Ⅰ 底質採取法 - 国立環境研究所
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24. 49 49 1 1 0000000 H2SiF 2 00 a 5 K 0557 A3 b 5 K 8223
25. 2 a 5 K 0557 3 b 4 9 1 2 b 9 4 9 1 2 c d 4 9 1 2 d e 2009 L 0 4 9 2 2 e f 000p
26. 0000000 pH6 8 0 JIS K 9007 17 09 JISK 9020 17 89 500mL h TOO 10y L 4 8 1 2 h i 5 9548 3 5 0 25g 75 100mL 3 1 5 0 02g 20mL p 000
27. 100mL b 4 a 0 5mL 5mL e 5mL 2 30mL 10 4 a 1 3 2 3 3 19 2 5mL 5 00 a 880nm 710nm b 000 5u g mL 1 8 mL 50mL 530 n e o 00000 50 40u g 50mL 40mL 200g L 40g L pH 40g L 1435 pH 3 _ 3 5mL 200 40 C 1
28. I 48 D DO x0 ULU JU 0 1mol L mL 0 005844 0 1mol L 00 1mL g k JIS K 8443 IU UO 0 6390 g 20g L 2 5mL 250mL g O D 100mL p 0 2g L JIS K 8495 U p ul ul Hl O 5 4 2 4 20mg JIS K 80347 100mL O T 0 5mL 0 1mol L
29. 30 20mmol L CODsed 2 a 0080000000000 20mmol L JIS K 8247 3 29 1 050 1 100mL 11 2 16 G4 30 b 50mmol L JIS K 8528 6 79 1L 000000 10g L 0 JIS K 8659 lg 10mL 100mL 1 d 0000000 0 0O 100g L 0 JIS K 8913 10g 100mL e 5 8637 26g JIS K 8625 0 29 1L 2 5 K 8005 13
30. 1 1 1 2 u 1 O 2 2 0000 21 0000 6km 22 200 300m 50m 50m 3 0000 2 3 10cm 10cm 3 4 pH
31. 34 1 000000 a b 00000000 1 1 109 10mm 2 ji 10mm 20 C b 2mm 3 H U 3100000000 0 nj 00000 jD Ud nang 2000000 000002mm 0000 4 0000 41 0000 1 000000 a 105 b 000000 0 001g
32. Et malli puru pod o0 um sss L ln n fn n n A O LE mz al ol oo ojojojojojajajaj y y olol olol e c3 r3 laa laa alo ExeExeaudmpgagaampgaggO 4 lama r3 r3 cceumuamiuuumuaum mes 3 r3 eai umi uu E mla laa 5 mla o ojal o a o ajo ojo aja 5 ol e ee cem L3 T mz o a a aa olol olol ola laa laa olola a a
33. 3 a b 000000 4 00000 8 10g 2mol L 100mL b C lg 4 5 1 1 4 e h d 100mL 4 5 1 1 4 e h 5 a 25mmol L b 4 d a c 4 1 1g mgN g 200 100 NH4 N a b xf TE x0 700 xw NH4 N moN g a 25mmol L mL b 25mmol L mL g mL 25mmol L 0 700 25mmol L 1mL mg a
34. 2mol L 2 00 a DDJISK 0557 A3 b 000000 qQ2mol L 4 5 2 1 2 b 1 50 0 100mL J IS K 8180 20mL d 5 K 8116 100g 700mL JIS K 8085 50mL 1L e 00000000 10 f 1 39 195mL J IS K 8541 5mL 00000000 700mL 80g L 70mL JIS K 8107 389 JISK 8983 N 12 5g 80g L pH 1L h 4 0000000000000 000 19 0 0 4 5 3 1 2 c i 000 N 1 00000000000000 00 0 1g L 0 4 5 3 1 2 d p 00000000 0 1mgN mL JIS K 8548 105
35. 45
36. 5 a 0000 b 000 25u gF mL O 0 20 60mL 100mL oer o dol e F c 00000 11 2mL min 500 200u L d 000000 4 1 1g mgF kg 67 6 00000000 4 9 1 6 a
37. t n 1 0 05 2 132 2 015 1 943 MDL MDL MDL 1 20 50 2050 s MDL MDL n 1 0 05 x s t n 1 0 05 n 1 596 t e nu 10 1 1 1 10 2 2 10 1 2 30 Ci C Cca H x100 30 e 00000000 10 1 1 1 10 20 eo 000000 10 60 10 d
38. I 44 CODsed 100mL 300mL 20mmol L 10mL 6 100g L 5mL 0 1mol L 1mL a g 4 1 1g CODsed mgO 500 1 CODsed b a xf x0 800 X100 XW CODsed mgO g a 0 1mol L mL b 0 1mol L mL 0 1mol L W g 0 800 0 1mol L 1mL mg 1 CODsed 3 2 2 400 60 10g 3 4 5 20mmol L 50mmol L 6 20mmol L 10mL 10mL 20mmol L 20mL 1 o b 100g L 25mL 3 7 10mL 0 25mol L 2mL
39. 4 00000 a 0000000 O 5 104 0 0 01g 500mL 250mL 9 5g L 100g L 1mL 2 a 200mL 20g L 20mL O 10mL EDTA 20mL 8 O 2 3mL min 49 5 150mL O 100g L 10mL 6 30 7 50 C 100mL 500mL 150mL 5g L 100mL uU Dg e 90mL 1 op 10 2 EDTA 100g L 1mL 35mg 3 EDTA EDTA 4 3mL min 5 15mm 6 100g L 1mL 14mg 7 pH 54
40. 5 a 0000 540nm b 000 2u gN mL 10 10mL 100mL c e mgN o 00000 O 0 20 2 9 100mL 10mL 10mL min 30mL 30mL 8 10mL 4 1mL N 1 1mL 20 540nm 100mL 000 d 4 1 lg mgN g 43 I 453 001 6 00000000 45 21 6 0000 ND 0 20 2u g 10m U gt 1000000000 10mL min 00000 30mL 0000 30mL 2000 540 nm 44 000 Ni90
41. 4 5 6 2 5 3mL min 7 1 5 00 a 4 10mmol L 25mL 1 1 2mL 8 b 10mmol L 1mL 9 c 4 a b 10 d 4 1 lg mg S g 1 S b a xf x0 1603 y S mg S g a 10mmol L mL b 10mmol L mL 10mmol L 4 a g 0 1603 10mmol L 1mL mg 8 9 0 1mol L 0 1mol L 10 24 I 43 000 6 00000000 EA DUDU 00mL 000000 axe EE a ad o ow 1 000 21591 0 0190 00 0000000 3000 500 200 30mL 0000000000 20m 000000 0 100g L 20mL 00000 2 5 3mL min 0
42. 46 lll 1 0000000 2 a 5 0557 3 b 2 1 250mL JISK 8951 500mL o 5 8905 69 JIS K 8533 Iil 0 24g 300mL 2 1 120mL JISK 8588 5g 500mL d 000000000 72g9 L 0 JIS K 9502 L 7 29 100mL og 10 e iuunnunnnnununn nunnnnununnununnun 5 1 f 00000 50u gP mL JIS K 9007 105 2 C 2 0 2197g 1 000mL 10 5u gP mL 50u gP mL 20mL 200mL h 0000000000 K 8721 E 0 19 100mL i 0000000000 2009 1 0 JIS K 8576 200g 1L j 0000000000 409 L 0 JIS K 8576 40g 1L k 1 35 JIS K 8951 2mL 70mL 3 4 00000 a 00 0000000 3 1 Dg 0 01g 10mL 5mL 10mL 5mL 60 5mL 2 30mL 5 B
43. 1 20 2 2 30 15 3 0000000 3 1 UDUD 1 000000 a 00000 b 2mm 000000 2 a 2mm b
44. NIES NIES CRM No 2 NIES CRM No 12 NIST NIST SRM 1646a Estuarine sedi ment NIST SRM 2704 River sediment NIST SRM 1939 River sediment NIST SRM 1941 Marine sediment NRCC NRCC MESS 1 Marine sediment NRCC BCSS 1 Marine sediment NRCC PACS 1 Marine sediment NRCC CS LHS LHS 2 Marine sediment PCBs NRCC HS 3 HS 4 HS 5 HS 6 Marine sediment BCR BCR CRM 277 Estuarine sediment BCR CRM 320 River sediment BCR CRM 462 Coastal sediment IAEA 356 Marine sediment
45. 43 000 1 0000000 1 O 1 300mL II 4 3 2 b 509 4 2 00 a 5 0557 A3 b K 8953 5g 500mL 115 K 8576 6g 300mL J S K 8960 70g 1L o 000000 1009 L 0 JIS K 8356 12g 100mL d ma aommol L rJIS K 8920 1 27g J S K 8913 5g 50mL 1L e 5 K 8637 26g JIS K 8625 0 2g 1L 2 5 K 8005 130 C 2 0 72g 0 001g 200mL 20mL 300mL JISK 8913 2g 145 5mL 5 100mL 10g L 1mL mL 0 1mol L f b 20 gt 1 100 200 2x x0 003567 a 9 b X 0 1mol L mL 0 003567 0 1mol L 1mL g f 10mmol L 000000000000 0 1mol L 20mL 22 I 43 000 DD 20m 9 000000 10g L 0JIiS K ss528000000000000019000 10m IJ 00
46. MDL n 1 0 05 x t n 1 0 05 MDL 5 0 2 1 000000000 tu n 1 0 050
47. 15mL O 25 2 30 11 12 O 620nm OmL 50mL Glo 10 pH 13 10mL 148 0 5mL pH6 8 10m pH6 8 pH 0 518 11 20 30 C 12 1 d 4 1 19 mgCN kg I 48 DODODO 6 00000000 481 0 0000 481 4000000000 000000000000000000 25mL 0 0 CNO 0 50 9u 0000000 50mLp 0000000000000 5g L0 10 25229100000 30000000000 620nm mgCN kg 59
48. 5 00 a 0000 638nm b 000 1u gCN mL 0 50 9mL 50mL 10mL 5 c c DU 4 25mL CN 0 50 9u g 50mL 5g L 1 148 pH 7 2 10mL 9 T 10g L 0 5mL 5 a 4 10mL 25 2 30 9 638nm 10mL 50mL pH7 2 10mL 6 d O00000 4 1 26 19 mgCN kg O 8 pH 70 8 9 20 300 I 48 DODODO 6 00000000 D DD 31000000080 50 10g 0 0190 0 D 0000000 5 0 250mL D O 0000 0000000 DUDU DUDU 0000 000000 200mL 0 g L 20mL E El ENE aoa GIG BA NO 000 10mL 0000020 3 min 00000 150mL O O CA 0000000 500mL 150mL 0000000000000 5g L0 0 0 100g L 1mL 56
49. 5 a 0000 b 000 O 0 1u gF mL 100mL 200mL pH 5 2 10mL 7 8 9 10 11 12 13 14 1u gF mL 100mL 10u gF mL 100mL 0 1mgF mL 100mL 200mL pH5 2 10mL 1u gF mL 0 1mgF mL I 1 aam O e 15 15 7 pH5 2 pH 5 2 8 0 1u gF mL
50. c 140 1454 5 C 4 d 3 5mL min 220mL e pH pH 5 00 6 0 40g L 5 f 250mL 3 4 5 a 0000 620 nm b 000 2u g F mL 2 25mL F 40 50u g 5 c 0 c 00000 30mL F7 4 50u g 50mL 5mL 10mL 1 e 20mL 1 30mL O 620nm d O00000 4 1 1g mgF kg 61 6 00000000 aul o ul a 00000 000 2H5g 001g 40mL lmL 40mL 0000 19 0000 140108000000 0000 30 5mL min b DUDU 30mL 50mL po000 00000000000000 20mL 62 492 1 0000000
51. 0 1mg g 100 105 250u 250u pod 000000000 4 a lg 100 1050 49 0 01mg 10mL
52. 4 1mL 5 N 1 1mL 20 e 540nm e 10mL ono d 000000 4 1 19 1 g 6 00000000 4 5 2 1 6 500 4 iml iml 2000 540 nm HUD 41 45 330 aq
53. 5 000000000 500 1 000g 4 ul 4 5 n 41 O 4
54. H2SiF 6
55. 1 4 2 1 b 10mm 2 DD a 10mm 0 001g b 105 110 40 C 3 00000000
56. 5 8 25mmol L b a c 4 1 1g mgN g 200 1 N mgN 9 a 25mmol L mL b 25mmol L mL 25mmol L V mL W g 0 700 25mmol L 1mL mg 00 2 25mmol L 10mmol L 4 4 1 lg mgN g N a b xf 200 x0 280 ues V W mgN g 10mmol L mL 10mmol L mL 10mmol L 5 V mL W g 0 280 10mmol L 1mL mg O 4 2 b 25mmol L 100mL 250mL O 5 2 b 25mmol L 00 3 2 6 25mmol L 500mL 25mmol L 6 50mL 5 7 4800 h 50mmol L 7 25mmol L 50mL 150mL 5 7 25mmol L 50mmol L mL 4 1 lg 4 5 1
57. A3 2 DO a JD JIS K 0557 b 4 5 1 1 2 c 4 5 1 1 2 d
58. 2 00 a 5 K 0557 3 b 4 9 1 2 b 4 9 1 2 o dj 0000000 4 9 1 2 9 H2SiF 6 e 00000000 0 2004 20g f DDD tn J IS K 8150 58g 1g 500mL 200g L pH 1L 0000000000 0 1mgF mL 4 9 1 2 f JIS K 8355 115 K 8284 100mL pH5 2 h 10 gF mL 200mL Y 0000000000 p mbi 200mL j 00000
59. 45 3 4 5 3 1 000000 Y 0000000 2mol L 1L 5mL op 10 C og 10 2 00 a 5 K 0557 A3 b 000000 2mol L 4 5 2 1 2 b 9 4 15 K 9066 4 2g JIS K 8180 60mL 80mL 200mL d 000 N 1 0 0000000000000000 19 0J1S K 8197 N 1 N 1 0 2g 200mL e 00000000 0 0 15 K 8019 105 1100 100 4 93g 1L f 000000000 0 24 gN mL 1mgN mL 10mL 1L 10mL 500mL 3 a b 00000 4 5 2 1 4 a b 100mL 4 5 2 1 4 a b 5 00 a 0000 540nm b 000 0 24 gN mL 1 10mL 10mL 10mL 4 5 3 1 5 0 mgN o 00000 O 0 20 2u g 10mL 10mL 40 4 5 3
60. 27 I 44 1 10 CODsed mgo CODsed b a xf 2 00 x a 0 25mol L mL b 0 25mol L mL 0 25mol L W 2 00 0 25mol L O 1mL mg 2 CODsed DO 000000 Qu 40000 EP 4 00000000
61. b 2mm 3 00000000 3100000000 10000000000 0000000000000 0000000 0000 2mm 17 33 0000 a 0000 1050 110 b 1050 110 C 1 1 10g 10mm 2 00 a 10mm
62. mgN g 200 1 N b a xf AU x0 700 XN N g b 25mmol L 50mL 50 mmol L mL a 50mmol L mL 50mmol L V mL w g 0 700 50mmol L 1mL mg O 6 2 b 25mmol L 7 50mmol L 30mL JIS K 8576 35g 4 5 2 5mL 1 000mL 000JIS K 8005 2kPa 48 lg 0 001g 200mL 20mL 300mL 1g L JIS K 8842 0 1g 95 100mL 130 5 50mmol L 50mmol L f f a TM s TEM SES 100 200 2xx0 004855 a 9 b x 50mmol L mL 0 004855 50mmol L 1mL g 32 I 451 000 6 00000000 000 3100000000 0 230 30mg 0 0190 0000000000 200m0 DO 10mL 000000 59 29 3000 000000 200mL O 200mL ooo 00 00000000 300mL 500mLp 50mL 5070 500g L 0000 100 20mL 33 45 12 000000000 1 0000000 4 5 1 N
63. e 0000 17 18 4 00000 4 9 1 4 a f
64. 4 00000 a 4 5 1 1 4 a d 9 b 4 5 1 1 200mL 50mL 10 c 4 5 1 1 4 f h 200mL 200mL d 30mL 4 5 1 1 4 b d 4 5 1 2 4 b c 9 0 032mg 10 25mmol L 50mL 5 00 a 630nm b 000 0 004 0 08mg 50mL 25mL 5 c o 00000 O 0 004 0 08mg 50mL 25mL 10mL e 10g L 5mL 20 25 30 11 630nm d O00000 4 1 90 19 g 11 200 25 06 30 30 35 45 1 6 00000000 000 0 NH 0 032mgD 0 0190 00 0000000000 200mL DO 10mL 000000 59 29 D ND 0 004 0 08mg 0000000 50 U 000 25mL 10mL 000000 o E 200mL DO 000000 000 00 DUDU 300mL pooo 200 000000000 50mL 20 25 C 30 630nm 00000000000 50041 DUDU 100mL 0 00 20mL ug 36 452 00000000 4 5 2 1 00000 1 0000000 2mo
65. 4 5 2 1 4 a d 5 a 0000 630nm b 000 4 5 1 2 5 b c 00000 4 5 1 2 5 9 O d 000000 4 1 lg 6 00000000 4 5 2 1 6 g 39 4 5 1 2 6
66. 1 0000000 250mL EDTA 4 2 00 a 5 K 0557 A3 b 000000000000 5g L 0JIS K 8799 0 5g JISK 8102 95 50mL 100mL o9 000000000000 0 100g L 0 JIS K 8588 10g 100mL d 5 K 8107 10g 20 g L 100mL e 5 9005 15 K 8356 l2g JIS K 8085 35mL 100mL 7 2 15 K 9020 17 8g 300mL 200g L pH7 2 500mL h TOO 109 L J0 JIS K 8318 p 0 629 50mL Y 400000000 00000000J SK 9548 3 1 5 0 3g JIS K 8500 N N 20mL 4 1 59 40 g L 20mL 1410 pH 7 100mL 10 C 20 j 0 1mol L 5 K 8550 17g 1 000mL 5 K 8005 600 1 NaCl 100 1 169g 200mL 20mL 50ml J IS K 8646 2g 100mL bmL 2g L IS K 8830 0 2g 100mL 3 4 0 1mol L 0 1mol L f b 20 1 f a x x x 100 200 x x0 005844 9 b 52
67. 3 5 140 00000 30
68. 4 a 3 000 5 000rpm 20 3 000 b 00000 9 0000 d 000 1987 pp127 1997 pp205 206 1996 pp28 39 1986 pp74 77 4 H 1 4 1 D mg kg H g kg mg g D 3 3 1 1 0 1 1 001 0000 u DUDU 96 0 1 0 D 96 0 1 0 0 uuu mg g 0 01 gogogogoo0000000000000sed mg g 0 1 mg g 0 01 mg g 0 01 mg g 0 01 uu t mg g 0 01 mg g 0 1 mg kg 1
69. 12 0 2 2 00000000000 0 D D gr 9 0 ppm NIES NIST NRCC BCR IAEA No 2 No 12 1646a 2704 MESS 2 BCSS 1 PACS 1 320 356 Pond Marine Estuarine Buffalo Marine Marine Harbour River Marine Sediment Sediment Sediment River Sediment Sediment Sediment Sediment Sediment Sediment 96 10 6 7 22 2 297 6 11 8 2 3 90 As 12 6 23 23 4 20 7 11 1 211 76 7 26 9 Ba 254 210 414 531 548 Cd 0 82 3 0 0 148 3 45 0 24 0 25 2 38 0 533 4 47 Ca 96 0 81 1 06 0 519 2 60 2 2 8 87 Ce 34 72 95 41 5 Cr 75 201 40 9 135 106 123 113 138 69 8 Co 27 16 6 5 14 0 13 8 11 4 17 5 19 15 0 Cu 210 104 10 01 98 6 39 3 18 5 452 44 1 365 Ga 5 15 20 Fe 96 4 31 2 008 4 11 6 53 4 5 2 41 Hg 1 3 1 16 0 04 1 47 0 092 4 57 1 03 7 62 MeHg 5 46 K 99 0 68 1 56 0 864 2 00 2 5 La 17 17 29 46 19 3 Li 18 47 5 73 9 Mg 1 46 0 388 1 20 2 0 Mn 770 837 234 5 555 365 229 470 800 312 Mo 1 8 2 85 1 9 12 9 0 6 4 87 Na 96 0 57 3 25 0 741 0 547 2 0 1 39 Ni 40 57 6 23 44 1 49 3 55 3 44 1 75 2 36 9 P 00 0 14 0 027 0 0998 0 11 Pb 105 101 11 7 161 21 9 22 7 404 42 3 47 Rb 42 69 38 100 71 0 S 90 0 352 0 397 Sb 2 0 0 3 3 79 1 09 0 59 171 0 6 8 33 Sc
70. b 4 1 1g mg g 1000 D0 mg g a b x W o 69 5 0000000000 0000 U D D I 410 00000000 200 30900 00 0 0190 00000 0000000 5600 80 C 30 80 5 C 00000000 3000000 0 000190 00000 70
71. d 4 5 1 1 2 e e 5 0 4 5 1 1 2 9 f 2009 L 0 20g 100mL 00000000000000 200g L 55mL JIS K 8798 25g 115 K 8034 6mL 200mL 10 5 h logLI I 7 12 8 10g L i t 1mgN mL JIS K 8116 JISK 8228 16 3 82g 1 000mL 0 10 p 00000 0 01mgN mL 1mgN mL 10mL 1 000mL 8 70 1294 10mL 200mL 10mL 300mL 100mL 10 2g 1 1 6mL 5 50mmol L 109 L 1mL 10mL N a xf m x0 001773 g L al 50mmol L mL fl 50mmol L 0 001773 50mmol L 1mL g 70 1256 mL 9 a 00000 4 5 1 1 3 b 00000 34
72. 0 1mgF mL o 00000 100mL 64 200mL pH5 2 10mL x b d 000000 4 1 1g mgF kg 6 00000000 4 9 1 6 a 200mL 10mL 49 3 00000000000 1 0000000 4 9
73. 500mL 80 2mL 6 80 e Q 80 C 5 30 30 0 0001g
74. 23
75. yn D 1 2 DD a o i j 3 000000 8 g h i j 4 o e nn o 000000 8 O OJIS K 0557 1 11 0 J 1S K 8180 71 0994 N 10 36 p E B EB ED LI D C 52 17 0 N 20 28 0000000 C 41 6 N 8 1 0 LEE ELTE EH 000000 O 00000 uu 0o00 uu 0000 000 0 O 0 001mg 99 99994 99 99994 99 999 q
76. 59000 0 00190 00 00 1 200 1050 1100 D 000000000 4000 1 0 00190 0 a b x10 20 0 001g 42 0000 1 000000 a 0 0 O O 600 259 b 600 25 1 D D 0 001g 2 a 3 3 2 b 5g 0 001g b 600 2520 O 2 0 001g c 0 100 e e 3 00000000 0000 poo000000 59000 0 00190 00 000000 000 600 25 C9 0 20 D 0000000 0 001 g0 00 a b mc M ai 4 3
77. 0 10g 95 100mL 9 00000000 0 0 oogL n JIS K 8576 JIS K 8102 250g 500mL 3 000000 451 1 4 00000 a 3 1 1 0 01g 200mL b 10mL 59 I 2g c 29 I 451 000 20m d
78. b 105 110 2 2 40 2mm 2 3 00000000 3100000000 100m0 000 1050 11061 20 OO 400 N O ju 3o 18
79. Il 4 7 TOC 1111 5mL z 2 500r pm ami 2 500rpm 10 203 1000 1055 2 825 C 5 a 0000 30 b 000 0 10 6 0mg 0 001mg wb 10 100mg 0 001mg 10 3 20 3 d 00 z 4 1 1g mg g W2 0 mg g a b x10 Xv 96 W1 W2 lI 4 7 TOC 6 00000000 a 100 105 C 2504 mp 1 D U D b 000000 19 ll 124111 000000 51 48 000000 481 4
80. poo 3100000000 00190 01000000 KMnos 40 60 5 0 0000 0000000 300mLD poeB0000000000 20mmol LO 100mL 0 000 00000000000 3009 L0 5mL 100mL 0000000 300 000000000000 0 20mmol L 10m 0000 30 000003000 p000000000 S0mmol LO 00000000006 NA kmnoap n Q0mmol L U 10mL oO 0030 70 10mL 009 5 mL 000000000 0 0 500mL 500mL 28 45 00 451 000 4511 00000 1 0000000 2 DD a 5 K 0557 A3 b 25mmol L J 9 K 8951 1 4mL 100mL 1L 5 K 8005
81. 6 00000000 4 5 2 10g Huu 2mol L 100mL 38 4 5 1 1 6 452 2 1 0000000 2mol L 2 a D0JISK 0557 b c 000000000 4 5 2 1 2 c dj 0000 00 0 4 5 1 1 2 e e 00000000 0 0 200g L 0 4 5 1 2 2 f f 0000000000000 0 4 5 1 2 2 9 9 000000000000 0000 10g L 0 4 5 1 2 2 h h 0 01mgN mL 4 5 1 2 2 j 3 000000 a 000000 b 0000 00000 4 00000 3 2mol L 4 5 2 1 2 b
82. 3 000rpm 20 1 VOC 3 00000000 10000 2mm 3 000 rpm 20 16 32 0000 1 a 00000 b 2mm 000000 2 00 a
83. g kg 5 g kg 5 u g kg 5 u g kg 1 0000000 u g kg 1 1 1 00000000000 3 0000 00000 UDUDnu MBASH mg kg 1 mg kg 1 mg kg 0 05 PCBs GC ECD mg kg 0 01 PCB u g kg 05 0 005 poo H g kg 0 5 0 005 u g kg 05 0 005 u g kg 0 5 0 005 u g kg 0 5 0 005 u g kg 0 5 0 005 u g kg 05 0 005 u g kg 05 0 005 u g kg 0 5 0 005 u g kg O0 5 0 005 a 000 H g kg 1 u g kg 1 Y DO0000000 H g kg 1 000 u g kg 1 p p LU LI u g kg 1 pp 000 u g kg 1 pp 000 u g kg 1 u g kg 1 H g kg 1 u g kg 1 000000 u g kg 1 00000 u g kg 1 u g kg 1 H g kg 1 H g kg 1 H g kg 1 trans 0 0000 H g kg 1 dst 0000 g kg 1 g kg 1 trans 0000 u g kg 1 dst 0000 u g kg 1 g kg 1 u g kg 1 g kg 1
84. 300m 0000 i 500mL b No PDDDODD A 300mm d 60000000000 500mL U 451 1 00000000 e 00000000 451 100000000000000000 50m 00000000 50m 50 700000000 50 100 e000000000000 00000000 5 7m mng en 140 00000000000 500mL00000000000000000 m i 30 na 00000 0 00023 0 03 32000 000000000 ua 100m0 JI 00000000 S00g L I 20m n0 0 0 5 5 po 1 451 51
85. mg g 0 02 mg g 0 1 uuu mg kg 0 1 mg kg 0 5 D mg kg 0 5 mg kg 5 D mg kg 5 uua mg kg 5 uua mg kg 0 5 mg kg 0 5 mg kg 0 2 uuu mg kg 0 2 mg kg 0 2 uua mg kg 5 mg kg 0 5 Doo mg kg 0 5 Bt mg kg 0 01 mg kg 0 01 I 1 0000 U 1 1 00000000000 00 2 DUDU L 00000 g kg 1 g kg 1 12 g kg 1 11 00000000 g kg 1 12 g kg 1 1111100000000 g kg 1 1 1 2 0 0000000 g kg 1 UUJupnununun g kg 1 u g kg 1 1370000000 g kg 1 u g kg 1 u g kg 1 0000 42 0000 0000 g kg 1 1270000000 g kg 1 u g kg 1 g kg 1 g kg 1 1 2 0 0 0 0 3 0 0 0 0 000 ODBCPO H g kg 1 uut u g kg 1 g kg 1 H g kg 1 u g kg 1 DDVPU H g kg 1 H g kg 1 u g kg 1 u g kg 1 H g kg 1 MEPR H g kg 1 g kg 1 0000000000 CNPO H g kg 1 Hu u g kg 1 u g kg 1 g kg 1 g kg 1 u g kg 1 u g kg 1 u g kg 1 g kg 1 u g kg 1
86. 1 7mmoa4 0 0 0000000 1 8mmol L J IS K 8622 0 143g JIS K 8625 0 191g 1L I Hl B d B H B H D O O 0 3mmot L 1 E U D U U 2 7mmol L JIS K 8622 0 025g JIS K 8625 0 286g 1L po0000000000 1 3mma 4 0 0000000000 1 3mmol4 0 000 O 30mmol 0 00000000 100g L m 0 p a d ur 59 2310 0 31g J IS K 8866 0 50g J IS K 8863 1 8690 JIS K 8032 100g 128mL JIS K 8295 5g 4mL 1L 2 5mmoad L 2 000 2 00000000 13 00000000 O O 2 4mmol L J 0 41590 JIS K 9704 2 2 1 3 0 291g 1L 0000 o f O 15mmol L 0 5mol L 6 30mL 1L e 25mmol L 0 5mol L 50mL 1L h 0 1mgrF mb 4 9 1 2 f i 0000000000 25u gF mD 0 1mgF mL 25mL 100mL 16 30mL 500mL 1L 66 3 000000 a 0000 b 0000 00000 1 2mL d 17 o 000000 ani
87. 5 K 9005 d 5 K 8885 1000 150 m 2 e 2 59 50mL 1 2 _ 3 N N 0 192g 1 10 4mL 200g L 4mL JIS K 8371 41g 400mL JIS K 8355 24mL 115 K 8034 400mL III 0 163g 145 10mL JIS K 8085 pH 4 7 1L f mL JIS K 8005 500 C 100 0 221g 1L 115 0030 F 100 00000000000 2u 9F mL gd 0 1mgF mL 10mL 500mL h 1 2 1 150 C 1 2u g F mL 10mL 3 a b 4 00000 8 20 5g 0 019 40mL 1mL 340mL b 19 60 4 9
88. dd mgCN mL 1 C a xf x5 204 X100 0000 cuni mgCN mL al 0 1mol L mL 0 1mol L HI 5 204 0 1mol L 1mL mg I pagado og ooo 1u GEN mb 1mgCN mL 10mL 1000mL 20g L 100mL 10mL 100mL Ig du lO LU LL 1mgCN mL J 3 a 48 10 00 b e YO D de J Big Jl ral ly At A z z x 2 r I 500 F Cr gu i 2 100 U 48 100000000 53
89. o 000 e 0000000 1 o 0000000 000000000 o 00000 MDL MDL Method Detection Limit
90. poo000000 1 2mL min 68 410 00000000 1 0000000 4 10 80 C 2 00 a 5 8848 b 5 8987 3 000000 a b 000000000 805 d DU D D 80 5 e 00000 80 C 5 30 0 0001g f 805 9 00000 0 0001g 4 a 0000 32 200 30g 0 01g 5 6
91. o 00000000000 e 000000000000 000000 00800 3 00000000000 a b PAOBO BO Dg ag gg 000 0000000000000 c pegada gg gg ago 00000000000 d 00000 D 1
92. 600 1 0 5300g 0 001g 20mL 25mmol L b 20 1 a x x x 100 200 x x0 002650 9 X 25mmol L mL 0 002650 25mmol L 1mL d 5 8962 d 5 K 8983 e DO000000000JI S K 8863 509 1L f K 8896 0 02g JIS K 8840
93. 0 1mV pH d 0000000000000000 d 3mol L 3mol L 100g L e 000000000000 25 63 4 00000 4 9 1 4 a f
94. H g kg 1 u g kg 1 g kg 1 g kg 1 g kg 1 u g kg 5 lal Bla P H g kg 1 0 1 1 00000000000 00 4 1 DUDU D DID Daupnaupnaunp g kg 0 3 DUIDDDDDDDUDDDU u g kg 0 3 poo000000 81 u g kg 1 0000000 u g kg 1 0000000 u g kg 1 u g kg 1 40000000 u g kg 1 g kg 10 u g kg 10 g kg 10 00000 n000 u g kg 25 u g kg 10 u g kg 10 00000 20000000 g kg 25 podo000000000 g kg 10 u g kg 10 000000 2 0 0000000 u g kg 10 000000 MU DUDUDUD g kg 5 4 u g kg 5 4 u g kg 5 4000000000 u g kg 5 4etpo0000000 u g kg 5 4 u g kg 5 poo000000 u g kg 50 poo000000 u g kg 5 24000000000 H g kg 5 u g kg 5 DUDU 4tp0000000 H g kg 1 po0000000 4n000000000 H g kg 1 4 u g kg 1 4000000000 H g kg 1 4etpoo0000000 H g kg 1 4n000000000 u g kg 1 poo000000 u g kg 10 poo000000 u g kg 1 24000000000 u g kg 1 u g kg 1 47a 00000000 H g kg 0 01 178 00000000 g kg 0 01 u g kg 0 01 2 0000
95. O 9 10 11 12 13 14 30 C 0 1 gF mL 1 lp mL 30 15 1p gF mL 110 0 1mgF mL 120mV 25 C 0 1u gF mL
96. 100mL Og L 20mL NO 10mL D Uu 0000020 3mL min 000000 90m 100mL 25mL CN 0 50 9u g0 0000000 50 10mL mgCN kg 48 2 1 0000000 00 0000000000 250mL 2 00 a JUD JIS K 0557 b 00000000000 0 Gg L r 4 8 1 2 b 00000000000 Qoog L r 4 8 1 2 c d EDTA 4 8 1 2 d e 4000 4 8 1 2 e f 000000000 009 4 8 1 2 f A3
97. 1 Jala F3 EEIELEIEILEIEILBIES nawan EL ESL E3 E3 E3 o lolo lolo OJOJIOIOJO OJIOJIOJOJOJOJOJO O r3 O O O OJO o jo o Jo o o o jo jo jo jo jo jo o jo jo o jo o o sisiszisris srisr sriE i RE RE ss a sr sr sr ir st E r3 N E3 r3 i o e N O E E mla mla r3 olo E iJ D o EIE mla mla 1 mla pea ns d L1 E l L E E E a r3 m al El LE CN L3 o r3 maa mla mla gjo sa E ml lam ma Bou mla mla mon mlm o2 e augu zlajz o c ala lng orlo fgagaoo loojoo aoao aoaaa gt x hn Soap r ao mojo oloo a ogo Ajo 000
98. ul l 4 51 5 VOC e 00000000 0000 DUDU 0000 3 DO DD DD DU UD
99. 1 000000000 0000000 2 000000 a 00000 0 SOPO Standard Operation Procedure 0 0 000800060 b
100. 0 lOomL 1000000000000 0000000000 3 000000 l 43 1090000000000000000000000000 000000000000 1000000 00000000 3000 500000000000 200ml 40000 BD D D DO O ED O FO LU Dg tL O 300mL 500mL 200mL L3 L3 E3 EJ p oana 0O U 43 1 00000000 4 DDDDD a 1 3000 500m D 00000 eg b 4100000000000 000000 9 a0000000 3000 500mL 200 30ml D DDD DD D D D d 000000000 009 20mL 0000000000000000000 e 00000000 145 5mL 0000000000000000000 A 100m g 00000000000000 000000000000 h 300000 2 0 000 2059000000000
101. 0 C 2 0 72g 0 001g 200mL 20mL 300mL JISK 8913 2g 145 5mL 5 100mL 10g L 1mL mL 0 1mol L f f a Rd AUN 100 200 2xx0 003567 a 9 b x 0 1mol L mL 0 003567 0 1mol L 1mL g 3 a 3 1 1 Q 300mL 3 0 01g 20mmol L 100mL 300g L 5mL b 30 4 c 50mmol L 100mL 3 7 10mL d 500mL 26 e f 9 h
102. 00000 0 1 gF mbi 200mL 6 500mL JIS K 8355 JIS K 8150 10u gF mL 20mL 0 1mgF mL 20mL 1u gF mL 20mL 58g 1 2 4g 200g L pH pH 5 01 5 5 1L 500mL JIS K 8355 57mL JIS K 8150 5890 JIS K 8288 0 3g 200g L pH pH 5 0 5 5 1L 3 a 0000000 b
103. 0000000 10m 00000 000000 10mmol L 25 mL 1 10 2mL 10mmol L 00000000000 pa00090000000 0 10000 25 I 4 4 44 sedi 1 0000000 CODsed
104. 00000000 1u GEN mbi 4 8 1 2 1 3 a 00000 4 8 1 3 8 b 4 00000 4 8 1 4 a 0 5 00 a 620nm b 000 1u gCN mL 0 50 9mL 50mL 10mL 5 c O o 4 25mL CN 0 5 9u g 50mL 5g L 1 148 pH6 8 10mL 10 T 10g L 0 25mL 5 57
105. 0000000000000 im 000000000 4 6
106. 110 C 100 0 7229 1L op 10 Qu gmL 0 1mgN mL 20mL 1L Y 0 5 2mm JO 40g 300mL 125 50mL 100mL 5 1 39 50mL 2 100mL 5 200mL 24 3 a 000000 b 00000 4 00000 4 5 2 1 4 a b 100mL 4 5 2 1 4 a b 42 4 5 3
107. 28 5 12 15 25 6 90 Se 0 72 0 43 1 09 0 214 0 76 Si 96 21 24 2 40 00 29 08 Sr 110 126 68 130 125 96 277 170 Th 5 8 9 2 18 Ti 0 64 0 34 0 456 0 457 0 5 0 22 U 2 0 3 13 6 3 20 V 250 134 44 8 95 252 93 4 127 105 55 5 343 738 438 172 119 824 142 977 000000000 13 0 2 3 000000000000000 NIST NIST NRCC NRCC River Sediment Marine Sediment Marine Sediment Marine Sediment SRM 1939 SRM 1941a HS 1 HS 3 g kg ug kg g kg pg kg Hexachlorobenzene 70 25 a HCH y HCH trans Chlordane Heptachlor epoxide 510 cis Chlordane 220 2 33 0 56 trans Nonachlor 270 1 26 0 13 cis Nonachlor Oxychlordane 2 59 Dieldrin 1 26 2 4 DDE 0 73 0 11 4 4 DDE 540 6 59 0 56 2 4 DDD 20 4 4 DDD 60 5 06 20 58 2 4 DDT 4 4 DDT 1 25 PCB 18 1 15 PCB 26 4200 290 PCB 28 2210 100 9 8 PCB 31 6860 6 2 PCB 44 1070 120 4 80 0 62 PCB 49 95 2 1 PCB 52 4480 6 89 0 56 PCB 66 930 68 1 4 PCB 95 75 1 1 PCB 99 4 17 0 51 PCB 101 820 110 1 6 1 62 0 21 PCB 105 365 0 27 PCB 110 9 47 40 85 PCB 118 510 100 1 1 PCB 128 100 187 0 32 PCB 138 570 13 38 0 97 1 98 0 28 PCB 149 92 1 1 PCB 151 2 62 0 48 0 08 PCB 153 176 1 9 2 27 0 28 PCB 156 0 93 0 14 PCB 170 110 3 00 0 46 0 27 0 05 PCB 180 160 5 83 4 0 58 1 17 0 15 PCB 187 180 7 0 PCB 194 1 78 0 23 0 234 0 04 PCB 206 3 67 0 87 P
108. 5 4 a 880nm 710nm 3 pH p 1 g L 4 1 V lug 0 35u 9 Do 2 III 0 03g d O00000 4 1 90 19 mgP g 46 I 46 000 6 00000000 a DO 2800000000000 00000000 0 00 3100000000 E 0000000 190 0190 0 DUDU 0000 0000000 100ml DO 10mL UD 5mL ERA gt 100mL UD 10mL sm Jut 0 0050 0 04mg 0000000 50 p000000000 2009 L 00000000000 409 10 podo00000000000000 0000350000000 00000000 40mL 00000 eor 5mL DUDU 0 D 30mL 3 5mL Doo 50mL uu 0o00 00 gt 880nm0 710nm uu 000 D D 47 b 000 3100000000 0000000 1e 0 019 0 0000 O D 30mL 0 1000000 000000 00050 B 48 0000000 1 0 100mL 46 6 a 00 0000 47 1 0000000 1 11
109. CB 209 8 34 0 49 0 334 0 10 Naphthalene 1010 140 9 0 0 7 Biphenyl 175 18 Fluorene 973 8 6 13 3 3 1 Phenanthrene 130 489 23 85 20 Anthracene 184 14 13 4 0 5 l Methylphenanthrene 101 27 Fluoranthene 190 981 78 60 9 Pyrene 170 811 24 399 Chrysene 51c 380 24 14 1 2 0 Triphenylene 197 11 Benz alanthracene 46 427 25 14 6 2 0 Benzo a fluoranthene 118 11 Benzo b fluoranthene 740 110 7 x 1 2 Benzo k fluoranthene 361 18 2 8 2 0 Benzo e P yrene 553 59 Benzo a P yrene 628 52 7 4 3 6 Perylene 452 58 Indeno 1 2 3 cd pyrene 525 67 5 4 1 3 Benz a h i perlene 501 72 5 0 2 0 Dibenz a i Janthracene 74 3 Dibenz a clanthracene 43 1 Dibenz a hlanthracene 1 3 0 5 Benzo b chrysene Picene 14 SOP
110. I
111. l L 2 0 0 a 0 0OJISK 0557 b Gmol L n J o 000000000 d p0000 10 0 4 5 1 1 2 e IS K 8121 149 1L 600 700 e 25mmol L 4 5 1 1 2 b f 0 4 5 1 1 2 f
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