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USER`S MANUAL - California Analytical Instruments, Inc.

1. 5 10 Shut off ALL gas flow Remove power from the instrument Remove the top cover retaining screws Remove all 4 tubes from the 4 way cross Remove the 4 screws securing the photodiode and reaction chamber from the oven Remove the photodiode electrical connector from the main circuit board Remove the chiller connection from the photodiode reaction chamber Separate the photodiode and heat sink assembly from the reaction chamber by removing the 4 Allen screws from the front of the heat sink Save the 2 black rubber O rings Separate the mounting plate and the glass filter from the reaction chamber Save the 2 Teflon spacers and O ring Separate the manifold from the gold reaction chamber NOTE the position of the holes in the Teflon gasket relative to the assembly screw holes The large hole is ozone 11 2 Assembly Procedure 1 Wash the reaction chamber glass filter and manifold separately in detergent using a test tube brush Be careful of the sample tube in the manifold Do not use abrasives 2 Dry by blowing clean with dry nitrogen 3 Reassemble the chamber assembly in reverse order per the above Make certain the sample tube is centered when assembling the manifold to the reaction chamber California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 66 of 86 Section 12 Model 650 Noxygen Analyzer 12 Troubleshooting 12 1 Ozone Air O Supply The Air O2
2. Note For Analyzers Sold After June 2007 Please See Addendum Starting After Page 86 of This Manual CAL Sa aye ay 1312 West Ene Avenue Orange CA 92865 4134 Phone 714 974 5560 Fax 714 921 2531 www gasanalyzers com Section 1 Model 650 Noxygen Analyzer 650 Quick Start Guide Plug in the analyzer and turn the power on 2 Connect the appropriate gas lines and vents to the analyzer Allow the analyzer to stabilize for at least one 1 hour During the analyzer s stabilization period setup the analyzer to the desired configuration a Set the analyzer s output as desired i From the Main Menu press F5 Setup then F7 System Settings i Press F3 output assignments to setup the output channels 1 Set to real time 2 Set channel 2 to NO 3 Set channel 3 to NO 4 Set channel 4 to O2 5 Press back to return to the system settings menu iii Press F4 output range to setup the output ranges 1 Set the Min and Max to zero 0 This will cause the outputs to default to the analyzer ranges 2 Set the outputs for milliamps mA or voltage V as desired a The mA setting will give 4 20 mA or 2 10V if 500 ohm resisters are installed b The V setting will give 0 20mA or 0 10V if 500 ohm resistors are installed 5 Connect all appropriate analog outputs a Pin 1 is the output common ground b Pins 2 3 4 and 5 are output channels 1 2 3 and 4 as setup in step 4 a
3. Haro Koo 47 Han H Dor 11 Figure 7 28 Span gas deviations Figure 7 29 Span gas deviations verifying 7 7 4 Relative Span Gas Deviation Relative span gas deviation is the actual deviation minus the deviation of the previous calibration related to the range limit of the calibrated range California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 34 of 86 Section 7 Model 650 Noxygen Analyzer 1 1 5 F4 Check Calibration Auto calib Cal Check 0 01 Mode HO Span Zero rangel purging Time 65 Hon Hoy 147 12 22 52 Figure 7 30 F4 Check calibration Figure 7 31 Check Calibration There is a default calibration Pressing F4 activates an automatic zero and span check for verification Def cal value Figure 7 32 F5 Reset calibration values Figure 7 33 Reset calibration values There is a default calibration Pressing F5 a new screen appears and asks if the user is sure to reset calibration values to the default calibration values F1 confirms and the calibration values are reset to default calibration values F2 leaves this menu without resetting to default values This function will overwrite all calibrations with factory values Also the linearization polynom will be overwritten with the factory values Lill F6 Range Select This allows a range change to be activated from the calibration menu Actual Rangel Figure 7 34 Range Select Figure 7 35 Range California Analytic
4. 18 Sample Pump If the analyzer is supplied with the optional internal sample pump itis always on in the measure mode It is turned off during calibration and may be manually turned off by putting the analyzer in standby 19 Sample Line Make certain the sample line is flushed before connecting to the analyzer sample inlet California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 59 of 86 Section 9 20 21 22 23 24 Model 650 Noxygen Analyzer Instrument Power Turn instrument power on and allow the reaction chamber and NO converter to stabilize before turning on the sample pump and or connecting the sample line Sampling System Prepare and check the sample system Check the sample pressure as indicated in the factory settings screen Air or O2 Pressure Check the Air O pressure for proper setting as indicated in the factory setting screen Readjust internal pressure as required Note Cylinder pressure should be set at 25 PSIG Zero amp Span Calibration Zero and span adjustment should be checked every 24 hours by either manual or automatic calibrations Reaction Chamber Assembly Dust water droplets or mist entering the reaction chamber assembly may cause drift due to contamination If the calibration procedure fails to bring the instrument to zero check the chamber for contamination 9 3 Shut Down Procedure 1 Turn off the zero span and air O2 cylinders 2 If t
5. California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 23 of 86 Section 5 Model 650 Noxygen Analyzer 5 1 The Main Menu Upon power up the CAI logo is first displayed and then the main menu appears as below NOTE Access Level Indication Diaanostics Setup Standby Figure 5 1 Main Menu on Power Up Screen NOTE F6 is not available because on initial start up the analyzer reverts to ONLY Level 1 access See Section 7 5 12 for setting Password information All functions can be selected with the cursor keys and activated by pressing the Enter key or directly with the function keys F1 through F7 A gt to the right of a function means that one or more sub menus are available If this sign is missing the function starts immediately after the activation NOTE Access level is 4 NOTE Access Level Indication Figure 5 2 Main User Menu Level 4 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 24 of 86 Section 6 Model 650 Noxygen Analyzer 6 Menu Structure There are 4 operating levels based on the level of your password This section shows the access rights of the single levels 6 1 User Functions Level 1 Main Menu SetpMenu Password Menu F5 Password F1 Enter password F10 Version i E F4 Calibrations ss FS Setup F7 Standb AA 6 2 Advanced User Functions Level 2 Main Menu SetupMenu HPasswordMenu_ F2 P
6. OgOppm Rangel 1 Fl Save valve E Fi Save value NOx 0 0 Fi Man Cal Mene 02 F2 Han Cal Menu 02 8 8 Z a CAI Tel 800 959 0959 Iz 2 versions opan Gas will be enabled and the observed results can be used to evaluate instrument performance Press F3 to toggle to the Diagnostic screen for additional information Press F1 to save the new value and complete the SPAN calibration for this Range Note The span gas value used for this range is highlighted and can be changed if necessary Use the Enter key and the numeric keys as required Press MAIN F1 to return to the MEASUREMENT screen to select other ranges and repeat the process or press F2 to return to the Manual Calibration screen California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 4 of 24 ADDENDUM 2 5 Range Limits F8 From the MEASUREMENT Screen CAI Tel 800 959 0959 2 versions The standard analyzer is factory configured with 4 Physical Ranges of 3 30 300 3 000 PPM The optional high level analyzer is factory configured with 4 Physical Ranges of 5 50 500 500 The operator can change the number of ranges and select a more convenient full scale concentration if required Note Do not exceed the maximum range set by the factory and always use ascending order as shown Example a For a single range instrument set Range to the desired value and all others to zero b For a two range instruments set Range
7. P M hhl x Ty 2 X Env LA wt a mg x ey a El i AE Figure 7 63 Set Autocalibration Cal Timing Figure 7 62 Select autocalibration time California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 44 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 20 F3 Set Auto Cal Ranges Figure 7 64 Clock and Timing Setup Screen 7 8 21 F4 Autocalibration on off ML Figure 7 65 F4 Toggles Auto Cal ON of OFF 7 8 22 Auto calibration Displays system time and status of autocalibration Figure 7 66 Autocalibration Status California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 45 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 23 F2 Displays TCP IP Address Figure 7 67 TCP IP Address 7 8 24 F3 Displays Output Signal Assignments Used to Adjust Analog Output Channels Figure 7 68 Output Assignments F4 Displays Output Ranges Used to Adjust Scale of Analog Output Channels 166 20 Figure 7 69 Output Ranges California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Operators Manual Page 46 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 26 F5 Turns Status Line On or Off The status line displays the AK Protocol action on the top line of the display Status Line Figure 7 70 Status Line 7 8 27 F8 Measure Settings This screen allows several of the system settings to be displayed and modified Figure 7 71 Menu Settin
8. The maximum length of measuring time is 9 seconds If the measured value was constant during calibration time it is checked to determine if this value deviates from the preceding value If the deviations are too large a warning Deviation error appears and the user can choose if the new value is saved or not At last the zero gas is flown a further time verifying time so it can be checked if the signal is still constant All of these times can be changed After zero gas calibration the same happens with span gas During auto calibration Calibration in progress is displayed It also shows which gas is flowing and which time runs When auto calibration has finished it is displayed If the span value of the selected range is O see section 5 6 1 then it will not be calibrated If one range is calibrated and the span value for the lower ranges is zero calibration parameters will be copied to this range To calibrate all ranges with the same span gas you must enter the gas concentration in the Span Gas Calibration screen for ALL RANGES You must also calibrate each range Offsets and scalars are NOT copied to other ranges Calibration in progress sd c pg Mode H Span Zero rangel purging Figure 7 13 Auto Calibration Screen California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 30 of 86 Section 7 Model 650 Noxygen Analyzer 7 6 2 F2 Manual Calibration 8 zc D m Bg all Fig
9. are present in the sampled gas 3 8 4 Gas Temperature When measuring high temperature gases take care that the maximum rating of the instrument 104 F 50 C is not exceeded 3 8 5 Pressure and Flow Rates The air or oxygen supply entering the instrument is controlled by an electronically controlled proportional flow EPC controller The regulator is factory adjusted for optimum analyzer performance The ozone supply Air or Os air cylinder pressure should be set at approximately 25 PSIG The sample entering the instrument is controlled by a factory set precision electronically controlled proportional flow EPC controller The EPC is factory set for optimum analyzer performance as indicated by the sample pressure If the analyzer does not contain the optional internal sample pump the sample gas entering the instrument should be at a pressure between 10 and 25 PSIG with a flow capacity at a minimum of 3 liters min If the analyzer contains the optional sample pump do not apply a pressurized sample The optional pump is capable of drawing a sample through a 4 inch heated sample line of approximately 75 feet The calibration span gas cylinder pressures should be set at 25 PSIG for delivery into the optional zero and span inlets located on the rear panel NOTE If the analyzer contains an optional internal sample pump the introduction of a pressurized sample gas in excess of 1 5 PSIG will damage the pump 3 8 6 Sample Gas Bypass Outl
10. press F5 Note For instruments with an internal Zero Solenoid select Calibration by Valves Main F5 F2 F4 Manual Zero 4 SENO B Manual zero 3 SMAH ll Zero gas Use F3 to Toggle ero gas Use F3 To Toggle Diagnostics Cal Wia Diagnostics Cal ia xliazina Current Temp amp Press 375 00 Ho H x R i 100 0 Ranae4 3000ppm ange PPM em E ee O 1 an al enu 02 BH jJ 7 rd a a Thu May 15 06 15 11 2008 l HO an La z Check Air EPC Coil VW 2 versions Zero Gas will be enabled and the observed results can be used to evaluate instrument performance Press F3 to toggle to the Diagnostic screen for additional information Press F1 to save the value and complete a ZERO calibration for this channel and range Press MAIN F1 to return to the MEASUREMENT screen to select other channels and ranges and repeat the process Or press F2 to return to the Manual Calibration Screen California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 3 of 24 ADDENDUM 2 4 Span From the MEASUREMENT Screen select the required range then press F6 Note For instruments with an Internal Span Solenoid select Calibration by Valves Main F5 F2 F4 Manual Span 3 SHET lEl Manual Span a2 SHET Z iran ga Use ES 5 Toggle Span gas Use F3 To Toggle iagnostics Ca Diagnostics Cal_Wia 3 7 m 0 0 lsing Current Temp amp Press Conc 0 0 0 T H Ox s Range4 S
11. s PEME 18A E ES FEN E ous wee ASER gt Ee ee C MOTOTS a EEN AE ouo s MOTOS D 3LOW38 8 EE E Oo 0t 10s 3LOVisu S 3oNvHOLnv B ae E 3oNvMOLDY S sos 6198 SONVHOLNY S 9 C a SVE NVdS 27108 OS PSONVHS gt svo 33d ECCE sos Os 3ONVM S x SYS ONSZ E m svo ouaz Sg fas las 23ONVHS y E v las v ids ISONvH S O E PIONVETS E AA Z UE auum b CE Ives ho MEUS ARE ne Qe pe 2 3 LC revive caera itl Wavy Lo M HN EO SVO NYdS CO LOG zo us 3ONYN SvO Ths vs SV dus e SL das 3ONVM SVO OYaZ D ES p PL dHS ZION VE S ono L das p EL des n y ON 2 O Lan 2 Zi Jus L GS FAVA YILYJANOS HATVA HILNZANOD LIM 2 Nds 2 be ade LL AS BATWA MOTJNSAO 4 AHATVACAMOd4udAO NVdS 2 O OM3Z 2 Di das Ol d8S JAWA ANO LIM 3ATVA AMO LEM Ouaz 2 voolnv 2 6 das We S dus 2 TWIOLNY_S gt O driind 2 gas b S das 8 O08 dnd 3 MOTO 5 idus d dus 4 O08 E MCOTS0 2 a O BONYYOLTY O 8 dts ba das goas 8 005 FONVHOLNY_O O WO gt 5_d88 p S dis 008 s ods Tw2 23 a PSION O EE Rr das v ods 008 TJONVM 2 O 3ONVH I das das E OUS S 008 PUONVM 2 O ZHONYE_O z das amp das 27008 P zons ZJ NYH O L3oNvM 7o das das 005 ee et Logs igoNvM O I d O OL TSNVOSNOVE Or osi OlHOSS32OHd S r i z E F 5 T Oz ADDENDUM TABLE OF CONTENTS ADDENDUM STARTING AFTER JUNE 2007 Section Title Page 1 0 IIE OGUICTION Rr C EE 2 0 Operation of Measurement Keys 2 1 OVE RANJE adaise a A EE LEO Aio E M C CE 24 Spansion 2 9 RANJE
12. to the lowest value Range 2 to the highest value and the others to zero 2 6 Span Values F9 From the MEASUREMENT Screen 1 SARA Use to define the concentration of the span gas that will be used to calibrate each range Note The span gas value used for this range is highlighted and can be changed if necessary Use the Enter key and the numeric keys as required California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 5 of 24 ADDENDUM 2 7 Outputs F10 From the MEASUREMENT Screen assignment C I Tel 800 959 0959 Use the 7 to select the desired Output Press Enter to select Use the 7 to select the desired Signal Press Enter to select Use this screen to define the signals and their location that will be monitored by a remote reordering device Note NO only active in the Switching Mode SEE TABLE D California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 6 of 24 ADDENDUM 3 0 NEW FUNCTIONS 3 1 Auto Start Up Main F5 F7 F7 Auto Startup 5 SHET El Auto Startup Off Wait for min l Calibrations 2 Startrange 4 Access Level I H Remote Manual anual HO HOx MHMode H O MAIN SAVE Hx 22 5 BACK SAVE Cheek Air Pressure Fr All key analyzer parameters are stored in a secure memory location and retained when power is removed In the event of an unexpected power failure it may be desirable to change
13. with the up and down cursor keys or entered directly Every input has to be concluded by pressing the Enter key again Then the input cursor disappears and a new range can be selected The changes are saved by leaving the screen by pressing Main or Back At the right side of the screen the range limits of the 4 ranges are displayed They cannot be changed in this screen Figure 7 39 Change span gas settings 7 8 2 F2 Calibration Settings In the calibration settings menu times deviations and methods can be changed CASE cali Hon How 17 12 32 99 zu Figure 7 40 Change Auto Calibration Settings California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 37 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 3 F1 Times There are four times in seconds for auto calibration that can be changed Purge measuring calibration and verifying time Changes are made and saved as above Figure 7 41 Setup times 7 8 4 F2 Measuring Deviations During auto calibration the measured value is only saved if it is within a certain time within an upper and a lower limit These two limits format a working window In the setup menu the deviation is in percent Figure 7 42 Measuring deviations 7 8 5 F3 Deviations Here you can change absolute and relative deviation in percent After auto calibration it is checked to assure the deviations are within this limit If the deviations are not in this limi
14. 4 F5 Auto range Manual Calibration F1 Flow zero gas F2 Flow span gas F3 Range select Display Deviations F1 Zero gas deviations F2 Span gas deviations F3 Zero gas deviations verify F4 Span gas deviations verify Check Calibration Reset calibration values Range select V Y Y NN y California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 20 of 86 Section 4 Model 650 Noxygen Analyzer Main Menu All access Setup All access F1 Span gas concentrations F2 Calibrations settings F3 Range limits F1 Measurement F2 Purge Analyzer F3 Diagnostics F4 Calibration F5 Setup F6 Remote Manual F7 Stand by F4 Alarms F5 Password F6 Linearization F7 System settings F8 Measure settings F10 Displays version Span gas concentrations Calibration settings F1 Times F2 Measuring deviations 96 F3 Deviation 96 F4 Calibration via values F5 Calibration via pump Range limits F1 Range 1 4 F2 Autorange Alarms Ill m Password Factory default vallues F1 Standard user F1 Standard user 111 F2 Extended user F2 Extended user 222 F3 Mainenance F3 Mainenance 333 F4 System operator F4 System operator 444 Systems settings Measure settings Displays version WJ NY NS NL YYY y y California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 21 of 86 Section 4 Model 650 Noxygen Analyzer 4 3 Keyboard _ Combined control numeral key
15. 5 coefficients can be changed for each range By pressing F2 the raw value can be displayed This is the value before linearization and offset span correction There are two values on the screen The value at the top is the linearized offset span corrected value and the other value is the raw value lal EE E E B Fl d i 3 JU Dra E a 2r Figure 7 56 Linearization Coefficients Figure 7 57 Range Raw Data with F2 7 8 17 F7 System Settings This screen allows all the system settings to be displayed and modified centrations tinas oe THT TY TY TI FEA Figure 7 58 system settings Figure 7 59 System Setup Screen California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 43 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 18 F1 Real Time Clock This brings up the clock time set screen auto cal and auto cal enable screens T Ld as E Mon How 17 xL Figure 7 60 Clock and Timing Setup Screen Figure 7 61 Set Clock Screen F1 brings up the clock set screen The current time may be set by using the cursor to highlight the entry and using the numeric keys to change the values 7 8 19 F2 Set autocalibration time F2 brings up the autocalibration time set As above the date and times can be set by using the cursor to highlight the entry and using the numeric keys to change the values pU I pm m E qeu Qm QV IET E d m d a Lar og ar ELI rant In EA EI i F F
16. ASYZ Respond System Time Command Response _ASYZ_KO_ AT90 Respond Lowpass filter time Command Response _AT90_KO_ _AT90 s t ADAL Diagnostic alarm limits Command Response _ADAL KO _ADAL s alf min_a1 max_ f12 max _ ADAL KO x _ADAL s x min x max Alarm Limits Air Pressure ASYZ s yymmdd hhmmss Description Respond system time yymmdd year month day each 2 characters wide no spaces hhmmss hour minutes seconds Description Respond lowpass filter time t filter time in seconds Description All alarms are responded Alarm limits of x Peltier Gas Temp Sample Pressure Cell Temp Oven Temp 2 3 4 Converter Temp 5 Diode Temp ATCP Query TCP IP settings Command Response ATCP KO ATCP s Zzz zzz Zzzz ZZZ ATCP s yyy yyy yyy yyy ATCP s xxxx AENT Query calibration gas flow setting Command Response _AENT_KO AENT s x California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc LN EPC Coil Sample Voltage EPC Coil Air Ozone Voltage Pump Temp Reserved Sample Content Description zzz TCP IP Address yyy TCP IP subnet mask xxxx TCP IP port Description x 10 Calibration through sample gas inlet pump y 11 Calibration through zero span valves Operators Manual Page 75 of 86 Section 13 Model 650 Noxygen Analyzer 13 5 Control commands SRES Command _SRES KO SPAU Command _SPAU_KO STBY Command _STBY_KO SNGA Command _SNGA_KO _SNGA_KO_Mn SEGA Comm
17. Calibration Settings sae rene rhe na e n oa er E Seo n depu t educi ue ttu d aoa e do aut 37 7 8 3 Fed II Srta dere otura ieee dhanh a 38 7 8 4 F2 Measuring Deviations savers prod pei tens Mier ae AA 38 7 8 5 ES IDS em 38 7 8 6 F4 Calibrations via Solenoids occcccccccccooccnnccnnnnccnonononncnnnnnnonnnnncnnnnnnnonnnannnnnnnnnnnnnnnns 39 7 8 7 E5 Galibrallom vid PIODG estaa ads 39 7 8 8 FS Range Brice 39 7 8 9 F1 Range 1 4 Change Upper Range LimMitS ooccccccccocccnnccccnoncnnnoconononnnnonnnnns 40 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 4 of 86 Section 1 Model 650 Noxygen Analyzer 7 8 10 F2 Change Auto Range Limits osse nnne nnns 40 7 8 11 AAA mA a a aaae e ada aieeaa aae ieoa 41 7 8 12 SSW eire uM C c URS 41 7 8 13 F1 Enter PASSWOlG initial ida 42 7 8 14 FZ Grange PASS WON s 2 252 022 0 9 22929 39559 0 corra elote oda Lien ao coder 42 7 8 15 FS Rese Passwords ui 42 7 8 16 ENS anZza ON a a 43 7 8 17 HAIR 43 7 8 18 a o e 44 7 8 19 FZ oeralitocallbrattem UNS sta llor 44 7 8 20 ES Ser Aulo Gal Rang OS el 45 7 8 21 F4 Autocalibration on off occccccoconncnnccononncononononnnnnonononnnnononanrnnnononanrnnnnnnnanrnnncnnnanenns 45 7 8 22 PAULO CANO AUIO dE ODE 45 7 8 23 E2 Displays TOP Address A ee eee 46 7 8 24 F3 Displays Output Signal ASSIGNMenNTS oooccccnncccccccconccnnncconononnnnnnnnnnononanennnnnnonn
18. Description Set converter off Only NO is measured Description Set converter on All kinds of NO are measured Description Activates dual measure mode Analyzer switches periodically between NO and NO mode and displays NO NO2 NO SFGR Reset calibration settings to factory default Converter on Command Response _SFGR_KO _SFGR_s SENT Set calibration gas flow Command Response _SENT_KO_x SENT s California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Description Reset all calibration settings to their factory settings Description x 10 Calibration through sample gas inlet pump y 11 Calibration through zero span valves Operators Manual Page 78 of 86 Section 13 Model 650 Noxygen Analyzer 13 6 Settings EKAK The four span gas concentration values are set Command Response Description EKAK_ KO M1 w w M2 x x M3 yy M4 zz EKAKSs Set end gas values EMBE The four measuring range end values are set Command Response Description EMBE KO EMBE s Set range limits M1 w w M2 x x M3 y y M4 z z EMBU The upper and the lower range switchover for autorange are set Command Response Description EMBU KO M1 w w W W M2 xx X X M3 EMBU s Set lower and upper range yy Y Y MA zz ZZ switchover limits EKEN Set new device identification Command Response Description _EKEN_KO_new device name EKEN s Set new device identification Maximum length of device name are 40 characters NOTE To change de
19. OFFSETS amp GAINS to zero and 1 respectively 3 4 Calibrate the Analog Outputs Main F5 F7 F8 D A Calibration Main F5 F7 F3 Output Assignment e Overview The 600 CLD Series is designed to provide four analog outputs that can be configured as 0 1 VDC 0 5 VDC 0 10 VDC 4 20 mA or 0 20 mA This screen Main F5 F7 F8 is used to select the scaling of the current mA or voltage 1 5 10 range that is required by a remote recording device The outputs can be calibrated to exactly match the results obtained on a PLC Recorder Data Logger or other remote recording device that may be connected to the analyzer The operator will first select the OUTPUT ASSIGNMENT Main F5 F7 F3 screen and choose the output that is set to be calibrated By selecting calibrate as the output all outputs of interest may be selected When calibration is competed the operator will return the outputs to their original assignment California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 9 of 24 ADDENDUM The D A CALIBRATION screen will then be used to complete the calibration procedure This screen provides a section that is used to record the zero signal corrections zero offset and a second area to record the 100 signal corrections Gain for each of the four output signals that may be defined to develop a voltage or current signal Since this is a Digital to Analog conversion the calibration will r
20. R3 O BYPASS MENU 650 NOXYGEN FLOW DIAGRAM Figure 14 1 Standard Analyzer California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 82 of 86 Section 14 Model 650 Noxygen Analyzer l Fi PRI 47 EPCV2 R5 Tm 5 Tq la RI QD a l l l MF1 ayo SAMPLEQ Oo 6 lt SVI WA sv2 VCV1 NOx Zero Q d F3 CONVERTER O R6 SV3 7 SpanE gt D 02 R K R3 R2 BYPASS o o Oe 650 NOXYGEN FLOW DIAGRAM W ZERO SPAN S V Figure 14 2 Standard Analyzer with Optional Zero Span Solenoids California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 83 of 86 Section 14 Model 650 Noxygen Analyzer MEM C C C PR1 J A 27 EPCV2 5 AS EXHAUST Ma CRI ES en MF1 P1 SU SAMPLE E lt WA NOx R6 02 R4x R3ok R2 BYPASS o PP M SO 650 NOXYGEN FLOW DIAGRAM W PUMP Figure 14 3 Standard Analyzer with Optional Sample Pump California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 84 of 86 Section 14 Model 650 Noxygen Analyzer a OZONE AS aro EXHAUST C R1 SVI M ZERO o lt CONVERTER E H6 F3 ie d gt lt i R49 R3I R2 dc BYPASS PP
21. are calculated for zero and for span gas A T T ES 2 E SHE 1 F1 shows zero gas deviations Display deus 3 SHET 2 F2shows span gas deviations 3 F3 Deviations of zero gas during verifying 4 F4 Deviations of span gas during verifying Figure 7 25 Display deviations screen F1 and F2 deviations are displayed in percent During calibration there is verification for zero and span gas With option F3 and F4 you can view the deviations during the verification time Absolute deviation is the absolute average difference from the saved value in ppm Relative deviation is the absolute average difference in percent related to the range limit California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 33 of 86 Section 7 Model 650 Noxygen Analyzer 7 7 1 Absolute Zero Gas Deviation Absolute zero gas deviation is zero gas content calculated by the factory polynom related to the range limit of the calibrated range SSeS Man How 1r Figure 7 26 Zero gas deviations Figure 7 27 Zero gas deviations verifying 7 1 2 Relative Zero Gas Deviation Relative zero gas deviation is the actual deviation minus the deviation of the previous calibration related to the range limit of the calibrated range 7 7 3 Absolute Span Gas Deviation Absolute span gas deviation is span gas bottle value minus span gas value calculated by the factory polynom related to the range limit of the calibrated range
22. bImlls seseesetesesteepe AA HOUSED MEME 2 0 SPAN NAUES nn eee ea ee eee ane aes ARRE 2 1 QUISO 3 0 New Functions ST AMO StA UNA E 9 2 Ala ms ON Oil Ss 2s pt A SANG A MAI A 9 4 Calibrate The Analog QUIDUIS at esa inan anto ee eet eene ere RASO 9 9 Dave Dala Archiving TME anno E TABLE EE 3 0 User Digital QUIDUIS eei A A ES TABLE Da PR AP EPA REA IO dea TABLE O ee uei eee dee Beis Call Analog OUUTE 4 0 Changes To Existing Functions MMM Al Saved or QOUISIGe LIImits sports RE RO 4 2 Calibration Deviations eere seo Ra ponere Por RO c eene eee 4 9 FOW Zero or opan GaS A eE p ee AS peus aciu seduce 4 4 Reset Calibration Valles e TABLE tU eO a EU Ie Eee I d Ee HERR California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 1 of 24 ADDENDUM 13 5 Starting With SERIAL NUMBER UOG6081 1 0 INTRODUCTION The Model 600 CLD Series Instruments starting with Serial Number U06081 have several new Hardware and Software features The Hardware includes the use of a new memory system isolation of the analog output signals and 15 relays that are used to buffer the many new digital output signals that are now available SEE TABLE D The available digital signals consist of a SERVICE group to externally monitor a number of parameters that provide insight for preventative
23. ii c If the output is set for voltages but there is no voltage output you will need to install a 500 ohm resistor between pin 1 and the channel you are trying to measure You will have to measure the voltage drop across this resistor 6 Press F1 from the analyzer s main Menu to get to the measurement screen a The individual NO NO and NO channels only work while measuring in dual mode Real time and O output continuously b Press F2 while in the measurement screen to get to dual measurement mode 7 Supply sample gas to the analyzer 8 The measurement screen should indicate the concentration of the sample gas If the concentration is incorrect the analyzer will need to be Zeroed and Spanned using your calibration gases Please reference the appropriate section of the manual for a description on how to zero and span the analyzer California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 2 of 86 Section 1 Model 650 Noxygen Analyzer TABLE OF CONTENTS LP INTOdUCUON etn 10 INEO UU I EE 10 iz WNP ACKING INSUUCTONS e ee e RT 10 iss Li leeeaedB iN iei ID ds 10 L4 Oontacb IMM 10 ko AWarranty Gerllll ale ias 11 La FO c 12 a A A TUI TENENTEM 12 Cree E AAPP bpm IM La RM MUR M LTEM 12 2 3 Model 650 CLD Paramagnetic Specifications oocccccoconccnnoconcnncononennconononnnonane
24. maintenance and diagnostics decisions A second STATUS group is provided to define the operation of the instrument such as Spanning Zeroing Calibrating and the Current Range 1 2 3 4 AUTO The Software includes modifications to existing functions changes to the Measurement screen additional Short Cut Keys and several New Functions that are listed as follows e MEASUREMENT Over Range 888888 Zero F5 Span F6 Range Limits F8 Span Values F9 Outputs F10 Note The operator can use these Short Cut Keys or continue to use existing procedures e NEW FUNCTIONS Auto Startup F5 F7 F7 ALARMS F5 F7 Use F6 to toggle ON OFF Offsets amp Gains F4 F3 F5 D A Calibration F5 F7 F8 Cal Analog Outputs F5 F8 Use F8 to toggle ON OFF Save Data Archiving Time F5 F7 F1 F5 Use ENTER to change record time User Digital Outputs F5 F9 e MODIFICATIONS Saved Not good F4 F2 F1 or F2 To flow Zero or Span Gas California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 2 of 24 ADDENDUM 2 0 OPERATION OF MEASUREMENT KEYS Note The amp Keys continue to be used to view a complete list of menu items 2 1 Over Range 888888 In the MEASUREMENT mode only any value that exceeds the range by more than10 will be displayed as 888888 2 2 Diagnostics Use F3 to toggle between MEASUREMENT and DIAGNOSTIC 2 3 Zero From the MEASUREMENT Screen select the required range for calibration then
25. may be used to establish several desirable special instrument start up parameters that define how the analyzer recovers from loss of AC power When enabled this screen will define the following n a Al arms NOx 43 7 Use F6 to toggle ON OFF The instrument has an extensive library of warning messages that will aid in the identification of various anomalous events and are displayed at the bottom of the screen These messages will assist in diagnostics and indicating the need for preventative maintenance This screen provides an option to disable these messages during initial start up or as may be desired for a particular application California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 8 of 24 ADDENDUM 3 3 Offset amp Gain Main F4 F3 F5 Offset and Gain B zero Span applied correction R Boe 1 Br angel a a Bandes 8 86 1 30 Rangest 0 00 1 00 Ranges O OO 1 00 Thu Ha 03 12 40 03 2007 F This screen can be used to provide an additional means to display calibration deviations The OFFSET is the value stored during zero calibration The GAIN is the value stored during span gas calibration using the operator defined calibration gas An increasing or decreasing change to the OFFSET or GAIN when used in conjunction with Deviations will provide insight to both short and long term changes to system performance Note Reset calibration values will reset
26. output amplifier 3 photo cell 6 meter indication Figure 10 3 Principle of operation Since the feedback current from the amplifier is proportional to the oxygen content of the gas sample the output signals that are produced by the amplifier will be accurate and linear The paramagnetic susceptibility of oxygen varies inversely as the square of the absolute temperature To provide compensation for changes in analyzer temperature a temperature sensitive element in contact with the measuring cell assembly is included in the feedback current circuit California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 63 of 86 Section 10 Model 650 Noxygen Analyzer 10 3 Cross sensitivity of gases The very high magnetic susceptibility of oxygen is the basis of the paramagnetic measuring principle In comparison to oxygen other gases have such a minor susceptibility that most of them are insignificant Exceptions to this are the nitrogen oxides However as these gases are in most cases present in a very low concentration the error is still negligible Example 1 The residual oxygen percentage is measured in a closed carbon dioxide CO2 atmosphere Nitrogen Nz is used for zero calibration According to the list of cross sensitivities the error for 100 96 CO at 20 C is 0 2796 In order to obtain a higher accuracy this means that for the zero calibration the reading should be adjusted at 0 27 with No in order
27. press F1 The following screen appears Figure 7 52 Access Level Screen F1 to F4 selects an access level Move the cursor to the access level to be modified You must enter the correct password for the access level desired The passwords for the various operation levels consist of three numbers that must to be entered on the numeric keypad If the code word is incorrect you are asked to re enter the codeword IMPORTANT TIP When a new analyzer is powered up it defaults to access level 1 User To operate ALL parameters and gain complete access select F4 Press the Enter key twice and enter 444 7 8 14 F2 Change Password The passwords can only be changed if you are in access level 4 After F2 enter your new 3 digit passwords Passuordi MEN Passuordz 222 Passwords 333 Password4 444 Figure 7 53 Passwords IMPORTANT TIP You MUST remember and record this new password If this is lost you will need to consult the factory for the default password 7 8 15 F3 Reset Passwords The passwords can only be changed if you are in access level 4 Reset passwords will revert back to the factory defaults California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 42 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 16 Linearization Pressing F6 on the Setup screen brings up the Linearization screen The analyzer can be linearized by a polynom with 5 coefficients By pressing F1 these
28. rra DA p pa 1 p L I e e T l an E yf s A tel ND a Figure 7 8 Main Menu User Level 4 Figure 7 9 Purge Screen Main Menu User Level 4 Operators Manual California Analytical Model 650 Noxygen Page 28 of 86 650 NOXO2 v9 0 doc Section 7 Model 650 Noxygen Analyzer 7 5 F3 Diagnostics F3 from the Main Menu activates the Diagnostics function As described in Section 7 1 3 F3 brings up the two diagnostics screens The Diagnostics screens may be brought up from EITHER the Main Menu or the Measurements screen NOTE Access level is 4 Figure 7 10 Main User Menu Level 4 7 6 F4 Calibrations F4 from the Main Menu activates the Calibrations screen Calibrations may be automatic or manual Deviations can also be displayed Calibration values can be reset to default values and the range to be calibrated can be changed Figure 7 12 Calibration Screen Level 4 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 29 of 86 Section 7 Model 650 Noxygen Analyzer 7 6 1 F1 Automatic Calibration From the Calibrations screen F1 starts automatic calibration If auto range is selected the actual range in use will be calibrated Auto calibration works as follows First zero gas is purged a certain time called purge time Then the measurement begins The measured value must be a minimum time called measuring time and within an upper and a lower limit to be saved as new offset value
29. some parameters until an operator can resume control This screen may be used to establish several desirable special instrument start up parameters that define how the analyzer recovers from loss of AC power When enabled this screen will define the following Wait The time delay in minutes before proceeding If Zero is selected the instrument will wait until all temperature warnings are cleared Calibrations The number of attempts to complete a successful calibration as required in the operator defined Deviation Tables If calibration is not successful the instrument will continue reporting results using the last completed calibration The analyzer will utilize the last completed calibration by selecting zero for Calibrations Starting Range When all defined actions are completed the analyzer will return to the Measurement Screen and at the range specified Access Level The user level at Start Up Remote Manual Put the analyzer in either Remote or Manual at Start Up NO NOx Mode Put the analyzer in NO or NOx or NO2 mode at Start Up California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 7 of 24 ADDENDUM 3 2 Alarms On Off Main F5 F7 All key analyzer parameters are stored in a secure memory location and retained when power is removed In the event of an unexpected power failure it may be desirable to change some parameters until an operator can resume control This screen
30. to compensate the error of COs Since the values of cross sensitivities are based on 100 volume of that particular gas the error at 50 by volume CO and 50 by volume No is 0 135 Example 2 Given the following gas composition at a temperature of 20 C 5 volume Oxygen O3 4100 00 x 10 x 5 45 0000 40 volume Carbon Dioxide CO 0 27 x 10 x 40 0 1080 196 volume Ethane C21 14 0 43 x 10 x1 0 0043 5496 volume Nitrogen N2 0 00 X 10 x 54 0 0000 Gives a reading 96 by volume of 44 8877 As this example shows the total error 5 000 minus 4 8877 is 0 1123 Note see Table 10 1 below for cross sensitivity values of typical gases California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 64 of 86 Section 10 Model 650 Noxygen Analyzer Table 10 1 Cross Sensitivity of gases All values based on nitrogen 0 oxygen 100 Gas Aosione RA df 0 63 AA Ammonia IN 9M stg Ethylene Oxide C HO2 o 1 O 054 060 CH OHCH OH Furan AA 988 988 _ _ Kypon kk os os o Carbon Monoxide co lt ovo oov Hen Ns S E ME Propylene Oxide CHO OO C Hg CH N_N AAA 0 00 Dose 19 AY E E Xenn Xe 0 95 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 65 of 86 Section 11 Model 650 Noxygen Analyzer 11 Reaction Chamber Servicing 11 1 Disassembly Procedure 1 A W N
31. to the analyzer Optional 7 Span Gas Inlet For feeding calibration gas to the analyzer Optional 8 Vent Exhaust from reaction chamber 1 4 inch tube fitting 9 X Output Connectors Analog Outputs and Remote Functions 10 TCP IP Port to Network Connector 11 Serial Port to Serial Connector 12 Filter Analyzer Filter Housing California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 51 of 86 Section 8 Model 650 Noxygen Analyzer 8 2 Main Connector Standard 28 Pin Connector 8 2 1 Main Connector Standard 28 Pin Connector Signal Function 1 6 Digital Output Ground Digital 20 _ Digital Input Span 8 DigialOutput Sense Range 22 Digital Output Zero Gas Flow 9 Digital Output SenseRange2 23 Digital Output Span Gas Flow 28 8 2 2 Auxiliary Connector Standard 28 Pin Connector Pin Signal Function_______ Pin Signal Function 6 Digital Output Ground Alarm 20 Digital Output Read Wet Mode 8 Digital Output Ch 1 Conc Alarm 22 _ Digital Output Read NO Mode __ 9 DigitalOutput Ch 2 Conc Alarm 23 Digital Input Set Wet Mode Digital Output Digital Input Set Overflow Mode 8 2 3 Digital Outputs RS 232 Standard 9 Pin DIN Connector Pin Funcio 1 DCDCarrierDetect 1 2 RxDReceiveData lt Grund 1 A Ground 7 California Ana
32. 1 Serial Interface and AK Commands ooocccnncccccccononnnccnnnnnnnonnnnaccnnonononononnannnnnnnnnnnonnnnos 68 18 22 MNAC ParamiStels qui 68 13 9 General AK Requirements is 69 pono Ee sts vetoes ces M 69 UorcmEseresiifelfeo nini RE E E kee needa eater adat 76 19 05 SOHO S exce tediiese dide emt acude tecum mint dan celduned a 79 3272 ooo AM o utc quehacer uPuRe te dete EERS ERSE 81 QU S 82 ET MODELES 50NOJOSR IOW DISOFAITIS asque idee eh ei ee nen te arene eia Dee 82 14 2 Electrical Block DIAQlA IM dee eet id Eu EH Eran nh Enea Ere ure et E mu E lu uale bes 86 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 6 of 86 Section 1 Model 650 Noxygen Analyzer Table of Figures Figure 3 1 AC Power Switch Connector and FUSC oves cre eet rev res a AAA 15 Eig re 3 2 EMI SUDDIOSSO usos devi eee ee LREUR D QNEE 15 Figure 4 1 Measurement Screen ccccccccsesssecccecceeeeeeeceeeeeeeueeuseeeeeeeessaeeseceeeeesseeaaseeeceeeesssaeaaeeeeeeesessaeaseeeeeeees 18 wis gas uM A VO ANC m 22 Figure 5 1 Main Menu on Power Up Screen occccccccccccnnccnnnccccconoonncnnnnnnnononnnnnnnnnnnonnnnncnnnnnnnnonnnannnnnnnnrnnarananennns 24 Figure 5 2 Mam User Menu Level 4 ios eaaet A A a Mud cR va Laveen E 24 Figure 7 1 Main Menu Screen cccccccsssssssecceceeceaeeeeeeceeeecaeuseeeceeeeessaeeeeseeeeeeseseeeeaeeeeeeessssaaeeeeeeeesessaaa
33. 1l 125 m EE ETE 1 00 i 1 00 10 HO O O Note These screens are used by the operator to define the maximum acceptable limits of the Zero and Span gas for both Manual and Automatic Calibrating 4 3 Flow Zero or Span Some analyzers have the above and the ability to flow Zero and Span Gas dM EM PESO Isl Manual calib 1 SARA PL pan Cal Span 0 08 0 08 oggle zero F4 Toggle span ZERO SPAN FS Measurements FS Cal zero OF F9 Cal spun 02 F amp Ranae pP e FT Ranae Down HOx HT u OZ a tc ra z CAI Tel 800 959 0959 F Thu Mary 15 6 22 23 2008 The above is shown using Zero SPAN Gas From Cal Screen use F2 or Main or Back From Main Menu use F4 F2 California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 21 of 24 ADDENDUM 4 4 Reset Calibration Values When the re set calibrations value function is used all recorded deviations will be set to zero Def cal value Span gas deus Span gas deus I Span gas devs verifying Span gas deviations Z1 measured 2uiation abs rel HN AF Rangel O 0 00 a pangess F OG 0 BB anges Ranges See 8 86 8 88 Range4 CAI Tel 800 959 0959 la Main F4 F3 F4 Main F4 F3 F2 Used to observe Auto Cal Results Used to observe Manual Cal results The above are the new deviations after the operator elects to re set the calibration values Cali
34. 2 _AKEN_s serialno AKEN K3 _AKEN s airpressure _AKEN K4 _AKEN s samplepressure ARMU Raw value Command Response _ARMU_KO _ARMU_s zz ATEM Temperatures Command Response _ATEM_KO _ATEM_s zz y y_ _ATEM KOx ATEM szz California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Description Device identification is responded Device model Device serial number Suggested input air pressure Suggested input sample pressure Description Haw value before linearization and offset span correction is responded Description All Temperatures in degrees Celsius are responded Temperature of x in degrees Celsius is responded Operators Manual Page 72 of 86 Section 13 Model 650 Noxygen Analyzer Description of x CLD DN Converter Temp 2 3 oo pome ADRU Pressures Command Response Description ADRU KO ADRU s zz yy All pressures are responded ADRU KO x _ADRU s zz Pressure of x is responded Description of x Sample Pressure Air Pressure Air Ozone EPC Coil Voltage Sample EPC Coil Voltage ADUF Flows Command Response Description _ADUF KO _ADRU s zz y y_ All flows are responded _ADUF_KO x _ADRU_s zz Flow of x is responded Description of x AGRD Polynom coefficients Command Response Description AGRD_KO Mn AGHRD s Mn a0 al a2 a3 a4 Polynom coefficients of range Mn are responded AANG Deviation from zero point after autocalibration Command Response Description _AANG_KO A
35. 5 6 1 User Funcions Level ia iia 25 6 2 Advanced User Functions Level 2 cococccccccccccnncccnncconnncconnnonnnonanncnnnnnnnannnnnnnos 25 6 3 Maintenance Functions Level 3 cooocccnnccccncconncconoconnnonnonanncnnnnnanonnnnonanonannonanonons 25 6 4 System User Functions Level 4 oooccccoccccccnccccnncconnnnnanconannonanonnnnnnonaninnaninnaness 25 7 Main Menu Function Descriptions ccooncconncconcnccnnncconaccnnanccnnnrrnnnnrnnanrnnanrrnnnnrnannrnaannnnas 26 TM FIMeasure Me Secada ici daneta todos eoe One tc aedes 26 TA FENO ONO Meare Mei adds 26 7 1 2 2 NONO Measurement oa 27 kes ESA NOS Io la 27 EA Dez TR 28 rao 2 UNOS Ana ra M TEE 28 Ta FS WIAGMOSIU GCS msi dida 29 10 nn PP a 29 7 6 1 F1 Automatic Calibration sex rn eto dis ald eee 30 7 6 2 F2 Manual CalibratiON oooonnccnnncccccoconnncnnnncnnnnnnonnnnnnnnnnononnnnnnnnnnnnonannnnnnnnnnonanans 31 Lfs Fo Display Devians M 33 T4 Absolute Zero Gas DeVIaHOF ias 34 2 Relative Zero Gas Deva Misas ba cotta oe ba caia da etel 34 TS Absolute Span Gas Deviation sessi 34 7 7 4 Relative Span Gas Devi ies 34 LAZO FAC heck Cal il 35 7 7 6 F5 Reset Calibration Values ooccccccccccconnccnnnnccconoonnncnnnonononononnnnnnonononannnnnnnnnnnnnnans 35 T FO Range Se Orito 35 EE eio E TT 36 7 8 1 Fl Span Gas GoncenttrallOD oo ufus ia 37 7 8 2 F2
36. 650 NOXO2 v9 0 doc Page 67 of 86 Section 13 Model 650 Noxygen Analyzer 13 AK Protocol Format The master computer and the Model 650 analyzer communicates via the RS232 serial link The Model 650 analyzer acts as a slave and only responds to commands Serial Interface Parameters 1 Baud from 300 to 9600 bps can be selected via the display 7or8 data bits 1 or 2 stop bits and the parity yes no 3 The data transmission is full duplex no echo with XON XOFF protocol The don t care byte byte 2 is adjustable factory setting 20H Command Format channel N always KO for the analyzer data bytes depending on the command 03H Answer Format same code as command package e g ASTZ 20H status O without error or 1 to 9 when error see also ASTF command parameter depending on the command 03H 13 1 Serial Interface and AK Commands The serial interface enables remote control of the Model 650 analyzer by a master computer It is implemented as an RS232 V24 interface and meets all requirements of the AK protocol A 9 pin male connector at the back of the unit is used to connect a master computer with the following pin assignment Pin 3 Txd transmit Pin 2 Rxd receive Pin 5 Gnd ground 13 2 Interface Parameters 9600 4800 2400 1200 600 300 baud Data bits Stop bit 1 or 2 1 byte adjustable e g 32 XON XOFF Active or not active California Analytical Model 650 Noxygen Opera
37. ANG s M1 z z da dr_ Deviation from zero point after M2 zz da dr M3 z z da dr autocalibration MA z z da dr California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 73 of 86 Section 13 Model 650 Noxygen Analyzer AAEQ Deviation from end point after autocalibration Command Response _AAEG KO AANG s Mi zz da dr M2 zz da dr M3 z z da _dr_ MA z z da dr_ AFDA Purge and Autocalibration times Command Response _AFDA KO SATK _AFDA sz yx w ZZ _AFDAKO_SSPL AFDA s zz APAR Request Autocalibration tolerance values Command Response _APAR KO SATK _APAR S ZZ y y X X W W AKAL Deviations from calibration Command Response _AKAL KO _ AKAL s M1 zz y y_X x_W w _ AKAL s M2 zz y y X X W Ww AKAL s M3 zz y y X X Ww w _AKAL_s M4 zz y y_X x_W w California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Description Deviation from end point after autocalibration Description Autocalibration times z Purge time y Calibration time x Total Calibration time w Verify time Z y X w in seconds Purge time will be responded Description Autocalibration tolerance value 96 z z Range 1 y y Range 2 x x Range 3 w w Range 4 Description Deviation ppm z z Zero gas relative to last calibration y y Zero gas factory calibration X X Span gas relative to last calibration w w Span gas factory calibration Operators Manual Page 74 of 86 Section 13 Model 650 Noxygen Analyzer
38. E C Status Group In Remote AutoRange Range 1 Range 2 Range 3 Range 4 In Calibrate In Zero In Span In Sample In NO Mode In NOx Mode 605 only In Wet Mode HCLD only In Overflow not used In NH3 Mode 605 only TYPICAL RELAY 600 SERIES ADDENDUM User DO Screen Display InRem AutoR R1 R2 R3 R4 InCal Zero Span Sample InNO InNOx InWet InOflow InNH3 Dieital Out These contacts 3 4 will drive continuously up to 500 MA using a customer voltage supply that does not to exceed 60 VDC California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 17 of 24 ADDENDUM e OPERATION Use Main F5 F9 to select the first seven outputs Use the 7 to select the desired output Press ENTER and use f to select desired item Press ENTER to save selection Note The 600 CLD has 15 user selectable isolated digital outputs from the list of 40 in TABLE B C User DO I Far Press F1 to observe the remaining eight outputs Program as desired per the above User DO II S SDE Z a Off a Off 10 Off ii off AAA i2 DET Set Unused x 13 Off Channel Off 14 off A ee i5 EZS FE t to Das HO 1 MAIN BACK to SAVE 02 0 0 Z CAI Tel 800 959 0959 lad California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 18 of 24 ADDENDUM 3 7 Cal Analog Output Main F5 F8 TEET Te r rag tim MEC mpensation DEM TE
39. EYPAD DISPLAYS e Scalable Analog Output e Auto Cal Times Voltages e Calculated NO values from empirically derived NO converter efficiencies SPECIAL FEATURES e Auto Ranging e Auto Calibration adjustable through internal clock 115 230 10 VAC 50 60 Hz 560 Watts DIMENSIONS _ _ _ _ 514 H x 19 W x 23 D Inches SPECIFICATIONS ARE SUBJECT TO CHANGE WITHOUT NOTICE California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 13 of 86 Section 3 Model 650 Noxygen Analyzer 3 Installation 3 1 General The instrument is designed for industrial applications These installation instructions are for a typical site Any questions regarding specific installation situations should be directed to Technical Service of California Analytical Instruments Inc 3 2 Site and Mounting NOTE The following precautions must be carefully observed 1 6 Select a site free from direct sunlight radiation from a high temperature surface or abrupt temperature variations This analyzer is not suitable for installation outdoors Select a site where the air is clean Avoid exposing the instrument to corrosive or combustible gases The instrument must not be subject to severe vibration If severe vibration is present use isolation mounts The instrument is designed for rack mounting Optional rack mount slides are available Do not install near equipment emitting electromagnet
40. Input GND analog A Input External Analog 1 A Input External Analog 2 A Output GND Isolated analog D Output Relay RTN 1 Es 3 r O oos O lt 0 10V 0 10V 9 10 11 12 use RTN 1 Status go CLOSED when active Alarms qo OPEN when present 13 14 15 16 use RTN2 17 18 19 20 use RTN 3 21 27 28 use RTN 4 D Output D Output D Output 6 Relay RTN2 7 Relay RTN 3 8 Relay RTN 4 COM 0 1 2 3 4 5 6 7 8 9 D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output D Output User Defined NO Relay 1 User Defined NO Relay 2 User Defined NO Relay 3 User Defined NO Relay 4 User Defined NO Relay 5 User Defined NO Relay 6 User Defined NO Relay 7 User Defined NO Relay 8 User Defined NO Relay 9 User Defined NO Relay 10 User Defined NO Relay 11 User Defined NO Relay 12 User Defined NO Relay 13 California Analytical Instruments Model 650 CLD Operators Manual January 10 2011
41. PP PP Se 650 NOXYGEN FLOW DIAGRAM W PUMP AND ZERO SPAN S V Figure 14 4 Standard Analyzer with Optional Sample Pump and Zero Span Solenoids California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 85 of 86 Model 650 Noxygen Analyzer 14 2 Electrical Block Diagram Section 14 Page 86 of 86 Operators Manual 5 a IX RCGNUM mem RUP ER AA DO cmm eR EUH dome SL P E EE 2002 po jSquisosQ Wepssupaw Ed LLEZOLL 18quinhj juatunaor y NIV MB LION e Oda Didi Ord ant 11047 Od3 LaSzidWvs dl LISTAS di MIvOd3 LISA dl 13847 dl 19H 009 MI SINAWNYLSNI TVOLLA TVNY VINSHOAETVOS g ASH AOL ar23 diat dnd WEL LAS dW3l 1130 n dil N3AO xeu dW31 EHN ZE awit zo 819 TL UN Hn B ausi SSTUHO_ E L SVO SIdMNS gt E ays B IAL ZO zH09 q iu T A SASI 9d3 3 SINIGd LSL eta Les Ed LMVHO dl issus EP luvH2 dL m OASI ELSE dW3l vo 1s dl po ad dl zn AS Ind eo dNOY di SONDY di WVSJgs PION Ine AGL 9 dW31 dgola CONV AG Ab G QA UST HN j SSNOITEIGNO2 TVNOIS i t 8 8 HMvHO dl 130 dL E 9 ino zo i SINIOd 1831 SOR Z Ada Ws 3 P er il OA c7 ser t ASIA y PLICA Oda we E dl _ E DR 2 be Las dl 7 4 LIST IAS dl Aavv ND E Av Iv Tyo Nvv 23 Wavy bo E
42. RES Limes Use F8 to toggle on off Normally during Auto Cal the Sample and Hold Outputs NO NOx and NO2 are held at the last process value If Cal Analog Output is set On then the values are not held and the Real Time value is Output California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 19 of 24 ADDENDUM 4 0 CHANGES TO EXISTING FUNCTIONS 4 1 Saved or Outside Limits During Manual Calibration the following screens will be displayed to indicate the instruments response to the value of the zero or span gas using the amount that the operator defined in the deviation table Manual Zero 5 SMAH sl Manual Span 1 SARA B Zero gas Use F3 To Toggle Span gas Use F3 To Togale Diagnostics Cal Uia Diagnostics Cal Uia Using Current Temp 2 Press Using Current Temp amp Pressx Saved Currentxxx Outside Deviation Limits HOX 0 00 Rangel OO ppm HO C Rang H x 0 0 Fi Save Value HOx O 1 an al enu Oz My f Fz Man al Menu 02 0 0 Z Thu Mar 15 06 16 17 2008 zd Th 2 The above is shown using Zero Gas From Measurement use F5 Zero or F6 Span From Main Menu use F4 F2 F1 Zero or F2 Span California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 20 of 24 ADDENDUM 4 2 Calibration Deviations MAIN F5 F2 F2 Deviations F3 Measuring Deviations 5 SHET LUN zl DevuiatianstZ Measuring devsiationELz
43. al Control The analyzer can be remote controlled by either a master computer or via contact closures The TCP IP and serial communication fully corresponds to the specifications of the AK protocol To change remote manual control press F6 in the main menu This toggles between remote and manual control Figure 7 78 Remote manual control Main Menu User Level 4 7 10 F8 Standby In Standby mode pump is turned off and the solenoids are closed The CAI logo is displayed l L Re Fm EEN ku dag ee oy Ee arn mode 1 m amp D m T 1 24 1j ee gu A ds a beg ud r q SERRE 1 mi T PE Figure 7 79 Standby selection Figure 7 80 Standby screen Main Menu User Level 4 Operators Manual California Analytical Model 650 Noxygen Page 50 of 86 650 NOXO2 v9 0 doc Section 8 Model 650 Noxygen Analyzer 8 Analyzer Components 8 1 Rear Panel The following details the rear panel connections Figure 32 Rear Panel Sample Gas Inlet Feeds sample gas to the analyzer 1 4 Inch Tube 2 Sample Gas Bypass Outlet Exhaust for sample 1 4 Inch Tube 3 Air Inlet For feeding hydrocarbon free air or oxygen to the ozone generator 4 Power Entry Module Power connection power switch fuse compartment 2 Amp 5 Rear Panel Power ON OFF Switch Turns ON OFF line power to instrument 6 Zero Gas Inlet For feeding hydrocarbon free zero air
44. al Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 35 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 F5 Setup From the Main Menu F5 brings up the setup menu Span gas concentrations calibration settings range limits alarms password linearization system and measure settings can be changed The Setup menu begins as shown below A description of each parameter is shown in the information box NOTE Use the down arrow key to obtain the additional setup parameters hom r How 172 17 239 Hon NOY Lf Life Sie l E oS NNI Decr ee ee nsi ERA AAA Sox TLTlInce 4 Figure 7 37 Setup menu 1 Figure 7 38 Setup menu 2 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 36 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 1 F1 Span Gas Concentration For calibration it is necessary to input the concentration of the span gas in ppm For every range the span gas concentration can be changed After pressing F1 in the setup menu a screen appears in which changes can be made Select with the cursor buttons the range to change The selected field turns black To change parameters switch to parameter input mode by pressing the Enter key The input cursor horizontal bar under the first character then appears in the active edit field black background The cursor can be positioned with the right and left cursor keys and the value displayed number or letter can be changed
45. alibrations settings F3 Range limits F4 Alarms F5 Password F6 Linearization F7 System settings F8 Measure settings F10 Displays version Remote Manual Stand By California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Model 650 Noxygen Analyzer F1 Toggles between NO and NO F2 Toggles on NO and NO F3 Displays Diagnostics Screen Sets analyzer in purge mode Diagnostics Ill EPC Coil V Sample Ozone Pressures PSIG Sample Air Gas Flow mL Min Sample Air F1 Starts auto calibration on range in use F2 Zero span calibration change range F3 Display deviations F4 Check calibration F5 Reset calibration values to factory default F6 Range change F1 Sets calibration gas values F2 Sets auto calibration times F3 Sets upper range limits F4 Sets range concentration limits F5 Set user password F6 Range change F7 Displays systems settings F9 Displays measure settings F10 Displays version Model S N Air press Sample press Software version Manual local control Toggles pump Operators Manual Page 19 of 86 Section 4 Model 650 Noxygen Analyzer Main Menu Calibration All access F1 Auto calibration F2 Manual calibration F1 Measurement F3 Display deviations F2 Purge Analyzer F4 Check calibration F3 Diagnostics F5 Reset calibration values F4 Calibration F6 Range select F5 Setup F6 Remote Manual F7 Stand by Auto calibration Range select F1 Range 1 F2 Range 2 F3 Range 3 F4 Range
46. ance We want you to be a member of our thousands of satisfied customers 1 2 Unpacking Instructions Open the shipping container and carefully remove the analyzer from the packing materials Inspect the instrument for any sign of damage Remove the Top Cover retaining screws Visually check for loose parts or connectors that are not properly seated Verify all circuit boards and circuit board connections are secure If all internal components look normal re install the cover 1 3 Reporting Damage Should there be any apparent damage to either the inside or outside of the instrument due to shipping or handling immediately notify the shipper The shipping container or packing materials should be retained for inspection by the shipper 1 4 Contact Information California Analytical Instruments Inc 1312 West Grove Avenue Orange CA 92865 714 974 5560 Fax 714 921 2531 Website www gasanalyzers com California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 10 of 86 Section 1 Model 650 Noxygen Analyzer 1 5 Warranty Certificate Subject to the exceptions and upon the conditions stated below California Analytical Instruments CAI warrants that the products sold under this sales order shall be free from defects in workmanship and materials for one year after delivery of the product to the original Buyer by CAI and if any such product should prove to be defective within such one year period CAI agrees at its opti
47. and SEGA KO SEGA K0 Mn SSPL Command SSPL KO Reset Response _SRES s Pause Response _SPAU s Standby Response _STBY_s Open valve for zero gas calibration Response SNGA S SNGA S Open valve for end gas calibration Response SEGA s SEGA s Purge Analyzer with zero gas Response _SSPL_s SLIN Linearization mode Command _SLIN_ KO Response _SLIN_s California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Description Heset Description Pause mode Description Standby mode Description Open valve for zero gas calibration of actual measuring range Open valve for zero gas calibration of range Mn Description Open valve for end gas calibration of actual measuring range Open valve for end gas calibration of range Mn Description Open valve for zero gas and purge the analyzer Description Change status to SLIN only for compatibility Operators Manual Page 76 of 86 Section 13 Model 650 Noxygen Analyzer SKOP Converter Check Command Response _SKOP_KO _SKOP_s Description Change status to SKOP and activate sample pump only for compatibility SWET Chiller off Wet mode measuring Command Response _SWET_KO _SWET s Description Switch chiller off SDRY Chiller on Dry mode measuring Command Response _SDRY_KO _SDRY s Description Switch chiller on SATK Start automatic calibration Command Response _SATK_KO _SATK_ SATK KO M
48. anged in the form of a dumbbell A single turn of platinum wire is placed around the dumbbell that is suspended in a symmetrical non uniform magnetic field gas out 1 quartz spheres dumb bell 3 mirror 2 platinum feedback coil 4 magnet pole pieces Figure 10 2 The Measuring cell in theory When the surrounding gas contains oxygen the dumbbell spheres are pushed out of the magnetic field by the change in the field that is caused by the relatively strong paramagnetic oxygen The torque acting on the dumbbell is proportional to the paramagnetic properties of the surrounding gas and therefore it can be used as a measure of the oxygen concentration The distortion of the dumbbell is sensed by a light beam and projected on a mirror attached to the dumbbell whereof it is reflected to a pair of photocells When both photocells are illuminated equally the output will be zero The output from the photocells is connected to an California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 62 of 86 Section 10 Model 650 Noxygen Analyzer amplifier which in turn is fed to the feedback coil of the measuring cell If the oxygen content of the gas sample changes the corresponding current output of the amplifier which is proportional to the oxygen content produces a magnetic field in the feedback coil opposing the forces and thereby causing the dumbbell to rotate 1 measuring cell 4 feedback amplifier 2 led light beam 5
49. anual January 10 2011 Page 14 of 24 ADDENDUM 3 6 User Digital Outputs e Overview The 600 CLD Series of instruments have 15 solid state optically coupled isolated relays that can be programmed by the operator to indicate the status of numerous digital conditions The available digital signals consist of a SERVICE group that can be used to externally monitor a number of conditions to aid in preventative maintenance and diagnostics SEE TABLEB amp D A second STATUS group is provided and is used to define the operation of the instrument such as Spanning Zeroing Calibrating and the current Range 1 2 3 4 AUTO etc SEE TABLE C amp D The individual output signals can be operator selected and set to a HOLD or CLEAR mode In the HOLD mode an activated signal is retained until the operator returns to the Digital Output Screen and selects the appropriate output signal and performs a manual CLEAR After performing a Clear Operation the operator must press F2 again to put the outputs back into the Hold mode User DO I 4 SENO AAA Set Unused Channels Off AE Clear x 15 DOts HO O 1 H CK to SAVE 02 0 0 amp B I s n i 01 90 39 2001 F z OQ PP MJ OEA A In the CLEAR mode the signal will automatically change state when the microprocessor detects that the noted condition no longer exists User DO II S SDEM Z 3 Off J Off 10 Off ii Hes HALA Ly OF Set Unused x 13 Off Cha
50. d by an expressly authorized officer of CAI California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 11 of 86 Section 2 Model 650 Noxygen Analyzer 2 Features 2 1 Description The CAI Model 650 NO O Analyzer is a highly sensitive chemiluminescent CLD gas analyzer and a reliable paramagnetic oxygen analyzer It measures oxides of nitrogen gas and dry basis oxygen concentrations in industrial and vehicle emission applications 2 2 Features General The Model 650 NO Oz analyzer has a 3 by 5 inch liquid crystal display and a 20 key data operation input keyboard The 16 bit microprocessor control board consists of the MSR Card with 16 digital inputs 16 digital outputs 16 analog inputs and 4 analog outputs The analyzer can be manually operated from the keypad or remotely via TCP IP or RS 232C communications After turning on the analyzer it needs at least 30 seconds for initialization During this time the screen is illuminated The analyzer is available with an optional internal heated sample pump and internal zero and span solenoids IMPORTANT TIP When the analyzer is powered up it defaults to access level 1 User To operate ALL parameters check the access level See Section 7 5 13 The contents of this operator s manual include 9 Specifications 10 Installation Requirements Mechanical amp Electrical 11 Operation amp Calibration Instructions 12 Reaction Chamber Description with Pr
51. d range Figure 7 47 Change Upper Range Limits 7 8 10 F2 Change Auto Range Limits Although the auto range limits are adapted automatically it is possible to define them manually Up means the value when the next higher range is selected in auto range mode down the value when the next lower range Is selected Figure 7 48 Change Auto Range Limits California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 40 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 11 Alarms Error reports are always displayed in the lowest line of the screen There are two pressures three temperatures one concentration and two voltages with alarm limits that can be defined The user can define the range limits and if exceeded will display an error message bA 1 hl nm LEM E TI E TTE WC TIL am Jn 17 P FE hi i Si 1 Figure 7 50 Set Concentration Pressure and Voltage Alarms 7 8 12 Password After turning on the analyzer you are in access level 1 To change the access level or to change the passwords press F5 Setup in the main menu and Press F5 Password again The following screen appears e m ki qe z r al P gt scr Han H ui i B L Li gd uat o8 x 7 Figure 7 51 Enter Change Password California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 41 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 13 F1 Enter Password To change access level
52. eaction Chamber Pre Amplifier California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 57 of 86 Section 8 Model 650 Noxygen Analyzer 8 9 Relay Board Connections J32 Connects to ip JA n Li a i B la Lal i s NEN s EE i Fa a LJ iji t HTAR AC Input J2 Power Supply 1 Power Supply 2 4 Power Supply 3 Ur oare fe Oven ester E Owens i California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 58 of 86 Section 9 Model 650 Noxygen Analyzer 9 Operation 9 1 Preparation for Operation Check that the external plumbing and wiring have been connected correctly as described in this manual NOTE The internal ozone generator requires approximately 1 hour of continuous operation for the analyzer to achieve full zero and span calibration stability 9 2 Operation 12 Power On Turn ON the power switch on the rear panel The digital display should illuminate 13 Introduce Ozone Supply Air or O2 Adjust the cylinder output pressure to 25 PSIG The internal air pressure is factory set to deliver the air pressure required for optimum analyzer performance as indicated in the factory settings screen 14 Air or O Pressure Settings Check the air pressure setting by referring to the diagnostic screen to check air pressure The pressure should read as indicated in the factory settings screen Note Zero and span calibrations may a
53. ections The tubing from the sampling system to the gas analyzer should be made from corrosive resistant material such as Teflon or stainless steel Even when the gases being sampled are corrosive themselves rubber or soft vinyl tubing should not be used since readings may be inaccurate due to gas absorption into the piping material To obtain fast response the tube should be as short as possible Optimum tube internal diameter is 0 16 inch 4 mm Couplings to the instrument are 1 4 Inch tube NOTE Be sure tubing and joints are clean Dust entering the instrument may cause it to malfunction California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 16 of 86 Section 3 Model 650 Noxygen Analyzer 3 8 Sampling Requirements 3 8 1 Filtration Dust must be eliminated completely Use filters as necessary The final filter must be capable of removing particles larger than 4 microns 3 8 2 Condensation Dew point of the sample gases must be lower than the instrument temperature to prevent accidental condensation within the instrument Bypass the sample through a dehumidifier to reduce the dew point to about 2 to 4 C or less If the sample contains an acid mist use an acid mist filter cooler or similar device to remove all traces of the mist 3 8 3 Presence of Corrosive Gases Useful service life of the instrument will be shortened if high concentrations of corrosive gases such as Clo SO Fe HCI etc
54. entration Pressure and Voltage AlarIMS ccccccccooccnnnccnnncccnoonnncnnnnnnnnnnnnncnonononononnnnnnnnns 41 Figure 7 51 Enter Change PasSWOLU seassa u e a a 41 Figure 4 92 A66855 Bevel SON ii e Tote o m CH T Evi d anus eos veda Urbes Dee truc coo vex 42 Foure 7 59 PaSSWOFOS A a 42 Figure 7 54 Linearization Screen cccccsccesecccccecceseeseeeeeeeeeeeeeeseceeeeeseuaeseeeeeeeeeesaeaaaeeceeeeeessueaseeeeeeeeessaaaseeeeeeees 43 Figure 7 55 Coefficients Range Select ooooncccnncccccccconnccnnnnconononncnnnnnnnononnnncnnnnnnnnnnnnnnnnnnnnnnnnnannnnnnnnnnnnnnnnaanennss 43 Figure 7 56 Linearization Coeficiente usd ita 43 Eig re 7 57 Range Raw Data WII Fla A vna uasa vnd oie t ND ad E 43 Figure 7 58 system Se INQS ooocccccoonnnococonnncconononcnnononcononnnonnnnnnn nennen nennen nnn nha nnn rsea atas se aris sais aranea sanas annis 43 Figure 7 59 System SelUp SCO ON ssl rfi alto sanas 43 Figure 7 60 Clock and Timing Setup Screen israse NE 44 Figure 7261 50 us oom ee eae de a ed oe d 44 Figure 7 62 Select autocalibration time oonccccccccnoccnnncnnncccononanncnnnnnnnonnnnnnnnnnnnonnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnannnennss 44 Figure 7 63 Set Autocalibration Cal Timing ccccccococnnccnnnnccnnononcnnnncnnnnnnnnnnnnnnnonononnnnnnnnnnnnnnnannnnnnnnnnnnnnnnnanennss 44 Figure 7 64 Clock and Timing Setup Screen occccccccccccnnccnnnnccncnnnnnncnonnnnnonnnncnnnnnnnnonnnnnnnnnnnnnonnnnnnnnnnnnnonnnnnnanennss 45 Figure 7 65 F4 Toggl
55. equire the completion of a simple trial and error procedure The operator will observe the results of a zero or span Gain signal generated by the analyzer to the remote recording device and select a correction factor The operator will save this value and then observe the results on the attached remote recording device The process of selection and saving for zero and span will be repeated until a satisfactory calibration is achieved For 0 1 VDC 0 5VDC 0 10VDC and a 0 20 mA outputs the Offset and Gain values are independent and do not interact With the 4 20 mA output the Offset zero and Gain span values interact and may require a few more trials The following is a table of typical values that can be used for start points for offsets and gains for different output types OUTPUT OFFSET GAIN 0 20 ma 0 000 0 927 4 20 ma 1 820 0 740 0 1 V 1 300 0 820 0 5 V 1 100 0 820 0 10 V 1 050 0 820 California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 10 of 24 ADDENDUM e Procedure 3 4 1 From the Main Menu press F5 F7 F3 to obtain following screen assignment 1 SARA Output Signal 3 4 2 Use the 7 to highlight the outputs that require calibration 3 4 3 Press enter so you provide access to all the menu of signals that are available Real Time NO NOx Calibration Sample Pressure etc 3 4 4 Select Calibration and press ENTER to complete the selection Note In the examp
56. ers and presented in PSIG via the diagnostics screen NOTE The correct pressures are determined by the factory for optimum analyzer performance and measured by N I S T traceable standards They are recorded on the Factory Settings Screen 10 1 3 Main Electronics Board The main electronics board contains the instrument power supplies and required instrument electronics A single transformer provides power to the main circuit board and includes provisions for 110 220 VAC at 50 60 Hz input 10 1 4 Relay Board The relay circuit board contains the logic circuitry required to control and switch the AC power to the required heaters and sample pump California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 61 of 86 Section 10 Model 650 Noxygen Analyzer 10 2 Principle of Operation Oxygen The paramagnetic susceptibility of oxygen is significantly greater than that of other common gases and consequently the molecules of oxygen are attracted much more strongly by a magnetic field than the molecules of the other gases Most of the other gases are slightly diamagnetic which means that their molecules are then repelled by a magnetic field nitrogen diamagnetic oxygen paramagnetic Figure 10 1 Magnetic Susceptibility of gases The principle of the magneto dynamic cell is based upon Faraday s method of determining the magnetic susceptibility of a gas The cell consists of two nitrogen filled quartz spheres arr
57. es Auto Gal ON of OFT re et ee ovi id 45 Figure 7 66 Autocalibration Status oooconnncconncccoconnccnnnncnonnonanncnnnnnonononnnnnnnnnnnonnnnnnnnnnnnnnnnnnnnnrnnnnnnnnnnnnnnnnennss 45 Figure 7 67 TOP IP Add ES Susurros toilet 46 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 8 of 86 Section 1 Model 650 Noxygen Analyzer Figure 7 69 O tput ASSIM Suera id 46 Figure 7 69 OUMPULR INGES crias lt PE 46 oi A ah i eae 47 Figure 7 71 Menu Settings Screen ccccccccccceccesessseecceeeeeeaeeeeeeeeeessaeeseseeeeeeeeseaeaseeeeeesessaeaaeeeeeeeesssaaaeseeeeees 47 Figure 7 72 Set NOs Purge and Measure TiMe cccccssesecccccssssececcceeeececccaeueeeeesaaeeeesseausececessaaeeeeessaageeeess 47 Figure 4 79 Ser Gonverter BINCIONCY six ece tasers AAA NA 48 Figure 7 74 Set TIMES d iae venu opes Codd edu ek 48 Figure 7 75 SO No NER I UU em 48 Figure 7 76 Analyzer Information Version ooccccooncnnccconnnccconnnnonononcnnonnnnononnnnonnnnnnnonannnononnnnnnnnnanenenannnnananans 49 Figure LSO Ware Ver Orellana 49 Figure 7 75 Remote mantal COMMON a e 50 Figure 7 79 Standby selection spiaire a e oa aE a a ANA EA 50 Figure 7 80 SLANG DY SCEE esn a lero pacense 50 Figure 8 1 Maj r Internal COMPONENTS ir e ea 54 Figure 8 2 Reaction Chamber Pre Ampllitier ccccccsssssecceceessececcceeeeceeceaeeeeesseaeeeesseaaecesessaaeeeeessaageeeess 57 Figure 8 3 Relay Board Co
58. et Vent A sample gas bypass outlet connector is located on the rear panel 4 Inch Tube Pressure at this outlet should be kept at atmospheric level ANY backpressure will cause an error in reading The vent outlet is located on the rear panel and may contain high levels of ozone which should be vented away from the instrument California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 17 of 86 Section 4 Model 650 Noxygen Analyzer 4 Basic Operation The operation of the digital microprocessor conforms to the guidelines of the AK committee originally developed in the German automotive industry Via the serial port of the MSR Card the analyzer can be remote controlled by a master computer The serial communication fully corresponds to the specifications of the AK protocol TCP IP communication is also available 4 1 Display The analyzer s LCD display includes 16 lines with 30 characters each The display also has background lighting that can be switched on and off via the Display key on the keyboard The following example shows the measurement screen which is formatted into 4 information areas Measurements Oo 3 Huto El 25 ppm 20 Ja Mon Apr 19 19 01 26 20684 Figure 4 1 Measurement Screen THE TOP INFORMATION AREA CONTAINS The AK Protocol Information This capability is for advanced uses and may be toggled on and off in the setup screen F5 Next to the symbol for the active operating mode
59. flow is controlled by an EPC valve lt requires 25 psig cylinder supply pressure and is factory set to deliver approximately 10 to 20 psig to the ozone capillary This pressure may be monitored by the diagnostics display The flow rate from the capillary is very low and will require a bubble flow meter to accurately determine proper flow 12 2 Sample Supply The sample flow is controlled by an adjustable electronic proportional pressure valve This valve requires a 10 to 25 PSIG sample supply pressure to deliver the proper pressure to the sample capillary This pressure may be monitored by the diagnostics meter at any time after inlet sample has been applied The sample flow rate from the capillary is very low and will require a bubble flow meter to determine proper flow rate If the pressure is properly set and a clogged capillary is suspected replace the sample capillary NOTE If the analyzer contains an optional internal sample pump the introduction of a pressurized sample gas in excess of 1 5 PSIG will damage the pump 12 3 NO NO Converter Several published test procedures require periodic NO efficiency tests to be performed on the converter to determine NO to NO conversion efficiency utilizing a NO generator The CAI Model NOxGen may be used for this procedure A short test using NO calibration gas is also defined in the U S Federal Register Title 40 Part 86 332 79 e California Analytical Model 650 Noxygen Operators Manual
60. fornia Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 22 of 24 Section 13 ADDENDUM TABLE D 600 SERIES CLD lO CHART 28 PIN MAIN CONNECTOR ASSIGNMENTS AO z Analog Output OC Open Collector SV z Solenoid Valve TTL z Transistor Logic OPTO 600 CLD HCLD 1 0 Type Analog Levels ping EN COM A Output GND Isolated analog Isolated Al A Output User Defined AO 1 1v 5v 10v mA A Output User Defined AO 2 1v 5v 10v mA A Output User Defined AO 3 1v 5v 10v mA A Output User Defined AO 4 1v 5v 10v mA Bi r Q D Output GND Digital D Output Sense Auto Range TTL low true D Output Sense Range 1 TTL low true D Output Sense Range 2 TTL low true D Output Sense Range 3 TTL low true D Output Sense Range 4 TTL low true oet Auto Range Control Range 1 Control Range 2 Control Range 3 Control Range 4 Auto Cal Calibrate Zero opan Sample D Output OC 24vdc if internal SV D Output OC 24vdc if internal SV D Output OC 24vdc if internal SV D Output 25 Local Remote TTL low true D Output 26 Read Cal Mode TTL low true D Output 2 Reserved D Output 28 Reserved O nete pas Bazaszs peo VNnN 00 Qvo lt California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 23 of 24 Section 13 ADDENDUM TABLE D CONT 600 SERIES CLD lO CHART 28 PIN AUXILLIARY CONNECTOR ASSIGNMENTS NO z Normally Open oPTO Signal CLD yo Type Analog LEVELS G WERE A
61. geseeeees 26 Figure 7 2 Measurements SCIGOll cus sed oin Linee i qd eger aco ex ia exped eins 26 Figure 7 9 Measurement Soren 27 Figure M caBes ieee 10 T ee Eom 27 Figure 7 5 Second Diagnostics Screen ooooocccnncccccnnnoncconnncnononnnnncnnnononnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnannnenns 27 Figure 7 6 Set TO AuUto R ANO iii a 28 Figure 7 7 Analyzer Ser to Range Suerte a da 28 Figure 7 8 Main Menu User Level 4b odes ea rev oi id 28 Figure 7 9 Purge Screen ssssesssssissssssseeeee nene ennnnnnnnn nnns R RR RR RR isis rise ssa nn sas i nasi isis ssa a sans nnns n 28 Figure 7 10 Main User Menu Level 4 cccccssscceceesseceessececeasececsaseeceeuseceneasecessaseeecsaeeensaseeenssaseeessageess 29 Figure 7 11 Main User Menu Level Visas Surtout ve iR Aire A qv ax eb AAA Ev ved reads 29 Figure 7 12 Calibration screen Eevel d ade ads ce abet OE ue uy tope da oe Dei ose ae 29 Figure 7 13 Auto Calibration Screen eeeeseissssssssssssseeseseeenn nnne nennen nnn nnns nn nna nnn nnn nsns naa anis nns 30 Figure 7 14 F2 M rn al Calibration ou inet ois sert a e a cnet eu oes 31 Figure 715 Manual Calibration SCree idt eres ineine ev or esos tov id 31 Eig re7 16 Manual zero gas callDralloLis u oiasosar buccina dct onal puru a dt Ea hana due 31 Figure 7 17 Manual Span gas calibration oooconnccnnnncconnonnnnnnnccnnononnnnnnnnnon
62. gs Screen 7 8 28 Set NO Mode Times Figure 7 72 Set NO Purge and Measure Time California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 47 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 29 F2 Converter Efficiency F2 on the Menu Settings screen allows the NO to NO converter efficiency to be set to the actual measured converter efficiency A value of 100 equals 1 00 F2 will prompt the operator through the NO efficiency test using a NO generator Figure 7 73 Set Converter Efficiency 7 8 30 Low Pass Filter Time Constant F3 on the Menu Settings screen allows the software time constant to be set between 1 and 60 seconds This is very useful in eliminating noise when measuring low level concentrations Figure 7 74 Set Time Constant 7 8 31 F4 Purge Time F4 on the Menu Settings screen the sets the purge time before continuing with a zero or span calibration Figure 7 75 Set Purge Time California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 48 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 32 F10 Displays the Current Analyzer and Software Versions This displays the analyzers information including the factory recommended air and sample pressure settings Figure 7 77 Software Version California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 49 of 86 Section 7 Model 650 Noxygen Analyzer 7 9 F7 Remote Manu
63. he analyzer contains the optional internal sample pump disconnect the sample line from the rear inlet port Do NOT turn off the sample pump or analyzer power at this point 3 A Allow the analyzer to draw in room air for approximately 5 minutes or flush out any remaining sample which may cause condensation as the analyzer cools 4 Turn off the optional internal sample pump by setting the analyzer to standby 5 turn off the analyzer power 6 Back flush the sample line and filter of any sample before disconnecting and powering down California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 60 of 86 Section 10 Model 650 Noxygen Analyzer 10 Functional Description 10 1 Operating Principle NO NO The California Analytical Model 650 Analyzer utilizes the chemiluminescent method of determination of oxides of nitrogen NO or NO in a sample gas In the NO mode the NO in the sample is quantitatively converted to NO by gas phase oxidation with molecular ozone produced by the UV reaction of cylinder air Generally 10 to 15 percent of these NO molecules are elevated to an electronically excited state This reaction is immediately followed by reversion to a non excited state and emission of photons The photons impinge on a photodiode detector PHOTODIODE which generates a low DC current directly proportional to the NO contained in the sample gas This current is amplified by a precision electrometer and
64. ic interference EMI NOTE A rear supporting brace or equivalent is required if the optional rack mount slides were not purchased California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 14 of 86 Section 3 Model 650 Noxygen Analyzer 3 3 Electrical All wiring is connected at the rear of the instrument The AC power is connected to the power fuse switch as shown below ell O Figure 3 1 AC Power Switch Connector and Fuse NOTE A defective ground may affect the operation of the instrument The output voltages are connected per Table 8 1 1 Shielded wiring is recommended for output signals CAUTION Electromagnetic interference EMI may affect the operation of the instrument Do not install the instrument in the vicinity of electrical noise such as high frequency furnaces electric welding machines etc If the instrument must be installed at such locations a separate power line must be used Noise from a relay or solenoid valve should be controlled by the use of an EMI suppressor RC circuit across the power wiring close to the noise generating component EMI Suppressor Figure 3 2 EMI Suppressor NOTE The EMI Suppressor must be located close to the noise source California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 15 of 86 Section 3 Model 650 Noxygen Analyzer 3 4 Analog Output Connections Appendix oee Appendix for connector pinouts located on
65. l alarm limits _EDAL KO x x min xmax _EDAL s Set alarm limits of x Alarm Limits Cell Temp Peltier Gas Temp EPC Coil Sample Voltage Sample Pressure gt 3 4 5 Reserved Sample Content Pump Temp 6 Diode Temp ETCP Set TCP IP Parameters DNE E 3 9 4 Converter Temp 10 EPC Coil Air Ozone Voltage 5 Command Response Description ETCP KO zzz zzz zzz zzz _ETCP s zzz TCP IP address ETCP KO _ yyy yyy yyy yyy yyy TCP IP subnet mask _ETCP_KO_xxxx xxxx TCP IP port All changes take effect after next power on cycle California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 80 of 86 Section 13 Model 650 Noxygen Analyzer 13 7 Abbreviations used Measuring range number M1 M4 Measuring Range 1 4 W W Numerical value ZZ Number t Numeric integer value Polynom coefficients s Gaus SAUS NENNEN SINE9J 75ZSATAZJAWEA NTL Date of format year month and day with 2 characters each and no spaces Time of format hour minute and second with 2 characters each and no spaces California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 81 of 86 Section 14 Model 650 Noxygen Analyzer 14 Appendix 14 1 MODEL 650 NO O Flow Diagrams MEME PRI ER L7 EPCV2 R5 AIR 02 DC C PEL e x EXHAUST c R1 m l e JAN MF1 SVI SAMPLE 2 C lt mE EPCV1 LE m E l 02 R4x
66. le below only Output 1 will be calibrated Record the name of these signals they will be restored Output CAI Tel 800 959 0959 Note Any or all of the four outputs can be selected for calibration This screen will not be used again until calibration has been completed California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 11 of 24 ADDENDUM 3 4 5 Press BACK to return to the SYSTEM SETUP screen Main F5 F7 3 4 6 Press F8 to obtain the following screen Main F5 F7 F8 3 4 7 Use the 7 to select the desired output press ENTER 3 4 8 Press F1 to select a ZERO signal and observe the results on the remote device 3 4 9 Change the offset value press BACK to save the new value 3 4 10 Press F8 to return to the D A Calibration screen and note the results on the remote device 3 4 11 Repeat steps 3 4 8 thru 3 4 10 until a satisfactory ZERO calibration is achieved 3 4 12 Complete steps 3 4 8 thru 3 4 10 for each of the remaining outputs that require calibration 3 4 13 Press F5 to produce a full scale 100 signal 3 4 14 Use the arrow keys to position the curser at the require GAIN value 3 4 15 Observe the results on the remote device and make a correction to the GAIN value for the output of interest Press BACK to save this new value 3 4 16 Press F8 to return to the D A calibration screen 3 4 17 Observe the results on the remote device and repeat the steps to cha
67. lso be initiated by an external computer or by remote contact closures 15 Zero Adjustment Flow zero gas through the instrument by selecting the calibration screen and select either manual or auto calibrate Perform a zero calibration for all ranges on both NO NO and O channels 8 Span Adjustment Flow span gas through the instrument by selecting the calibration screen and select either manual or auto calibrate Perform a span calibration for all ranges on both NO NO and O channels NOTE The correct calibration gas values must be entered The instrument is available from the factory with four ranges 16 NO NO Function The analyzer switches the NO converter in and out of the sample stream and is controlled from the measurement screen In the NO mode the sample bypasses the converter and the resultant analysis produces the value of NO Only in the sample In the NO mode the sample passes through converter and the resultant analysis produces the value of NO NO NO in the sample The analyzer will also display the values of NOx NO and NO The NO mode may be switched in and out remotely by a contact closure or computer Remote control wiring is terminated in the rear panel connector See Appendix 17 Sample Pressure Check With sample gas flowing through the instrument check the sample pressure setting by referring to the diagnostic screen The sample pressure should read as indicated in the factory pressure settings screen
68. lytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 52 of 86 Section 8 Model 650 Noxygen Analyzer 8 2 4 Digital Outputs TCP IP 8 Pin RJ 47 Connector IMPORTANT TIP For direct connect to a PC a crossover cable is required Connection to a hub requires a straight cable California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 53 of 86 Section 8 Model 650 Noxygen Analyzer 8 3 Internal Component Locations Figure 8 1 Major Internal Components Electronics Includes instrument electronics See Main Electronic Board 2 NO NO Solenoid Valve Switches flow between the NO and NO mode 3 Optional Internal Sample Pump Provides sample to analyzer Not shown 4 Ozonator Contains UV Lamp 5 Ozonator High Voltage Supply Produces High Voltage to UV lamp 6 Proportional Flow Pressure Regulator Regulates flow of ozone 7 Proportional Flow Pressure Regulator Regulates flow of sample 8 Reaction Chamber amp Detector Assembly 9 NO NO Converter Converts NO to NO for total NO 10 Relay Control Board Provides AC Voltage to Heaters Pump and UV Transformer 11 Paramagnetic Oxygen Sensor Measures oxygen content of sample California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 54 of 86 Section 8 Model 650 Noxygen Analyzer 8 4 Main Electronics Board Potentiometers RP1 to RP17 z ES i E m P UB am ha E
69. n H n rt da a S T i m Lm F i i um n 1 i i i P LN mac fs PEU a AH amies i pT sip EAH Tm na re ae EE P EE m iE pt p LUI iii Yu T LL CL A 8 5 Main Electronic Board Potentiometers HP1 EPC 9 5V Sample Set HP10 Chiller Zero Temp Set HP2 EPC 9 5V Air Set HP11 Chiller Span Temp Set RP3 03 Cutoff RP12 Chiller Temp Set RP4 Cell Temp Set HP13 12VDC Adjust RPS Oven Temp Set RP14 Sample Pressure Set RP6 Pump Temp Set HP15 Air Pressure Set HP7 Converter Temp Set HP16 Not Used HP8 O2 Temp Set HP17 Not Used HP9 NH3 Temp Set HP18 PGA Balance NOTE Potentiometers are clearly labeled on both sides of the PCB California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 55 of 86 Section 8 Model 650 Noxygen Analyzer 8 6 Main Electronics Board Connectors Test Points Voltage Output Clearly Resistor Stand wis PE en ex i PE ni my T Lg i mz fui EL n3 KI TT up ate En TS ui 3 E E EMT ui LI iii Y iiid Th Pee it 8 7 Main Electronic Board Connectors J5 J7 J9 J11 J13 Relay Board UPA PGAZero j 000000 NOTE Connections are clearly labeled on the PCB California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 56 of 86 Section 8 Model 650 Noxygen Analyzer 8 8 Reaction Chamber To Pressure Power Input Inverting Amplifier Adiust Main Zero Board Adjust Figure 8 2 R
70. n _SATK s SEMB Set measuring range Description Start automatic calibration of all ranges Start automatic calibration using range Mn Command Response SEMB KO Mn SEMB s SARE Auto range on Description Set measuring range Autorange is disabled Command Response SARE KO SARE s SARA Auto range off Command Response _SARA_KO SARA s Description Set auto range on Description Set autorange off SREM Remote mode for AK commands Command Response SREM KO SREM s Description Set device in remote mode SMAN Manual control to control device manually Command Response SMAN KO0 SMAN s Description E Set device in manual mode California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Operators Manual Page 77 of 86 Section 13 Model 650 Noxygen Analyzer SMGA Start measuring Command Response _SMGA_KO _SMGA_s SNKA Saves measured value as new offset Command Response _SNKA_KO _SNKA_s SEKA Saves measured value as new span value Command Response _SEKA_KO SEKA s SENO Converter off Command Response SENO KO _SENO s SNOX Converter on Command Response _SNOX_KO _SNOX_s SNO2 Converter on Command Response _SNO2_KO _SNO2 s Description Start measuring Turn on pump for sample gas Description Saves measured value of actual range as new Offset if zero valve is opened Description Saves measured value of actual range as new span value if span valve is opened
71. nans 46 7 8 25 F4 Displays Output RANGES cccocoocccccnncccccncoonccnnnnnononannnnnnnnnnonnnnnnnnnnnnnnonnnnnnnnnnnnnnnnans 46 7 8 26 F5 Turns status Line On ol Of oai peces dis 47 7 8 27 ES Measure SEUNG S uiii lc 47 7 8 28 Set NO Mode TNES ass aaa iaa 47 7 8 29 F2 Converter Ef ICIENCy coooocoonncnnccccocononccnnnnnonononanncnnnnononnnnncnnnnnnnnononannnnnnnnnnonans 48 7 8 30 Low Pass Filter Time GCOHSLtaliboeco eee c peus eo teo di eee sodes eumd s dus teo latas 48 7 8 31 PA Purge las cU 48 7 8 32 F10 Displays the Current Analyzer and Software Versions 49 549 Fe Remotes Manual Cont io 50 UD FSSD 90 0 Analyzer COmDponenls ooi oi iaa NECEM 51 all A O dta a DEA ER 51 8 2 Main Connector Standard 28 Pin Connector occccoccccccccnnccncnncoconononononocannnnnnanononos 52 8 2 1 Main Connector Standard 28 Pin CONNEeCTOT cooooonnccnnncccnccnnonccnnnnncnnnnnaancnnnnnnnnnnnos 52 8 2 2 Auxiliary Connector Standard 28 Pin Connector ccoooooonnccnnncccnccnnnnccnnnnnnnonnnancnnnnnnos 52 8 2 3 Digital Outputs RS 232 Standard 9 Pin DIN Connector 52 8 2 4 Digital Outputs TCP IP 8 Pin RJ 47 Connector cooooocccncccnccnooccccnnccnnnnnnancnnnnnnnnnnnos 53 8 3 Internal Component LOCAtiONS ooccccccccccnnccconnnnnononnonnnconccnnnnnnnennonnnnnnnnonanennnonaness 54 8 4 Main Electronics Board P
72. nd content and for the period but not in excess of one year stated on the label at the time of delivery or 90 days f CAI may from time to time provide a special printed warranty with respect to a certain product and where applicable such warranty shall be deemed incorporated herein by reference g CAI shall be released from all obligations under all warranties either expressed or implied if any product covered hereby is repaired or modified by persons other than its own authorized service personnel unless such repair by others is made with the written consent of CAI IT IS EXPRESSLY AGREED THAT THE ABOVE WARRANTY SHALL BE IN LIEU OF ALL WARRANTIES OF FITNESS AND OF THE WARRANTY OF MERCHANTABILITY AND THAT CAI SHALL HAVE NO LIABILITY FOR SPECIAL OR CONSEQUENTIAL DAMAGES OF ANY KIND OR FROM ANY CAUSE WHATSOEVER ARISING OUT OF THE MANUFACTURE USE SALE HANDLING REPAIR MAINTENANCE OR REPLACEMENT OF ANY OF THE PRODUCTS SOLD UNDER THIS SALES ORDER SOME STATES DO NOT ALLOW THE EXCLUSION OR LIMITATION OF INCIDENTAL OR CONSEQUENTIAL DAMAGES SO THAT THE ABOVE LIMITATIONS OR EXCLUSIONS MAY NOT APPLY THIS WARRANTY GIVES YOU SPECIFIC LEGAL RIGHTS AND YOU MAY ALSO HAVE OTHER RIGHTS WHICH VARY FROM STATE TO STATE Representations and warranties made by any person including dealers and representatives of CAI which are inconsistent or in conflict with the terms of this warranty shall not be binding upon CAI unless reduced to writing and approve
73. nge the GAIN value by repeating steps 3 4 14 thru 3 4 16 as needed for each output 3 4 18 Return to the OUTPUT Assignment screen F5 F7 F3 from the main menu and change the output signals from CALIBRATE to their original values as defined in step 3 4 1 California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 12 of 24 ADDENDUM 3 5 Save Data Archiving Time Main F5 F7 F1 F5 Archive Time is the Time in seconds between each set of data points If zero no data is stored in the SEC data files The SEC data files are in CSV format for direct import into Excel CAI can provide the tools necessary to download these files Use ENTER to change recording time SEE TABLE A California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 13 of 24 ADDENDUM TABLE A 600 SERIES CLD DATA ARCHIVE FILES Time Date Month Year Error Index TimeStamp NO Conc NO2 Conc NOx Conc NH3 Conc Concentration Detector Volts Range Auto Manual Span Gas Offset Gain Sample Pressure Sample Flow Sample EPV Volts Air Pressure Ozone Flow Ozone EPC Volts Diode Temp Cell Temp Oven Temp Pump Temp Converter Temp Dryer Temp O2 Detector Temp NH3 Conv Temp O2 Concentration O2 Detector Volts O2 Offset O2 Gain Wet Dry Meas Mode Local Remote Converter California Analytical Instruments Model 650 CLD Operators M
74. nnections ooooonnccnnncccccnoncnnnnncnnnnnnanncnnnnnonononnnnennnnnnnnnnnnnnrnnnnnrnnnnnnnnnnnnnnnonnnananennss 58 Figure 10 1 Magnetic Susceptibility of gases occcccccccccooonnncnonnnonononanncnnnnnnononnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnannnnnns 62 Figure 10 2 The Measuring Cell In teory ss a E Pere ave sos Ye Ea ve or E ee inean 62 Figure 10 3 Principle of operatio nhu esie gebeten A a s duds 63 Figure 14 1 Standard Analyzer ccccccccssssseccccseeeeeccceeueececcseeueeeeescuaueeceeeseaaeeeeesaaseceseseuaeceesessaeeeessssagseeees 82 Figure 14 2 Standard Analyzer with Optional Zero Span Solenoids ooocccccccoooonncccnnccnnnononnccnnnononnannnnnnnnnnnos 83 Figure 14 3 Standard Analyzer with Optional Sample Pump oooocccnnnccccccnnncnnnnccnonononnccnnnncnonnnnnnnnnnonnnnnnannnnnns 84 Figure 14 4 Standard Analyzer with Optional Sample Pump and Zero Span Solenoids 85 Tables Table 10 1 Cross Sensitivity Of GASCS cier ii 65 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 9 of 86 Section 1 Model 650 Noxygen Analyzer 1 Introduction 1 1 Overview Congratulations and thank you You have just purchased one of the most reliable gas analyzers in the world Before using the analyzer please familiarize yourself with its operation by reading this manual lf you have any questions please do not hesitate to call California Analytical Instruments for assist
75. nnels Off i4 Off A xxx xxx i E Fi I to T DO s HO O 1 MAIN BACK to SAVE 02 g u z CAI Tel 38001 959 0959 F California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 Page 15 of 24 ADDENDUM The operator can select from the following the desired SERVICE or STATUS groups that are to be digitally monitored Index O CO NO OF C N 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 26 TABLE B Service Group Sample Pressure Failure Air Pressure Failure Oven Temp Failure hcld only Converter Temp Failure Pump Temp Failure Diode Temp Failure Cell Temp Failure Peltier Gas Temp Failure hcld only O2 Temp Failure 650 only EPC Coil Sample Failure EPC Coil Air Failure Range overflow ADC Range Overflow ADC Range Underflow Range 1 is not calibrated Range 2 is not calibrated Range 3 is not calibrated Range 4 is not calibrated Reaction chamber pressure Low concentration Warning High concentration Warning NH3 Converter Temp Failure 605 only dummy text for RTC General Alarm Cal Alarm California Analytical Instruments Model 650 CLD Operators Manual January 10 2011 User DO Screen Display SampleP AirP OvenT ConvT PumpT DiodeT CellT DryT O2T SEV AEV OR AO AU R1NC R2NC R3NC RANC RCP LoC HiC NH3T Off GenAlarm CalAlarm Page 16 of 24 Index 25 27 28 29 30 31 32 33 34 35 36 37 38 39 40 TABL
76. nnnnnnnnnnnnnnnnnnannnnnnnonnnnnnnnnanennos 31 FOUE o Range sele resol oa 32 Figure 2219 Selected range una AN ee eo ea 32 Figure 7220 58 ECC ra o o o a 32 Figure 7 21 Selected range 3 sesasine naiai a a aaa a ana a ai aap aaa oan a iina anin 32 Figure 7 22 Selected range A aean cedo eter A is 32 Figure 7 29 Selected auto anderson 32 Eigure 7 24 F3 Display deviations od 33 Figure 7 25 Display deviations screen ssssssisssssssssssesseeee nennen nennen nennen hann nsns nnne 33 Figure 7 26 Zero gas OSMA ON castell tie Etude toa diosa ees cds pesas 34 Figure 7 27 Zero das deviations VENIS 34 Figure 7 28 opan gas deviation S cn ud ih aa e ea 34 Figure 7 29 Span gas deviations VerifyiNQ cccccccooconcncconnncconononnncnnnonononanncnnnnnonnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnennns 34 Figure 7 30 F4 Check callblallOrizes iiu racio pecie seers oases Does ipee Bent facts sio utc quieti eoi io bem e ticus 35 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 7 of 86 Section 1 Model 650 Noxygen Analyzer Figure 7 91 Gheck Calibration zii tto oet ida 35 Figure 7 32 F5 Reset calibration valles u2iii eon pe dite Ue esie Poeta Ev cs Fave rad a bus di ici 35 Figure 7 39 Resetcalibration Values uri tods 35 Figure 7 34 Range Seletin inie E rae EEA E A A AAE eE AOA EA 35 FOUG T S9 PANO 6 aeaa aaao 35 Fig re 7 36 Mainmenu User levela oa a eee Ae N 36 Figure 7 387 CU MEn de ete 36 Figure 7 38 Setup me
77. nu 2 2 c cc0 ceccccceecsecedeeeccecesccessseeecenescdeecsedeeceesescceseaesectecseccouseececesscccedeeseecceessstecedveseeess 36 Figure 7 39 Change span gas SettidgS cccccccccccoconnccnncnonononnncnnnnnnnononnnnnnnnnnnnnnnnnnnnnnnnnnnnnnannnnnnnononnnnnnannennss 37 Figure 7 40 Change Auto Calibration Settings cccccccccoconncnnnnccnonononncnnnnnnnnononancnnnnnnnnnnnnnnnnnnnnnonnnnananenons 37 Eigure 7 Setup ulTies Lc a D escas 38 Figure 7 42 Measuring deviations llsssesessssssssseseeseee nennen nnne nennen nnne nennen na nnns nnn ann nens nnns nnns 38 Figure 7 43 Absolute versus relative deviations cccccsssccccceessececcceeeececccaeusececeeaeeeeeseaueeeeessaaeeeeeessaseeeess 38 Figure 7 44 Calibrations via internal solenoid valves oooccccccconcnncccconncnnnonnnnncnnnncnnnnnnnonononnnnnnnnnnranonononanenss 39 Figure 7 45 Galibrallon Via roD uiuere o O dd o ae 39 Figure 7 46 Change Range Limits c ooconnncccnncccccconccnnnncnnononnnncnnnnnonononnnnnnnnnnnnnonnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnnanenos 39 Figure 7 47 Change Upper Range Limits ccccccccocccnncccconcnncncnoncnnnononancnnnnnnnnncnnnnnnnnnnnnnnonnnnnnnnnnanrnnnnnnonannnss 40 Figure 7 49 Change Auto Range LIM vecs eet te e t oet D teer eis eei een erat 40 Figure 7 49 Set Temperature Alarms cccccccccssessececcceeseceecccaueeecceseuseeeeceeauseeeesseuaeeeecssaueeeeessagseeeesssagseeees 41 Figure 7 50 Set Conc
78. ocedures for Disassembly of its Component Parts 13 Function Explanation of the Electronic Circuitry 14 Electrical Block Diagram California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 12 of 86 Section 2 Model 650 Noxygen Analyzer 2 3 Model 650 CLD Paramagnetic Specifications DETECTORS Chemiluminescence CLD Photodiode Paramagnetic Os 0 1 to 3 000 ppm NO or NOx Four user definable ranges Higher andes Available qua Request M RESOLUTION DETECTION LIMIT Better than 1 096 of Full Scale NOISE JLessthanO S eofFullScale ADDITIONAL INTERFERENCE CO 1000 ppm NA HCN 28 ppm N A SO 500 ppm N A DATA NH 10 ppm N A N50 201 ppm N A Carbon Material 205 C gt 98 to 100 Efficiency Ultraviolet Lamp UltravioletLamp o AIR OR O REQUIREMENTS Dry air less than 0 01 ppm NOxat 250 cc Min 25 psig NO NO Control soir dci Cycle Remote NOx mode by dry contact OUTPUTS AVAILABLE scalable to 0 10 V or 4 20 mADC RS232 and TCP IP General Fault TTL Logic Ground True DISCRETE ALARMS Calibration Failure TTL Logic Ground True High Concentration 2 each TTL Logic Ground True e Converter Temperatures e Air Pressures Flow Rate and e Cell Temperatures EPC Control Voltage e Photodiode Temperatures e Sample Pressure Flow Rate and EPC Control Voltage e Factory Settings e Passwords 4 Full e TCP IP Address e Scale Range Select DIGITAL DIAGNOSTICS K
79. on either i to correct by repair or at CAl s election by replacement with equivalent product any such defective product provided that investigation and factory inspection discloses that such defect developed under normal and proper uses or ii to refund the purchase price The exceptions and conditions mentioned above are as follows a components or accessories manufactured by CAI which by their nature are not intended to and will not function for one year are warranted only to give reasonable service for a reasonable time which constitutes reasonable time and reasonable services shall be determined solely by CAI A complete list of such components and accessories is maintained at the factory b CAI makes no warranty with respect to components or accessories not manufactured by it in the event of defect in any such component or accessory CAI will give reasonable assistance to Buyer in obtaining from the respective manufacturer whatever adjustment is authorized by the manufacturer s warranty c any product claimed to be defective must be returned to the factory transportation charges prepaid and CAI will return the repaired or replaced product freight collect d ifthe product claimed to be defective requires on site repair such warranty labor will be provided at no charge however transportation and living expenses will be charged to Buyer e ifthe product is a consumable or the like it is warranted only to conform to the quantity a
80. otentiometers occcoccccocncoccccccncconnconnncnnonnnnnnnnononncnanonons 55 8 5 Main Electronic Board Potentiometers sess 55 8 6 Main Electronics Board Connectors occcccccnncccccconcconnnoconnnnconnononanonononnnnonanononannnnnos 56 California Analytical Model 650 Noxygen 650 NOXO2 v9 0 doc Operators Manual Page 5 of 86 Section 1 Model 650 Noxygen Analyzer 8 7 Main Electronic Board Connectors cccccccocccnccccncnnnononnnnnnnnnnonnnnonconnononennnnnnnnnnnonennnnnss 56 8 9 REACCION Na MD o S D 57 9 9 Relay Board Connections immer it 58 Oe OCS AU ON EE E LTD E 59 Ls Preparauomndor DOFQUOLD use A ia 59 A ON TEE 59 9 3 nut Dow PrOCGSdllle sra ita 60 10 Fu u ctonal DesriptlOM ssoi E 61 10 1 Operating Principle NO NOb oocccncccccconcccnocononcnccnncnnnnconcononnnnnononnnnnonancnnnonannnnnonancnnonnns 61 10 1 1 Reaction einem IM a cd 61 10 1 2 mI E MD TU UR 61 10 1 3 Main Electronics Board ML 61 10 1 4 Relay BO al ee la aa er 61 10 22 Prneipleor OperailOn Oxy Gen dieta 62 10532 Cross senslitvity Ol Odds es ici elit dal cloaca 64 11 Reaction Chamber Servicing ee eceeee eee ieeeen eie eene enean n enhn anna n nnnm 66 11 1 Disassembly Procedure monito 66 ID NAM ASSemDy Procede m RE TTE 66 127 TROUDIESNOO UNO etc 67 20 OZE All Ode SU ai 67 12 2 Sample SUD dd aa ee a 67 123 NONO Converter uie icio es aid 67 13 AK Protocol FO Mati its 68 13
81. presented to digital panel meter and recorder output In the NOx mode the sample is first routed to the NOx converter where the NOs component is reduced to NO The complete sample is analyzed by the PHOTODIODE as above 10 1 1 Reaction Chamber The sample and ozone are delivered to the reaction chamber via the unique regulated flow system described below The sample and ozone are mixed together at the center of the chamber where the reaction takes place The sample is vented from the chamber through a 1 8 inch stainless steel tube The chamber contains a red filter which is sealed with an integral O Ring The chamber assembly is O Ring mounted to the PHOTODIODE The complete chamber and PHOTODIODE assembly is housed in an RFI shielded enclosure 10 1 2 Flow System The basic function is to deliver highly regulated flows of sample and air or O2 to the ozonator and reaction chamber assemblies The EPC valve delivers approximately 15 PSIG to a pre set capillary and consequently accurately predetermines the ozone flow rate The air supply cylinder should be set to 25 psig The sample is presented to the reaction chamber via a precision factory set electronically controlled proportional pressure valve through a capillary This pressure is factory set at approximately 3 85 PSIG A close coupled bypass capillary minimizes dead volume and improves response time Sample inlet pressure and regulated air pressures are monitored by internal pressure transduc
82. ropped for integers If you switch from Manual to Remote at the device it remains in Manual mode until a SREM KO is received by the control computer On the display this mode is indicated by REME Remote enable on the status line In manual mode query commands via the serial interface are possible at any time 13 4 Scans AKON Command _AKON_KO Measured concentration value Response Description AKON s ZZ y y X X W W Measured concentration value is responded z z Current measured value y y NO x x NO2 w w NOx y y X X w w are only used in dual measure mode Otherwise O O will be returned California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 69 of 86 Section 13 Model 650 Noxygen Analyzer AEMB Set measuring range Command Response Description _AEMB_KO _AEMB_s Mn Current measuring range is responded AMBE Measuring range limit Command Response Description _AMBE KO _AMBE s M1 w w M2 _x x_M3 yy All existing measuring range limits are M4 z z responded AMBE KO Mn AMBE s Mn zz Range limit of Range Mn is responded AKAK Calibration gas concentrations Command Response Description AKAK KO AKAK s M1 w w M2 x x M3 y y All existing calibration gas values are M4 z z responded AKAK KO Mn AKAK s Mn zz Calibration gas value of Range Mn is responded AMBU Upper and lower range switchover values for auto range Command Response Description _AMBU KO _AMBU_s M1 w w W W M2 x x X Lo
83. s To the main menu Display lighting 6 i on off P p baca Der the last menu Delete key End input open selected field for input Switch over of the keyboard Arrow keys for selecting the functions and numeral control keys editing fields and for scrolling possible input values Figure 4 2 Keyboard 4 3 1 Operation with the Cursor Keys and the Enter Key When operating the unit with the cursor keys you select the various functions with the up down cursor keys and start them with the Enter key This method is particularly suitable for less proficient users since the system displays a short on line help for nearly every function selected The actual cursor position is shown as a black horizontal bar TIP If you are not yet familiar with the screens and their fields just press any cursor key after a screen appears This moves the cursor from field to field and displays the corresponding online help 4 3 2 Operation with the Function Keys When using the function keys Fl though F10 functions are directly accessed by pressing their corresponding function keys This method is suitable for the advanced user since it is faster than the operation with the cursor keys 4 3 3 Read Change Parameters To read and or change parameters you must switch to the parameter input mode by pressing the Enter key after calling the corresponding parameter screen The input cursor horizontal bar under the first charac
84. sed value At the predetermined time it will switch to the NO mode through converter and read and display the NO value while the last 15 second NO average is displayed The top value will be real time values and will change between NO and NOx The difference between the two average values is shown as NO2 All three values are sent to the analog and digital outputs Figure 7 3 Measurement Screen 7 2 F3 Diagnostics F3 activates the diagnostic screen where pressures flow rates temperatures and EPC control voltages are displayed in real time The units are psig degrees C ml min and voltage Use the arrow key to switch between diagnostic screens Figure 7 4 First Diagnostics Screen Figure 7 5 Second Diagnostics Screen California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 27 of 86 Section 7 Model 650 Noxygen Analyzer 7 3 Select Range With the arrow keys the ranges 1 to 4 can be selected and locked in which will disable the auto range capability Continue pressing the arrow keys will recycle the analyzer back to auto range The range and or auto range is displayed on the measurement screen lf the limits are exceeded while not in the auto range mode a warning Over Range appears on the screen Figure 7 7 Analyzer set to Range 3 7 4 F2 Purge Analyzer F2 from the Main Menu activates the Purge analyzer function if equipped i E n L D7T1 zx mR
85. ss 13 SAEC mm 14 SUPE CITIES 14 32 Se ana MON ul ET 14 So AICO UNG Al grag E e ts 15 3 4 Analog Output Connections Appendix occccccoccccccconnoncccnoconnnonononcnnnnnnnnnonanonnnonaness 16 S NEEC oC E O E Re re ee te re en ree ee ee ee ee 16 3 0 Gas Handling EQUIP A so uie todos tots toot a edat tatio sete ood aac 16 Su GAS CONECO S usce imi tei rx ta esco 16 3 8 Sampling Hequlremiente succi eec terre ot ets ero oo Le iie ese ci mu Fei eder dun 17 3 8 1 FNMA OMs E C aborts 17 3 8 2 GondensalO Mariara baba ba oca 17 3 8 3 Presence of Corrosive Gases S ciaiue a a a E A 17 3 8 4 Gas TEMPE total daa 17 3 8 5 Pressure and FIOWRalOS dnd unice mte ttes benug sanand ast mls tiic vata os tnu avus GA do aa Me gud 17 4 Basic Oper atom iii 18 AA O 18 A O E A oe ectmeciesssn andi hectadecbace 19 ABa A 22 4 3 1 Operation with the Cursor Keys and the Enter Key cc sssseeeeeeeeeeeeeeeeeeeeeeeaes 22 4 3 2 Operation with the Function KeyS ooccccccccoccnnnccnnnncccnononnccnnnnononnnanncnononononanncnnnnnnns 22 4 3 3 Read Change Parameters cccccccccnocnccnnnnccccononnnonnnnnnnnnnnccnnnnnnonnnnnnnnnnnnnnonannnnnnnnnnonnnans 22 5 Operating SIEUCIUTO idas 23 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 3 of 86 Section 1 Model 650 Noxygen Analyzer Sls Me Man eC tds 24 6 Men Structure asias 2
86. t a warning Deviation error appears Figure 7 43 Absolute versus relative deviations California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 38 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 6 F4 Calibrations via Solenoids Calibrations can be made by using the solenoids for zero and span gas or by using the pump Calibration via valves means that the zero gas is flown by the zero gas solenoid and the span gas is flown by the span gas solenoid Figure 7 44 Calibrations via internal solenoid valves 7 8 7 F5 Calibration via Probe Calibration via probe means that the zero and the sample gas is flown by the sample pump the solenoids for zero and span gas are not used Ml m om ki uit BE Han Hovy Figure 7 45 Calibration via probe 7 8 8 F3 Range Limits There are 4 different ranges The user can define the upper range limits in ppm Hon How 17 Figure 7 46 Change Range Limits California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 39 of 86 Section 7 Model 650 Noxygen Analyzer 7 8 9 F1 Range 1 4 Change Upper Range Limits In this menu the upper range limits can be changed The new settings are saved by pressing MAIN or BACK The auto range limits are automatically adapted This means that if the upper range limit of range 1 for example has reached 90 of the upper range limit in the auto range mode it is switched automatically to the secon
87. ter then appears in the active edit field black background The cursor can be positioned with the right and left cursor keys and the value displayed number or letter can be changed with the up and down cursor keys or entered directly Every input has to be concluded by pressing the Enter key again which causes the cursor to disappear California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 22 of 86 Section 5 Model 650 Noxygen Analyzer 5 Operating Structure The analyzer s operation can be divided into four operating levels The current level is always displayed as a stack of 1 to 4 horizontal bars in the top right corner of the screen In the access level menu you can choose between the following operating levels F1 User operating level 1 F2 Advanced user operating level 2 F3 Maintenance operating level 3 F4 System user operating level 4 A password can be assigned to each operating level Only the system user who normally has the highest operating priority can assign the password At the factory the default passwords for the CAI analyzers are set as follows User 111 Advanced user 222 Maintenance 333 System 444 The default setting can be changed only by the system user This manual is written to include all information for the advanced system user TIP Because of the user settings some of the parameters shown in this manual may not appear on your analyzer Check the access level
88. the analyzer rear panel Remote range identification and range selection are obtained via the rear panel connections When a range is selected the corresponding control line is pulled low to zero VDC Ranges not selected will remain at approximately 5 VDC When remote range control is selected on the front panel switch a contact closure is provided at the rear panel connector Remote range selection is made by connection of the control line for the desired range to the analyzers zero VDC line provided in the connector Five VDC is also provided Remote NO On is selected by connection to the common line This contact closure turns on the NOx function by flowing the sample first through the NO NO converter 3 5 Gases 1 Air or O2 Ozone Air lt 1 ppm C in pressurized cylinder 2 Nitrogen or zero air in pressurized cylinder 3 Standard span gas es near full scale concentration with a nitrogen balance in a pressurized certified cylinder 3 6 Gas Handling Equipment 1 Pressure regulators for zero gas Air or N2 ozone supply air or O2 and span gas cylinders 2 Corrosive resistant gas tubing NOTE High levels of NH greater than 10 PPM NH may reduce the NO to NO Converter s conversion efficiency to a level that is unacceptable It is therefore recommended that the customer purchase a commercially available NH scrubber and install it in the path of the sample gas prior to its introduction into the analyzer 3 7 Gas Conn
89. the device status is indicated The status field is also displayed on all other screens SARE Autorange enabled SMGA Measuring gas is flowing SMAN Device is in manual operation status SWET What The level of Password Entry is shown on the right with 1 to 4 horizontal lines THE LARGE INFORMATION AREA CONTAINS The date portion of the screen THE THIRD INFORMATION AREA CONTAINS The help information for the parameter selected ranges etc THE LOWER INFORMATION AREA CONTAINS The time and date and any error condition The symbol in the bottom right corner indicates the keyboard mode In the example shown the keyboard is in the function key mode For input fields the mode is usually switched to numerical input Then an N appears in the lower right of the screen This symbol is displayed on all screens California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 18 of 86 Section 4 4 2 Menu Tree Main Menu All access F1 Measurement F2 Purge Analyzer F3 Diagnostics F4 Calibration F5 Setup F6 Remote Manual F7 Stand by V NN NY gt Measurement F1 NO NO O F2 Dual Mode F3 Diagnostics Up down range Purge Analyzer Diagnostics I Temperatures e Cell Diode e Oven Pump e 02 Calibration F1 Auto calibration F2 Manual calibration F3 Display deviations F4 Check calibration F5 Reset calibration values F6 Range select Setup F1 Span gas concentrations F2 C
90. tors Manual 650 NOXO2_v9 0 doc Page 68 of 86 Section 13 Model 650 Noxygen Analyzer 13 3 General AK Requirements 1 If the command message contains no error the acknowledge message contains the echo of the function code and the error status number 1 to 9 If the transfer was faulty or the function code unknown the answer contains four question marks example 0 If the displayed value is not valid a is placed in front of the measured value example AIKG 0 9999 If a control or adjusting command is sent via the serial interface while the measuring device is in Manual mode it sends an answer like SLIN O KO OF If a channel does not exist the answer for control and adjusting commands is e g ATEM 0 3 NA in which 3 is the number of the sub channel If the device is busy with a running function SLIN for example every arriving control command is ignored except SRES and STBY and the response message is e g SMAN 0 BS If In the mode SINT an additional SINT KO command is received the integrator is reset to O and the integration is restarted If the command message contains data that the measuring device cannot process ESYZ KO ABC for example the response message is ESYZ 0 SE A syntax error is recognized if the data does not match the expected format or if the parameters do not fit the expected size Numbers are in floating point format with decimal point The decimal point can be d
91. ure 7 14 F2 Manual Calibration From the Calibration screen F2 starts manual calibration If auto range is selected calibration is not possible and the appropriate range can be selected In the manual calibrations menu five options are possible F1 Flow zero gas 2 F2Flow span gas 3 F3 Range select 4 F4Flow zero O 5 F5 Flow span O Figure 7 15 Manual Calibration Screen When zero or span gas is flown the measured value can be saved by pressing F1 If the screen is left by pressing the buttons Main or Back the measured value is not saved Solenoids are closed by pressing F2 Figure 7 16 Manual zero gas calibration Figure 7 17 Manual Span gas calibration California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 31 of 86 Section 7 Model 650 Noxygen Analyzer From the manual calibration menu the range to calibrate can be chosen by pressing F3 F i mmm Cn c4 chm tu erg C d 40 40 im m m AI E R a Figure 7 18 Range select iu io iTi easuremenTt L Aailbratlcocrniz Range select Selected ranae Ranaez 300 ppm SMGA Figure 7 22 Selected range 4 Figure 7 23 Selected auto range California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 32 of 86 Section 7 Model 650 Noxygen Analyzer 7 7 FS3Display Deviations Figure 7 24 F3 Display deviations After every calibration the deviations
92. urge Analyzer F5 Passwod o O F10 Version F4 Calibrations ss F5 Setup F7 Stadby 0 0 0 0 0 O 6 3 Maintenance Functions Level 3 icis AAA Menu Concentration password Clock Analyzer password on off p F1 F2 F4 ibrati F5 7 Settings ee peee ION Settings F7 Stand F10 Version 6 4 System User Functions Level 4 All function described in this manual may be accessed from Level 4 California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 25 of 86 Section 7 Model 650 Noxygen Analyzer 7T Main Menu Function Descriptions 7 1 F1 Measurements The measurements screen is activated by pressing F1 on the Main Menu screen Figure 7 1 Main Menu Screen 7 1 1 F1 NO or NO Measurement The NO NO content is displayed in ppm Pressing F1 switches between measuring the sample gas for NO or NO only When the converter is off only NO is measured When the converter is on NO is measured Figure 7 2 Measurements Screen California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 26 of 86 Section 7 Model 650 Noxygen Analyzer 7 1 2 F2 NO NO Measurement The F2 function activates the hold and sample feature which allows the analyzer to automatically switch between NO and NO measurement The time duration for the sample read is set up in the Setup Menu The analyzer will read and display the NO converter is bypas
93. vice identification you must first rename the device to RESET Now a name up to 40 letters can be given NOTE The device name must not have any blanks between i e CAI CLD is not allowed You can use underlines i e CAL_CLD EGRD Set polynom coefficients Command Response Description EGRD KO0 Mn a0 al a2 a3 a4 EGRD s Set polynom coefficients of range Mn EFDA Set autocalibration and purge times Command Response Description EFDA KO SATK zy x w _EFDA s Set autocalibration times z Purge time y Calibration time x Total calibration time w Verify time Z y X w in seconds EFDA KO SSPL z _EFDA s Set analyzer purge time to z seconds California Analytical Model 650 Noxygen Operators Manual 650 NOXO2 v9 0 doc Page 79 of 86 Section 13 Model 650 Noxygen Analyzer EPAR Set autocalibration tolerance values Command Response Description EPAR KO SATK zz y y X X w w EPAR Ss Autocalibration Tolerance value z z Range 1 y y Range 2 x x Range 3 w w Range 4 ESYZ Set System Time Command Response Description ESYZ KO yymmdd hhmmss ESYA s Respond system time yymmdd year month day each 2 characters wide no spaces hhmmss hour minutes seconds ET90 Set Lowpass Filter Time Command Response Description ET90 KO t ET90 s Set lowpass filter time t filter time in seconds EDAL Diagnostic alarm limits Command Response Description EDAL KO al1 min al mas al2max _EDAL s Set al
94. wer and upper range switchover X M3 y y Y Y MA zz ZZ value of auto range are responded ASTZ Normal device status Command Response Description _ASTZ KO ASTZ s SREM STBY SENO SARE Device status is responded _SDRY California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 70 of 86 Section 13 Model 650 Noxygen Analyzer Possible states SHEM STBY SENO SARE SDRY SMAN SPAU SMAN SARA SWET SMGA o measuring gas SNGA zero gas SATK SNGA zero gas during autocal SATK SEGA end gas during autocal SLIN AAA SSPL AA SKOP AA California Analytical Model 650 Noxygen Operators Manual 650 NOXO2_v9 0 doc Page 71 of 86 Section 13 Model 650 Noxygen Analyzer ASTF Error status Command Response _ASTF KO _ASTE s f1 12 f3 f15 Errors 1 Sample Pressure Failure Air Pressure Failure Oven Temp Failure 2 3 Converter Temp Failure 5 Pump Temp Failure Diode Temp Failure 10 11 13 14 Description Current error number is responded 10 EPC Coil Sample Failure EPC Coil Air Failure Range Overflow ADC Range Overflow ADC Range Underflow 5 Range 1 is not calibrated Cell Temp Failure Range 2 is not calibrated Peltier Gas Temp Failure 15 7 1 LM Range 3 is not calibrated 9 Reaction Chamber Temp Failure Range 4 is not calibrated AKEN Device identification Command Response _AKEN_ KO _AKEN s devicename _AKEN K1 _AKEN_s model _AKEN_ K

USER`S MANUAL - California Analytical Instruments, Inc.

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