select Channel gt Set Minimum or Maximum Value e Use t and to increment or decrement the numeric value e Press to validate and save the new minimum value Table 3 4 Analog Output Zero to Full Scale Table Output Zero Value Full Scale 100 Value 03 Zero 0 Range Setting Range Status Recommend not to change the setting for this output Intensity A User set alarm min value User set alarm max value Intensity B User set alarm min value User set alarm max value 3 42 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Table 3 4 Analog Output Zero to Full Scale Table Output Noise A Noise B Flow A Flow B Pressure Bench Temp Lamp Temp O3 Lamp Temp Choose Signal To Output Zero Value Zero 0 Zero 0 User set alarm min value User set alarm min value User set alarm min value User set alarm min value User set alarm min value User set alarm min value Operation Instrument Controls Menu Full Scale 100 Value Range Setting Range Setting User set alarm max value User set alarm max value User set alarm max value User set alarm max value User set alarm max value User set alarm max value Other Measurements and Analog Inputs if the I O expans
177. ompensation is on then both pressure readings are the same If pressure compensation is off a pressure of 760 mm Hg is used as the default pressure even though the actual pressure is 753 4 mm Hg The example that follows shows that actual reaction chamber pressure is 753 4 mm Hg Send pres Receive pres 760 0 mm Hg actual 753 4 flags This reports 8 hexadecimal digits or flags that represent the status of the ozonator gas mode and alarms To decode the flags each hexadecimal digit is converted to binary as shown in Figure B 1 It is the binary digits that define the status of each parameter In the example that follows the instrument is reporting the instrument is in local mode the temperature compensation and pressure compensation are OFF the gas mode status is Sample gas units are ppb and intensity B is in high alarm Send flags Receive flags 00028000 Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual B 11 C Link Protocol Commands Alarms a i Convert to binary l p r e sg i gt SAA COIN JOE wee we ie x E NVE LOD Le se g 8 Pa 8 Ba VA l l 7 es ojlolilollo oiioioiol lollollollo fojfojfi fo iioiioio o fo fojfo lollolilollo ojfojfojfo II II Il l J l l J l J J l l l l J Not Used a Alarms lodes Oz Lamp lemp Er J r Bench Lamp Temp O local S e E Bench lemp 01 remote Daea S Pressure 10 servic
178. onds standard cycle or every four seconds fast cycle Every cycle the two solenoid valves switch the sample gas and reference gas streams between the two cells One cell contains sample gas the other cell contains reference gas and vice versa During a standard cycle the cells are purged for seven seconds and measurements are taken for three seconds During a fast cycle the cells are purged for three seconds and measurements are taken for one second During every cycle the instrument calculates the natural logarithm of the sample gas frequency to reference gas frequency ratio in each cell and averages these results to optimize instrument accuracy These logarithms provide the basis for calculating the ozone concentrations The logarithms are stored in a rolling stack of 30 logarithms which are averaged by the Instrument e averaging time function The background values for O3 are corrected for temperature pressure and span and are subtracted from the ozone calculated to yield a corrected value 7 4 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Output Communication Electronics Motherboard External Connectors Thermo Fisher Scientific System Description Electronics The front panel display serial and Ethernet data ports and analog outputs are used to communicate the results of the measurement calculations The front panel displays the O3 concentration The display is updated every ten seconds
179. onnector An RJ45 connector is used for the 1OMbs Ethernet connection supporting TCP IP communications via standard IP V4 addressing The IP address may be configured for static addressing or dynamic addressing set using a DHCP server Any serial port protocols may be accessed over Ethernet in addition to the serial port The external accessory connector is not used in the Model 497 Primary Standard This port is used in other models to communicate with smart external devices that may be mounted hundreds of feet from the analyzer using an RS 485 electrical interface Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Chapters Optional Equipment The Model 497 Primary Standard is available with the following options e Zero Air Source on page 8 1 e Teflon Particulate Filter on page 8 1 e I O Expansion Board Assembly on page 8 1 e Terminal Block and Cable Kits on page 8 2 e Cables on page 8 2 e 25 Pin Terminal Board Assembly on page 8 3 e Mounting Options on page 8 3 Zero Air Source The zero air source option is a convenient system for generating pollutant free zero gas for O3 monitoring requirements This option includes the pump filter filter holder and Silastic tubing Teflon Pa rticulate A 5 10 micron pore size two inch diameter Teflon element is available for Filter the Model 497 Primary Standard This filter should be installed just prior to the SAMPLE
180. or codes For associated part numbers refer to External Device Connection Components in the Servicing chapter Note able 8 2 provides the color coding for both 25 pin cables and 37 pin cables Color codes for pins 1 25 are for 25 pin cables color codes for pins 1 37 are for 37 pin cables a Table 8 1 Cable Options Description Cable Length DB37M to open end Six feet DB37F to open end Six feet DB25M to open end Six feet RS 232 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific 25 Pin Terminal Board Assembly Mounting Options Thermo Fisher Scientific Optional Equipment 25 Pin Terminal Board Assembly Table 8 2 Color Codes for 25 Pin and 37 Pin Cables Pin Color 1 BLACK 2 BROWN 3 RED 4 ORANGE 5 YELLOW 6 GREEN 7 BLUE 8 VIOLET 9 GRAY 10 WHITE 11 PINK 12 LIGHT GREEN 13 BLACK WHITE 14 BROWN WHITE 15 RED WHITE 16 ORANGE WHITE 17 GREEN WHITE 18 BLUE WHITE 19 VIOLET WHITE Pin 20 21 22 23 24 25 Color RED BLACK ORANGE BLACK YELLOW BLACK GREEN BLACK GRAY BLACK PINK BLACK End color codes for 25 pin cables continue for 37 pin cables 26 2i 28 29 30 31 2 33 34 Sa 36 S PINK GREEN PINK RED PINK VIOLET LIGHT BLUE LIGHT BLUE BROWN LIGHT BLUE RED LIGHT BLUE VIOLET LIGHT BLUE BLACK GRAY GREEN GRAY RED GRAY VIOLET LIGHT GREEN BLACK The 25 pin terminal board assembly is included with the optional I O expansion board Refer Terminal
181. or enters the flow value on this screen to perform the calibration a e Inthe Main Menu choose Service gt Select Flow Calibration A or B gt Span e Use EW and to move and change the value e Press to save set to value as actual value Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 75 Operation Service Menu Te TER L piyi LLI cure ts CHOMGE VALLE Restore Default Flow Calibration The Restore Default Calibration A screen allows the user to reset the flow calibration configuration values to factory defaults The Restore Default Calibration B screen functions the same way e Inthe Main Menu choose Service gt Select Flow Calibration A or B gt Set Defaults e Press to warn user and enable restore with al e Use to overwrite pressure sensor calibration parameters with factory default values when pressed after 4a Temperatu re Calibration The Temperature calibration screen allows the user to view and set the ambient temperature sensor calibration The temperature calibration is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician e In the Main Menu choose Service gt Temperature Calibration 3 76 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operat
182. ore a large range of detector frequencies are acceptable for proper operation of the instrument The nominal values are 65 to 120 kHz These frequencies can be monitored from the Intensities screen in the Diagnostics menu l Press to display the Main Menu 2 Use t Tt to scroll to GE press aa gt Ire scroll to Intensities and press The Intensities screen appears Degradation of detector frequencies to below 65 kHz indicates either a dirty cell or low lamp output In addition to degrading the measured detector frequency dirt in the cells can decompose the ozone and give erroneous readings Therefore the cells should first be cleaned and the frequency re measured If the frequencies are still low the lamp output can be increased by using the Lamp Setting screen in the Service mode If the frequency cannot be set above 65 kHz replace the lamp 1 Press m to display the Main Menu 2 Use to scroll to Service press EE gt to scroll to Lamp Setting and press The Lamp Setting screen appears If the Service Mode is not displayed on the Main Menu use the following procedure to display it a At the Main Menu press to scroll to Instrument Controls gt press sl E to scroll to Service Mode gt and press e The Service Mode screen appears b Press to toggle the Service Mode to ON c Press nl gt nl to return to the Main Menu Model 497 Primary Standard Instruction Manual T
183. ote mode in order to change instrument parameters via remote However the command set mode remote can be sent to the analyzer to put it in the remote mode Report commands commands that don t begin with set can be issued either in the remote or local mode For information on changing modes see Chapter 3 Operation The commands can be sent in either uppercase or lowercase characters Each command must begin with the proper instrument identification number ASCII character The command in the example that follows begins with the ASCII character code 170 decimal which directs the command to the Model 497 and is terminated by a carriage return CR ASCII character code 13 decimal B 2 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands If an incorrect command is sent a bad command message will be received The example that follows sends the incorrect command set unit ppm instead of the correct command set gas unit ppm Send set unit ppm Receive set unit ppm bad cmd Commands The save and set save params commands stores parameters in FLASH It is important that each time instrument parameters are changed that this command be sent If changes are not saved they will be lost in the event of a power failure Table B 1 lists the 497 Primary Standard C Link protocol commands The interface will respond to
184. possible values of this example will be 0 through 3 The translation list shows the words which correspond to each input value the zeroth value appearing first 0 gt local 1 gt remote etc The selection list shows that only the first two values in this case are to be shown to the user when the button is pressed The T button indicates full translation input code to string and user selection number to output string Wat B 48 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Record Layout Definition This is a line that starts a new column the xC or AL Comp 6 11x off on Tset temp comp Ben This shows that the bitfield end the second part of a bitfield specification is optional The bitfield will be one bit long starting in this case at the eleventh bit Background 7f 8Bd ddd set 03 bkg Sein This shows the use of indirect precision specifiers for floating point displays The background value is taken from the 7th element and the precision specifier is taken from the 8th If the asterisk were not present it would indicate instead that 8 digits after the decimal point should be displayed Model 497 Primary Standard Instruction Manual B 49 C Link Protocol Commands Record Layout Definition B 50 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Appendix C MODBUS Protocol This appendix provides a description of
185. power cord 2 Ifthe instrument is mounted in a rack remove it from the rack 3 Remove the cover 6 8 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Fuse Replacement Thermo Fisher Scientific 10 KS Servicing Fuse Replacement Disconnect the plumbing connections at the rear of the measurement bench Disconnect the connectors that pass through the center of the partition panel Remove two screws from the left side of the case viewed from rear Remove one screw from the bottom front of the case Remove one screw from the top front of the partition panel While holding the case securely loosen the captive screw at the rear of the measurement bench and pull the measurement bench from the rear of the case Remove the screw at the top rear of the partition panel securing the top of partition panel to the measurement bench and lower the panel being careful not to put excessive tension on the cables Replace the measurement bench by following the previous steps in reverse Use the following procedure to replace the fuse Equipment Required Replacement fuses refer to Replacement Parts List on page 6 4 Turn instrument OFF and unplug the power cord Remove fuse drawer located on the AC power connector If either fuse is blown replace both fuses Model 497 Primary Standard Instruction Manual 6 9 Servicing Pump Replacement 4 Insert fuse drawer and reconnect power
186. pply e Photometer lamp power supply e Optical bench temperature thermistor e Pump e Sample Reference Solenoid Valves Model 497 Primary Standard Instruction Manual 7 1 System Description Hardware Motherboard Ozonator Pump Ozonator Board a Output Board Photometer Board I O Expansion Board Optional CG _ ER Fan solenoid Assembly D d i Sample Valve Reference Valve Y mi IN d W SL Ss SSS a ss At Ke 3 H IC i gt H o J r Power Supply F z EL Measurement Interface Board Flow Transducer B Flow Transducer A Detector Assembly A Detector Assembly B Photometer Lamp Lamp Heater Optical Bench Pressure Transducer Assembly Optical Bench with Photometer Lamp Detector System Flow Transducers Pressure Transducer Figure 7 1 Hardware Components The optical bench has two airtight chambers that contain the sample and reference gases with a common photometer lamp at one end and two individual detectors at the other end The photo diode in each detector transmits light intensity information to the measurement interface board for sample measurement computations Flow transducers monitor the flow of the sample and reference gases and transmit the data to the measurement interface board The pressure transducer measures the pressure of the sample gas 7 2 Model 497 Primar
187. pump only adjust the span setting 6 32 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Servicing Pressure Transducer Calibration A rough check of the pressure accuracy can be made by obtaining the current barometric pressure from the local weather station or airport and comparing it to the pressure reading However since these pressures are usually corrected to sea level it may be necessary to correct the reading to local pressure by subtracting 0 027 mm Hg per foot of altitude Do not try to calibrate the pressure transducer unless the pressure is known accurately 1 Remove the cover 2 Disconnect the tubing from the pressure transducer and connect a vacuum pump known to produce a vacuum less than 1 mm Hg 3 From the Main Menu press to scroll to Service gt press gt A to scroll to Pressure Calibration gt and press ER The Pressure Sensor Cal screen appears Note If Service is not displayed refer to Accessing the Service Mode on page 6 4 then return to the beginning of this step 4 At the Pressure Sensor Cal screen press to select Zero The Calibrate Pressure Zero screen appears 5 Wait at least 10 seconds for the zero reading to stabilize then press to save the zero pressure value 6 Disconnect the pump from the pressure transducer 7 Press nl to return to the Pressure Sensor Cal screen 8 At the Pressure Sensor Cal screen
188. r WARNING The service procedures in this manual are restricted to qualified service representatives If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired a Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Remove the instrument cover 2 Tape the thermistor plugged into the measurement interface board to a calibrated thermometer Note Since the thermistors are interchangeable to an accuracy of 0 2 C and have a value of 10K ohms at 25 C an alternate procedure is to connect an accurately known 10K resistor to the thermistor input TEMP on the measurement interface board and enter the temperature reading A 1 C change corresponds to a 5 change in resistance thus this alternative procedure can be quite accurate as a check however it clearly is not NIST traceable 3 From the Main Menu press to scroll to Service gt press gt to scroll to Temperature Calibration gt and press Ce The Calibrate Bench Temp screen appears Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 17 Servicing I O Expansion Board Optional Replacement I O Expansion Board Optional Replacement Note If Service is not displayed refer to Accessing the Service M
189. r Calibration Use the following procedure to calibrate the flow transducer Equipment Required Flow sensor WARNING The service procedures in this manual are restricted to qualified service representatives If the equipment is operated in a manner not specified by the manufacturer the protection provided by the equipment may be impaired a Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Remove the cover 2 Disconnect the pump cable from AC PUMP connector on the measurement interface board 3 From the Main Menu press to scroll to Service gt press gt to scroll to Flow A Calibration or Flow B Calibration gt and press e Depending on your selection the Flow A Sensor Cal or Flow B Sensor Cal screen appears For this procedure Flow A Sensor Cal is used Note If Service is not displayed refer to Accessing the Service Mode on page 6 4 then return to the beginning of this step 4 At the Flow A Sensor Cal screen press to select Zero The Calibrate Flow A Zero screen appears 5 Wait at least 10 seconds for the zero reading to stabilize then press to save the zero flow value Model 497 Primary Standard Instruction Manual 6 35 Servicing Ozonator Lamp Replacement Ozonator Lamp Replacement A 10 11 Reconnect the pump cable to the A
190. rd Photometer Board Sy I Dr Power Supply d Gt Rice Measurement Team mr Interface Board CNL IE rm els IT D E S Gi Y A UJ ee Ze KL Leg mm CH l y oh IL Lamp Heater Optical Bench Pressure Transducer Assembly Figure 6 2 Component Layout Model 497 Primary Standard Instruction Manual Flow Transducer B Flow Transducer A mT aA Eo eh on 4 Tei E Sach TI Detector Assembly B Log an Poo e A i D i ER i CL Detector Assembly A 6 7 Servicing Removing the Measurement Bench and Lowering the Partition Panel Removing the Measurement Bench and Lowering the Partition Panel REMOVE SCREWS Pass Through Connectors Partition Panel The measurement bench can be removed and the partition panel can be lowered to improve access to connectors and components Refer to the following steps when a procedure requires lowering the partition panel see Figure 6 3 Remove Screw LOWER PANEL Remove Hidden Screw Figure 6 3 Removing the Measurement Bench and Lowering the Partition Panel Equipment Required Philips screwdriver Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Turn instrument OFF and unplug the
191. rding to Table B 6 If the mode is incorrect the instrument responds with can t wrong settings The example that follows reports that the O3 range is 50 ppb Send range 03 Receive range oi 0 5000E 2 ppb set range selection set high range selection set low range selection These commands select the O full scale range according to able B 6 The example that follows sets the O3 full scale to 2 000 ppb Send set range 03 5 Receive set range oi 5 ok Table B 6 Range Settings Code ppm mg m 0 0 05 0 1 1 0 1 0 2 2 0 2 0 4 3 0 5 1 4 1 2 5 2 4 6 5 10 7 10 20 8 20 40 g 50 100 10 100 200 11 200 400 12 C1 C1 13 C2 C2 14 C3 RF custom range range 1 2 3 B 30 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Measurement Configuration This command reports the user defined value of custom range 1 2 or 3 The example that follows reports that custom range 1 is defined to 55 0 Send custom 1 Receive custom 1 5500E 2 ppm set custom range value set custom 1 value set custom 2 value set custom 3 value set custom 1 range value set custom 2 range value set custom 3 range value These commands are used to set the maximum concentration for any of the three custom ranges 1 2 or 3 to range value where value is a floating point number representing concentration in ppm or mg m The example that follows sets the custom
192. rds screen is used to select the starting point to display the number of records back to view e Use and gt to move the cursor left or right e Use t and to increment or decrement the numeric value e Press to set the starting record and continue to the record display screen The Record Display screen read only displays the selected records e Use e and to view all the items in the record e Use and to view records at different times Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 19 Operation Instrument Controls Menu Date and Time The Date and Time screen is used to set a start date and time for which to view logged data For example if 20 JUN 2005 10 00 is entered then the first logged data record that is displayed is the first record after this time If set to one minute logging this would be at 20 JUN 2005 10 01 e Use and to increment or decrement the selected field e Use ER to advance to next field e Press to set the date and time of the first record to be displayed and continue to the record display screen The Record Display screen read only displays the selected records e Use e and a to view all the items in the record e Use and to view records at different times 3 20 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Erase Log Operation Instrument Controls Menu The
193. registers These registers are 16 bits each and are organized as shown below All of the values are reported as 32 bit IEEE standard 754 floating point format This uses 2 sequential registers least significant 16 bits first The request specifies the starting register address and the number of registers Registers are addressed starting at zero Therefore registers numbered 1 16 are addressed as 0 15 The register data in the response message are packed as two bytes per register with the binary contents right justified within each byte For each register the first byte contains the high order bits and the second contains the low order bits Request Function code 1 Byte 0x03 or 0x04 Starting Address 2 Bytes 0x0000 to maximum allowed by instrument Quantity of Registers 2 Bytes 1 to maximum allowed by instrument Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual C 5 MODBUS Protocol Function Codes C 6 N Quantity of Registers Response Function code Byte count Register value Error Response Function code Exception code 1 Byte 1 Byte N x 2 Bytes 1 Byte 1 Byte 0x03 or 0x04 2 xN n NorN l Function code 0x80 01 IIlegal Function 02 IIlegal Address 03 lllegal Data 04 Slave Device Failure Here is an example of a request to read registers 10 13 Request Field Name Function Starting Address Hi Starting Address Lo No of Registers HI No of Registers Lo Response F
194. ring indicating the data formats for data that is sent out in response to the erec lrec srec and related commands The example that follows shows a typical response For details on how to interpret the strings see Record Layout Definition later in this appendix Send lrec layout Receive rec layout ze s lx Ar f SF f ZF f f SF AF AT f At SE ak flags no nox hino hinox pres pmtt intt rctt convt smplf ozonf pmtv Irec mem size srec mem size These commands report the long and short records that can be stored with the current settings and the number of blocks reserved for long and short records To calculate the number of short records per block add 2 to the number of records and then divide by the number of blocks The example that follows shows that 7 blocks were reserved for long records and the maximum number of long records that can be stored in memory is 1426 Send lrec mem size Receive lrec mem size 1426 recs 7 blocks Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual B 21 C Link Protocol Commands Datalogging lrec per srec per These commands report the long and short records logging period The example that follows shows that the short record logging period is 5 minutes Send srec per Recelve srec per 5 min set srec per value set srec per value value 1 5 15 30 60 These commands set the long and short records logging period to value in minutes The example that follows s
195. rt 1 CTS RS485 IN NC NC Serial Port 2 RX RS485 IN Serial Port 2 TX RS485 OUT NC Ground NC Serial Port 2 RTS RS485 OUT Serial Port 2 CTS RS485 IN NC AC HOT AC NEUT AC Ground AC HOT AC NEUT AC Ground AC HOT AC NEUT AC Ground Thermo Fisher Scientific Troubleshooting Connector Pin Descriptions Table 5 4 Front Panel Board Connector Pin Diagram Connector Reference Pin Signal Label Designator Description MOTHER di 1 Ground BOARD Ground LCLK LCD Signal Ground Ground LLP LCD Signal LFLM LCD Signal LD4 LCD Signal LDO LCD Signal co co N O o A O N 10 LD5 LCD Signal 11 LD1 LCD Signal 12 LD6 LCD Signal 13 LD2 LCD Signal 14 LD7 LCD Signal 15 LD3 LCD Signal 16 LCD Bias Voltage SI 5V 18 Ground 19 Ground 20 LCD_ONOFF LCD Signal 21 Keypad Row 2 Input 22 Keypad Row 1 Input 29 Keypad Row 4 Input 24 Keypad Row 3 Input 25 Keypad Col 2 Select 26 Keypad Col 1 Select 21 Keypad Col 4 Select 28 Keypad Col 3 Select 29 Ground 30 Ground 31 Ground Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 5 13 Troubleshooting Connector Pin Descriptions Table 5 4 Front Panel Board Connector Pin Diagram continued Connector Reference Pin Signal Label Designator Description 32 Ground 33 24V 34 24V LCD DATA J2 1 DO DV LCD Signal 2 LD1_5V LCD Signal 3 IO DV LCD Signal 4 LD3_5V LCD Signal 5 LCD_ONOFF_5V
196. rument Controls gt Communication Settings gt Baud Rate e Use t and to scroll through a list of choices e Press to save the new baud rate Instrument ID The Instrument ID screen allows the operator to edit the instrument ID The ID is used to identify the calibrator when using C Link or MODBUS protocols to control the calibrator or collect data It may be necessary to edit the ID number if two or more of the same calibrator are connected to one computer Valid Instrument ID numbers are from 0 to 127 The Model 492 Primary Standard has a default Instrument ID of 49 For more information about the Instrument ID see Appendix B C Link Protocol Commands or Appendix C MODBUS Protocol e Inthe Main Menu choose Instrument Controls gt Communication Settings gt Instrument ID 3 28 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Communication Protocol Streaming Data Configuration Thermo Fisher Scientific Operation Instrument Controls Menu e Use and to increment or decrement the ID value e Press to save the new instrument ID Che Communication Protocol screen is used to change the communication g protocol for serial communications In the Main Menu choose Instrument Controls gt Communication Settings gt Communication Protocol e Use and to scroll through a list of choices e Press to save the new protocol The Streaming Data Configur
197. s enables the pressure reading of Cell B with either sample or reference gas to be determined Pump pressure is used to test the pump Selecting any of these menu items will disturb the analog outputs e Inthe Main Menu choose Service gt Pressure Check Sample Pressure The Sample Pressure screen read only displays the pressure of the sample gas in Cell B e Inthe Main Menu choose Service gt Pressure Check gt Sample Pressure Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 67 Operation Service Menu Reference Pressure The Reference Pressure screen read only displays the pressure of the reference gas in Cell B e Inthe Main Menu choose Service gt Pressure Check gt Reference Pressure Pump Pressure The Pump Pressure screen read only is used to test the pump The solenoids are energized such that there is no flow in Cell B The flow rate for Cell B drops to zero and the pressure reading should drop below 390 mmHg in less than 20 seconds This indicates the effectiveness of the internal pump After 20 seconds if the pressure is greater than 390 mmHg or the flow is greater than 0 010 LPM the words PUMP PROBLEM DETECTED appears After 20 seconds if the pressure is less than 390 mmHg and the flow is less than 0 010 LPM the words PUMP OK appears e Inthe Main Menu choose Service gt Pressure Check gt Pump Pressure 3 68 Model 497 Primary Standard Instruction Man
198. s sets the current custom level 4 concentration B Benn _Reports sets the current custom level 5 concentration B lamp Reports sets the current photometer lamp setting B 10 lamp setting Reports the current photometer lamp setting B 10 lamp temp Reports the current bench lamp temperature B 10 lamp voltage bench Reports the bench lamp voltage Is volts B 11 lamp voltage oz Reports the ozonaor lamp voltage is volts B 11 layout ack Disables stale layout layout changed indicator 7 B 40 le left Simulates pressing left pushbutton B 28 level Sets the instrument in custom levels 1 2 3 40r 5 B 33 list din Lists current selection for digital input B 18 list dout Lists current selection for digital output B 18 list Irec Lists current selection Irec logging data B 18 list sp Lists current selection in the scratchpad list B 18 list srec Lists current selection srec logging data B 18 list stream Lists current selection streaming data output B 18 list var aout Reports list of analog output index numbers and variables B 43 list var din Reports list of digital input index numbers and variables B 43 B 6 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Command list var dout low avg time low 03 low 03 coef low range low sp conc Ir Irec Irec format Irec layout Irec mem size Irec per malloc Irec malloc srec manual me menu mode no of Irec no of srec 03 03 bkg 03 coef
199. selected analog output The operator must connect a meter to the output and adjust output until it reads the value shown in the set output to field e Inthe Main Menu choose Service gt Analog Out Calibration gt Select Channel gt Calibrate Full Scale e Use the and to increment or decrement the numeric value Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Service Menu e Press to save the value Analog Input Calibration The Analog Input Calibration menu is a selection of 8 analog inputs if the I O expansion board option is installed to calibrate and allows the user to select the calibration action zero or span The analog input calibration is visible only when the calibrator is in service mode For more information on the service mode see Service Mode earlier in the chapter Note This adjustment should only be performed by an instrument service technician a e Inthe Main Menu choose Service gt Analog Input Calibration Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 79 Operation Service Menu Analog Input Calibrate Zero The Analog Input Calibrate Zero screen allows the user to calibrate the zero state of the selected analog input In the Main Menu choose Service gt Analog Input Calibration gt Select Channel gt Calibrate Zero Hook up a voltage source of 0 V to the analog input channel e Press to save the valu
200. set dhcp on Receive set dhcp on ok format This command reports the current reply termination format The example that follows shows that the reply format is 00 which means reply with no checksum according to Table B 8 Send format Receive format 00 set format format This command sets the reply termination format where format is set according to able B 8 The example that follows sets the reply termination format to checksum Send set format 01 Receive set format 01 ok Table B 8 Reply Termination Formats Format Reply Termination 00 lt CR gt 01 lt NL gt sum xxxx lt CR gt where xxxx 4 hexadecimal digits that represent the sum of all the characters bytes in the message host name This command reports the host name string Send host name Receive host name ISERIES set host name string This command sets the host name string where string is 1 13 alphanumeric characters Send set host name analyzero1 B 38 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Communications Configuration Receive set host name analyzero1 ok instr name This command reports the instrument name Send instr name Receive instr name 03 Analyzer 03 Analyzer instrument id This command reports the instrument id Send instrument id Receive instrument id 49 set instrument id value This command sets the instrument id to value where va
201. ssor software tasks are organized into four areas s Instrument Control e Monitoring Signals e Measurement Calculations e Output Communication Model 497 Primary Standard Instruction Manual 7 3 System Description software Instrument Control Monitoring Signals Measurement Calculations Low level embedded processors are used to control the various functions on the boards such as analog and digital I O and heater control These processors are controlled over a serial interface with a single high level processor that also controls the front panel user interface The low level processors all run a common piece of firmware that is bundled with the high level firmware and loaded on power up if a different version is detected Each board has a specific address that is used to identify to the firmware what functions are supported on that board This address is also used for the communications between the low level processors and the high level processor Every tenth of a second the frequency counters analog I O and digital I O are read and written to by the low level processor The counters are accumulated over the past second and the analog inputs are averaged over that second The high level processor polls the low level processors once per second to exchange the measurement and control data The instrument includes a sample solenoid valve and a reference solenoid valve The instrument can be configured to measure O3 every ten sec
202. st strap must be worn while handling any internal component a Equipment Damage Some internal components can be damaged by small 1 Turn instrument OFF unplug the power cord and remove the cover 2 Remove the three ribbon cables and the two wire connector from the front panel board 3 Pop off the board from the two top mounting studs and remove the board by lifting it up and off the slotted bottom support 4 Replace the front panel board by following previous steps in reverse LCD Module LCD Module Screws Front Panel Board Mounting Studs 2 Ribbon Cables 3 ae f Two Wire Connector Bottom Support Figure 6 10 Replacing the Front Panel Board and the LCD Module LCD Module Use the following procedure to replace the LCD module Figure 6 10 Replacement Equipment Required Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 6 23 Servicing LCD Module Replacement LCD module Philips screwdriver CAUTION If the LCD panel breaks do not to let the liquid crystal contact your skin or clothes If the liquid crystal contacts your skin or clothes wash it off immediately using soap and water gt Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a gt Do not remove the LCD panel or frame from the LCD module The L
203. t ETX gt lt BCC gt lt STX gt DA lt ETX gt lt BCC gt The data query string is valid and will be answered with data transmission only if the command starts with lt STX gt which is followed by the characters DA and the lt address gt if present matches the Instrument Address and the command is terminated with either lt CR gt with no checksum or lt ETX gt followed by the correct checksum lt BCC gt Sample Data Reply String in response to Data Query Command DA In response to a valid data query command DA the instrument responds in the following format lt STX gt MD02 lt SP gt lt address gt lt SP gt lt measured valuel gt lt SP gt lt status gt lt SP gt lt SFKT gt lt SP gt lt address 1 gt lt SP gt lt measured value2 gt lt SP gt lt status gt lt SP gt lt SFKT gt lt EITX gt lt BCC gt The response uses the same command terminators as used by the received command i e if the received command was terminated with a lt CR gt the response is terminated with lt CR gt and if the command was terminated with a lt ETX gt lt BCC gt the response is terminated with lt ETX gt and the computed checksum lt BCC gt The 02 after the MD indicates that two measurements are present in the reply string a 03 for three measurements and so on this will also determine the length of the reply string Model 497 Primary Standard Instruction Manual D 5 Geysitech Bayern Hessen Protocol Geysitech Commands lt address
204. t the O3 span gas concentrations used by the auto calibration routine to value where value is a floating point representation of the gas concentration in current selected units The gas units are the same as those chosen by the user The example that follows sets the O3 span gas concentration to 123 4 ppm Send Set 03 gas 123 4 Receive set 03 gas 123 4 ok B 26 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific C Link Protocol Commands Calibration o3 bkg These commands report the current O3 background The example that follows reports that the O3 background is 5 5 ppb Send 03 bkg Receive 03 bkg 5 5 ppb set 03 bkg value These commands are used to set O3 background to user defined values to value where value is a floating point representation of the background in current selected units The example that follows sets the O3 background to 5 5 ppb Send set no bkg 5 5 Receive set no bkg 5 5 ok set cal detectors This command is used to balance the output for both detectors so that they read the same value Send set cal detectors Receive set cal detectors ok sp conc high sp conc low sp conc These commands report span concentration in single range mode or the high and low span concentrations in dual or auto range mode If the mode is incorrect the instrument responds with can t wrong settings The example below reports the span gas concentration in single rang
205. t to full scale set to zero or reset to normal Full scale sets the analog outputs to the full scale voltage zero sets the analog outputs to 0 volts and normal operation The example below shows the selected output state ALL is set to normal e Inthe Main Menu choose Diagnostics gt Test Analog Outputs gt ALL Voltage Channel 1 6 or Current Channel 1 6 e Press or to set output e Press e to reset to normal Instrument Configuration The Instrument Configuration screen displays information on the hardware configuration of the calibrator Note If the calibrator is in service mode pressing on the item will toggle it yes or no with the exception of purchased options such as dilution and auto calibration a e Inthe Main Menu choose Diagnostics gt Instrument Configuration e Press to toggle instrument configuration in service mode only Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 57 Operation Alarms Menu Contact Information The Contact Information screen displays the customer service information e Inthe Main Menu choose Diagnostics gt Contact Information Alarms Menu The alarms menu displays a list of items that are monitored by the calibrator If the item being monitored goes outside the lower or upper limit the status of that item will go from OK to either LOW or HIGH respectively If the alarm is not a level alarm the status will go
206. tandard Instruction Manual 3 47 Operation Instrument Controls Menu Use and to move the cursor up and down e Press to save the new value te CHANGE VALUE o SAVE User Value The User Value screen allows the user to set the output value for the corresponding input voltage for the selected table point in the conversion table from 9999999 to 99999999 The default table is a two point table with point 1 0 00 V 000 0 U and point 2 10 00 V 10 0 U e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Analog Input Config gt Select Table Point gt User Value e Use e and ER to move the cursor left or right e Use and 4 to move the cursor up and down e Press to save the new value te CHANGE VALUE o SAVE Screen Contrast The Screen Contrast screen is used to change the contrast of the display Intensities between 0 and 100 in increments of 10 are available Changing the screen contrast may be necessary if the calibrator is operated at extreme temperatures 3 48 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Instrument Controls Menu e Inthe Main Menu choose Instrument Controls gt Screen Contrast e Use and to increment or decrement the screen contrast e Press to accept a change Service Mode The Service Mode screen is used to turn the service mode on or off The service mode locks out any remote actions and inclu
207. tant information to alert you to potential safety D amage Alerts hazards and risks of equipment damage Refer to the following types of alerts you may see in this manual Safety and Equipment Damage Alert Descriptions Alert DANGER WARNING CAUTION Equipment Damage gt gt E xvi Model 497 Primary Standard Instruction Manual Description A hazard is present that will result in death or serious personal injury if the warning is ignored a A hazard is present or an unsafe practice can result in serious personal injury if the warning Is ignored a The hazard or unsafe practice could result in minor to moderate personal injury if the warning is ignored The hazard or unsafe practice could result in property damage If the warning Is ignored Thermo Fisher Scientific Preface Safety and Equipment Damage Alerts in this Manual Alert Description WARNING If the equipment is operated in a manner not specified by A the manufacturer the protection provided by the equipment may be impaired The service procedures in this manual are restricted to qualified service personnel only a The Model 497 Primary Standard is supplied with a three wire grounding cord Under no circumstances should this grounding system be defeated a CAUTION If the LCD panel breaks do not to let the liquid crystal A contact your skin or clothes If the liquid crystal contacts your skin or clothes wash it off immediately using soap and wa
208. ter Equipment Damage Do not attempt to lift the analyzer by the cover or other A external fittings some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a This adjustment should only be performed by an instrument service technician a Handle all printed circuit boards by the edges only Do not remove the panel or frame from the LCD module M The LCD module polarizing plate is very fragile handle it carefully Do not wipe the LCD module polarizing plate with a dry cloth it may easily scratch the plate a Do not use Ketonics solvent or aromatic solvent to clean the LCD module use a soft cloth moistened with a naphtha cleaning solvent Do not place the LCD module near organic solvents or corrosive gases a Do not shake or jolt the LCD module Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual xvii Preface FCC Compl lance Changes or modifications to this unit not expressly approved by the party responsible for compliance could void the user s authority to operate the equipment Note This equipment has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment
209. the board 3 Remove the two screws from the top of the board 4 Pop off the board from the bottom mounting studs and remove the board 5 To install the new ozonator board follow previous steps in reverse Service Locations For additional assistance service is available from exclusive distributors worldwide Contact one of the phone numbers below for product support and technical information or visit us on the web at www thermo com adi 1 866 282 0430 Toll Free 1 508 520 0430 International 6 40 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific Hardware Chapter7 System Description This chapter describes the function and location of the system components provides an overview of the software structure and includes a description of the system electronics and input output connections and functions e Hardware on page 7 1 describes the analyzer components e Software on page 7 3 provides an overview of the software organization and detailed information on the software tasks e Electronics on page 7 5 describes the system boards assemblies and connectors e I O Components on page 7 8 describes the input and output communication functions and components The Model 497 Primary Standard components include e Optical bench with photometer lamp e Detector system e Flow transducers e Pressure transducer e Ozonator assembly e Oczonator lamp power su
210. the command strings outlined below Table B 1 C Link Protocol Commands Command addr dns addr gw addr ip addr nm alarm bench lamp temp max alarm bench lamp temp min alarm bench temp max alarm bench temp min alarm conc 03 max alarm conc 03 min alarm intensity a max alarm intensity a min alarm intensity b max alarm intensity b min alarm level 1 Description Reports sets domain name server address Reports sets default gateway address Reports sets IP address Reports sets netmask address Reports the bench lamp temperature alarm maximum value Current setting Reports the bench lamp temperature alarm minimum value Current setting Reports the bench lamp temperature alarm maximum value Current setting Reports the bench temperature alarm minimum value current setting Reports the concentration 03 alarm maximum value current setting Reports the concentration O03 alarm minimum value current setting Reports the current setting of maximum intensity alarm level for cell a Reports the current setting of minimum intensity alarm level for cell a Reports the current setting of maximum intensity alarm level for cell b Reports the current setting of minimum intensity alarm level for cell b Reports current alarm level 1 offset from the concentration as the alarm trigger point for that level Model 497 Primary Standard Instruction Manual Page B 36 B 36 B 36 B 37 B 12 B 12 B 13 B 13
211. tics Menu The Analog Input Readings screen read only displays the 8 current user scaled analog readings if the I O expansion board option is installed e Inthe Main Menu choose Diagnostics gt Analog Input Readings The Analog Input Voltages screen read only displays the 8 raw analog voltage readings if the I O expansion board option is installed e Inthe Main Menu choose Diagnostics gt Analog Input Voltages The Digital Inputs screen read only displays the state of the 16 digital inputs e Inthe Main Menu choose Diagnostics gt Digital Inputs Model 497 Primary Standard Instruction Manual 3 55 Operation Diagnostics Menu Relay States The Relay States screen displays the state of the 10 digital outputs and allows toggling of the state to either on 1 or off 0 The relays are restored to their original states upon exiting this screen e Inthe Main Menu choose Diagnostics gt Relay States Test Analog Outp uts The Test Analog Outputs menu contains a number of digital to analog converter DAC calibration items Channel choices include all analog outputs 6 voltage channels and 6 current channels if the I O expansion board option is installed e Inthe Main Menu choose Diagnostics gt Test Analog Outputs 3 56 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Operation Diagnostics Menu Set Analog Outputs The Set Analog Outputs screen contains three choices Se
212. tion Manual xiii Tables Operating Status for Model 49i and 49i Primary Standard ee D 8 Error Status for Model 49i and 49i Primary Standard cesceeesseeeeees D 8 XIV Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Thermo Fisher Scientific About This Manual This manual provides information about operating maintaining and servicing the analyzer It also contains important alerts to ensure safe operation and prevent equipment damage The manual is organized into the following chapters and appendices to provide direct access to specific operation and service information e Chapter 1 Introduction provides an overview of product features describes the principles of operation and lists the specifications e Chapter 2 Installation describes how to unpack setup and startup the analyzer e Chapter 3 Operation describes the front panel display the front panel pushbuttons and the menu driven software e Chapter 4 Preventive Maintenance provides maintenance procedures to ensure reliable and consistent instrument operation e Chapter 5 Troubleshooting presents guidelines for diagnosing analyzer failures isolating faults and includes recommended actions for restoring proper operation e Chapter 6 Servicing presents safety alerts for technicians working on the analyzer step by step instructions for repairing and replacing components and a replacement parts
213. tment One cell excessively contaminated Defective detector Dirty cells Light adjustment Action Check that the instrument is plugged into the proper source 115 or 220 volts Check instrument fuses Check power supply voltages using a voltmeter Readjust Lamp Setting From the Service Mode menu choose Lamp Setting Interchange detectors at Measurement Interface Board connectors to determine if detector is defective Check for 1 7 volt peak to peak waveform at lamp current check point on Lamp Power Supply Board Readjust lamp setting From the Service Mode menu choose Lamp Setting Clean cell Interchange detectors at Measurement Interface Board connectors to determine if detector is defective Clean cells Check for 1 7 volt peak to peak waveform at lamp current check point on Lamp Power Supply Board Thermo Fisher Scientific Table 5 1 Troubleshooting General Guide continued Malfunction Cell A or B noise excessive Cell A and B noise excessive Pressure transducer does not hold calibration Output signal noisy Slow response Thermo Fisher Scientific Possible Cause Lamp Lamp heater 15 volt power supply Foreign material in one cell Defective detector Foreign material in cells Lamp failure 15 volt power supply Pressure transducer Recorder Sample is varying Foreign material in cell Sticky solenoid valve Averaging time Contaminated optical
214. ts user selected measurement data via the serial port in real time for capture by a serial printer data logger or PC 7 10 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific RS 232 Connection RS 485 Connection Thermo Fisher Scientific System Description 1 0 Components A null modem crossed cable is required when connecting the analyzer to an IBM Compatible PC However a straight cable one to one may be required when connecting the analyzer to other remote devices As a general rule when the connector of the host remote device is female a straight cable is required and when the connector is male a null modem cable is required Data Format 1200 2400 4800 9600 19200 38400 57600 or 115200 BAUD 8 data bits 1 stop bit no parity All responses are terminated with a carriage return hex 0D Refer to Table 7 1 for the DB9 connector pin configuration Table 7 1 RS 232 DB Connector Pin Configurations DB9 Pin Function 2 OT CO WN Ww RX TX RTS CTS Ground The instrument uses a four wire RS 485 configuration with automatic flow control SD Refer to Table 7 2 for the DB9 connector pin configuration Table 7 2 RS 485 DB Connector Pin Configuration DB9 Pin Function 2 or wo N CO receive receive transmit transmit ground Model 497 Primary Standard Instruction Manual 7 11 System Description 1 0 Components 7 12 Ethernet Connection External Accessory C
215. u choose Averaging Time e Use t and to scroll through a list of choices e Press to save the averaging time Calibration Fa CtOrs Calibration factors are used to make minor compensations to the O3 Menu concentration when the Model 497 Primary Standard is being precisely matched to a NIST traceable O3 calibrator The Calibration Factors menu displays the calibration factors e In the Main Menu choose Calibration Factors 3 12 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific 0 Background 0 Span Coefficients Thermo Fisher Scientific Operation Calibration Factors Menu The O3 Background is used to make small adjustments to the zero level This adjustment should only be made when the Model 497 Primary Standard is being precisely matched to a NIST traceable O3 calibrator Normally the Model 497 Primary Standard does not require any background compensation e In the Main Menu choose Calibration Factors gt O3 Background e Use Jand to increment or decrement the proposed background value e Press to save the new background The O3 span coefficients is s used to make small adjustments to the output level This adjustment should only be made when the Model 497 Primary Standard is being precisely matched to a NIST traceable O3 calibrator Normally the Model 497 Primary Standard does not require any compensation Note The concentration value will show ERROR if the measur
216. u displays a list of the 16 digital inputs available and allows the user to select the logic state and instrument parameter for the relay selected Note The digital inputs must be asserted for at least one second for the action to be activated a e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Digital Input Settings e Use and to move the cursor up and down e Press to select a choice Logic State The Logic State screen is used to change the I O relay to either normally open or normally closed The default state is open which indicates that a relay connected between the digital input pin and ground is normally open Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 3 39 Operation Instrument Controls Menu and closes to trigger the digital input action If nothing is connected to the digital input pin the state should be left at open to prevent the action from being triggered e Press to toggle and set the logic state open or closed Instrument Action The Instrument Action screen allows the user to choose the instrument action that is tied to the selected digital input e Inthe Main Menu choose Instrument Controls gt I O Configuration gt Digital Input Settings gt Select Relay gt Instrument Action e Use and to scroll through a list of choices e Press to save the new selection for the relay Analog Output Configuration The
217. ual 2 5 Installation Connecting External Devices Table 2 1 UU Terminal Board Pin Descriptions continued Pin Signal Description 3 Analog2 4 Analog ground 5 Analog3 6 Analog ground 7 Analog4 8 Analog ground 9 Analog5 10 Analog ground 11 Analog6 12 Analog ground Pin 15 16 17 18 19 20 21 22 EK 24 Signal Description Power_Fail_NO TTL_Input1 TTL_Input2 TTL_Input3 TTL_Input4 Digital ground TTL_Input5 TTL_Input6 TTL_Input7 Digital ground D O Terminal Board Figure 2 5 shows the recommended method for attaching the cable to the terminal board using the included tie down and spacer Table 2 2 identifies the connector pins and associated signals See Detail A See Detail B Assembled Connector Detail A Figure 2 5 D O Terminal Board Views 2 6 Model 497 Primary Standard Instruction Manual Detail B Thermo Fisher Scientific Installation Connecting External Devices Table 2 2 D O Terminal Board Pin Descriptions Pin Signal Description Pin Signal Description 1 Relay1_ContactA 13 Relay7_ContactA 2 Relay1_ContactB 14 Relay7_ContactB 3 Relay2_ContactA 15 Relay8_ContactA 4 Relay2_ContactB 16 Relay8_ContactB 5 Relay3_ContactA 17 Relay9_ContactA 6 Relay3_ContactB 18 Relay9_ContactB 7 Relay4_ContactA 19 Relay10_ContactA 8 Relay4_ContactB 20 Relay10_ContactB 9 Relay5_ContactA Z Solenoid_Drive_Output1 10 Relay5_ContactB 22 24V 11 Relay6_ContactA 23 solenoid_Drive_O
218. ual Thermo Fisher Scientific Lamp Setting Detector Calibration Thermo Fisher Scientific Operation Service Menu The Lamp Setting screen is used to adjust the detector intensities The display shows the intensities of Cell A and Cell B The next line of the display shows the current lamp setting Adjust the lamp setting until the intensities are about 100 kHz Note This adjustment should only be performed by an instrument service technician e Inthe Main Menu choose Service gt Lamp Setting e Use and to increment or decrement the numeric value e Press to save the new lamp setting The Detector Calibration screen is used to set the calibration factors for detector A and detector B Calibration factors are computed so that both detectors read 100 000 Hz on zero air If either detector reads lower than 75 000 Hz or higher than 125 000 Hz this calibration will not be successful It is crucial that the lamp intensity be set such that both detector intensities fall inside this range before performing this calibration Model 497 Primary Standard Instruction Manual 3 69 Operation Service Menu Note This adjustment should only be performed by an instrument service technician a e Inthe Main Menu choose Service gt Detector Calibration Intensity Check The Intensity Check menu is used to manually control the flow of reference or sample gas through either Cell A or Cell B This enables the intensity an
219. ubsequent semicolon I Indicates a button which pops up a selection list with input translation That is the values read are translated before they are compared to the selection list options L Indicates a button which pops up a selection list without any translation The output value is number of the selected option T Indicates a button which pops up a selection list with output translation The number of the option selected is used as an index into the translation table to generate an output string N Indicates a button which only sends the subsequent command to the instrument No user prompting happens The following string through an optional or the end of the line is the command which is to be sent to the instrument upon the completion of the button selection The command string should normally contain print style formatting to include the user input If a is present it indicates a command which is sent to the instrument upon successful completion of the button command to update the value field This is not currently used Some examples Un is the C syntax for an end of line character Concentrations n Model 497 Primary Standard Instruction Manual B 47 C Link Protocol Commands Record Layout Definition This is a single text only line Au This is a single blank line 03 3s n This is a line which appears slightly indented The text field is 03 the value is taken from the third element
220. uild the pump Figure 4 2 To replace the pump see Pump Replacement in the Servicing chapter Equipment Required Flatblade screwdriver Pump rebuild kit flapper valve and diaphragm amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a Equipment Damage Some internal components can be damaged by small 1 Turn instrument OFF unplug the power cord and remove the cover 2 Loosen the fittings and remove both lines going to the pump 4 6 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Preventive Maintenance Leak Test and Pump Checkout 3 Remove the four screws from the top plate remove top plate flapper valve and the bottom plate S2 Top Plate S e Flapper Plate Bottom Plate Diaphragm Figure 4 2 Rebuilding the Pump 4 Remove the screw the securing the diaphragm to piston and remove diaphragm 5 Assemble the pump by following the previous steps in reverse make sure the Teflon white side of the diaphragm is facing up and that the flapper valves cover the holes of the top and bottom plate 6 Perform the Leak Test and Pump Checkout procedure described in this chapter Leak Test and Pump Use the following procedures to test for system leaks and checkout the Checkout pump External Leaks Use the following procedure to test for leaks around the fittings Thermo Fisher Scientific
221. ull Scale 8 Use until the meter reads the value shown in the Set Output To line then press to save the value Use the following procedures to calibrate the analog inputs after replacing the optional I O expansion board These procedures include selecting analog input channels calibrating them to zero volts and then calibrating them to full scale using a known voltage source Use the following procedure to calibrate the input channels to zero volts 1 From the Main Menu press to scroll to Service press gt to scroll to Analog Input Calibration and press ECH The Analog Input Cal screen displays Note If Service is not displayed refer to Accessing the Service Mode on page 6 4 then return to the beginning of this step a 2 At the Analog Input Cal screen press to scroll to a channel and press 4 3 With the cursor at Calibrate Zero press The screen displays the input voltage for the selected channel Model 497 Primary Standard Instruction Manual 6 15 Servicing Analog Input Calibration 6 16 Make sure that nothing is connected to the channel input pins and press to calibrate the input voltage on the selected channel to zero volts The screen displays 0 00 V as the voltage setting Press gt to return to the Analog Input Cal screen and repeat Steps 2 through 4 to calibrate other input channels to zero as necessary Continue with the Calibrating the Input Channels to Full
222. unding system be defeated a Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component Figure 6 1 If an antistatic wrist strap is not available be sure to touch a grounded metal object before touching any internal components When the instrument is unplugged the chassis is not at earth ground a Handle all printed circuit boards by the edges a Do not remove the LCD panel or frame from the LCD module The LCD polarizing plate is very fragile handle it carefully Do not wipe the LCD polarizing plate with a dry cloth it may easily scratch the plate Do not use alcohol acetone MEK or other Ketone based or aromatic solvents to clean the LCD module use a soft cloth moistened with a naphtha cleaning solvent Do not place the LCD module near organic solvents or corrosive gases a Do not shake or jolt the LCD module a Model 497 Primary Standard Instruction Manual 6 3 Servicing Firmware Updates Firmware Updates Accessing the Service Mode Replacement Parts List Figure 6 1 Properly Grounded Antistatic Wrist Strap The firmware can be updated by the user in the field via the serial port or over the Ethernet This includes both the main processor firmware and the firmware in all low level processors Refer to the Port manual for the firmware update proce
223. using until it bottoms Pull lamp out approximately 1 16 inch to allow for expansion when the lamp warms up and tighten the Allen screws on the clamp Slide the insulation onto lamp against the ozonator assembly Re connect the ozonator LAMP connector to the ozonator board 10 Replace the cover and reconnect power Use the following procedure to replace the ozonator lamp heater Equipment Required Model 497 Primary Standard Instruction Manual 6 37 Servicing Ozonator Lamp Heater Replacement Ozonator lamp heater Allen wrenches 3 32 inch 7 64 inch Philips screwdriver Heat conductive compound Equipment Damage Some internal components can be damaged by small amounts of static electricity A properly grounded antistatic wrist strap must be worn while handling any internal component a 1 Turn instrument OFF unplug the power cord and remove the cover 2 Unplug heater cable from the LAMP HEATER and LAMP connectors on the ozonator board Figure 6 13 3 Disconnect plumbing from the ozonator 4 Remove the two screws securing the ozonator to the floor plate and remove the ozonator 5 Remove bottom flange of ozonator housing 6 Remove ozonator lamp heater block from ozonator by removing four Allen screws 7 Coat new lamp heater block with thin film of heat conductive compound 8 Install new ozonator lamp heater block by following the above procedure in reverse 9 Re install the instrument cover 6 38
224. utput2 12 Relay6_ContactB 24 24V 25 Pin Terminal Board The 25 pin terminal board is included with the optional I O Expansion Board See Detail A See Detail B Detail A Detail B Assembled Connector Figure 2 6 25 Pin Terminal Board Views Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 2 1 Installation Startup Table 2 3 25 Pin Terminal Board Pin Descriptions Pin Signal Description Pin Signal Description 1 lOut1 IS Analog In 2 GND_ISO 14 Analog_ n2 3 Ou 15 Analog_ n3 4 GND_ISO 16 GNDD 5 lOut3 17 Analog Ind 6 GND_ISO 18 Analog_In5 l lOut4 19 Analog_ n6 8 GND_ISO 20 GNDD d Out 21 Analog_ n7 10 GND_ISO 22 Analog Int 11 lOut6 Zs GNDD 12 GND_ISO 24 GNDD Sta rtup Use the following procedure when starting the instrument 1 Turn the power ON 2 Allow 90 minutes for the instrument to stabilize 3 Set instrument parameters such as operating ranges and averaging times to appropriate settings For more information about instrument parameters see the Operation chapter 2 8 Model 497 Primary Standard Instruction Manual Thermo Fisher Scientific Chapter3 Operation This chapter describes the front panel display front panel pushbuttons and menu driven software e Display on page 3 2 describes the LCD graphics display e Pushbuttons on page 3 3 describes the various front panel pushbuttons and the expected key actions for each e Softwar
225. uuae dwe7 o enuen Y Mou o giv ue sumes WwW0D u wn suj MOOIun jaon suods y Fo INSS ld smoj4 s6um s Puffoeeg pIOMSSEed SNOWY yooyuy su uU duet yousg ainssaid uo esu dwo said piomssed abueyd ISCH 10 9919q duet Ee sduat uolesuedwos duet s jnejeg e9 1SN jeseay Sebueu wojsnd 8S u wn suj MOO Huas due duet due o GITT dwnd ja09 O ebuey P1OMSSEd 18S yd9YUD NSS ld p 99 q SURV UuOISI9A WesBOld S A07 WOo sng Dag To oui Bay sun SED 01 U0 10 0e oul BEE SSES SR sonsoubelq EEN ten e E ebuey nual ulen ugoe UNY U9919S Lol H S U9919S dn 13MO0d Operation Software Overview Power Up Screen The Power Up screen is displayed on power up of the Model 49 Primary Standard The Self Test is displayed while the internal components are warming up and diagnostic checks are performed Thermo SCIENTIFIC iSeries Please wait while Ecot ing Run Screen The Run screen displays the Oz concentration The status bar displays sample cal solenoid valve or internal ozonator time and alarm status The word ZERO on the bottom left of the display indicates the calibrator is in zero mode Other modes appear in the same area of the display as LEVEL 1 LEVEL 2 LEVEL 3 LEVEL 4 and LEVEL 5 or blank to signify manual mode as shown below In manul mode use TI and to increase and decrease the O3 output concentration ree to scroll through manual zero or custom levels 3 6 Mode
226. w a alarm minimum value current setting Reports the sample flow b alarm maximum value current setting Reports the sample flow b alarm minimum value current setting Reports the current setting of the concentration 03 alarm trigger action minimum alarm Reports analog current output range per channel Retrieves analog voltage input data per channel Reports analog voltage output range per channel Reports sets averaging time Reports sets current baud rate Reports bench temperature Balances the output of both detectors Sets auto calibrates high range 0 coefficient Sets auto calibrates low range Q3 coefficient Sets auto calibrates 03 background Sets auto calibrates 03 coefficient Reports the current lamp intensity for cell a Reports the current lamp intensity for cell b Page B 14 B 14 B 14 B 14 B 15 B 15 B 15 B 15 B 16 B 16 B 16 B 16 B 16 B 40 B 40 B 41 B 8 B 37 B 9 B 27 B 25 B 25 B 25 B 25 B 17 B 17 Thermo Fisher Scientific Thermo Fisher Scientific Command clr records clr srecs contrast copy Irec to sp copy sp to Irec copy sp to srec copy sp to stream copy srec to sp copy stream to sp custom date default params dhcp diag volt iob diag volt mb diag volt mib dig in din do down dout dtoa en enter er erec erec format erec layout flags flow a flow b format C Link Protocol Commands Table B 1 C Link Protocol Commands continue
227. wer Monitor Ground Thermo Fisher Scientific Troubleshooting Connector Pin Descriptions Table 5 3 Motherboard Connector Pin Descriptions continued Connector Reference Pin Signal Label Designator Description FRONT PANEL J18 1 Ground BD 2 Ground 3 LCLK LCD Signal 4 Ground 5 Ground 6 LLP LCD Signal 7 LFLM LCD Signal 8 LD4 LCD Signal g LDO LCD Signal 10 LD5 LCD Signal 11 LD1 LCD Signal 12 LD6 LCD Signal E LD2 LCD Signal 14 LD7 LCD Signal 15 LD3 LCD Signal 16 LCD Bias Voltage p 5V 18 Ground 19 Ground 20 LCD_ONOFF LCD Signal 21 Keypad Row 2 Input 22 Keypad Row 1 Input 23 Keypad Row 4 Input 24 Keypad Row 3 Input 75 Keypad Col 2 Select 26 Keypad Col 1 Select 2 Keypad Col 4 Select 28 Keypad Col 3 Select 29 Ground 30 Ground 31 Ground 32 Ground Thermo Fisher Scientific Model 497 Primary Standard Instruction Manual 5 11 Troubleshooting Connector Pin Descriptions Table 5 3 Motherboard Connector Pin Descriptions continued Connector Label RS232 RS485 A RS232 RS485 B AC IN AC 24VPWR AC INTF BD 5 12 Model 497 Primary Standard Instruction Manual Reference Designator PLA PJ1 PJ2 PJ3 Pin 33 34 ch lU wo N gt OO OD N O ooo FP O N gt O WO N O o A WO N W N Signal Description 24V 24V NC Serial Port 1 RX RS485 IN Serial Port 1 TX RS485 OUT NC Ground NC Serial Port 1 RTS RS485 OUT Serial Po
228. y Standard Instruction Manual Thermo Fisher Scientific Ozonator Assembly Ozonator Lamp Power Supply Photometer Lamp power Supply Optical Bench Temperature Thermistor Pump Sample Reference Solenoid Valves Thermo Fisher Scientific Software System Description Software The internal ozonator operates on the photolytic principle The ozone level produced is a function of light intensity at 185 nm and gas flow The light intensity is varied by changing the current into the lamp The gas flow is held constant by a pressure regulator followed by a capillary The ozonator lamp power supply generates high voltage AC and contains heater control circuits for the ozonator lamp The photometer lamp power supply generates high voltage AC and contains heater control circuits for the photometer lamp The optical bench temperature thermistor is used for maintaining the optical bench at a constant temperature The pump draws the zero air through the optical bench Note Total flows of less than 1 LPM 2 scfh should be avoided since the flush time would be excessive Total flows of greater than 3 LPM should also be avoided since there would not be enough residence time in the converter to ensure greater than 99 conversion of the ozone a The sample reference solenoid valves allow sample gas to pass through Cell A and reference gas through Cell B or vise versa depending upon which cycle the instrument is performing The proce

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