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UNITYplus Installation Planning

1. 7 Figure 3 Magnet leg antivibration systems leg placement and sizes 7 Figure 4 Typical radial distances at which 5 gauss levels exist 10 Figure 5 Typical vertical stray fields for 400 54 500 51 600 51 and 750 51 magnets 12 Figure 6 Internal wiring of gradient cabinet sess 19 Figure 7 Stray field plots for 200 54 and 200 89 magnets sss 42 Figure 8 Stray field plots for 300 54 and 300 89 magnets ss 43 Figure 9 Stray field plots for 400 54 and 400 89 magnets ss 45 Figure 10 Stray field plots for the 500 51 magnet sese 46 Figure 11 Stray field plots for 600 51 magnets esee 47 Figure 12 Stray field plots for 750 51 magnets sse 49 Figure 13 10 gauss warning sign Pub No 87 250302 00 csse 51 Figure 14 5 gauss warning sign Pub No 87 250303 00 eeeeseeeeeteeeee 51 Figure 15 Magnet area danger sign Pub No 87 250301 00 n 52 UNITYplus Installation Planning Guide 87 195320 00 G0994 List of Tables Table 1 Cabinets dimensions and weights essere 2 Table 2 Magnet dimensions and weights essere 3 Table 3 System accessories dimensions and weights esses 4 Table 4 Ceiling minimum height ses
2. n 29 Monitor Degaussing Coil Recommended sess 29 Computer Preparation nennen entente nennen nnnesen 30 Magnetic Field Considerations for Computers and Peripherals 30 SUN COMPULSTS 2 5 PD 30 SuirPeripher ls ie rr e e rg pae ilo 31 SUNOS Media allocare 31 SunOS Installation e D TOT Re Eee 31 Sun Documentation rne deer ee teer te reete ideata 32 Computer Preparation Checklist ui 32 Configuration and Peripherals i 33 Collecting System and Network Information sese 33 System Configuration Type i 33 Selec ng a Hostiam esie Maiella tbe lait 33 Obtaining the IP Address ire 34 Selecting a Subnet Mask ii 34 Selecting the Name Service Type i 34 Entering the Hostname and IP Address of the Name Server 34 Doman Name eet rete lierna 34 Setting the Time Zone ione treten ceti db erred 34 Disk L yout nenion a e e i er e nee 34 Pre Installation Worksheet essent 35 Receiving Preparations sse eee eene 36 Postdelivery Instructions i 37 Inspecting for Shipping Damage eese 37 Moving the Systema ote de etie ei di v d eredi rn 37 Appendix A Installation Checklists 39 PredehVety 5 es
3. 13 Ambient Temperature and Humidity i 16 Ventilation cirie ii lia le OD eo etes tie 17 Maximutn Altt de 1 liane iaia 17 Installation Site Preparation eene 18 Line Voltage Variations idu tete o P a ete 18 Uninterrupted Power Supply UPS sess 18 Electrical Outlets eiecti rete Re Ra dee in 18 Separate Air Sources for System Options esser 20 Compressed Air Supply rri re er re Ia te eere nte 21 AC Power and Air Conditioning iii 22 Compressed Nitrogen Gas enne eere 23 Telephones iege Ep ier t Pre CU ee p lille te 23 Electrostatic Dischargest i i oce Hr eret ola 23 Installation Supplies and Equipment i 24 Liquid Helium Supply s ieri aaa rat 25 Liquid Nitrogen Supply 5 ilaria 26 Helium Gas Supply ill ete e tette 27 Nitrogen Gas Supply for Magnet Installation see 27 Face Mask and Thermal Gloves sess 28 Heat G n sila reti te rt eite vli P Pet rara ile 28 Nonterromagnetic Ladder te er er teat 28 Horst ere rhet Pe P erige tren P RD Cadre dara 28 Isopropyl Alcohol and Acetone Systems with an Oxford Magnet 28 Cryogenic Equipment Rack Recommended sess 28 87 195320 00 G0994 UNITYplus Installation Planning Guide iii Electrical Power Surge Protector Recommended
4. Postdelivery Instructions on page 37 for further instructions and safety precautions Ji 2 Upon delivery check for shipping damage but do not open any shipping crates except with direct instructions from an authorized service representative Examine crates for shipping damage Note any apparent damage on the carrier s waybill and contact the insurance company As soon as possible move the shipment to a clean dry location preferably the installation site Move the crates in an upright position Do not drop or mishandle The crates are packed with G force and tip and tell indicators that record mishandling If one or more crates cannot be moved into the installation site because of doorway clearance leave the affected crate in a clean safe dry location Again do not open any crate except with direct instructions from an authorized service representative In particular the crate containing the magnet has components that could be irreparably damaged if opened incorrectly Contact Varian to schedule the visit of an installation engineer after the shipment is moved to the installation site the utilities are installed and non Varian installation parts and supplies listed in the Installation Supplies and Equipment section are received For installations in the United States telephone the Installation Department at 415 424 6361 For installations in other locations contact the nearest Varian sales or service off
5. on page 63 lists peripherals that can be used with Varian UNITYplus NMR spectrometers These devices fall into a number of compatibility categories ranging from fully tested to unknown which are described in Appendix E Most of the products in the fully tested category are available from Varian This information is provided solely as a courtesy to those users who wish to purchase their own peripherals or who may already have these items Products in other categories are not sold by Varian and Varian assumes no responsibility for their purchase or use but provides this information solely for your discretionary use Collecting System and Network Information The Solaris installation program asks you to supply some system and network information before installation begins You can save time by collecting this information now before booting from the Solaris 2 3 CD ROM Use the Pre Installation Worksheet on page 35 to record your system information Each field on the worksheet is described below If your system is not connected to a network you need to know or create only the hostname root password and the time zone If your system is on a network you need additional information that is described in this section If unsure contact your network administrator System Configuration Type You are asked to configure your computer as one of the following server standalone or dataless client A server is a system that
6. 0 2 H field 0 25 E field 0 25 H field 0 25 E field 0 25 H field 0 005 E field 0 05 H field 0 1 E field 0 1 H field 0 E field 0 H field 0 E field 0 H field 0 E field 0 H field 0 05 E field 0 05 H field 0 E field 0 01 H field 0 05 E field 0 02 H field 0 05 E field 0 05 H field 0 05 E field 0 05 H field 0 E field 0 005 H field 0 E field 0 H field 1 0 E field 1 0 H field 1 0 E field 1 0 H field 2 0 E field 2 0 H field 2 0 E field 2 0 H field 1 0 E field 1 0 H field 1 0 E field 1 0 H field 1 7 E field 1 7 H field 1 7 E field 1 7 H field 1 0 E field 1 8 H field 1 0 E field 1 0 H field 100 watts 20 ms pulse 14 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements Table 9 IEEE ANSI C95 1 1991 standard for RF radiation levels Frequency MHz E Field mW cm H Field mW cm 50 1 0 4 0 75 1 0 1 8 125 1 0 1 0 150 1 0 1 0 200 1 0 1 0 300 1 0 1 0 500 1 7 1 7 600 2 0 2 0 750 2 5 2 5 87 195320 00 G0994 UNITYplus Installation Planning Guide 15 Installation Site Requirements Ambient Temperature and Humidity Table 10 lists the required ambient temperature ranges temperature stability and humidity levels for the site For optimal performance the ambient temperature around the magnet should not vary Magnet homogeneity is optimized if the ambient temperature stability is maintained for the duration of an experiment and b
7. System Cable Lengths and Room Layouts Cable Lengths for Systems With Ultraenmr Shims m rd Interface box HIM l Magnet Host Computer Standard Cabinet Shim 24m Power 8 ft Supply 1 8 m 6 ft 5 2 m 17 ft 1 5 m 5 ft Power Source The Ultraenmr Shims system consists of three components Shim tube equipped with a heavily shielded 7 m 20 ft cable Shim power supply Interface HIM box equipped with a shielded 3 m 10 ft cable The illustration above details the cable length requirements for the Ultra nmr Shims system The requirements can be expressed in terms of the following configurational constraints The shim power supply contains a floppy disk and must therefore be at least outside the 5 gauss line of the magnet The typical placement of the shim power supply is at the end of the console farthest from the magnet In general the shim power supply should be closest to the rf cabinet since the cable carrying the analog ZO signal and the homospoil TTL control line comes from the bottom of rf cabinet and must be connected to the back of the shim power supply The usable length of this cable Part No 00 968378 00 is 1 8 m 6 ft and therefore limits the distance that the shim power supply can be from the rf cabinet The distance from the shim power supply to a source of power should be within 1
8. 5 m 5 ft since the length of the power cord on the shim power supply is 1 5 m 5 ft The distance between the shim power supply and the shim tube which is installed in the magnet bore must be less than or equal to 5 2 m 17 ft The interface box must be within 2 4 m 8 ft of the shim power supply and should be situated next to the Sun host computer to facilitate interactive shimming and locking 56 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix D System Cable Lengths and Room Layouts Minimum Space for 200 54 or 300 54 System Without Options 220 Vac 20 A Outlet Paes 200 300 O E Cabinet Outlet Magnet 120 Vac Outlet iB c E Room dimensions are about 3 6 m x 3 3 m 12 ft x 10 7 ft The standard cabinet is 111 cm x 78 cm 44 in x 31 in Typical table size is 183 cm x 76 cm 72 in x 30 in The magnet is 69 cm x 69 cm 27 in x 27 in A distance of 1 7 m 5 3 4 ft should be maintained around the magnet to prevent interference with electronic components A distance of 1 m 3 ft should be maintained around the standard cabinet If space permits the alternate arrangements shown in subsequent layouts in this appendix are recommended Not drawn to scale 87 195320 00 G0994 UNITYlus Installation Planning Guide 57 Appendix D System Cable Lengths and Room Layouts Standard Layout for 200 54 or 300 54 System Without Options 120 Vac Outlets 220 Vac 20A Standard Outlet Cabin
9. B 200 06 299 96 399 94 499 95 599 95 749 94 19E 188 22 282 20 376 29 470 39 564 45 705 56 3p 80 98 121 42 161 90 202 39 242 85 303 56 Hc 50 31 75 43 100 58 125 73 150 87 188 59 Ee 39 75 59 59 79 46 99 33 119 20 148 98 H 30 71 46 04 61 40 76 15 92 09 115 11 I5N 20 28 30 41 40 54 50 68 60 80 76 03 REC 14 00 18 66 23 33 28 00 35 00 87 195320 00 G0994 UNITYplus Installation Planning Guide 13 Installation Site Requirements The results of the tests shown in Table 8 found that rf emissions from Varian NMR equipment were not detectable or at levels far below the IEEE ANSI C95 1 1991 Standard levels which are shown in Table 9 Table 8 Results of rf emissions tests on Varian NMR equipment NMR Experiment Frequency RF at Probe MHz mW cm RF at Amplifier IEEE ANSI mW cm C95 1 1991 UNITY plus 600 Carbon observe tpwr 58 pulse Carbon observe tpwr 63 pulse 50 ohm load Proton observe tpwr 63 pulse Proton observe tpwr 63 pulse 50 ohm load UNITYplus 500 Carbon observe tpwr 63 dpwr 63 pulse terminated Carbon observe tpwr 63 pulse 50 ohm load Proton observe tpwr 63 pulse Proton observe tpwr 63 pulse 50 ohm load UNITYplus 300 Cross polarization 300 watts 2 ms pulse Cross polarization 150 150 600 600 125 125 500 500 75 300 0 E field 0 H field 0 E field 0 H field 0 E field 0 H field 0 E field 0 H field 0 E field 0 05 H field 0 01 E field
10. Client Standalone Hostname Example mysystem IP Address Example 195 5 2 15 Subnet Mask Example 255 255 255 0 Name Service Choices NIS NIS or none Name Server Hostname Example ourserver Name Server IP Address Example 195 5 2 25 Domain Name Example ourdomain Time Zone Examples US Mountain US Pacific US Eastern Disk Layout Examples c0t0d0s0 swap c0t0d0s1 usr c0t0d0s6 Use the default proposed by the installation program 87 195320 00 G0994 UNITY plus Installation Planning Guide 35 Receiving Preparations Receiving Preparations The method of shipping and the current conditions at the destination determine the extent of the receiving preparations The Varian Order Acknowledgment form indicates the shipping method for the order The following service is usually provided Air Freight System is delivered to unloading dock or other easily accessible outside unloading point Factory to destination transit time is about two days not including time to clear customs Motor or Moving Van System is delivered to an easily accessible interior location or any interior location to which freight can be easily transported by movable dolly Excluded is transport in elevators that cannot support the weight of the shipment or up stairways Factory to destination within the United States is about eight days Confirm that the local shipping company uses a vehicle that
11. Contact an electronic professional for advice on quality surge protection in your area Monitor Degaussing Coil Recommended The display monitor can gradually become somewhat magnetized due to its proximity to the magnet This condition can be corrected with a degaussing coil If the host computer system will be located near the edge of the 1 2 gauss stray field of the magnet it will be necessary to have the degaussing coil 87 195320 00 G0994 UNITYplus Installation Planning Guide 29 Computer Preparation Computer Preparation Varian UNITYplus spectrometers are operated using a Sun Microsystems computer which may have been purchased from Varian or separately In either case certain preparations are required Some of these preparations have been outlined previously in the section Electrical Outlets The following sections contain additional considerations Magnetic Field Considerations for Computers and Peripherals The spectrometer host computer system and storage media in other words streaming magnetic tape cartridge must be located at a sufficient distance from the magnet that the magnetic field cannot damage the data For a Sun workstation this specification is less than 5 gauss The distances at which this gauss level is present are different for each kind of magnet and must be taken into account when planning the room size See the field plots in Appendix B on page 41 for typical distances at which various gauss levels exi
12. G force indicator 37 39 gradient power cabinet 19 graphics boards 31 grounding 23 GX graphics 31 hard disk default layout 34 hard disk drives 31 heat gun 28 helium gas supply 27 helium supplies 1 high altitudes 16 hoist 28 host computer 30 host computer and magnetic fields 30 hostname 33 humidity level 16 imaging module 22 installation department 39 installation equipment 24 installation site preparation 18 installation site requirements 2 installation supplies 24 internal hard disk drive 31 Internet Protocol network address 34 IP address 34 isopropl alcohol 28 laboratory size 4 ladder 28 lifting equipment 2 line conditioner 18 line voltage variation 18 liquid helium supply 25 liquid nitrogen supply 26 magnet crate 37 39 magnet field homogeneity 8 magnet transport 36 magnetic field considerations for computers 30 magnetic field exposure 11 magnetic field warning signs 50 magnetic interference 4 8 man command 32 memory size 31 microimaging module 19 21 modem connection 23 monitor degaussing coil 29 moving crates 1 39 moving equipment 36 UNITYlus Installation Planning Guide 67 Index moving the system 37 moving van delivery 36 name service 34 NFS server 33 NIS or NIS server 34 nitrogen gas 23 nitrogen gas supply 27 nitrogen supplies 1 Object Code License Form 39 oil filter 21 on line documentation 32 opening cr
13. Location Sample Changer 120 Vac Outlets o E e a x E a MOY Service Access The room dimensions are about 5 2 m x 6 7 m 17 ft x 22 ft The standard cabinet is 111 cm x 78 cm 44 in x 31 in The imaging and high power solids cabinets are 55 cm x 78 cm 22 in x 31 in each Typical table size is 183 cm x 76 cm 72 in x 30 in The magnet is 80 cm 32 in in diameter The sample changer is about 64 cm x 69 cm 25 in x 35 in A distance of 3 m 10 ft should be maintained around the magnet to prevent interference with electronic components A distance of 1 m 3 ft should be maintained around the cabinets Service requirements for the imagining and solids outlets are described in the Installation Site Preparation section Not drawn to scale 87 195320 00 G0994 UNITY plus Installation Planning Guide 61 Appendix D System Cable Lengths and Room Layouts Typical Layout for 600 51 System Es 7 220 Vac 20A Outlet b Service N f Space q 3 f f 600 MHz f y Magnet 1 1 i Typical 5 Gauss Horizontal Zone Typical 10 Gauss Horizontal Zone Room dimensions are about 6 1 m x 6 1 m 20 ft x 20 ft The standard cabinet is 111 cm x 78 cm 44 in x 31 in Typical table size is 183 cm x 76 cm 72 in x 30 in The magnet is 97 8 cm 38 5 in in diameter A minimum of 3 m 10 ft should be maintained around the magnet to prevent interferen
14. as a ceiling value Radio Frequency Environment The site should be checked for radio frequency interference rfi at or near the operating frequencies of the spectrometer and most common nuclei listed in Table 7 The level of any interference should be attenuated to an electrical field strength of less than 150 uV m at the site of the magnet Interference is not uncommon when two spectrometers are located in the same room referenced to the same power system or operating at the same frequency Radio Frequency Emissions from Varian NMR Equipment RF emissions from Varian NMR equipment has been measured and compared with the IEEE ANSI C95 1 1991 Standard for Safety Levels with Respect to Human Exposure to RF Radiation The rf tests included general measurements of systems with particular interest directed toward amplifiers transmitter boards and probes With maximum power applied tpwr 63 and dpwr 63 measurements were taken both one foot away and as close as possible to the rf source while the source was installed in the console or magnet Table 7 Spectrometer and nuclei operating frequencies Spectrometer frequency ranges in MHz Proton Frequency Frequency Ranges 200 12 to 309 5 300 12 to 309 5 400 12 to 489 5 500 12 to 609 5 600 12 to 609 5 750 12 to 989 5 Operating frequency in MHz for most common nuclei 200 MHz 300MHz 400 MHz 500 MHz 600 MHz 750 MHz Mule System System System System System System
15. damaged An overly dry atmosphere also tends to create an electrostatic charge As with any system based on integrated circuits the system is susceptible to static spikes both those generated on the power line and those generated in the lab area that must be suppressed 87 195320 00 G0994 UNITYplus Installation Planning Guide 23 Installation Supplies and Equipment Installation Supplies and Equipment The installation engineer will need the following non Varian supplies and equipment during installation Liquid helium supply Liquid nitrogen supply Helium gas supply Nitrogen gas supply Face mask and thermal gloves Heat gun Nonferromagnetic ladder Hoist systems with a Oxford magnet Isopropyl alcohol and acetone systems with a Oxford magnet In addition the following items are recommended Cryogenic equipment rack Electrical power surge protector Monitor degaussing coil Manuals reference rack Details about each item are presented in the following sections Locating a reliable local source of liquid helium and nitrogen is particularly important As soon as possible after ordering a system make arrangements for an initial delivery and an on going supply of liquid helium and nitrogen 24 UNIT Yplus Installation Planning Guide 87 195320 00 G0994 Installation Supplies and Equipment Liquid Helium Supply To prevent unnecessary loss of the supply request delivery just prior to the schedul
16. dispatch 415 856 6139 fax technical support International Asia Southeast Varian Pacific Inc Hong Kong Tel 3 724 2836 Australia Varian Pty Ltd Mount Waverley Victoria Tel 3 543 8022 Austria Varian Ges M B H Voesendorf Bei Wien Tel 1 69 55 45 Belgium NV Varian Benelux S A Zaventem Tel 2 721 4850 Canada Varian NMR Instruments Mississauga Ontario Tel 905 819 8181 China Varian China Ltd Beijing Tel 1 256 5634 France Varian S A Orsay Tel 16 986 3838 Germany Varian GmbH Darmstadt Tel 6151 7030 Italy Varian SpA Segrate Milano Tel 2 753 1651 66 UNITYplus Installation Planning Guide North American Service Varian NMR Instruments 6440 Dobbin Rd Suite D Columbia MD 21045 410 964 3065 site planning assistance 410 964 3080 fax Japan Varian Instruments Ltd Tokyo Tel 3 204 1211 Korea Varian Korea Ltd Ansan City Kyunggi Do Tel 2 561 1624 7 Latin America North Varian S A Mexico D F Tel 5 514 9862 Latin America South Varian Industria E Comercio SP Brazil Tel 11 533 0444 Netherlands Varian Benelux B V Amsterdam Holland Tel 20 10 47 05 Sweden Varian AB Solna Stockholm Tel 8 82 00 30 Switzerland Varian AG Zug Tel 42 44 88 44 United Kingdom Varian Associates Ltd Surrey England Tel 932 24 37 41 Other International Varian Associates Inc Sunnyvale CA Tel 408 734 5
17. existing computer the server s name can be displayed by entering the command ypwhich The server s IP address and other information can be displayed by entering the command ypcat hosts grep ypwhich Again note the use of back quotes Domain Name The domain name is the name assigned to a group of computers that are administered together All computers in the group domain are accessed by the same NIS or NIS maps Your network administrator should be able to provide the domain name Or the domain name can be found by entering the command domainname Setting the Time Zone Solaris software uses world time zones and automatically adjusts the system clock for daylight savings time if appropriate Time zones are specified by name such as US Central Disk Layout Your computer must contain at least one hard disk drive If only one disk drive is installed use the default layout provided by the software If more than one drive is installed accept the default layout or select the drive to receive the software during the installation process See the Software Installation Manual 34 UNITYplus Installation Planning Guide 87 195320 00 G0994 Pre Installation Worksheet Computer Preparation Write down your system and network information here in preparation for the questions that are asked during the installation process Category Your Configuration System Configuration Type Choices Server Standalone or Dataless
18. firmly secured to avoid movement caused by magnetic field attraction Provide a flowmeter that measures 280 to 1400 liter hr 10 to 50 ft3 hr and a hose barb that fits 5 mm 3 16 in ID Tygon tubing Nitrogen Gas Supply for Magnet Installation During installation one cylinder of nitrogen gas is required for precooling the magnet and for transfer of liquid nitrogen A magnetic nitrogen gas container can be used provided the unit remains outside the 5 gauss limit of the magnet and the cylinder is firmly secured to prevent attraction to the magnet If the system is equipped with the variable temperature accessory a nitrogen gas supply is required If a fixed source is not available obtain a nitrogen gas cylinder with pressure regulator The gas must be dry and chemically pure with a flow rate through the pressure of 19 LPM 40 SCFH at 207 kPa 30 psig For low temperature operation use prepurified grade gas 99 99 85 C dew point CAUTION To avoid movement caused by magnetic field attraction helium gas and nitrogen gas cylinders made of magnetic material must be kept outside the 5 gauss limit of the magnet and firmly secured Table 17 Helium gas supply Magnet field Helium gas MHz cylinders 200 54 200 54 LH235 200 54 LH365 200 89 300 54 300 54 LH235 300 54 LH365 300 89 400 54 400 54 LH365 400 89 500 51 600 51 750 51 MWnn ne vd NNN NYY VY WN 87 195320 00 G0994 UNITYplus Installation Planning Guid
19. ft Table 11 Liquid helium displacement for room ventilation considerations Magnet Bore LHe Maximum MHz mm Volume liters 750 51 440 600 51 138 500 51 68 400 89 81 400 54 LH365 74 400 54 74 300 89 65 300 54 LH365 74 300 54 LH235 74 300 54 30 200 89 65 200 54 LH365 74 200 54 LH235 74 200 54 30 87 195320 00 G0994 UNITYplus Installation Planning Guide 17 Installation Site Preparation Installation Site Preparation Verify the configuration with a Varian representative before designing the room layout Site preparation must conform with federal state and local codes which take precedence over recommendations in this guide Approval by a building inspector may be necessary Line Voltage Variation UNITYplus spectrometers require one line tap at 220 Vac single phase Measure and record the ac line voltage for 48 hours using a suitable power line analyzer such as the BMI Model 4800 or equivalent Provide a copy for the Varian installation engineer Requirements are the following Long term voltage variations slow average do not exceed 7 of nominal line tap voltages Short term voltage variations sag or surge with a duration between several milliseconds and several seconds do not exceed 10 of nominal line tap voltage Line transients impulse with a duration between 1 us and 800 us not to exceed 50 V peak above or below nominal line tap voltage These transients must be measured at the power pl
20. in the air supply is a problem you should consider installing a prefilter with an automatic drain to help prevent overload of the filter In extreme cases an air dryer assembly may be necessary The source should include a reservoir and be capable of delivering the air pressures in kilopascals or pounds per square inch gauge and flow rates in liters per minute or standard cubic feet per hour after filtering as given in Table 13 The installation engineer will install on your air termination fitting a Varian supplied assembly that includes a 0 to 400 kPa 0 to 60 psi pressure gauge a reduction valve a standard 20 micron air filter a coalescing oil filter 99 9 percent oil removal efficiency and an air line to the magnet Table 13 Compressed air supply source System Configuration Pressure Flow Rate 200 300 or 400 system with liquids only no options air source needed for spin probe cooling VT and eject Normal operation 240 kPa 35 psig 27 LPM 57 SCFH During sample eject 240 kPa 35 psig 45 LPM 95 SCFH 500 or 600 system with liquids only no options air source needed for spin probe shim cooling VT and eject Normal operation 310 kPa 45 psig 27 LPM 57 SCFH During sample eject 310 kPa 45 psig 48 LPM 102 SCFH System with wideline module Same as above System with third fourth rf channel Same as above System with CP MAS or CRAMPS 620 kPa 90 psig 80 LPM 170 SCFH System with Doty probe 414 kPa
21. interference with electronic components distance of 1 m 3 ft should be maintained around the cabinets Service requirements for the third rf imaging and solids outlets are described in the Installation Site Preparation section Not drawn to scale 87 195320 00 G0994 UNITYlus Installation Planning Guide 59 Appendix D System Cable Lengths and Room Layouts Recommended for 400 54 or Any 89 mm System Without Options 120 Vac Outlets Disk Drives Table Standard 220 Vac Cabinet 20A Outlet Magnet Front Widebore Magnet 120 Vac 20 A Outlet X Service Access TAA The room dimensions are about 4 4 m x 4 6 m 14 5 ft x 15 2 ft The standard cabinet is 111 cm x 78 cm 44 in x 31 in Typical table size is 183 cm x 76 cm 72 in x 30 in The magnet is 80 cm 32 in in diameter A minimum of 3 m 10 ft should be maintained around the magnet to prevent interference with electronic components A distance of 1 m 3 ft should be maintained around the standard cabinet Not drawn to scale 60 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix D System Cable Lengths and Room Layouts Recommended for 400 54 500 51 or Any 89 mm System With Options Imaging Outlet 220 Vac 30 A 3rd RF Solids 3 Phase Outlet Outlet Outlet 120 Vac 20 A Outlet Imaging Cable to Magnet Approx Location Standard 120 Vac Cabinet i 20A Outlet Widebore Magnet Sample Changer Alternate
22. mT equivalent to 600 gauss whole body or 600 mT 6000 gauss to the extremities Table 6 Stray field data for Oxford and Varian magnets Magnet Type Radial Distance cm Axial Distance cm Hom GE UG Die LOGE e io Moner Quiside CL cm to CL cm 750 51 115 50 32 155 76 53 54 6 0 5 58 4 600 51 70 a a 96 48 35 44 0 45 9 500 51 57 a a 79 41 b 39 1 36 2 400 89 56 a a 81 42 b 38 5 362 400 54 39 a a 59 b b 332 362 300 89 40 a a 59 b b 35 7 362 200 89 a a a 56 b b 35 1 362 300 54 a a 38 b b 23 9 28 0 200 54 a a a 33 b b 23 9 28 0 a Where no radial position is given the point is within the cryostat body b The axial point is in the cryostat bore Compare with the magnet center line CL distance c To be determined 87 195320 00 G0994 UNITYlus Installation Planning Guide 11 Installation Site Requirements 2 80 m 400 lt Typical 5 gauss 3 45 m 500 vertical zone 4 55 m 600 7 60 m 750 Typical 10 gauss 2 24 m 400 vertical zone 2 70 m 500 3 60 m 600 6 04 m 750 Centerline to floor 400 54 1 16m 500 51 1 24m 600 51 1 35 m 750 51 1 38m Magnet room floor Figure 5 Typical vertical stray fields for 400 54 500 51 600 51 and 750 51 magnets 12 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements on a daily 8 hour time weighted average basis A flux density of 2 teslas 20 000 gauss is recommended
23. of the standard power stick for running up the magnet field If one of the larger capacity liquid helium storage dewars is used with the magnet however additional ceiling clearance may be necessary In general the ceiling height must be at least twice the height of liquid helium storage dewar above the floor Oxford magnets can be provided with optional hinged top loading components that reduces the minimum ceiling height requirements Contact Oxford for details Most of the antivibration vibration isolation systems add nothing to the ceiling height requirements with the exception of the 200 54 and 300 54 magnets when placed on an antivibration table system For these cases add 20 cm 8 in to the ceiling height requirements Table 4 Ceiling minimum height Magnet Bore Ceiling Minimum With Optional Helium MHz mm cm in Level Sensor cm in 200 54 252 99 Not applicable 200 54 LH235 321 126 5 365 cm 144 in 200 54 LH365 321 126 5 365 cm 144 in 200 89 311 122 5 355 cm 140 in 300 54 252 99 Not applicable 300 54 LH235 321 126 5 365 cm 144 in 300 54 LH365 321 126 5 365 cm 144 in 300 89 311 122 5 355 cm 140 in 400 54 321 126 5 365 cm 144 in 400 54 LH365 321 126 5 365 cm 144 in 400 89 321 126 5 344 cm 135 5 in 500 51 311 122 5 345 cm 136 in 600 51 334 131 2 Includes flexible helium level probe 750 51 400 157 5 87 195320 00 G0994 UNITYplus Installation Planning Guide 5 Instal
24. to the floor The antivibration system used with these magnets incorporates the dampening mechanism as an integral part of the magnet leg Although in normal operation these antivibration legs are stable for added safety Varian requires that they be anchored to the floor after installation Anchoring to a floor is a standard procedure for many types of equipment and Varian expects that the customer s plant maintenance personnel can usually accomplish it The anchoring requires four 2 5 inch embedments for each leg 36 x 36 Platform 3 leg pads 6 x 6 Figure 2 Platform antivibration system leg placements and sizes A B C 3 leg pads on floor 11 x 15 3 leg pads on floor 4 leg pads on floor R 19 72 9 x 11 9 x 11 a ba R 24 94 2d br ond Pa R 21 125 E a 4 f v Magnets Il Magnet 200 89 300 89 Magnet 750 51 400 54 400 89 600 51 i eS 500 51 and 27 PRX E 4 gt N P DI lt Sace N N ig _ Figure 3 Magnet leg antivibration systems leg placement and sizes 87 195320 00 G0994 UNITYplus Installation Planning Guide 7 Installation Site Requirements anchored using 0 5 inch bolts Details are provided in the Antivibration System Installation Manual this note is provided for information purposes only Floor Vibration Requirements The floor mustbe sufficiently rigid to reduce the vibration from adjacent dynamic loads to a negligible level defined as no single p
25. under its patent rights nor the rights of others Inclusion in this document does not imply that any particular feature is standard on the instrument UNITYplus and ASM 100 are trademarks of Varian Associates Inc Sun and the Sun logo are trademarks of Sun Microsystems Inc SPARC and SPARCstation are trademarks of SPARC International Tygon is a trademark of DuPont Company Ethernet is a trademark of Xerox Corporation Oxford is a registered trademark of Oxford Instruments Ltd Other product names are trademarks or registered trademarks of their respective holders Table of Contents Introduction caos atta ni ao I 1 Safety Precautions 3 3 0 0 asic ern ee engen lin ede ge e Heels 1 Installation Site Requirements nne 2 Acce ssibility of Site intet tete d tete AIR E 2 SES VA ante ita qe pae rie 4 Ceiling Height Requirements i 5 Structural Strength of Floor 6 Magnet Weight Distribution No Antivibration System 6 Magnet Weight Distribution With Antivibration System 6 Antivibration Bolt Down Requirement sees 7 Floor Vibration Requirements nentes 8 Magnetic Enyironment oerte ern neret re ei ses sabaveesdenas 8 Safety Hazards of Strong Magnetic Fields eeeeeneeeeeeeeeeeeeeeeees 10 Radio Frequency Environment i 13 Radio Frequency Emissions from Varian NMR Equipment
26. 00 Ib such as pushcarts hand trucks gas cylinders Presence or movement of ferromagnetic objects over 450 kg 1000 Ib such as small delivery trucks automobiles pallet movers forklifts elevators Presence or movement of ferromagnetic objects over 34 000 kg 75 000 Ib such as trains large trucks Objects affected by the magnetic field 15 gauss line or closer 5 to 15 gauss 2 to 5 gauss 1 to 2 gauss Cardiac pacemakers ferromagnetic implants unrestrained ferromagnetic objects such as tools keys elec tronic equipment analog watches magnetic data storage media credit cards Cardiac pacemakers electronic equipment such as shielded CRTs computers shielded image intensifiers shielded pho tomultiplier tubes Very sensitive electronic equipment such as unshielded im age intensifiers photomultiplier tubes Extremely sensitive electronic equipment such as linear ac celerators electron microscopes CRTs 87 195320 00 G0994 UNITYplus Installation Planning Guide Installation Site Requirements Safety Hazards of Strong Magnetic Fields The potential safety hazards of strong magnetic fields to devices such as certain pacemakers must be understood and planned for A set of plots indicating the magnitude of the stray fields for each type of magnet is included in Appendix B on page 41 These plots show typical levels of stray field Actual levels may vary and should be checked after a particular magnet h
27. 10 Ib from crate to crate Long hold magnets are designated by LH and a number that represents hold time in days 87 195320 00 G0994 UNITYplus Installation Planning Guide 3 Installation Site Requirements If it is not possible to gain access to the installation site unless the system is uncrated contact a Varian service representative for further instructions Do not uncrate the system except with direct instructions from an authorized service representative Site Size The site must be large enough to allow free access to all sides of the system and magnet for operation maintenance and cryogenic service Table 1 Table 2 and Table 3 list the dimensions of the system components and Appendix D System Cable Lengths and Room Layouts on page 54 contains floor plans for the NMR laboratory area or room The plans are suggestions and not specifications AII cabinets have casters for easy movement which allows the system to be placed in a location as small as that illustrated in the section Minimum Space for 200 51 or 300 51 System Without Options in Appendix D on page 54 as long as sufficient space exists for the cabinets to be moved to provide for access to all sides For comfort and convenience however and to provide space for an automatic sample changer or other options the larger layouts shown in Appendix D on page 54 are highly recommended The minimum dimensions do not include compensation for external magnetic an
28. 370 87 195320 00 G0994 accessibility of site 2 acetone 28 air conditioning 16 22 air freight delivery 36 air source 21 air ventilation 17 altitude 17 ambient temperature 16 ambient temperature ranges 16 antistatic spray 23 ASM 100 sample changer 20 boiloff 25 building inspector 18 cable lengths 54 55 56 cardiac pacemaker wearers 8 carpeting 23 cautions defined 1 CD ROM unit 31 ceiling height 5 centerline to floor distance 12 codes 18 color CRTs 8 compatibility of peripherals 63 compressed air supply 21 computer preparation 30 configuring peripherals 33 CP MAS option 20 22 CP MAS options 19 CRAMPS option 20 CRAMPS multipulse module 22 crate unpacking 37 cryogenic equipment rack 28 dataless client 33 daylight savings time 34 degaussing coil 29 delivery of supplies 2 delivery responsibility 1 delivery services 36 Desktop SPARC manual set 32 dewars 25 differential amplifier box 54 55 56 distance centerline to floor 12 documentation 32 domain name 34 domainname command 34 Doty probe 21 electrical grounds 19 electrical outlets 18 electrical power surge protector 29 electrostatic discharge 23 equipment rack 28 external hard disk drive 31 face mask 28 87 195320 00 G0994 Index floor coverings 23 floor structure strength 6 floor vibration 8 flowmeter 27 flutter tube 28 FOB block 37 gate valve 21 gauss levels 41
29. 4 Appendix B Stray Field Plots 600 51 magnet field values in gauss Axial distance from magnet CL m 0 5 1 0 1 5 2 0 2 5 3 0 3 5 Radial distance from magnet CL m Figure 11 Stray field plots for 600 51 magnets 87 195320 00 G0994 UNITYplus Installation Planning Guide 47 Appendix B Stray Field Plots 48 UNITYplus Installation Planning Guide 87 195320 00 G0994 Axial distance from magnet CL m Appendix B Stray Field Plots 0 5 1 0 1 5 2 0 2 5 3 0 3 5 4 0 Radial distance from magnet CL m Figure 12 Stray field plots for 750 51 magnets 4 5 5 0 750 51 magnet field values in gauss 5 5 6 0 87 195320 00 G0994 UNITYlus Installation Planning Guide 49 Appendix C Posting Requirements for Magnetic Field Warning Signs Appendix C Posting Requirements for Magnetic Field Warning Signs 50 The strong magnetic fields that surround a superconducting magnet are capable of causing death or serious injury to individuals with implanted or attached medical devices such as pacemakers or prosthetic parts Such fields can also suddenly pull nearby magnetic tools equipment or dewars into the magnet body with considerable force which could cause personal injury or serious damage Moreover strong magnetic fields can erase magnetic media such as tapes and floppy disks disable the information stored on the magnetic strip of automated teller machine ATM and credit cards and damage some watches To warn of the pre
30. 5 468 1030 300 89 200 80 95 37 25 95 37 25 416 916 400 54 200 80 95 37 25 95 37 25 468 1030 400 54 LH365 200 80 95 37 25 95 37 25 468 1030 400 89 200 80 95 37 25 95 37 25 571 1256 500 51 200 80 95 37 25 95 37 25 571 1256 600 51 206 81 121 49 120 48 998 2235 750 51 272 108 210 84 210 84 3000 6614 Magnets as shipped with crate and pallet removed and stand or legs attached Magnet Bore Height Width Depth Magnet Weight Moi MHz mm cm in cm in cm in Weight AMIANO kg lb kg Ib 200 54 158 62 76 30 66 26 136 300 544 1200 200 54 LH 235 235 92 5 69 27 69 27 400 880 556 1225 200 54 LH 365 235 92 5 69 27 69 27 400 880 556 1225 200 89 225 88 5 79 3D 79 31 300 660 456 1005 300 54 158 62 76 30 66 26 152 335 560 1235 300 54 LH 235 235 92 5 69 27 69 27 400 880 556 1225 300 54 LH 365 235 92 5 69 27 69 27 400 880 556 1225 300 89 225 88 5 79 31 79 31 350 770 506 1115 400 54 235 92 5 69027 69 27 400 880 556 1225 400 54 LH 365 235 92 5 69 27 69 27 400 880 556 1225 400 89 246 97 79 31 79 31 530 1166 660 1456 500 51 240 94 5 79 31 79 31 540 1190 671 1480 600 51 259 102 98 38 4 98 38 4 1070 2365 1211 2670 750 51 331 3 130 4 116 8 46 0 116 8 46 0 3000 6614 3000 6614 Dimensions and weights are typical and can vary 5 cm 2 in or 4 5 kg
31. 5 Europe U K 220 240 15 Microimaging Module The gradient power cabinet of the microimaging module contains three Techron gradient amplifiers a VME card cage and a power distribution unit PDU and requires considerable electrical power Customers must therefore provide a dedicated three phase 30 power line to a wall mounted circuit breaker and wiring from the circuit breaker to the PDU All wiring must conform to local electrical codes For three phase wiring configuration and requirements check with your Varian representative The 5 m 16 5 ft 5 conductor cable to the PDU is supplied by Varian without connectors Figure 6 shows the internal wiring of the gradient cabinet As shown in Table 12 Techron units come in four different models corresponding to the four input voltages Varian recommends the 208 model for U S installations and the 380 model for European installations The customer must communicate the choice of power input voltage and mains frequency 50 Hz or 60 Hz to Varian well in advance of the spectrometer shipping date so that the correct Techron models will be included Note that by using internal jumpers the Techron 208 can be converted to the 240 model and the 380 model can be converted to the 416 model VME Card Cage 100 Techron Techron Techron voltage a 250 Gradient Amp Gradient Amp Gradient Amp selector 240 X Y Z 3 cable fso fo fao fre to circuit breaker Power Distributi
32. 51 600 51 The bottoms of the stands consist of a large annular base as shown in Figure 1C Magnet Weight Distribution With Antivibration System This section describes weight distribution for magnets installed with antivibration systems The weights of the magnets including stands and antivibration systems are given in Table 1 200 51 300 51 magnet The antivibration system consists of a square table supported by three legs See Figure 2 for leg placements and sizes A B C i _ 115 75 500 51 R 12 875 Wo lt 24 23 125 600 51 R 0 75 500 51 leg pads 21 5 6 5 O D 18 215 600 51 annular base bM d Magnets Magnets Magnets 200 54 200 89 400 89 300 54 300 89 500 51 400 54 600 51 LH magnets Figure 1 Plan views of floor contact points of magnet stands 6 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements 200 89 300 89 400 54 400 89 500 51 600 51 750 51 magnets The antivibration system for these magnets consists of dampening equipment integrated into the magnet legs All of these magnets except the 600 51 are supported by three legs as illustrated in Figure 3A and Figure 3C The 600 51 is supported by four legs as illustrated in Figure 3B Antivibration Bolt Down Requirement For 200 89 300 89 400 54 400 89 500 51 600 51 or 750 51 magnets as well as LH magnets with an antivibration system the magnet legs must be bolted
33. 60 psig 50 LPM 106 SCFH System with microimaging module Gradient coil cooling 310 kPa 45 psig 50 LPM 106 SCFH Probe cooling 310 kPa 45 psig 20 LPM 42 SCFH 87 195320 00 G0994 UNITYplus Installation Planning Guide 21 Installation Site Preparation AC Power and Air Conditioning Use Table 14 to help determine maximum surge current line conditioning and air conditioning requirements The surge current can be reduced by setting the rf amplifier s to the off position using the rf amplifier switch on the rear panel and then switching on the spectrometer power and turning on each rf amplifier separately A filter on the air conditioning unit intake and special air filtration is required in installations exposed to corrosive gases salt air or unusual dirt or dust conditions The air conditioning system requires a power line separate from the spectrometer system Table 14 Maximum air conditioning requirements For standard systems and host computers Power Surge Current Power System kW A Factor BTU hr 200 300 400 500 MHz standard 1 7 78 0 925 5800 system leading 600 MHz standard system 1 8 78 0 925 6150 leading Host computer monitor peripherals 0 9 3100 Decay time 150 ms 7 Leading and lagging is the phase relationship between voltage and current i Conversion of the unit of heat energy between BTU and the amount of system power is calculated 1 kilowatt hour 2 3413 BTU Measur
34. 65 300 300 400 89 300 300 500 51 400 300 600 51 1000 600 750 51 2000 1200 87 195320 00 G0994 UNITYplus Installation Planning Guide 25 Installation Supplies and Equipment Liquid Nitrogen Supply Table 16 lists the recommended quantities of liquid nitrogen Liquid nitrogen storage containers suffer a loss of contents from boiloff so request delivery of the supply just prior to the scheduled visit of the installation engineer Provide an adaptor for connecting 9 mm 3 8 in ID rubber tubing to the container For low temperature operation using the variable temperature accessory a refrigerant is required Most commonly this is liquid nitrogen in the VT cooling bucket Table 16 Initial on site liquid nitrogen supply Magnet Field Initial Supply MHz liters 200 54 130 200 54 LH235 325 200 54 LH365 325 200 89 325 300 54 130 300 54 LH235 325 300 54 LH365 325 300 89 325 400 54 325 400 54 LH365 325 400 89 325 500 51 325 600 51 700 750 51 1500 26 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Supplies and Equipment Helium Gas Supply Table 17 lists the recommended number of helium gas cylinders Each cylinder should hold at least 8000 liters 285 ft3 The helium gas must be the highest purity available no less than 99 995 or U S Bureau of Mines Grade A A magnetic helium gas container can be used provided the unit remains outside the 5 gauss limit of the magnet and the cylinder is
35. Installation Planning Guide UMTYplus NMR Spectrometer Systems Pub No 87 195320 00 Rev G0994 nuclear magnetic resonance instruments NOTICE Varian Inc was acquired by Agilent Technologies in May 2010 This document is provided as a courtesy but is no longer kept current and thus will contain historical references to Varian For more information go to www agilent com chem E Agilent Technologies Installation Planning Guide UNITY plus NMR Spectrometer Systems Pub No 87 195320 00 Rev G0994 Applicability of manual Varian UNITYplus NMR spectrometer systems Technical writer Dan Steel Copyright 1994 1995 by Varian Associates Inc Nuclear Magnetic Resonance Instruments 3120 Hansen Way Palo Alto California 94304 1030 All rights reserved Printed in the United States The information in this document has been carefully checked and is believed to be entirely reliable However no responsibility is assumed for inaccuracies Statements in this document are not intended to create any warranty expressed or implied Specifications and performance characteristics of the software described in this manual may be changed at any time without notice Varian reserves the right to make changes in any products herein to improve reliability function or design Varian does not assume any liability arising out of the application or use of any product or circuit described herein neither does it convey any license
36. L Mete tenete med dide redes 39 Postdelivery cess detecte eee vett eee tree dte red 39 Appendix B Stray Field Plots 41 Appendix C Posting Requirements for Magnetic Field Warning Signs 50 Warning S19ns 2e er ee tte tre el pr et peii ted 50 Public Access Areas ini v FER RELIER IRR WE Re Re PUER UP HP 50 Safety Traming etd e reo iii 51 Appendix D System Cable Lengths and Room Layouts 54 Cable Lengths for 200 500 MHz Systems Without Options 54 Cable Lengths for High Field Systems and Systems With Options 55 Cable Lengths for Systems With Ultraenmr M Shims ees 56 Minimum Space for 200 54 or 300 54 System Without Options 57 Standard Layout for 200 54 or 300 54 System Without Options 58 Recommended for 200 54 or 300 54 System With Options 59 Recommended for 400 54 or Any 89 mm System Without Options 60 Recommended for 400 54 500 51 or Any 89 mm System With Options 61 Typical Layout for 600 51 System sess 62 Appendix E Peripheral Compatibility 63 iv UNITYplus Installation Planning Guide 87 195320 00 G0994 Explanation of Status Listing 63 Printer and Plotter Compatibility esee 63 Hewlett Packard ThinkJet HP2225D sene 63 Hewle
37. any of the computers listed here are acceptable Computers must have 8 megabytes MB of RAM or more One or more up to three hard disks internal and or external can be present with a minimum total disk space of 207 MB Monitors can be any size monochrome or color Graphics can be plain or the GX version the GX version provides higher performance Graphics higher than GX that is GXplus GS GT are not used by Varian software Varian has not performed a full evaluation of higher lever graphics boards and cannot guarantee complete compatibility Sun Peripherals Sun operating system software SunOS as discussed below is shipped on a CD ROM and can be installed either locally on a computer to which the CD ROM unit is attached or remotely You must have a CD ROM drive available for installation of SunOS a CD ROM drive is not automatically included with the computer or with a spectrometer purchase Varian VNMR software is provided on 1 4 inch and 8 mm tape and instructions are only provided for installing it locally or remotely To install VNMR software you must have available either directly connected to the computer or to a computer to which that computer is networked a 1 4 inch or 8 mm tape drive SunOS Media Sun computers whether purchased from Sun or from Varian include the UNIX right to use license In general they do not have the operating system media included some Sun computers purchased through Varian do inc
38. aration Obtaining the IP Address Your computer must have a unique Internet Protocol IP network address if your computer is to be attached to a network Consult your network administrator about the address If the software is being installed on a computer that is already connected to a network the command ypcat hosts grep uname n can be used to display the IP address of your computer Note the use of back quotes in this command Selecting a Subnet Mask The subnet mask is a number that is used to split IP addresses into the network Internet and host parts If your site does not use multiple subnets use the default number otherwise consult your network administrator For a computer connected to a network the command cat etc netmasks can be used Selecting the Name Service Type The name service prompt allows choosing between NIS NIS and none If you choose NIS or NIS you need to enter the hostname and the IP address of the computer from which you receive the service If you choose none you are not prompted for additional information Ask your network administrator what name service the network uses Entering the Hostname and IP Address of the Name Server If you select either NIS or NIS as the name service type it is assumed that there is a different computer on the network that is the current NIS or NIS server You are asked to enter the hostname and IP address of the server that provides the name service On an
39. as been installed Cardiac pacemaker wearers should refrain from entering a zone that would subject a cardiac pacemaker to a magnetic intensity that could cause adverse effects In some instances this zone might include space on the floors directly above and below the magnet Figure 4 indicates the typical 5 gauss level zone for each magnet bore size For assistance in determining the effect of a system on pacemaker consult the pacemaker user s manual contact the manufacturer or confer with a physician to determine the effect on a specific pacemaker Actual levels vary and should be checked after a particular magnet has been installed Varian provides signs warning of magnetic field hazards Refer to Appendix C on page 50 for an explanation of the types of signs and the sign posting requirements Additional signs are available from Varian at no charge 750 51 6 04 m 600 51 3 607 Magnet center Magnet Bore 5 gauss field MHz mm m Figure 4 Typical radial distances at which 5 gauss levels exist 10 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements Since the magnetic field exists both horizontally and vertically the effect of the field on persons electronic equipment computers and other objects located above and below the magnet must also be considered Pacemaker hazard and other signs warning that a magnetic field is present may be needed in the space on the next floor above the mag
40. ates 37 39 operating frequency 13 Order Acknowledgement form 37 39 pacemaker hazard 10 PDU 19 peripheral compatibility 63 peripherals 33 printers and plotters 63 terminals 64 postdelivery checklist 39 postdelivery instructions 37 posting requirements 50 power conditioning system 18 power distribution unit 19 power line analyzer 18 power stick 5 predelivery checklist 39 prefilter 21 pregnancy hazard 11 preinstallation worksheet 35 preloaded SunOS 31 pressure gauge 21 printer and plotter compatibility 63 receiving preparations 36 reproductive hazard 11 rf interference 4 13 right to use license 31 room layouts 54 safety precautions meaning 1 sales centers 66 sample changer 20 scheduling installation 39 server 33 service centers 66 Ship By date 39 shipping crate damage 37 shipping damage 37 shipping method 36 signs 50 site survey 39 size of site 4 software compatibility 30 Solaris collecting system and network information 33 68 UNITYplus Installation Planning Guide versions compatible with VNMR 30 Solaris installation preinstallation worksheet 35 solids modules 19 SPARCstation computers 30 standalone 33 step down transformer 18 stray field plots 10 12 41 streaming tape cartridge 30 structural floor loading rating 6 subnet mask 34 Sun computer models 30 Sun computers 30 architecture and SunOS versions 30 Sun operating system softwa
41. ce with electronic components A distance of 1 m 3 ft should be maintained around the cabinets The service space should be at least 132 cm 52 in Service requirements are described in the Installation Site Preparation section Not drawn to scale 62 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix E Peripheral Compatibility Appendix E Peripheral Compatibility Explanation of Status Listing Fully tested Varian has fully tested this product and believes it to be fully compatible Configuration and use of the product is documented in Varian manuals We guarantee current compatibility and every effort will be made to ensure compatibility with future products e g future software releases Compatibility tested Varian has performed a brief compatibility test of this product and knows of no incompatibilities but does not support the product nor guarantee current or future compatibility Customer tested At least one Varian customer has reported successfully using this product no Varian experience Non functional Varian has reason to believe that this product will not work with our products Unknown Varian has no experience with this product Printer and Plotter Compatibility Hewlett Packard ThinkJet HP2225D Description Dot matrix printer plotter Required configuration Serial interface Status Fully tested Hewlett Packard QuietJet HP2227A Description Dot matrix printer plotter Statu
42. ctrometer system including preparing the computer system Using the predelivery and postdelivery checklists provided and following the information presented should bring about a smooth transition from delivery to installation Varian s delivery responsibility ends at Varian s factory shipping dock or at the customer s receiving dock depending upon the type of insurance obtained by the customer In either case the customer must provide a moving crew to move the shipping crates holding the system from the delivery truck or storage location to the installation site Certain supplies not provided by Varian such as helium and nitrogen supplies must be obtained by the customer before the Varian installation engineer can start the installation This guide describes these supplies in detail We at Varian make every effort to ensure that the ownership of your new NMR spectrometer is a lasting and pleasurable experience If you have any questions or problems please call your local sales representative listed in Appendix F Varian Sales and Service Centers on page 66 of this guide or to contact the factory at the following address Varian Nuclear Magnetic Resonance Instruments Customer Support Group 3120 Hansen Way MS D 421 Palo Alto CA 94304 1030 Telephone 415 424 4643 Safety Precautions This guide contains important warnings and cautions that you should read and follow carefully These safety precautions have the following f
43. d rf interference that may be present Each individual site must be analyzed to ensure optimum system performance Table 3 System accessories dimensions and weights SMS Autosampler system Height Width Depth Weight Conzano cm in cm in cm in kg Ib With crate and pallet 23 50 Crate and pallet removed 71 28 34 3 13 5 34 3 13 5 17 38 UNITYplus work table i Height Width Depth Weight VORREHIUROR cm in cm in cm in kg Ib In carton 31 12 198 78 91 36 53 117 Assembled 67 26 5 183 72 76 30 48 107 Ultraenmr Shims accessory I Height Width Depth Weight che cm in cm in cm in kg Ib Interface HIM Box 13 5 27 11 20 8 Power Supply 86 34 55 5 22 78 5 31 68 150 4 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements Ceiling Height Requirements The ceiling must provide sufficient headroom to insert the liquid helium transfer tube into the magnet dewar and the storage dewar The height of the ceiling or that part of the ceiling located directly above the magnet without obstructions such as lighting and heating ducts must be equal to or greater than the minimum heights in Table 4 On 600 MHz magnets minimum ceiling height includes a flexible helium level sensor probe These ceiling minimums allow enough headroom to insert the standard helium flutter tube and refill transfer tubes into the magnet dewar They also allow use
44. e 220 Vac 120 Vac For 200 54 and 300 54 magnets the minimum distance from the nearest edge of the closest cabinet to the centerline of the magnet is 1 5 m 5 ft For 200 89 300 89 400 89 400 54 and 500 51 magnets this distance is 3 m 10 ft the maximum length of the cable Drawing is a rear view and not drawn to scale 54 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix D System Cable Lengths and Room Layouts Cable Lengths for High Field Systems and Systems With Options See Text Monitor Printer 00 lo O 71 Periph D Q 000 Q Q Q p Imaging l Standard Cabinet High Power Gorda on LLLI table E E st t o E Q O O Oo O Cabl 115 Vac See Text 48 a s 15 ft Differential 3m 3m Amplifier Box 10 ft ion 10 ft Cable Cable Cable Q O o 208 220 240 220 Vac 208 240 380 416 115 Vac Vac Vac 3 Phase For 500 600 and 750 MHz systems and 300 and 400 MHz systems with high power solids the minimum distance from the centerline of the magnet to the edge of the nearest cabinet is the maximum length of the cable which is 3 meters 10 ft A cable from the imaging cabinet to the magnet passes on the other side of the cabinets and is not shown here A gap of 15 cm 6 in is left between the standard cabinet and the options cabinets Drawing is a rear view and not drawn to scale 87 195320 00 G0994 UNITYlus Installation Planning Guide 55 Appendix D
45. e 27 Installation Supplies and Equipment Face Mask and Thermal Gloves If cryogenic helium or nitrogen contact living tissue a serious injury similar to a burn can occur Order appropriate safety coverings for use during dewar servicing including a mask that protects the face completely and loose fitting thermal gloves WARNING Avoid helium or liquid nitrogen contact with any part of the body If liquid helium or nitrogen contact living tissue a serious injury similar to a burn can occur Never place your head over the helium and nitrogen exit tubes on top of the magnet If helium or nitrogen contacts the body seek medical attention especially if the skin is blistered or the eyes are affected Heat Gun Order a 120 Vac 20 A heat gun Dayton Model 27046 or equivalent for thawing ice accumulation and drying out moisture on dewar servicing equipment Nonferromagnetic Ladder Acquire a 90 to 120 cm 3 to 4 ft nonferromagnetic ladder for reaching the top of the dewar while inserting and removing the helium transfer tube The ladder should be sturdy and self supporting with rubber feet A somewhat taller 120 to 180 cm 4 to 6 ft ladder is recommended for widebore and 400 500 and 600 MHz magnets Hoist A hoist must be available to remove the magnet from the crate assemble it and move it into place The capacity of the hoist depends on the weight of the magnet being installed Table 2 on page 3 specifies magnet weights Allo
46. e 5 Table 5 Interaction between common objects and a magnetic field 9 Table 6 Stray field data for Oxford and Varian magnets sss 11 Table 7 Spectrometer and nuclei operating frequencies sess 13 Table 8 Results of rf emissions tests on Varian NMR equipment 14 Table 9 IEEE ANSI C95 1 1991 standard for RF radiation levels 15 Table 10 Ambient temperature and relative humidity sess 16 Table 11 Liquid helium displacement for room ventilation considerations 17 Table 12 Models of Techron gradient amplifiers sess 20 Table 13 Compressed air supply source seen 21 Table 14 Maximum air conditioning requirements eee 22 Table 15 Initial on site and short notice liquid helium supplies 25 Table 16 Initial on site liquid nitrogen supply een 26 Table 17 Helium gas supply iii 27 Table 18 Sun systems architecture SunOS and Solaris versions 30 Table 19 Stray field data for NMR magnet systems sse 41 87 195320 00 G0994 UNITYplus Installation Planning Guide vii viii UNITYplus Installation Planning Guide 87 195320 00 G0994 Introduction This guide assists in selecting and preparing a site to install a Varian UNITYplus NMR superconducting spe
47. e System Operation Manual contains information to operate your spectrometer and interact with UNIX The Sun computer also comes with the Desktop SPARC manual set which provides user level documentation on the basic features of UNIX Additionally SunOS contains extensive on line documentation accessed by the man command For these reasons full Sun UNIX documentation is not included with the purchase of a Sun computer whether from Varian or another source Full documentation is available from Sun through SunExpress SX 09 but such documentation is definitely not required for installation or use of the system Computer Preparation Checklist J Sun computer is SPARCstation ELC IPC IPX or SPARCstation 1 1 2 10 Classic or LX Hard disk drive is 207 MB or larger 150 MB 1 4 inch tape unit or 8 mm tape unit is installed or available on a networked computer CD ROM drive is installed or available on a networked computer LL LL Sun operating system media is available CD ROM If you have purchased the Sun computer from a source other than Varian Copy of current Software Installation Manual in house Computer installed and configured according to Varian specifications LLL Sun operating system installed and configured according to Varian specifications 32 UNITYplus Installation Planning Guide 87 195320 00 G0994 Computer Preparation Configuration and Peripherals Appendix E Peripheral Compatibility
48. eak vibration greater than 20 ug for 400 500 600 750 MHz and long hold magnets or 100 ug 200 and 300 MHz magnets acceleration from 0 to 100 Hz Measurement is made with an Ono Sokki Model CF 200 field FFT analyzer or a Hewlett Packard Model 3561A signal analyzer or equivalent using 16 rms time averages and with a seismic accelerometer with 10 V g sensitivity Wilcoxen Model 731 or equivalent Magnetic Environment The site must have a minimum of environmental magnetic fields Common sources of magnetic interference are fluctuating loads on adjacent power lines radio or television transmissions heavy duty transformers elevator motors and similar electromagnetic devices Allow a separation of at least 4 6 m 15 ft between the magnet and other high field electromagnets elevators or forklift trucks Similar separation distances must also be maintained between the magnet and anything that can cause a detrimental effect on the field homogeneity or the structural integrity of the magnet Conditions that could interfere with the magnet include but by no means limited to a wall with metal sheathing or steel studding a concrete support column with steel reinforcing bars and a storage area containing steel dewars for cryogenic storage Each site must be carefully analyzed to ensure optimum performance of the system See Table 5 for examples of objects that affect or are affected by the magnetic field The CRT in color monitors need
49. ed visit of the Varian installation engineer Table 15 lists the quantities of liquid helium recommended at installation CAUTION Specity that supply dewars be made of nonmagnetic materials A magnetic supply dewar next to the magnet can damage the magnet solenoid A magnetic supply dewar can also be pulled into the magnet possibly damaging the magnet or causing the magnet to quench The amount of loss due to boiloff as the magnet is cooled varies An initial supply of liquid helium about 5096 more than the amount expected to be necessary for cooling down the magnet is usually adequate however an additional supply for delivery on short notice is also advisable should the initial amount be insufficient Table 15 shows the quantities recommended When ordering for the 200 54 or 300 54 system be sure that the supply dewar has a diameter less than 84cm 33 in This is necessary because these magnets use a rigid transfer tube that must be inserted into the storage dewar and magnet dewar simultaneously without bending All other magnets use a flexible transfer tube that inserts into most sizes of supply dewars Table 15 Initial on site and short notice liquid helium supplies Magnet Bore Initial Supply Short Notice MHzmm liters Supply liters 200 54 200 150 200 54 LH235 300 300 200 54 LH365 300 300 200 89 300 200 300 54 200 150 300 54 LH235 300 300 300 54 LH365 300 300 300 89 300 200 400 54 400 89 300 300 400 54 LH3
50. ements are only for the standard acquisition and rf console which does not share an ac power branch with the host computer 7 Measurements are only for the host computer The computer does not share an ac power branch with the acquisition rf console For systems equipped with the following modules increase the heat output of the standard system by the maximum amounts shown System kW BTU hr SMS Autosampler 0 18 615 CP MAS 0 1 340 Wideline module 1 0 3413 CRAMPS multipulse module 1 0 3413 Complete solids module 1 7 5800 Additional rf channel 0 5 1700 Ultraenmr Shims 0 75 2600 Microimaging module 1 5 5120 22 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Preparation Compressed Nitrogen Gas During operation of the variable temperature accessory a compressed nitrogen gas supply from a cylinder or a fixed line is required that is dry oil free magnetically clean for example free of rust and with a dew point of 193 C 80 K The flow and pressure rates through the regulators are the same as those listed for the compressed air supply Telephones We recommend that at least one telephone line be located in the immediate vicinity of the spectrometer It should be modem quality This line may serve as a normal telephone some of the time and as a modem connection at other times It might be desirable to have two telephone lines one of modem quality and one regular The latter could s
51. erve as a telephone to enable the operator to discuss the spectrometer system as it operates The other line could be permanently connected to a modem making use of the remote communication capabilities that are inherent in UNIX Varian software does not require or support modem communication Electrostatic Discharges Electrostatic discharges under 15 kV generally will not result in any perceivable errors or problems Discharges over 15 kV however can result in loss of data and or errors that are perceivable to the operator Discharges over 25 kV can cause damage to the equipment To prevent electrostatic discharge damage the system should be installed on vinyl covered floors and be properly grounded If carpeting is installed the carpet should contain only a small percentage of nylon and be installed over antistatic pads Alternatively regular use of a good quality antistatic spray will help considerably in alleviating the problem Whenever a printed circuit board must be touched or handled the person should wear grounded wrist straps CAUTION Many components in the system contain highly sensitive electronic devices that must be protected from electrostatic discharges by proper floor coverings and grounding practices A person walking across a nylon carpet or wearing synthetic fabrics can generate an electrostatic charge that can discharge to the next object that is touched If this happens to be the system the system components can be
52. et 200 300 Magnet W Service Access 120 Vac 20 A Outlet S The room dimensions are about 4 4 m x 4 6 m 14 5 ft x 15 ft This arrangement provides comfortable access for operator and service personnel The standard cabinet is 111 cm x 78 cm 44 in x 31 in Typical table size is 183 cm x 76 cm 72 in x 30 in The magnet is 69 cm x 69 cm 27 in x 27 in A distance of 1 7 m 5 3 4 ft should be maintained around the magnet to prevent interference with electronic components A distance of 1 m 3 ft should be maintained around the standard cabinet Not drawn to scale 58 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix D System Cable Lengths and Room Layouts Recommended for 200 54 or 300 54 System With Options utlet Imaging Outlet 220 Vac 20A Solids 3 Phase Outlet O Imaging Cable to Magnet Approx Location Standard A 120 Vac Cabinet i 20A Outlet 120 Vac 20A Outlet 120 Vac Outlets n d a x e a NN Service Access The room dimensions are about 4 4 m x 5 5 m 14 5 ft x 18 2 ft The standard cabinet is 111 cm x 78 cm 44 in x 31 in The imaging and high power solids cabinets are 55 cm x 78 cm 22 in x 31 in each Typical table size is 183 cm x 76 cm 72 in x 30 in The magnet is 69 cm x 69 cm 27 in x 27 in The SMS autosampler is about 79 cm x 79 cm 36 in x 36 in A distance of 1 7 m 5 3 4 ft should be maintained around the magnet to prevent
53. etween shimming Sunlight should never shine on the magnet or the area surrounding the magnet If necessary install an air conditioning system to maintain the required conditions Keep the air conditioning system operating continuously to stabilize the temperature and humidity surrounding the spectrometer system The air flow from the room heating and cooling system must not blow on the magnet Do not allow moisture to collect on in or around the system At high altitudes above 5000 ft the cooling efficiency for the electronics is lower This can be compensated for by lowering the room temperature by one or two degrees from the room temperature specification Table 10 Ambient temperature and relative humidity Temperature Relative Humidity Mode C F Noncondensing Operational 17 to 24 60 to 75 20 to 80 Optimum 20 68 40 to 60 Stability 1 0 x18 Non operational 20 to 60 4t0140 8 to 80 16 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements Ventilation Air ventilation must be adequate to displace the liquid helium gas during a quench especially when using any type of volatile liquid for variable temperature experiments Consult with a safety engineer on this subject See also Table 11 which lists the amount of liquid helium for each magnet Maximum Altitude The maximum altitude during operation is 2440 m 8000 ft The maximum during storage or transport is 9100 m 30 000
54. ice listed in Appendix E of this guide 87 195320 00 G0994 UNITYplus Installation Planning Guide 39 Appendix A Installation Checklists 40 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix B Stray Field Plots Appendix B Stray Field Plots This appendix shows stray field plots for each magnet listed as MHz mm The axial and radial distances shown are measured in meters from the magnet centerline CL The values are typical but may vary between individual magnets Gauss levels should be checked after a particular magnet has been installed The values in Table 19 were copied from Oxford technical manuals Table 19 Stray field data for NMR magnet systems 87 195320 00 G0994 Magnet Axial Distance m from Magnet Radial Distance m from Magnet Systems Center Line Center Line MHz mm 5 gauss l0 gauss 25 gauss 5 gauss l0 gauss 25 gauss 200 54 1 82 1 45 1 05 1 47 1 20 0 90 200 89 2 65 2 05 1 49 2 00 1 60 1 15 300 54 2 20 1 75 1 26 1 70 1 30 0 97 300 89 2 75 2 20 1 63 2 20 1 75 1 26 400 54 2 80 2 24 1 65 2 20 1 76 1 29 400 89 3 80 3 00 2 21 3 05 2 40 1 74 500 51 3 45 2 70 2 00 2 75 2 20 1 60 600 51 4 55 3 60 2 67 3 60 2 85 2 10 750 51 7 60 6 04 4 45 6 04 4 79 3 53 UNITYplus Installation Planning Guide 41 Appendix B Stray Field Plots Axial distance from magnet CL m Axial distance from magnet CL m 200 54 magnet field values in gauss 0 5 1 0 1 5 2 0 Radial distance from
55. lation Site Requirements Structural Strength of Floor Contact plant engineer structural engineer or registered civil engineer to confirm that the magnet and antivibration system as applicable does not exceed the structural floor loading rating The site floor also must have sufficient structural strength to support the combined weight of the spectrometer system and moving equipment during installation Table 1 and Table 2 list magnet and system weights Magnet Weight Distribution No Antivibration System This section describes weight distribution for magnets without antivibration systems The weights of the magnets including stands are given in Table 1 200 54 and 300 54 magnets The plan view of the magnet stand illustrated in Figure 1A shows how the two rectangular legs contact the floor The magnet stand has four adjustable feet of 11 61 cm 1 8 sq in each total 45 16 cm or 7 Sq in so the point loading is relatively high Because of the overall light weight of these magnets however this is usually not a concern except in areas with a soft floor covering 200 89 300 89 400 54 and long hold magnets The stands for these magnets consist of three legs as shown in the plan view in Figure 1B Since the legs are hollow the actual surface contact with the floor is only 167 74 cm 26 sq in total which creates relatively high point loading This is only a concern however if the floor covering is soft 400 89 500
56. llation Planning Guide 37 Postdelivery Instructions 38 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix A Installation Checklists Appendix A Installation Checklists Predelivery Use the following checklist to prepare for delivery of the system Refer to this manual for further instructions and safety precautions Consult knowledgeable individuals such as plant facilities personnel for assistance in implementing these instructions yi jo 13 14 15 J6 Check the SHIP BY date on the Varian Order Acknowledgment form Use this date as a target for completing installation preparations Select the site for installing and operating the system Note a site survey is standard with many UNITYplus spectrometer systems Prepare the installation site including electrical outlets compressed air supply and air conditioning Make any computer preparations required Order supplies and equipment for installation and startup operation Make arrangements for workers and equipment to move the system upon delivery to the installation site Read carefully sign and mail to Varian the Object Code License Form Note that acceptance of the products on the Order Acknowledgment form will constitute acceptance of the terms stated in the Object Code License Form whether the form is signed or not Postdelivery Use the checklist below to plan for handling the instrument after delivery Refer to
57. lude a CD ROM that is a CD ROM containing the relevant version of SunOS Media is separately purchased One copy of the media on hand for the installation is required and this media must be for the relevant version of SunOS currently 4 1 3 for all computers except SPARCclassic and SPARCstation LX 4 1 3C for SPARCclassic and SPARCstation LX You may purchase the CD ROM from Varian Part No 00 993277 00 for 4 1 3 or Part No 00 901451 00 for 4 1 3C you may purchase it from Sun through SunExpress phone 1 800 USA4SUN Sun P N SX 21 CD ROM or you may borrow it from another computer this is completely legal because of your right to use license SunOS Installation The Software Installation Manual contains complete instructions for configuring the Sun computer and installing the Sun operating system software according to Varian specifications Sun computers operating either as a host or as a separate data station require specific setup and configuration for SunOS installation that are not met by the preloaded configuration supplied by Sun with the computer If you have purchased your computer from Varian Varian assumes full responsibility and will install both the Sun operating system software and the VnmrS and or VnmrX software subject to the constraints discussed above under SunOS Media and Sun Peripherals If you have purchased your Sun from another source you are responsible for configuring the hardware and i
58. magnet CL m 200 89 magnet field values in gauss 1 60 2 00 0 5 1 0 1 5 2 0 Radial distance from magnet CL m Figure 7 Stray field plots for 200 54 and 200 89 magnets 42 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix B Stray Field Plots 300 54 magnet field values in gauss Axial distance from magnet CL m 0 5 1 0 1 5 2 0 Radial distance from magnet CL m 300 89 magnet field values in gauss Axial distance from magnet CL m 0 5 1 0 1 5 2 0 Radial distance from magnet CL m Figure 8 Stray field plots for 300 54 and 300 89 magnets 87 195320 00 G0994 UNITYlus Installation Planning Guide 43 Appendix B Stray Field Plots 44 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix B Stray Field Plots 400 54 magnet field values in gauss Axial distance from magnet CL m 0 5 1 0 1 5 2 0 2 5 Radial distance from magnet CL m 400 89 magnet field values in gauss Axial distance from magnet CL m 0 5 1 0 1 5 2 0 2 5 3 0 Radial distance from magnet CL m Figure 9 Stray field plots for 400 54 and 400 89 magnets 87 195320 00 G0994 UNITYlus Installation Planning Guide 45 Appendix B Stray Field Plots 500 51 magnet field values in gauss Axial distance from magnet CL m 0 5 1 0 1 5 2 0 2 5 3 0 Radial distance from magnet CL m Figure 10 Stray field plots for the 500 51 magnet 46 UNITYplus Installation Planning Guide 87 195320 00 G099
59. may extend vertically to adjacent floors and additional signs may be needed there 3 Post magnet area danger signs Figure 15 at each entrance to the magnet area Be sure each sign is outside the 5 gauss perimeter Be aware that stray magnetic fields can reach beyond the published distances when two or more magnetic fields intersect or when the field extends over large ferromagnetic masses or structures steel doors steel construction beams etc In this case the customer must measure the stray field using a gaussmeter to determine how far the 5 and 10 gauss fields actually extend contact a scientific instrumentation supplier for information on acquiring a gaussmeter If you need additional signs request them from Varian by telephoning 1 800 544 4636 in the United States or by contacting your local Varian office in other countries Public Access Areas In addition to posting signs Varian strongly recommends that customers block or restrict access to public areas containing a 5 gauss or higher stray field In some facilities these areas might include company lobbies or sidewalks outside the building UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix C Posting Requirements for Magnetic Field Warning Signs A10 GAUSS WARNING STRONG MAGNETIC FIELD Tools and Equipment Strong magnetic fields are present that can make magnetic items suddenly fly towards the magnet which could cause personal injury or
60. mended that surge protection be provided Standard Two Cabinet System The standard two cabinet system requires a dedicated single phase continuous duty 220 Vac 7 50 60 Hz power line with 20 A minimum service Terminate this line within 3 m 10 ft of the left side looking from the rear of the standard cabinet with a fused quick disconnect switch box or circuit 18 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Preparation breaker Run a separate insulated low resistance earth ground to the main electrical service entrance ground Solid State NMR Modules No extra electrical services are required for solids modules that do not require the third cabinet such as CP MAS Solids modules that require the third cabinet such as Wideline and CRAMPS Multipulse require an additional 208 220 240 Vac single phase 30 A dedicated line A spectrometer system with complete liquids and solids capability CP MAS Wideline and CRAMPS Multipulse requires an electrical supply with one 220 Vac single phase 20 A outlet and for the standard cabinet and one 208 220 240 Vac single phase 30 A outlet for the high power solids cabinet VT CP MAS Option requires a dedicated single phase continuous duty 50 60 Hz power line as shown in the following table In addition the customer must supply a 3 prong polarized plug compatible with the site voltage Installation Site Voltage Vac Minimum Service A U S 110 125 1
61. net and on the floor below the magnet Figure 5 shows the typical extent of vertical fields for the 400 500 600 and 750 MHz magnet systems drawing is not to scale NMR workers are exposed to high levels of static magnetic fields At this time no conclusive evidence exists indicating adverse health effects at current exposure levels Current exposure levels are generally indicated as levels equal to or less than those in Table 6 on page 11 Although some studies suggest a link between magnetic field exposure and adverse reproductive effects the body of medical data available is not clear enough to draw any firm conclusions regarding risks to pregnancy In other words static magnetic field associated with the NMR spectrometer magnets are not considered by the scientific community at this time to comprise a risk to pregnancy or a reproductive hazard The American Conference of Governmental Industrial Hygienists ACGIH article entitled Threshold Limit Values and Biological Exposure Indices 5th ed states the following TLVs Threshold Limit Values refer to static magnetic flux densities to which it is believed that nearly all workers may be repeatedly exposed day after day without adverse health effects These values should be used as guides in the control of exposure to static magnetic fields and should not be regarded as a fine line between safe and dangerous levels Routine occupational exposures should not exceed 60 milliteslas
62. nowledgment form determines owner responsibility FOB PALO ALTO Transfer of ownership occurs when the shipment leaves the factory The customer is responsible for claims for shipping damage Upon request Varian will provide assistance in filing claims FOB DESTINATION Transfer of ownership occurs at customer s point of receipt Varian is responsible for claims for shipping damage Damage discovered fifteen or more days after delivery generally cannot be recovered Such damage will be at the expense of the customer Moving the System CAUTION Move the crates in an upright position Do not drop or mishandle The crates are packed with G force and tip and tell indicators that record mishandling Be especially careful about moving the magnet crate If one or more crates cannot be moved into the installation site because of doorway clearance leave the affected crates in a clean safe dry location Do not open any crate except with direct instructions from an authorized service representative If possible move the crates in an upright position with a forklift or hydraulic pallet mover directly to the installation site Should it appear necessary to uncrate one or more units because of doorway or passage clearance contact your Varian service representative for further instructions To avoid unnecessary expense be sure moving personnel and equipment are ready for the shipment on the delivery day 87 195320 00 G0994 UNITYplus Insta
63. ns also require a separate regulated air source or nitrogen gas for variable temperature operation with 620 kPa 90 psig pressure at the wall Dewpoint should be 193 C 80 K and oil removal greater than 99 5 Filtration should be to 0 6 microns Contaminated air can cause extensive damage to the probe The minimum flowrate at the wall is 80 Ipm Table 12 Models of Techron gradient amplifiers Model Wall 30 PDU Techron Card Cage 10 208 208 Vac 60 amp 60 A breaker 208 Vac select 120 Vac 240 240 Vac 60 amp 60 A breaker 240 Vac select 120 Vac 380 380 Vac 30 amp 30 A breaker 380 Vac select 240 Vac 416 416 Vac 30 amp 30 A breaker 416 Vac select 240 Vac 20 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Preparation Compressed Air Supply The house compressed air supply must provide a source of air that is clean dry and free of contaminants with a dew point of 40 C 40 F minimum Install a gate valve on the permanent outlet of the air supply line The gate valve must be rated at least 860 kPa 125 psi or 9 kg cm If the house line pressure is greater than this level the valve must be rated at a level that exceeds the house pressure Attach to the valve a minimum 1 cm 0 4 in pipe terminated with a 1 4 inch male NPT Make the pipe long enough so that its termination fitting is within 4 5 m 15 ft of the planned location of the magnet In areas where humidity is high or where moisture
64. nstalling the SunOS software according to the instructions contained in the Software Installation Manual you can request a free copy 87 195320 00 G0994 UNITYplus Installation Planning Guide 31 Computer Preparation through Varian Technical Support or through your local Varian sales and service organization Installation will not start until the computer system is properly configured however you are not expected to install the Varian VnmrS and or VnmrX software There is an exception If you have purchased a Sun computer from a source other than Varian and if you have a knowledge of UNIX system administration and if that computer came with SunOS preloaded it is possible to reconfigure the preloaded SunOS so that it can be used for VNMR operation In this case only a copy of the SunOS media is not required Guidelines but not step by step instructions are contained in the Software Installation Manual for the case of a two disk system A single 207 MB hard drive system does have sufficient room to install VNMR on top of the preloaded SunOS although only a small amount of space to store NMR data will remain Varian installers are not trained to perform these operations If you have purchased the Sun computer from Varian you must have a copy of the SunOS CD ROM available for the installer to use Sun Documentation The Varian manual Software Installation Manual contains full step by step instructions for installing SunOS and Solaris and th
65. on Unit PDU Figure 6 Internal wiring of gradient cabinet 87 195320 00 G0994 UNITYplus Installation Planning Guide 19 Installation Site Preparation SMS Autosampler System requires a 120 or 220 Vac single phase continuous duty 50 60 Hz power line 15 A minimum service within 2 7 m 9 ft of the magnet Ultraenmr Shims accessory requires 110 120 Vac power at 60 Hz 750 W and cannot drop below 100 V For 220 240 Vac at 50 60 Hz use a Gemini step down transformer For 200 Vac at 50 60 Hz use a special isolation transformer with a 200 Vac tap Pulsed Field Gradients accessory uses standard system power and requires no special electrical outlets Other Accessories and Test Equipment At least six outlets are needed within 1 8 m 6 ft of the host computer standard cabinet and magnet The outlets must have ground connections and should provide a minimum of 2 30 kVA at the local single phase line voltage 120 Vac at 20 A or 230 Vac at 10 A Separate Air Sources for System Options The vibration isolation table and antivibration legs require a separate regulator supplied by Varian The air pressure requirements are the same as the spectrometer system Using the spectrometer or sample changer regulator with the antivibration system causes the magnet to vibrate A system equipped with a vibration table or vibration isolators for the magnet also requires a separate air source and regulator The CP MAS and CRAMPS solids optio
66. ormat and meaning WARNING Warnings are used when failure to observe instructions or precautions could result in injury or death to humans or animals or significant property damage CAUTION Cautions are used when failure to observe instructions could result in permanent damage to equipment or data 87 195320 00 G0994 UNITYplus Installation Planning Guide 1 Installation Site Requirements Installation Site Requirements Factors to consider when selecting the installation site include Accessibility to the delivery location Site size and ceiling height Floor rigidity and structural strength Magnetic and radio frequency environment Ambient temperature and humidity Air ventilation Each item is described in detail in the following sections Accessibility of Site The installation site must be accessible from the delivery location with adequate clearance for system crates and moving equipment throughout the access route Refer to Table 1 Table 2 and Table 3 for the dimensions and weights needed for calculating vertical horizontal and turning clearances and evaluating the structural strength of passageways Moving the larger crates of the system requires a forklift or hydraulic pallet mover which must be considered when calculating accessibility The site must also provide adequate access for the routine delivery of supply dewars containing liquid helium and nitrogen For an installation site at a different level f
67. patible but not recommended Computer Compatibility Sun SPARCsystem 600 MP series Description Sun multiprocessor server computers Status Compatibility tested Comments Tested as workstation only status as host unknown Tested running SunOS 4 1 2 64 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix E Peripheral Compatibility Terminal Emulator Compatibility TextTerm Graphics Description Source Status VersaTerm Pro Description Status Tektronix 4107 4207 emulator for Macintosh computers Mesa Graphics 505 672 1998 Compatibility tested Tektronix 4105 emulator for Macintosh computers Non functional X Server Software Compatibility MacX Description Source Status eXodus Description Source Status 87 195320 00 G0994 X server software for Macintosh computers Apple Computer Compatibility tested X server software for Macintosh computers White Pine Software 603 886 9050 Compatibility tested UNITYplus Installation Planning Guide 65 Appendix F Varian Sales and Service Centers Appendix F Varian Sales and Service Centers Varian s staff of thoroughly trained service specialists throughout the world is your assurance of always receiving prompt attention United States Varian Associates Inc Nuclear Magnetic Resonance Instruments 3120 Hansen Way M S D 421 Palo Alto California 94304 1030 415 424 6361 installation scheduling 800 356 4437 sales service
68. pendix C Posting Requirements for Magnetic Field Warning Signs ADANGER STRONG MAGNETIC AND RADIO FREQUENCY FIELDS ARE PRESENT DUET TECH LT ERE Tale Tools and Equipment ATM Credit Cards Strong magnetic fields are Strong magnetic fields are present that could erase present that could make some magnetic media such as magnetic items suddenly fly floppies and tapes disable ATM towards the magnet body which and credit cards and damage could cause personal injury or some watches serious damage Do not take such objects closer Do not take tools equipment to the magnet than the or personal items containing 5 GAUSS WARNING signs steel iron or other magnetic materials closer to the magnet than the 10 GAUSS WARNING signs Figure 15 Magnet area danger sign Pub No 87 250301 00 52 UNITYplus Installation Planning Guide 87 195320 00 G0994 Appendix C Posting Requirements for Magnetic Field Warning Signs 87 195320 00 G0994 UNITYplus Installation Planning Guide 53 Appendix D System Cable Lengths and Room Layouts Appendix D System Cable Lengths and Room Layouts Cable Lengths for 200 500 MHz Systems Without Options Monitor Printer oe ps FIG SF PL SO p Ko Standard Cabinet Magnet Plotter V 9 See Text oo 120 Vac 4 6 m 15 ft Cable See Text Differential Amplifier Box 3 m 10 ft Cabl
69. provides network services such as file transfer and storage space A standalone system is a system that contains its own hard disk and bootup files A dataless client sometimes called diskless client is a system without its own hard disk and uses an NFS server for the operating system storage and other services For the purposes of VNMR you will install your system as a standalone system Selecting a Hostname A computer on a network is often called a host Its hostname is the name that uniquely identifies the computer If you already have a version of UNIX installed you can use the command uname n from within a C Shell to display this information for a Sun computer When choosing a hostname make sure the name you select is unique within both your local area network and if applicable your name service domain In many networks the choice of a hostname is left up to the owner of the computer subject to the requirement of uniqueness A hostname can be up to 64 upper case or lower case characters It is strongly recommended that you use all lower case characters in the hostname because some networking software that might be used in other computers on the network could require lower case hostnames Choose a name that starts with a lower case letter followed by any combination of lower case letters numbers or hyphens The name however cannot end with a hyphen 87 195320 00 G0994 UNITYplus Installation Planning Guide 33 Computer Prep
70. re SunOS 31 Sun peripherals 31 SunExpress 31 SunOS versions compatible with VNMR 30 SunOS and VNMR Software Installation Manual 32 SunOS and VNMR Software Installation Manual 31 SunOS Media 31 supplies 24 supply dewars 25 surge protection 18 surge protector 29 System Operation Manual 32 Techron gradient amplifiers 19 telephone jack 23 temperature stability 16 terminal compatibility 64 test equipment outlets 20 thermal gloves 28 third rf channel 21 tip and tell indicator 37 39 transfer of ownership 37 transfer tube 5 25 28 uname n command 33 uncrating system 4 van delivery 36 variable temperature accessory 23 Varian sales and service centers 66 ventilation 17 vertical magnetic fields 11 vibration in floor 8 vibration table 20 VME card cage 19 VNMR compatibility with SunOS and Solaris 30 voltage variations 18 VT accessory 26 27 warning signs 10 50 warnings defined 1 wideline module 22 321 world time zones 34 87 195320 00 G0994 Index ypcat hosts grep uname n command 34 ypwhich command 34 87 195320 00 G0994 UNITYplus Installation Planning Guide 69
71. rom the delivery location be sure that the lifting equipment such as an elevator is capable of handling the combined weight and size of the shipping crates and the moving equipment Table 1 Cabinets dimensions and weights Cabinets as shipped with crate and pallet Height Width Depth Weight COPIE cm in cm in cm in kg Ib Standard UNITYplus 148 6 58 5 135 53 102 40 285 630 High power solids 168 66 81 32 102 40 285 630 Microimaging 168 66 81 32 102 40 240 530 Components unpacked with crate and pallet removed Height Width Depth Weight Component cm in cm in cm in kg Ib Standard UNITYplus 124 5 49 110 7 43 6 78 30 7 272 600 High power solids 142 3 56 55 3 21 8 78 30 7 lt 272 lt 600 Microimaging 142 3 56 55 3 21 8 78 30 7 227 500 2 UNITY plus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements Table 2 Magnet dimensions and weights Magnets as shipped with crate and pallet Magnet Bore Height Width Depth Weight MHz mm cm in cm in cm in kg Ib 200 54 120 47 79 31 88 35 132 290 200 54 LH235 200 80 95 37 25 95 37 25 468 1030 200 54 LH365 200 80 95 37 25 95 37 25 468 1030 200 89 200 80 95 37 25 95 37 25 368 810 300 54 120 47 79 31 88 35 142 313 300 54 LH235 200 80 95 37 25 95 37 25 468 1030 300 54 LH365 200 80 95 37 25 95 37 2
72. s Fully tested Hewlett Packard DeskJet Description Ink jet printer plotter Status Fully tested Hewlett Packard LaserJet IIl HP33449A Description Laser printer plotter Required configuration 2 MB memory expansion Status Fully tested Comments PostScript cartridge can be used and produces faster plotting Hewlett Packard LaserJet 4 Description Laser printer plotter Required configuration Standard 2 MB memory Status Fully tested IBM Lexmark Color Jetprinter PS 4079 Description Inkjet printer plotter Required configuration Standard 4 MB memory Status Fully tested 87 195320 00 G0994 UNITYplus Installation Planning Guide 63 Appendix E Peripheral Compatibility Hewlett Packard HP7475 HP7475A Description Single sheet 11x17 plotter Required configuration Interface option 001 RS 232C CCITT Status Fully tested Hewlett Packard HP7550 HP7550B Description 11x17 plotter with automatic sheet feed Required configuration B size media handling kit P N 17092A recommended Status Fully tested Hewlett Packard DraftPro HP7570A Description D size 25x39 plotter Status Fully tested Terminal Compatibility GraphOn 240 GO 240 Description Monochrome terminal Required configuration Mouse 1001C ET Status Fully tested Tektronix 4207 TEK 4207 Description Color terminal Required configuration 3 button mouse Option 4M Status Fully tested Comments 4205 4107 4105 also com
73. s to be degaussed in magnetic fields above 1 to 2 gauss Above 5 gauss color monitors may need additional shielding to prevent display distortion Sun computers and peripherals are also affected by the magnetic field refer to Computer Preparation on page 30 for a discussion of magnetic field considerations WARNING Cardiac pacemaker wearers must remain more than 4 5 m or 15 ft 6 1 m or 25 ft for the 750 51 away in all directions from the magnet until safety is clearly established An NMR superconducting magnet generates strong magnetic and electromagnetic fields that can inhibit operation of some cardiac pacemakers resulting in death or serious injury to the user Consult the pacemaker user s manual contact the manufacturer or confer with a physician to determine the effect on a specific pacemaker Varian provides signs with each system to warn pacemaker wearers of this hazard Post the signs at least 4 5 m or 15 ft 6 1m or 25 ft for the 750 51 from the magnet 8 UNITYplus Installation Planning Guide 87 195320 00 G0994 Installation Site Requirements Table 5 Interaction between common objects and a magnetic field Objects that affect the magnetic field 15 gauss line or closer 5 to 15 gauss 2 to 5 gauss 1 to 2 gauss All ferromagnetic construction materials except small amounts of steel reinforcing bar normally not exceed ing 11 kg m 2 5 Ib ft Presence or movement of ferromagnetic objects over 45 kg 1
74. sence and hazard of strong magnetic fields the customer is responsible for posting clearly visible signs warning of magnetic field hazards This responsibility includes measuring stray fields with a gaussmeter Radio frequency emissions may also pose a danger to some individuals The rf emission levels from Varian NMR equipment have been measured and compared to the IEEE ANSI C95 1 1991 standard For further information refer to the Installation Planning Guide for the system Warning Signs To help customers meet this posting responsibility Varian provides warning signs These signs must be posted according to the following requirements before the magnet is energized 1 Post 10 gauss warning signs Figure 13 along the 10 gauss perimeter of the magnet so that a sign can be easily seen by any person about to enter the 10 gauss field from any direction The back of each sign lists typical 10 gauss distances Note that the stray field may extend vertically to adjacent floors and additional signs may be needed there A sign is not required if the 10 gauss field extends no more than 30 cm 12 in beyond a permanent wall or no more than 61 cm 24 in beyond the floor above the magnet 2 Post 5 gauss warning signs Figure 14 along the 5 gauss perimeter of the magnet so that a sign can be easily seen by any person about to enter the 5 gauss field from any direction The back of each sign lists typical 5 gauss distances Note that the stray field
75. serious damage Do not take tools equipment or personal items containing steel iron or other magnetic materials closer to the magnet than this sign Dewars The stray field of the magnet can pull a magnetic dewar into the magnet body causing serious damage Use only nonmagnetic stainless steel dewars Do not use iron or steel dewars during servicing Pul Na 57 25090200 80694 10 Qaus Waring Si II variane Figure 13 10 gauss warning sign Pub No 87 250302 00 STRONG MAGNETIC FIELD Pacemaker Metallic Implant Hazard Strong magnetic and rf fields are present that can cause serious injury or death to persons with implanted or attached medical devices such as pacemakers and prosthetic parts Such persons must not go closer to the magnet than this sign until safety at a closer distance is identified by a physician or device manufacturer Magnetic Media ATM Credit Cards Strong magnetic fields are present that can erase magnetic media disable ATM and credit cards and damage some watches Do not take such objects closer to the magnet than this sign Pul No 87 250908 00 80604 Gauss Waning Sgn I variane Figure 14 5 gauss warning sign Pub No 87 250303 00 Safety Training Customers must provide on site training about magnetic field hazards to any person who may be exposed to 5 gauss or stronger stray fields 87 195320 00 G0994 UNIT Yplus Installation Planning Guide 51 Ap
76. st for particular magnets but be aware that these distances will vary somewhat for each magnet and should be checked after a magnet is installed Sun Computers Varian currently supports the Sun computer models shown in Table 18 This table also lists the versions of SunOS and Solaris that are compatible with VNMR Other models that have been sold in the recent past are fully documented in the installation manuals including the SPARCstation 1 and SPARCstation 1 If you Table 18 Sun systems architecture SunOS and Solaris versions Sun System Sun Architecture SunOS Version Solaris Version SPARCstation 20 Sun 4m 4 1 3 Ul 4 1 4 2 3 2 4 SPARCstation 5 SPARCclassic Sun 4m 4 1 3C 2 3 2 4 SPARCstation LX 4 1 3_U1 4 1 4 SPARCstation 10 Sun 4m 4 1 3 4 1 3_U1 2 3 2 4 4 1 4 SPARCstation IPX Sun 4c 4 1 2 4 1 3 2 3 2 4 SPARCstation IPC 4 1 3 U1 4 1 4 SPARCstation ELC SPARCstation SLC SPARCstation 2 SPARCstation 1 SPARCstation 1 SPARCstation 330 Sun 4 4 1 1 4 1 2 Not Supported 4 1 3 SunOS 4 1 4 referred to as Solaris 1 1 2 requires a DMA compatible HAL 7 SunOS 4 1 3C referred to by Sun as Solaris1 1C only works with the SPARCclassic and LX i Using 4 1 3 on a Sun 4 requires building a new kernel and modifying the setacq program 30 UNITYplus Installation Planning Guide 87 195320 00 G0994 Computer Preparation purchase a computer from a source other than Varian or plan to use an existing computer
77. tt Packard QuietJet HP2227A sese 63 Hewlett Packard DeskJet 63 Hewlett Packard LaserJet III HP33449A i 63 Hewlett Packard LaserJet 4 63 IBM Lexmark Color Jetprinter PS 4079 sese 63 Hewlett Packard HP7475 HP74754A sss 64 Hewlett Packard HP7550 HP7550B see 64 Hewlett Packard DraftPro HP7570A sse 64 Terminal Compatibility ii 64 GraphOn 240 GO 240 i 64 Tektronix 4207 TEK 4207 sess 64 Computer Compatibility i 64 Sun SPARCsystem 600 MP series ii 64 Terminal Emulator Compatibility esent 65 Textlerm Graphics ete eren on cite 65 Versalerm 3Pro ideo ee etie ee tere 65 X Server Software Compatibility essere 65 CIO d 65 eXodlis Wed eet dete vete etie desee ei i 65 Appendix F Varian Sales and Service Centers eese 66 United States i eee e pete perde eet eite perdere edens 66 International eet ete E eere e eee Pea e eva eise ded 66 Index adest eaae amu ea 67 87 195320 00 G0994 UNITYplus Installation Planning Guide V vi List of Figures Figure 1 Plan views of floor contact points of magnet standS 6 Figure 2 Platform antivibration system leg placements and sizes
78. ug with a load connected that draws the same power as the spectrometer AC line frequency does not vary by more than 0 5 to 1 0 Hz The purchase of a line conditioner and regulator is strongly recommended By providing protection against transients and improving line regulation total system up time will improve and the electronic components within the system will last longer In many locations a good power conditioning system will pay for itself within a few years Contact a local power consultant for suitable equipment in your area Uninterrupted Power Supply UPS If your site experiences frequent and short less than 10 minutes power outages you may want to consider a UPS UPS systems are limited in how long they can supply power when house power is out Consider the placement of a UPS when planning your lab If you want to use one UPS it must have output for 208 Vac and 120 Vac and it must be placed such that both the NMR console and the host computer can use it Electrical Outlets Host Computer and Peripherals The host workstation and accessories require a minimum of six 120 Vac single phase power outlets Locations with ac voltages over 132 Vac should check with their local Varian service center for power outlet requirements Locations with ac voltages over 125 Vac might need at least one step down transformer To minimize ground loop interference these outlets should all be on the same 20 A service It is strongly recom
79. w a safety factor of at least 10096 above the weight shown The hoist can be a chain hoist suspended from a moveable mechanism such as an A frame or it can be permanently fixed above the area designated for the magnet such as a beam Consult your plant facilities department or authorized Varian representative to ensure that adequate facilities are available Isopropyl Alcohol and Acetone Systems with an Oxford Magnet Obtain 1 pint 500 cm each of isopropyl alcohol and acetone These solvents are needed to clean the magnet parts before assembly Cryogenic Equipment Rack Recommended Various items are used around the magnet for routine maintenance and handling These include helium transfer tube flutter tube Tygon tubing stingers and so on To protect the cryogenic equipment from damage and to keep it conveniently available provide a rack to hold the items A 1 2 m x 2 4 m 4 ft x 8 ft peg board hung on a laboratory wall with wood or plastic pegs works very well 28 UNIT Yplus Installation Planning Guide 87 195320 00 G0994 Installation Supplies and Equipment Electrical Power Surge Protector Recommended To protect the delicate electrical components of the computer system monitor disk drive unit CPU base etc a good quality surge protector should be inserted in the power circuit serving the components A single surge protector with six outlets will suffice if the components are located relatively close to one another
80. will allow the magnet to be transported in an upright position for all transport methods that will be used See Tables 1 through 3 for dimensions and weights of major system components Contact the shipping company locally about the service usually rendered If moving equipment will be required at the site obtain help from the plant facilities department or an outside moving service Sea freight or motor freight without air cushion suspension is not recommended for long distance delivery of systems 36 UNITYplus Installation Planning Guide 87 195320 00 G0994 Postdelivery Instructions Postdelivery Instructions When the system is delivered follow the instructions below to inspect for shipping damage before moving the crates Do not open any crate Inspecting for Shipping Damage CAUTION Do not open any crate except with direct instructions from an authorized Varian service representative In particular the crate containing the magnet has components that could be irreparably damaged if opened incorrectly When the shipment arrives make an immediate visual inspection of the outside of each crate for damage Take the following steps if any damage is found 1 Note the nature of the damage on the carrier s waybill 2 Request an inspection and written damage report by a representative of the carrier 3 Forward a copy of the damage report to the local Varian representative In case of damage the FOB block on the Varian Order Ack

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