Analytical Circle No.30（2003.9）
Contents
1. 95000000000 G TK Labot S Sunny LIMITED vay 10 00000000000000200000000000000000 gt 000000000000000000000000000000000 gt 0000000000000000000000 20000000 0000 000000 OO OO 00000000 KW 0000000 N 000000 No 308 10141 0000000000 1 468 0000 305 10151 39 0001 3002 10161 1 20 0001 309 10171 10 28 00012. 460 6 eU O L 2 U 10 6 ell u 00 300 0 000000 20ppm BOB IB d B 000 000 26000 60441 1120221 l1 Methoxy PMS 600000060 1 5 460 DET o 000000 Histamine 1000 30 000 207k Q amp A
3. 00 000 2 0 00000000000000000000000000 Wako Analytical Circle No 30 vrocsrau EBEE CHEMICAL DCSIGN 5 0 s C 000000000 000000000000 000000000000000000000 21215 7 Rack mounted Desk Top EE wlx f Small Scale 0 00 Middle Scale 0 00 Loroe Scole 0 00 5 1 2000 00000 0000 00000000 0000 2 0000000 CI 00000000 00000 0000 0000 O 0 0000000 0000 000000000 00 00 000000000000000 000000 0000 B Pocket PC 0 1 08000001 00 O EA TEIE 0 0 0 o O O L
4. Wako Analytical Circle No 30 KE 0000000000000000000000 00000000000000000000000 00000000000000000000000 000000000000000000000000000 0100060000000000000000 2 00000000000000000000000000 Wako 000000000000000000000000000 remaemascaaa a 016 00346 000000000000000000 Acetone 00000000000000000000000000 000000000000000000000000000 500 079000675808 es D 0000000000000000000 01 100 000000000 01 1 0000100000001 000 an 04 1 0000400100000000 Lot 0 000000000000060000 320012000 000000000 000000 Bs a I ooo UUDUIUDUUU 50Kg 00000000 3069 _ 010 1000Kg 100Kg 20 100Kg Ul 5009 0000000 500Kg 00000 1000 9 000000000000000060 10 DE o Eo E 130 0000 Mon 0000000 00000000000000000 10Kg 0000000000000000000
5. G M L O MARAM I LIP 8 7 98080 1 Llaki Pt LIW Lp L Li 0 038 KUNI L LIYA LL Llaki 2 k 540 8605 812 80 06 6203 3741 2103 0023 85135 A 03 3270 8571 R 77 092 622 1005 82 285 6381 8 052 772 07880 A 045 476 2061 4 8 641 1271 298 58 2278 it 022 222 3072 011 271 0285 1000000 0120 052 099 00000000 0120 052 806 URL http www wako chem cojp 03 91150 Kk
6. 0 lavi 18 5 2 0 150 45 000 49 000 0 00 2 0 250 48 000 52 000 3 0 150 45 000 49 000 3 0 250 48 000 52 000 4 0 150 45 000 49 000 4 0 x250mm 48 000 52 000 4 6 150 45 000 49 000 5 4 6 250 48 000 52 000 20000 DDD 00 0000000 00000000 000000000 00000000000000000000000 000000000 18 50000000000000000 30 50000000000 0000000000000000000000 0000000000000 Wi Navciss Navi C30 5 18 5000000 000000000 0 95 00 000000 5 mil LULU LD Ea A 0o00 A 00000000 A 100080 9 0000 00 ETD Wako A
7. 5 Column size 4 6mm x 250mm Eluent 20 2 2 5 Flow 1 0ml min 435 C ase amp 2 Detection UV 210nm 0 04AUFS g En Sample 1 Acid 2 Tartaric Acid 11 17 9 5 17 Formic Acid 4 Lactic Acid 5 Acid 6 Citric Acid 70Fumaric Acid 8 Succinic Acid 9 Acid 10 JPropionic Acid J 110Levulinic Acid 3 C18 A 30 50 000000000000 00000 0 18 5 0 22 500000 1 0000000000 45 18 4 HPLC Conditions DU Column size 4 6mm x 250mm Eluent 100 18 5 Navi 22 5 Navi C30 5 Flow rate 1 0ml min Temp 3556 A 5 Detection UV 295 0 064 5 3 3 Sample 10 d Tocopherol I 20 d 7 t 1 d Tocopherol g 1 4 d 4 4 JU L J zoh L LJ C18 C18 co c18 DO C18 G TK Wako Analytical Circle No 30 gases 000000000 ENA 5 19 Histamine KIKKOMAan WAS N S 00000 00000 0 00000 000 000 60 0000 00000 0005 0
8. g 00000000000000000 50Kg 00000000000000 00 300Kg 00000 5 00000 000000 200 ___ 400 000000 400 040 00000 000000 1000L 000000000000000000000000 00000 gooo 2000 000000000000000000000000 00000 000000 20001 000000000000000000000000 00000 ___ 0965 100000 0000 OOL 100001 0000000000000000000000 50 m 0000000000 1 0000000 0000000000 100Kg 90 300Kg G MI Wako Analytical Circle No 30 70 7 5 3 h uma m UZZLE E mail ed 45 00000 T 000000000 1 9 10000 10 300000000000 HUUDUUHUUUU 3 9 19000 000000 00 150 100 100 0000 0 00 000 0000 00 000000000 3 1 2 0 0000000 000 00000000 00000 0000000000 0 0 0 0000 00 00 0 0000 00 06 6203 1999 0
9. 5 16 0000 0000000 291 41751 50 13 0000 635 04191 PTFEQ 1 100 19 2001 KN B Wako Analytical Circle No 30 JUD UD UI MJRFVY 1008 0 15 28901010 0000 _ 2000 00 0 5 No 7 1 0 No 8 2 0 No 9 5 0 No 10 10 0 5 061 01631 0000000000000000 40000 00000 3 3001 206 06701 000000000 10000 00000 2 9000 200 09021 000000000 100000 00000 2 9000 KN H 21 C100 14 CnH gt n 1 SOsNa 10 14 3 0 HPLC Conditions C11 Column Wakopak Navi C18 5 4 6 250mm Eluent 0 1mol L NaClO40 CH3CN H200 65 33 Flow Rate 1 0mL min at 40 Detection 221nm 284nm Inj vol 20u L Sample Sodium Alkylbenzenesulfonate C10 14 2 0 LU 1 0
10. 0 10 20 Time min mpi Sodium Decylbenzenesulfonate Standard Solution 1mo ml methanol solution 00000 1 5 1 192 13121 Sodium Undecylbenzenesulfonate Standard Solution 10000 1 5 1mg ml methanol solution Sodium Dodecylbenzenesulfonate Standard Solution F i 1mo ml methanol 00000 1lmix5A Sodium Tridecylbenzenesulfonate Standard Solution 1 7 methanol solution 00000 1mix5A Sodium Tetradecylbenzenesulfonate Standard Solution 1mg ml methanol solution 00000 1 5 KN H Wako Analytical Circle No 30 L 79277 100 T Ju X u 2 2 U 100 0000000000 2400000 AARAA 0 00000000000 10 J 0 5 AO gt Est 1000 00 100 mi 0
11. 60 000 NEW 126 BDE 126S 3 3 4 4 5 1 60 000 127 1275 3 3 4 5 5 60 000 NEW 128 1285 2 2 3 3 4 4 1 27 000 131 1315 2 2 3 3 4 6 60 000 NEW 138 1385 2 2 3 4 4 5 1 27 000 139 1395 2 2 3 4 4 6 1 0m 60 000 140 1405 2 2 3 4 4 6 HexaBDE 1 60 000 NEW 141 1415 2 2 3 4 5 5 60 000 NEW 142 1425 2 2 3 4 5 6 1 48 000 144 1445 2 2 3 4 5 6 1 48 000 153 1535 2 2 4 4 5 5 1 27 000 154 1545 2 2 4 4 5 6 1 0 27 000 155 1555 2 2 4 4 6 6 HexaBDE 1 27 000 156 1565 2 33 4 4 5 60 000 NEW 158 1585 2 3 3 4 4 6 1 60 000 159 1595 2 33 4 5 5 60 000 NEW 160 1605 2 3 3 4 5 6 1 48 000 EE EO 1 60 000 166 1665 2 3 4 4 5 6 1 27 000 167 1675 23 4 4 5 5 60 000 NEW 168 1685 2 3 4 4 5 6 1 0m 60 000 NEW 60 000 NEW 181 1815 2 2 3 4 4 5 6 1 48 000 182 1825 2 2 3 4 4 5 6
12. UJU DUDUDE oli 00 00000000000 0000000 0000 5 0 0000000000 000002001000000 0000000 5 00 0000000000 1 00 000000000000000 mam au a 0 100 000000000000000 1 00 MUG 0 100 000000000000000 00000000000 0 100 0 100 00000 000 0000000 304 14401 100 100 10 5 0000 20 30 000 000000 306 145811 100 Aqua Testi 10001 000000 3 000 309 09441 02 00000000000000 _ 5 6000 300 09471 BL4BLB 1 7000 304 13421 01 0000 0000 5 0001 Wako Analytical Circle No 30 _ ZI gt 0 0 0 0 BDE 000000 2 1 0015 2 MonoBDE 1 0m 15 000 2 BDE 002S 3 1 0ml 15 000 3 BDE 003S 4 MonoBDE 1 0ml 15 000 4 BDE 004S 2 2 DiBDE 1 0m 27 000 6 0065 2 3 DiBDE 1 0m 27 000 7 0075 2 4 DiBDE 1 0m 15 000 8 BDE 008S 2 4 DiBDE 1 0m 15 000 9 BDE 009S 2 5 DiBDE 1 0m 48 000 10 BDE 010S 2 6 DiBDE 1 0m 15 000 11 BDE 011S 3 3
13. 00000 0000000 HB 10000 000 00000 15 0000000 _ 0000000 69 10000000000 39 00000 0 99 k 2200000000 69 b 4400000000 4 59 00000 999 gt 20000000000000 39 00000 0 99 1000000 00000 000 00000 11000 1 1100 2 20 10 0 1 2000 0000000000000000 000 HUU HUO OTH H 2 4 6 Trichlorophenol 2 Propyzamide Anthracene 40 N N Bis 1 methylethyl benzamide 5 Lenacil 6 Bis 2 ethylhexyl phthalate E S a e o lt T C Z 0 10 20 30 40 0 10 20 30 40 ODODO iti 910 9 9 101913 295 41651 P resep Multilayer Silica 000000 57 18 0001 299 42151 Adapter 10 15 0000 295 42251 Column Adapter 1 4 0000 Wako Analytical Circle No 30 900000000 00000000000 00000 00000000000 0 00000 0000000000 lt ii 00000 0000000000 Doo 29099 41551 Presep Active Carbon blend
14. 1 017 60 000 NEW 183 1835 2 2 3 4 4 5 6 HeptaBDE 1 48 000 184 1845 2 2 3 4 4 6 6 60 000 185 1855 2 2 3 4 5 5 6 1 0m 48 000 190 1905 2 3 3 4 4 5 6 1 0 27 000 191 1915 2 3 3 4 4 5 6 1 60 000 NEW 1 0 60 000 203 2035 T Ioa N 1 0m 60 000 204 2045 T 1 0m 60 000 NEW 205 2055 1 0m 60 000 208 2085 1 0 75 000 NEW 209 2095 1 27 000 50 o mlin Isooctane solution KN B ULTRA Scientific 5 ULTRA Scientific O0 0 15090010 ISO Guide 25 00000000000 E Polychlorinated Terphenyls Chlorinated Terphenyls Purity 95 99 Compound Catalog Unit 4 chloro o terphenyl RTP 019 10mg 4 chloro p terphenyl RTP 002 20mg 2 4 dichloro p terphenyl RTP 014 20mg 2 5 dichloro o terphenyl RTP 005 10mg 2 3 5 6 tetrachloro p terphenyl RTP 015 10mg 2 4 4 6 tetrachloro p terphenyl RTP 010 10mg 2 3 4 5 6 pentachloro p terphenyl RTP 016 10mg tetradecachloro o terphenyl RTP
15. 27 000 51 0515 2 2 4 6 TetraBDE 1 0m 27 000 53 BDE 053S 2 2 5 6 TetraBDE 1 0 60 000 55 0555 2 3 3 4 TetraBDE 1 0m 60 000 NEW 58 BDE 058S 2 3 3 5 TetraBDE TOM 60 000 NEW 62 BDE 062S 2 3 4 6 TetraBDE 1 0ml 48 000 66 BDE 066S 2 3 4 4 TetraBDE 1 0 27 000 67 0675 2 3 4 5 1 0m 60 000 NEW 68 BDE 068S 2 3 4 5 TetraBDE 1 0 60 000 69 0695 2 3 4 6 TetraBDE 1 0m 27 000 71 BDE 071S 2 3 4 6 TetraBDE 1 0m 27 000 72 0725 2 3 5 5 1 0m 60 000 73 BDE 073S 2 3 5 6 TetraBDE 1 0m 60 000 74 BDE 074S 2 4 4 5 TetraBDE 1 0m 60 000 NEW 75 0755 2 4 4 6 TetraBDE 1 0m 27 000 76 BDE 076S 2 3 4 5 TetraBDE 1 0m 60 000 77 BDE 077S 3 3 4 4 TetraBDE 1 0m 27 000 78 0785 3 3 4 5 1 0ml 60 000 79 BDE 079S 3 3 4 5 Tom 60 000 80 BDE 080S 3 3 5 5 TetraBDE 1 0m 60 000 81 BDE 081S 3 4 4 5 TetraBDE 1 0m 60 000 Wako Analytical Circle 30 50 o mlin Isooctane solution 00000000000000000 0 AccuStandard 2090000000000000000000000 0 BDE 0000000 ni 85 BDE 085S 2 2 3 4 4 PentaBDE 1 0 27 000 86 BDE 086S 2 2 3 4 5
16. 22 ODSIJUIDDDUDUDUDUDDUDUDDUDUDUUUDU A 5 5 1 000000 2 1 4 00000 0 000 SHIUBDUUUDUUDUUunu 5 000000 1 2 00000 955000000000000 3 0000000000000 Wako Analytical Circle No 30
17. 1 0 60 000 87 BDE 087S 2 2 3 4 5 PentaBDE 1 60 000 NEW 88 0885 2 2 3 4 6 1 48 000 97 0975 2 2 3 4 5 1 60 000 NEW 98 0985 2 2 3 4 6 60 000 NEW 99 0995 2 2 4 4 5 PentaBDE 1 27 000 100 1005 2 2 4 4 6 PentaBDE 1 27 000 101 1015 2 2 4 5 5 PentaBDE 1 60 000 NEW 102 1025 2 2 4 5 6 1 0 60 000 103 1035 2 2 4 5 6 1 48 000 104 1045 2 2 4 6 6 60 000 NEW 105 1055 2 3 3 4 4 1 0m 60 000 NEW 106 1065 2 3 3 4 5 60 000 NEW 108 1085 2 3 3 4 5 1 0m 60 000 NEW 109 1095 2 3 3 4 6 1 0m 48 000 114 1145 2 3 4 4 5 1 0 60 000 NEW 115 1155 2 3 4 4 6 1 0 48 000 116 1165 2 3 4 5 6 1 27 000 118 1185 2 3 4 4 5 1 60 000 119 1195 2 3 4 4 6 1 27 000 120 1205 2 3 4 5 5 1 017 60 000 NEW 121 1215 2 3 4 5 6 1 60 000 Pempe 1 0 60 000 124 BDE 124S 2 3 4 5 5 PentaBDE 1 0m 60 000 125 1255 2 3 4 5 6
18. DiBDE 1 0m 15 000 12 BDE 012S 3 4 1 0ml 15 000 13 BDE 013S 3 4 DiBDE 1 0 27000 14 BDE 014S 3 5 1 0m 60 000 15 BDE 015S 4 4 DiBDE 1 0ml 15 000 16 0165 2 2 3 TriBDE 1 0m 60 000 NEW 17 BDE 017S 2 2 4 TriBDE 1 0m 27 000 18 BDE 018S 2 2 5 TriBDE 1 0m 48 000 19 BDE 019S 2 2 6 TriBDE 1 O In 27 000 20 BDE 020S 2 3 3 TriBDE 1 0m 60 000 NEW 22 BDE 022S 2 3 4 TriBDE 1 0ml 60 000 NEW 25 BDE 025S 2 3 4 1 0m 27 000 26 BDE 026S 2 3 5 1 0 48 000 27 BDE 027S 2 3 6 TriBDE 1 0m 27 000 28 BDE 028S 2 4 4 TriBDE 1 0 15 000 29 0295 2 4 5 TriBDE 1 0m 60 000 NEW 30 BDE 030S 2 4 6 TriBDE TO 15 000 31 BDE 031S 2 4 5 1 0m 48 000 32 BDE 032S 2 4 6 TriBDE 1 0m 15 000 33 BDE 033S 2 3 4 TriBDE 1 0m 15 000 34 BDE 034S 2 3 5 TriBDE 1 0m 60 000 35 BDE 035S 3 3 4 1 0m 15 000 36 BDE 036S 3 3 5 TriBDE 1 0 60 000 37 BDE 037S 3 4 4 1 0m 27 000 38 BDE 038S 3 4 5 TriBDE 1 0m 60 000 39 BDE 039S 3 4 5 TriBDE 1 0m 60 000 40 BDE 040S 2 2 3 3 TetraBDE 1 0m 60 000 NEW 42 BDE 042S 2 2 3 4 TetraBDE 1 0m 60 000 NEW 46 BDE 046S 2 2 3 6 TetraBDE 1 0 60 000 47 0475 2 2 4 4 TetraBDE 1 0m 27 000 48 BDE 048S 2 2 4 5 TetraBDE 1 0ml 60 000 NEW 49 BDE 049S 2 2 4 5 TetraBDE 1 0m 48 000 50 BDE 050S 2 2 4 6 TetraBDE 1 0
19. 00 O 00 000 O 00 000 10000 00 0 290000 000100 0 0 e 0000000000000000000000000000 0000000000000 0000000 000000000000000000 0000000000000000000000000000 2 0000000000000000000000000000 0020 0 0000000000000 00000000100000000000000000006 0000000000000000000000000000 0000000000000 000000 0000000000000000000000000000 0000000000000000000000 000000000 000000000000000000000000 OA 0 000000000000000000 000 00000 nL 0000000000005 2 00000 0000000000000000000000 033200 9 0000000000000000000000000000 11100000000000000000000000000 000 000000000 00000 000000000000000000000000 00000000000000000000000000000 00000 0000 00000000000000000 99 0000000000000 000000000000000 0000000000000000000000000000 00000000000000000000000000000 100000000666000000000000006 000000000000000000000000 0000000000000000000000000000 0000000000000000000000000000 1273000000000000000000000000 EA 160000000000 99 00000000000000000000000000000 000000000 00 0 00 0 2000000000000000
20. 012 25mg ULTRA Scientific Kit contains three ampules 1 x 1 1 of each Aroclor 100 g mL in Hexane Aroclor 5442 Aroclor5460 Aroclor5060 RTP 1A Kit U H Wako Analytical Circle No 30 0167 F 0 0 5 21001 150 40 180000 15 16600 0 0 CORPORATION Veratox For DON 5 5 NEOoGEN Veratox For DON 5 500000000000 DONO 0000000000000 gt 000000 gt 00000000 PUDUDUDUDUDUDUDUDUDUDUDU gt 100000 gt 0000000000 gt D gt 09 D D gt 000000 0 1 ppm 0 25 2 5 ppm 0 0 25 0 5 1 3ppm w sz z E n sil Wako Analytical Circle 30 controls samples l 8331 Veratox for DON 5 5 DON 38 80 0001 8010 5 Aflatoxin 18 26 0001 8
21. 030 Veratox for Aflatoxin 40 61 0001 8041 Veratox for Aflatoxin Single Test 16 36 0001 8031 Veratox for Aflatoxin High Sensitivity 38 61 0000 8044 Aflatoxin Column 5 50 113 000 8310 Agri Screen for DON DON 20 41 0001 8330 Veratoxfor DON 10 10 DON 38 80 0001 8810 5 for Fumonisin JUD 20 42 0001 8830 Veratox for Fumonisin 38 80 0000 8610 Veratox for Ochratoxin 38 80 0000 8210 Veratox for T 2 Toxin T 2 38 80 0001 8110 Veratox for 2 38 80 0000 E 5 DENKO AgraQuant DON 000000000000 5 0000000000000000 PIU gt 10000000000 gt 000000 gt 0000000050000 5 gt 00000000000000 gt 00000000000 gt 0000000000000 gt 00000000 200000 gt 00000 gt 0000000000000000 050 000000000000 y y 00000 0 000000000000 00000000000000000 V gt 000000000000000 4 00000000000 44 gt YYYYYYY YYYYYYY 00 450 0 000000000 7000 DON g
22. ANL IC yU Ce Wakopak Navi DDOD S Histamine 000000000000 2 QSA s 3 1000 HAOHAOA u 0 0 0 0 0 ULTRA Scientific 000000 lt O 00000000 Labot S CHEMICALDESIGN 18 u amp lt U Z Wako 00000 0000000000 00000 0000000000 15 03110 0000000000000000000 15 0312 0 0 0 000000000 00000000000000 5 00000 0000000000 0000000000000 26800000000000000 00000 B B B DD E ____ 00400 ___ unan Ian 10000 0000000 00000 0000000000 00000 00000 0000000000 _____ _____ 00000
23. ed Silica Gel JUDDUUD 10 22 0001 293 41451 Carbon impregnated Silica 28 0000 0000000000000 00000 0000000000 Toluene 100m 100 200m DFO OCDD O 5ng 0 50no mlil 0 1 5ng 50no 0 1 Co PCB 1400 s m 00000000 00000000000 0000000000000 0000000 1090 O OUL O ODOL 100 1000000 T4CDDs P5CDDs Hexane0 50m Toluene0 50m Toluene 0 150m 50 100m 100 200m H6CDDs H7CDDs O8 CDDs T4CDFs DFO OCDD Co PCB 1400 000000000 1901 CO0000000000 00000 0000000000 lt 00000 0000000 50 9 0 1 5ng 50 0 1 P5CDFs H6CDFs H7CDFs OCDF T4CBs P5CBs H6CBs H7CBs CAN D U 1 000000000000000000000 0 0 0 0 0000000000000 100 0 JiS 03110 15 0312100000000 lt unu 0000000000000000 0 I 293 42551 Activated
24. nalytical Circle No 30 Navi C18 5 C22 500 00000000 24 6 34 698 26 339 15 0 14 023 HPLC Conditions Column size 4 6 mm x 250 mm 20 0 25 0 30 0 35 0 25 0 30 0 L35 0 10 0 20 0 25 0 L 30 0 Eluent CHaCN 10mM KH2POA pH 7 0 C30 5 30 70 v v Flow rate 1 0 25 35 C _ Detection 254nm 0 16AUFS _ Sample 10 Uridine 54 8 s 45 45 59 20 3 53 30 Phenol 4 2 4 6 Trimethylpyridine 50 Methyl Benzoate D C18 C18 DI C18 18 50 225 0000 000000000000 18 50 00000000 5 0 00000000000 15 0 20 0 HPLC Conditions
25. t 00000 25 5 l DON 0 0 00 00000000000000 000000 i Y Y gt 0000000000000000 00000000000000000 YY YY JUDDDUUUBDDUUuDUDuupnUuu DONO 29400000000 DONO O U OE UJUUUUDU 2 8 C 000 ON 633 04491 AgraQuant DON 48 48 Well gogog DON 42 000 632 04503 AgraQuant DON 96 96 Well 80 0001 AgraQuant Romer Labs nc J 0000 000 0 013 10361 yi 10 22 0001 010 17691 0000 58 0000 024 07761 10mg 15 700 0033 08011 ur 10mg 27 000 048 18631 Deoxynivalenol 24 0000 046 20401 Diacetoxyscirpenol 10 16 0001 060 03563 10 0001 1 064 03561 H rumonisin 42 0001 063 03411 B2 10mg 39 900 063 01711 Fusarenon X Standard 10 21 0000 141 04661 20 0000 150 02111 Ochratoxin from Aspergillus ochraceus 5 mg 42 0001 209 08251 13 0000 G W Wako Analytical Circle No 30 EN gt gt gt Wakopak X OWako
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