confirm pesticide and environmental pollutants with confidence
Contents
1. 3 4 5 6 Pentachlorobiphenyl BZ 117 68194 11 6 15 2 3 4 5 6 Pentachlorobiphenyl BZ 121 56558 18 0 16 2 3 4 5 6 Pentachlorobiphenyl BZ 125 74472 39 2 JJJJJJJ J J77 EEF 17 2 3 4 5 Tetrachlorobiphenyl BZ 61 33284 53 6 Home 18 2 3 4 5 Tetrachlorobiphenyl BZ 63 74472 34 7 a at a R28 To review our full line of analyzers visit agilent com chem appkits Perform highly sensitive multi residue target analysis in complex matrices using these built in features Flexible comprehensive MRM Database contains over 1000 pesticides and pollutants and is optimized with up to 8 MRM transitions to minimize matrix interference It also includes a tool that makes it easy to build methods based on your own list Integrated Capillary Flow Technology CFT Boost your multi residue screening productivity with the Agilent Pesticide and Environmental Pollutant Analyzer 3 0 Top two transitions of Methamidophos 141 0 gt 95 0 l TT eee a eee 45 46 47 backflush promotes shorter analysis times lower chemical background longer column life and less frequent ion source cleaning to medium matrix interference overlapping peak gives incorrect ion ratio strong matrix interference overlapping peak gives inaccurate quantitation result improve uptime Multimode inlet MMI with large volume injection enhances trace level detection and adds flexibility by including hot or cold split s2. 300000 RT range of analytes 200000 4 296 min Initial run 4 72 psi 4 064 min Trim 1 meter 4 72 psi 4 297 min Relock 4 42 psi Auto RTL tuning following inlet or column maintenance enables your lab to start analyzing samples faster Reversing column flow using CFT backflush eliminates the need to bake columns at the end of the run to remove heavy materials CFT backflush also reduces system cycle time minimizes source cleaning and provides stable baselines and retention times for target analytes Cleaning out high boilers a real problem a 4e Run time gt 75 min A D to clean the column 100000 LAU 40 t 50 60 70 80 Oven ramps to 320 C to bake off late eluters Here CFT reduced the cycle time for target analytes in milk extract Choose from four fast configurations to meet your most complex analytical challenges Part No Backflush Method RunTime Dimensions Backflush G3445B 41 1 Flexible Constant Pressure CP 40 min 30 m column x 0 5 m restrictor Post column G3445B 415 Fast CP 20 min 15m column x 0 5 m restrictor Post column G3445B 412 Fast Constant Flow CF 20 min 15 m column x 15 m column Mid column G3445BH414 Selective CF 20 min 5 m column x 15 m column Mid column Configured with a 240 V GC oven to allow rapid temperature ramps for oven and inlet programs Bleed line Schematic diagram for the G3445B 415 Analyzer Constant pressure CP backflush methods are designed
3. 5 1 LowRes 0 1 0 572614108 Control Panel 95 enol 2 992 false LowRes 65 LowRes 0 1 0 211618257 Manage MRM Tables G9250AA_Database A 1 01 Micrd jichlorobenzene 1 2 3 249115827 false 146 LowRes 111 1 LowRes 0 1 1 Home Insert Page L Formulas a Review View MASSHUNTER REPORTING Developer chlorobenzene 3 2 3 249115827 false Waku ote oa eee erortForclAOndnber 50 chlorobenzene 1 2 3 249115827 false es aan ai 0 1 0 503750 prze 2 NI 3 398068884 false _ Ja a F HoN 72 lexachloroethane e 1 i b ae 3 398068884 false file for import 5 0 1 0 484693878 Create Quant method D MRM Table et aie cee id i 3 72 3 398068884 false 9 Lo to O u 0 1 0 3214285 fipboard Agana Eaa japhthalene 3 837 false 1 LowRes tes 1 jome owRes Yes lo fe Target japhthalene 3 837 false View Methods lt japhthalene 3 837 false 8 c E 92 i amidophos 3 920985396 false 1 Compound Name CAS a My Target Compound List 92 lethamidophos 3 920985396 false es 79 LowRes 0 1 0 733333333 3 920985396 false tes 64 LowRes 0 1 2 3 4 4 5 5 Hexachlorobiphenyl BZ 167 52663 72 6 arg 92 1 lethamidophos f 1 0 48 2 2 3 4 4 5 6 Hexachlorobiphenyl BZ 166 41411 63 6 ari Create New Target List 53 ugenol 4 503 false uaa eee E 0 1 1 3 2 3 4 4 5 6 Hexachlorobiphenyl BZ 168 59291 65 5 ar agen dee ase hiontas 5 Oe eoleee 4 2 3 4 4 5 Pentachlorobiphenyl BZ 114 74472 3
4. 7 0 ar Sai as ageno age a a S i 5 2 34 4 5 Pentachlorobiphenyl BZ 118 31508 00 6 ar vie AEM dle a T E EEE able gt ae a 6 2 3 4 4 5 Pentachlorobiphenyl BZ 123 65510 44 3 95 Trichlorophenol 2 4 5 4 553523315 false tes 0 1 0 643939394 G9250AA Version A 1 01 7 2 3 4 4 6 Pentachlorobiphenyl BZ 115 74472 38 1 Manage Target Lists 52 jiphent 4 667017646 false tes j 0 1 1 52 phen 4 667017646 false 1 LowRes ye 0 1 0 588548602 52 Biphen 4 667017646 false 155 1 LowRes to v 0 1 0 126498003 Add Compounds 34 inphos 4 844 false 127 LowRes os 0 1 1 z inphos aq 8 2 3 4 4 6 Pentachlorobiphenyl BZ 119 56558 17 9 4 844 false 127 LowRes owRes 0 1 0 385714286 9 2 3 4 4 Tetrachlorobiphenyl BZ 60 33025 41 1 ii 34 ii 4 844 false 192 LowRes O 0 1 0 385714286 Im Numbers _ pores 19 ephate 4 864231372 false 136 LowRes owRes 0 1 1 10 2 3 4 4 Tetrachlorobiphenyl BZ 66 32598 10 0 4 864231372 false 142 LowRes O 0 1 0 230769231 11 2 3 4 5 5 Pentachlorobiphenyl BZ 120 68194 12 7 ephate Build MRM Table 19 ephate 4 864231372 false 124 9 LowRes owRes 0 1 0 179487179 4934 91 lorme 4 93 false O owRes 0 1 1 91 1 ei 12 2 3 4 5 5 Pentachlorobiphenyl BZ 124 70424 70 3 4 93 false Ll tes owRes 0 1 0 335714286 35 24934 91 6 Chlormephos 4 93 false owRes owRes B 0 1 0 189285714 4 EEEE 13 2 3 4 5 6 Pentachlorobiphenyl BZ 116 18259 05 7 14 2
5. POLLUTANTS WITH CONFIDENCE The Mea sure of Confidence Guil Agilent Pesticide and Environmental Pollutan E Powered by superior technology these factory configured chemically tested analyzers put you on the fast track to measuring trace contaminants in complex matrices Concern about trace level food and environmental pollutants is driving the demand for rapid reliable identification of chemical residues Meeting this challenge requires the fast deployment of technologies that can differentiate pesticides PAHs and other targets from organic interferences Agilent s Pesticide and Environmental Pollutant Analyzer 3 0 lets you accurately confirm target pesticides while reducing the time required from start up to results It combines the leading edge innovations of Agilent s 890B GC and 7000C Series Triple Quadrupole GC MS with a comprehensive MRM database to transform your results trom acceptable to exceptional Customize to get you on the FAST TRACK The system includes the following components that save time and maximize performance e 1000 compound MRM database with 8000 optimized transitions e Graphical User Interface GUI that facilitates the building of target compound lists and MassHunter acquisition and quantitation methods e Retention Time Locked RTL method that provides reliable peak identification and quantitation e Che
6. ckout sample for field verification of chromatographic performance e Capillary Flow Technology CFT and backtlush for faster cycle time and reduced maintenance e Quick start guide that allows you to quickly utilize Agilent s advanced technologies and get outstanding analytical results immediately after installation e CD ROM with system specific methods checkout data files and user manual oe Agilent Technologies Technology innovations deliver superior analytical performance Consistent retention times Automated Retention Time Locking Auto RTL Reliable target identification requires the precise matching of retention times RTs to database indices Auto RTL precisely matches RTs from column to column instrument to instrument and lab to lab for methods that have the same nominal parameters Using five 5 calibration runs Auto RTL automatically adjusts column flow for constant pressure and constant flow backflush methods so you can be sure that retention times match your original analytical method Remove heavy sample components Capillary Flow Technology CFT Backflush Injecting heavy matrix samples can place high boiling compounds at the head of the column Such materials can move slowly through the column and elute during subsequent runs causing analyte interferences They can also build up near the column head which degrades chromatographic performance and increases the need for tedious column trimming 400000
7. for simplicity and ease of use 15 m Column Restrictor or a splitter Bleed line Schematic diagram for the G3445B 414 Analyzer Constant flow CF backflush methods offer the highest sensitivity for trace pesticide multi residue analysis 5 m Column 15 m Column or a splitter Powerful software tools simplify the creation of compound lists and analytical methods When developing acquisition and quantitation methods you must In addition a new Graphical User Interface GUI guides you through build a target list that includes retention times and MRM transition the creation of methods for your specific analysis You can then use data for specific compounds The MRM Database simplifies this MassHunter s Compound List Assistant to optimize time segments and process by providing retention times and transition data for more than dwell times 1000 compounds User friendly menus help you build a target compound list Quickly create MassHunter Acquisition and Quantitation methods G9250AA_DatabaseA x id 9 X G9250AA_Database A 1 01 Microsoft Excel Developer ert Pagelayout Formulas Data Review View MASSHUNTER REPORTING Developer j Normal 2 Normal 3 Normal_Sheet1 3 Sann u As v E wrap Text General H EET F BE EB PH Bmergeacener WS onditional 1 For Q Master MRM Table Agilent Technologies MRM Database je 2 992 false owRes 66 1 LowRes 0 1 Save MRM Table 95 je 2 992 false owRes 6
8. plitless capabilities Superior GC MS MS selectivity and sensitivity eliminates false results and simplifies data review for improved productivity Productivity tools to help you make the most out of every analysis Agilent autotune batch at a glance data review and parameter less integrator streamline your data review and processing Put your lab on the productivity fast track Contact your local Agilent Representative or Agilent Authorized Distributor Call 800 227 9770 in the U S or Canada or visit agilent com chem appkits This information is subject to change without notice Agilent Technologies Inc 2014 Printed in U S A October 15 2014 5990 6045EN Orange Pear Two alternative transitions of Methamidophos i l 95 0 gt 64 0 i l l WDS ee 4 5 4 6 4 7 45 46 47 minimum matrix interference minimum matrix interference The G9250AA database has up to 8 transitions for each compound This allows the user to choose alternative transitions to minimize matrix interferences and improve quantitation results Ordering information Choose one of the following options when you order an Agilent 7000C Series Triple Quadrupole GC MS with an Agilent 7890B GC analyzer system Flexibility driven setup e G3445B 411 40 minute run 30 m column x 0 5 m restrictor post column backflush e G3445B 415 20 minute run 15 m column x 0 5 m restrictor pos
9. t column backflush Performance driven setup e G3445B 412 20 minute run 15 m column x 15 m column mid column backflush e G3445B 414 20 minute run 5 m column x 15 m column mid column backflush For customers who already own an Agilent GC MS MS system e G9250AA rev A 1 01 Pesticides and Environmental Pollutants MRM database with Graphical User Interface Agilent also offers Single Quadrupole GC MSD pesticide analyzers for broad screening at D to 100 ppb Each is equipped with CFT Backflush Deconvolution Reporting Software and RTL Pesticide and Endocrine Disruptor library Go to agilent com chem library brochure 5990 5310EN for details g Agilent Technologies
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