AB Sciex - IonSense
Contents
1. 5 Preparing the Source Region ss 5 Attaching the Vapur Interface VV 6 Inserting the Ceramic lon Transfer Tube into the Vapur Interface 7 Attaching the DART SVP source to the Vapur Interface ccceccceeeeeeeeeeeeeeees 8 Attaching the Mounting Ring 3200 4000 5000 only cc eeeeeeeeeeeeeeeeneees 9 Operation nn 11 Recommended Operating Parameters ccccccceecceceeceeseeeeeeeeeesaeeeesaeeeesaeeeeeas 11 FROUIDICSIMOOUING ser a da aa do e oo odadaioniiodun 11 VISIO RARES ee 11 Replacement Parts ccccecccseccseeecseeeneeeseeeeeeeeseeeseeeeeueesseeseuesseeeseeeseueeseeeseeesaes 12 FRO VISION AIS TON ad de te dant de ae de 12 3 Scope of Delivery This chapter lists the components of the ABI Sciex Interface Standard System Components 1 Sl 200 A R ABI Sciex Flange Assembly 2 SI 999 14 VAPUR Pump Kit 1 4 3 JG10019 Graphite Vespel Ferrule 4 SI 200 INT 5500 Sciex Interlock Plug installed on SI 200 A R 5 Sl 200 CC A Sciex Contact Closure Cable 6 SHSH SS188 M6 12mm M6 x 12 Socket Cap Screws Configuration Dependent Components 1 Varies Ceramic Tubes 2 JVLC ACCUTOF A PLATE SUPPORT YOKE ACCUTOF ASSEMBLY NOTE See VAPUR Interface Ceramic Tubes Reference Sheet 7 5 038 for ceramic tube lengths available on ionsense com NOTE Only for 3200 4000 and 5000 Models 4 D Functional Description The ABI Sciex Interface2. 5 8 with new pictures 12
3. Gas CUR 10 0 Collision Gas CAD 7 dependent on MRM tune lonSpray Voltage IS 0 0 Temperature TEM 0 0 lon Source Gas 1 GS 1 0 0 lon Source Gas 2 GS 2 0 0 Interface Heater ON Suggested Ranges for the Compounds Tab compound specific Declustering Potential DP 0 200 V Entrance Potential EP 1 12 V Collision Energy CE 5 130 V Collision Cell Exit Potential CXP 0 58 V Resolution Q1 Unit Resolution Q3 Unit Troubleshooting Pressure is too high 1 Check the vapur pump settings See the DART Vapur Pump Optimization Protocol 7 5 052 for details available on ionsense com 2 Check the ceramic tube spacing to ensure a 2 mm gap See page 8 for further details Maintenance No special maintenance is required for the ABI Sciex Interface 11 Replacement Parts S1 999 14 VAPUR Pump Kit 1 4 JG10019 Graphite Vespel Ferrule O1 200 CC A Sciex Contact Closure Cable SI 9xxx 4 7 Ceramic Tubes NOTE See VAPUR Interface Ceramic Tubes Reference Sheet 7 5 038 for ceramic tube lengths available on ionsense com Revision History Template Revision 1 Revision History DCR Description of Change Effective Date Initial Release 11 11 2013 2 221 Updated to new format User 7 2 2015 Manual Template _Rev1_7 5 111 Deleted models on page 1 Updated copyright page Deleted disclaimer sentence above table of contents Deleted pumping requirements Deleted and re wrote pages
4. SI 200 GIST DART AB Sciex Interface Manual User Manual Manual Revision 2 Document 7 5 058 IOS nsc Your source for open air mass spectrometry lonSense Inc 999 Broadway Suite 404 Saugus MA 01906 Copyright 2005 2015 by lonSense Inc All rights reserved The information in this document has been carefully checked and is believed to be reliable However no responsibility is assumed for inaccuracies Statements in the document not intended to create any warranty expressed or implied Specification and performance characteristics of the hardware and software described in the manual may be changed at any time without notice lonSense Inc reserves the right to make changes in any product herein in order to improve reliability design or function lonSense does not assume any liability arising out of application or use of any product or circuit described nor does it cover any license under its patent rights or the rights of others The apparatus and application of the apparatus described in this document is protected by US Patent Number 6 949 741 and used under license additional patents pending All trademarks are properties of their respective owners Table of Contents Scope of Delivery 4 Standard System Components ccccccsecccceeeecceeeeeeeeeeseeseeseeeesseeeesegeeesseeeesaeeees 4 Configuration Dependent Components 4 UROCNORAMDESCAIPTIOMSS a a a ie None 5 LS LE SLA ee ee ee 5 CULO a
5. ferrules making sure to set a 2 mm gap between the tube and the APC Inlet To easily set the 2 mm gap push the ceramic tube against the Sciex inlet secure the Swagelok fitting with ferrule and then mark the tube with a pencil Pull the tube out as shown in Image 3 above so that a 2 mm gap is created inside the interface Attach the black rubber pumping line from the diaphragm pump over the barbed pumping port fitting on the side of the Vapur interface Figure 7 Pumping Port Attaching the DART SVP source to the Vapur Interface Attach the base of the source directly to the bottom of the flange with the two M6 x 12 mm socket cap screws provided with the flange t we t ri Figure 8 Attaching the source to the interface Attaching the Mounting Ring 3200 4000 5000 only Sicex 3200 4000 5000 models require a mounting ring before the DART SVP source can be installed Install the two alignment screws into the top right and bottom left holes on the flange piece Use the two M6 x 12 mm socket cap screws to attach the base of the source to the mounting ring Figure 11 Attaching the source to the mounting ring Slide the mounting ring over the alignment holes and tighten the captive screws on the mounting ring i gp a a Figure 12 Attaching the mounting ring to the interface 10 Operation Recommended Operating Parameters lon Source Turbo Spray Curtain
6. transfers the ions created by the DART source to the mass spectrometer and allows the DART source to mount on the mass spectrometer Safety Caution The surface of the flange can get hot Installation Preparing the Source Region First before installing the DART interface place the Sciex Instrument in Standby mode Then carefully remove all gas and electrical connections from the AB Sciex APCI source and remove the source from the instrument The source area should look like the one in the figure below Carefully remove the cover plate and set that aside Caution the cover plate may be very hot _ Figure 2 AB Sciex Source Region Once the AB Sciex source and cover plate are removed the DART flange can be installed Attaching the Vapur Interface Check that the set screw on the back of the flange is completely inserted into the flange s 1 Figure 3 Set Screw Orientate the interface so that the turning rods circled in red in the picture below line up with the keyholes on either side of the source region The interlock plug should also line up Figure 4 Turning Rods Next gently place the interface over the source region and turn the handles downward locking the interface in place Figure 5 Installed Interface Remove the Swagelok nut from the front of the Vapur interface and insert the ceramic ion transfer tube Secure the ceramic tube with one of the provided graphite Vespel
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