Jetstream Series
Contents
1. self Test 2 self Test EP self Test FEYBOAFD Ok Operation Jetstream Series If the instrument passed successfully the test the display will show choose function if not please shut off wait 5 seconds and repeat the power on procedure If the procedure fails a second time see error messages page 19 ERROR keyboard 1 if you pressed a key during the test switch off and on again ERROR temp sensor 3 Send your instrument to be repaired 5 2 Configuration 9 2 1 Leak sensor Setting the sensitivity of the solvent leak detector G Leaksenser 1 leak 00 2 Enter the desired sensitivity Range 00 99 00 solvent leak detector switched off 99 maximum sensitivity Leaksensor 5 leak 50 es choose function For more details please see Maintenance page 21 10 Jetstream Series Operation A WARNING Ignition of flammable chemicals Beware of ignition hazard when using flammable chemicals such as organic solvents Always check the following conditions If an abnormality is found stop operation immediately Leakage of solvent or waste solution Leakage of solvent inside the instrument Inadequate ventilation of the laboratory room This instrument is not explosion proof Although aqueous solvents or organic solvents having an ignition point of 70 C or higher are use2. 12 5 3 2 Temperature programming with internal timer 13 5000 UCM CR ye e 16 5 7 Error EY A PA 19 yr Yal ENO EAA e 0000 20 n D 21 Til LeakeDetection Tesi PTOtOCOluuuuuuudRR YARD DR alada 21 752 1cinperatute COM CCUOM coseno S N 23 7 2 1 Temperature Auto Cal brat on Feature 23 7 2 2 Manual Temperature Correction 24 Sedasa ado Prolocolusaaaaaa Ma a d 26 9 E lt Declaration of Conformity masada de EEE E 21 O re nv nb ors 28 General description Jetstream Series 3 GENERAL DESCRIPTION The Jetstream Series HPLC Column Thermostats are specifically designed for the analytical needs in chemical and biological research as well as routine laboratories The use of thermo electrical elements Peltier offers the possibility of heating and cooling Therefore not only very rapid changes of temperature can be attained but also analyses independent of ambient temperature The temperature regulation 1s microprocessor controlled via the control module or an external computer Software which has been developed especially for HPLC needs allows an optimization of the analyses Safety To prevent any damages there 1s an inbuilt watch dog which three times per second checks the proper function of the temperature control Jetstream Series Inst
3. HPLC PELTIER COLUMN THERMOSTATS Jetstream Series Technical Handbook Rev 2 14 Generalities Jetstream Series 1 GENERALITIES This manual has been updated to the actual Jetstream Series standard It now covers all the features of the actual Jetstream series models All rights concerning this manual are reserved to the editors The authors and editors do not assume any guarantee for the correctness of this manual Nor they will assume any responsibility or liability for defective specifications und resulting consequences The designations used in this manual could be trademarks even though not mentioned as such The contents of this manual could be subject to changes any time and without notice Despite of the carefulness with which the texts and graphics have been composed mistakes could still have occurred The authors would be grateful for any improvement proposition or indication of mistakes Impression June 2008 Jetstream Series Content 2 CONTENT til 2 cn i 3 775 4 2111 N Mes r 5 MANE AMO Us a b 2 7 OOC imi 2 OMOLU 7 270 Oh E A 8 5 e pe e 8811 a 8 5 C OnT OUI e np RR NV 10 5567 10 E ie ka olma 1 5 3 Pro ramiming the T Nermostat sanalda en Makal kanin aza lala 12 5 3 1 Enter a fix temperature 1sothermall
4. L eak field will increase Turn the adjusting knob counter clockwise with a screwdriver to decrease the sensitivity the value in the L eak field will decrease The audio alarm signal is disabled during this operation The leak detection test procedure is recommended to be done at least once a year ENTER Enter to exit the menu 27 Jetstream Series Maintenance 7 2 Temperature correction 7 2 1 Temperature Auto Calibration Feature The new Auto Calibration Feature provides you with the possibility of having your thermostat calibrate itself directly n the laboratory After following the instructions below you thermostat will start a self calibration and control routine for 8 hours see fig 7 2 1 a Room temperature should be stable 22 23 C Press and enter 0 C When 0 C is displayed exit with os 2 Enter 9 5 6 and close with LO 3 The instrument goes through following temperature values 85 70 60 50 40 30 20 10 05 C 4 As soon as the measurements are done the display shows choose function again Switch off for 15 sec and on to activate the changes fig 7 2 1 a C 90 Hr G L 20 lo LY 1 0 80 70 60 50 40 30 TH ee Maintenance Jetstream Series 7 2 2 Manual Temperature Correction Because of the precision of the instrument it
5. contact your service agent After having located and eliminated the source of the error you may continue with this key EAKSENSOR ALARM 2 Solvent is leaking Check column and its connections After having located and eliminated the source of the error you may continue with this key 3 Instrument failure T SENSOR ALARM Contact your service agent 19 Addendum Jetstream Series 6 ADDENDUM Thermostat fan If the oven is not in use both internal fans will automatically turn off after 2 or 3 minutes Idle status If choose function displayed the instrument is 1n idle status cooling and heating elements are switched off as well as the fans after 2 or minutes power consumption 1s reduced to a minimum Power off Programs will not get lost if power 1s switched off Temperature profile The temperature change in the column is approximately 2 3 C min Please take this into consideration by programming and leave sufficient time for the temperature to stabilize Displayed Temperature There is a highly precise temperature sensor PT1000 inside the chamber designed similar to a column Please consider this when comparing with a standard temperature probe 1 e air circulation Erase inputs You only have to overwrite old inputs by new entries 20 Jetstream Series Maintenance 7 MAINTENANCE 7 1 Leak Detection Test Protocol The inside temperatu
6. DUSTRIAL ELECTRONICS Hauptplatz 4 2103 Langenzersdori Austria submitted by EMV Testhaus GmbH Gustav Hertz Strafie 35 94319 Straubing To the judgement of the products with regard to electromagnetic compatibility according following regulations EN 500891 1 EN 55022 1987 Class B EN 50082 2 IEC 801 2 3 4 5 ie 28 Dezember 1995 ae fs aa zz 3 faciurer Signature Testlab 1 z Technical Data Jetstream Series 10 TECHNICAL DATA PMID STATUES AOC 5 85 C Tempera e ae E E E 0 1 C Temperature 51 1 225 0 02 C measured n a 25cm test column Temperature change eee 2 39C min Nominal voltage 100 230VAC Nominalfregueney e 47 63Hz Power ONUR yalad aad 72W Main fuse in drawer close to power connector A Caution To protect against fire type and rating Small flat screwdriver A WARNING Beware of explosion Can cause serious injury High concentration of organic solvent vapor may lead to explosion Do not allow flammable chemicals to leak A CAUTION Beware of high temperature Can cause burns Column oven remains hot for g a while even after power off bihi d li Before accessing inside of column oven make sure it has cooled down sufficiently _ 28 hazard replace fuses with those of the same
7. LATION PROTOCOL Date Ser No Responsible for Installation Please stick to the follow up procedure as explained below to guarantee the proper setup for your column thermostat Select a flat and stable place not submitted to shocks to setup your column thermostat The room temperature should be 17 to 28 C the relative air humidity between 35 and 85 not condensing Please check for sufficient aeriation of the instrument The column thermostat should not stand near a source of heat or in the sun Connect the by packed power cord with the thermostat and a security socket 90 230 V 50 60 Hz and 10A Fuse Please don t use multiple sockets with other instruments also connected to it Connect the control unit with the keyboard connection on the rear side of the instrument and turn the power switch ON The instrument is now performing a self test If afterwards the display shows choose function the column thermostat has been properly set up Signature 26 Jetstream Series CE Declaration of Conformit 9 CE DECLARATION OF CONFORMITY EQUIPMENT Column Thermometer TYPE JETSTREAM 2 Declaration No 255 698 This declaration of conformity is according to article 7 3 and article 10 2 of the Council of European Communities of 3 May 1989 The protection requirements according the Council Directive article 4 and Annex Ill are kept This declaration is given from the manufacturer WO IN
8. able do not use organic solvents having an ignition point below 70 C 5 2 2 T Lock Setting T Lock temperature to prevent destruction of temp sensitive columns T LOCK input 1 temp 002 2 Enter the desired T LOCK temperature 05 85 C 00 C gt T LOCK function inactive T LOCK input 2 Le JLo temp 60 C 11 Operation Jetstream Series 5 3 Programming the Thermostat A CAUTION Touching hot part could result in burns The column oven becomes hot and can severely burn you if touched Before column replacement open the column oven door and wait until the inside temperature in the column oven decreases down to room temperature 5 3 1 Enter a fix temperature isothermal Press Display 1 choose function 2 rel Manualmode g set 00 C 3 Enter the desired temperature 1 e 39 C Manualmode 9 set dc MANUAL set 39 C act 32 27 act XX XX actual temperature In addition the display shows the actual status temperature lower than set heating modus temperature higher than set cooling modus L L set temperature attained TLOCK Pressing this key you reduce the set temperature by one degree If you keep pressing it it will have a repetition effect once a second Pressing this key you increase the set temperature by one degree If you keep pressing it it will have a repetition effect once a second Pressing this key you quit the manual sett
9. ach temperature Slope 01 98min k Programmode 8 deltaT 10 Example 60 C 30 C 10min 20min 15min The oven will keep a temperature of 30 C for 10 minutes than linearly increase it in 20 min to 60 C and keep it for 15 minutes Pr 00 Temperature for 10 Min at 30 C l bli i 202 i D 9 Lo 1Lo delta _17 Operation Jetstream Series Pr 01 increase to 60 und keep it 15 Min gt Lo Pr No i 4 Le Lo Temp 6 clock by input 99 temperature will be endlessly maintained minimum is minute 8 Lo delta t time to raise temp from 30 to 60 C Control unit calculates a slope of 1 5 C min 9 e Now enter next program step or enter following closed loop program closed loop program If you want the temperature profile to repeat itself automatically you can program a closed loop In the example above select prog 2 with clock 00 Please make sure to program sufficient time to allow the thermostat to return to its initial temperature before you make your next analysis To start this program select prog 0 press START and ENTER 18 Jetstream Series Operation 5 4 Error messages If the system detects some kind of error 1t sends a repeated alarm signal 1 Temperature limit has been reached rr T LOCK k ri kiki ALARMI kkk Check programming or selected maximum temperature If wide apart
10. allation 4 INSTALLATION Backside View JETSTREAM Series Installation Jetstream Series 4 1 Location Select a place which 1s stable level and not submitted to shocks The room temperature should be 17 to 28 C the relative air humidity between 35 and 85 not condensing Please take care that the Jetstream does not stand near a source of heat or in the sun Make sure the location offers a sufficient aeration of the instrument Do not expose the Jetstream to alkaline or aggressive vapours During periods of great temperature differences between in and outside let the unit equilibrate for a few hours before installation especially in winter time 4 2 Connections You need the following connections at the location you want to install the unit A security socket with 90 230V 50 60 Hz and 10A fuse A WARNING Electric shock in contact with inside of instrument Beware of electric shock Potentially dangerous voltages are present within the instrument WARNING Electric shock due to improper grounding This instrument is classified as 1 in IEC1010 1 Annex H and plug connected type in IEC1010 1 so connect the power cable to a grounded 3 wire outlet Please do not use a multiple socket with other instruments also connected to it Use the by packed power cord or a similar one Connect the control unit with the keyboard connection on the rear side of the instrument and fix it with the screws Turn the s
11. ect program l prog 00 14 Jetstream Series Operation select program Lo prog 00 slope act program time POOF 10 HEAT sel 30 act 25 Slope positive slope v negative slope 5 No slope Timer function active Time Time left in the actual function 14 Slope function With this key you may quit the slope function and activate the timer function 4 Timer function With this key you may quit the programming function With this key you may decrease the program by one With this key you may increase the program by one Please make sure that sufficient time is programmed to allow the thermostat to reach the desired temperature in this time Typically a 2 3 C min rise should be planned If the programmed time is too short to reach the upper temperature the programmed time will prevail and the oven might not reach the desired temperature _15 Operation Jetstream Series 5 3 3 Temperature curves The Jestream models are able to calculate linear temperature in decreases Press Display choose function prog 00 ir r Programmode Enter the program number Programmode 2 Lo prog 00 py ik 3 Programmode temp 00 C Enter desired temperature in C ow Programmode 5 time 00 Enter dwell time after ramp 01 98min r cl il 6 time toa j a germe 16 Jetstream Series Operation Enter time to re
12. ing mode DE Jetstream Series Operation 5 3 2 Temperature programming with internal timer The following example shows how to program temperature steps In this example we assign Program 0 to start from let us say 30 C stay for 10 minutes and then increase to 40 C maintain it for 10 minutes and come back to initial temperature of 30 C Press Display Programmode l prog 00 Enter program number 2 0 Programmode prog 00 PFrogrammede 3 temp 00 C Enter desired temperature in C 05 85 C mw Froqram mede 5 time 00 Enter duration in min 01 98min P iode mM imi Qrammode 13 Operation Jetstream Series FProgrammode 6 deltaT 00 no input necessary see pages 17 18 R choose function Input of program 0 is now completed In order to enter the next program step you only need to increase program by one set temperature to 30 C clock to 10 minutes Following this procedure up to 99 temperature profiles can be stored To come back to start temperature increase again next program by one negotiate all entries and for time Time 00 go back to program 0 Sequence will be automatically repeated Time 99 stay at final temperature set with CL 99 Temp 00 stops the temperature program Starting the program In order to start the program press the START key enter the program number 0 and press ENTER sel
13. ment Next the default settings for the leak detector are displayed Actual Settings Leak V 20 The built in solvent leak detector is automatically in function after the instrument has been switched on and attains its full functionality after approx 3 minutes You can adjust the sensitivity with the key of the control unit For more details see 5 2 2 Adjustments Please do take into consideration that the sensitivity alters with temperature You might have to readjust it after having gathered experience As soon as the acoustic alarm is audible the power to the heating cooling element is shut off Whenever you solved your leak problem and you are ready to start again e simply press the key on the control unit the instrument will work as usual For more details see 5 4 Error statements Jetstream Series Operation The actual setting for the T Lock temperature will be displayed next Actual Settings T LOCK OF This feature 15 considered to prevent destruction of temperature sensitive columns caused by handling errors You may want to adjust a maximum temperature the thermostat should not override Whenever this temperature has been reached the power to the heating cooling unit will be switched off and a warning will appear on the display For more details see 5 2 and 5 4 The instrument then continues the self test During this self test please do not hit any key self Test
14. re of the oven should be 20 30 Celsius Equipment to be used Syringe 50 ul 300 ul MEOH Instrument Condition After power on please wait 3 5 minutes before you can go on with the test procedure Instrument at 20 30 C in working condition not Standby mode internal fan on Instrument position vertical front door and all 8 holes with stoppers as shipped model Jetstream Plus closed Injection of MEOH Insert syringe horizontally through stopper on right side close to the bottom Jetstream II Plus or between sealings Jetstream Plus so that the tip of the syringe is approx in center of the inner chamber please do not try to inject directly into leak detection sensor by extreme placement of syringe inject and afterwards close hole with stopper Open the door for 2 minutes between the two test to let remaining Methanol from the first test routine evapour completely Test results 50 ul MEOH no alarm should be triggered 300 ul MEOH alarm should be triggered x Maintenance Jetstream Series If leak detection fails choose function 19 15 7 If the value L is greater than 100 an alarm will be triggered You can adjust the value L eak with the potentiometer on the rear panel Potentio meter But also the setting in section 5 2 1 affects the sensitivity Turn the adjusting knob clockwise with a screwdriver to increase the sensitivity the value in the
15. should only be calibrated by your service agent However you may do it yourself 1f you need values correlating with your temperature measurement The temperature values can be corrected at the following points 05 10 20 30 40 50 60 70 85 C Measure the actual temperature for all those settings and write down the differences to the set temperatures You now have your own correction table which you can enter with the following procedure Enter the following keys 9 Le set value corr D splay 05 gt 0 0 The correction value for 5 C is shown on the display TLOCK If you do not want to change it go to the next value with If you want to change it press Enter your correction value with numerical keys maximum 2 5 C 1 at 85 C you can only correct gt 1 C or 2 5 C Change the sign to minus with to plus with 24 Jetstream Series Example set temperature 05 10 20 30 Display Display e g Maintenance measured temperature correction value 5 1 0 1 10 0 0 0 19 8 0 2 29 6 0 4 set value corr 05 gt 00 set value corr 05 gt 0 1 0 1 by 5 C means the reference value will be decreased by 0 1 C Close the entry with es With scroll downwards with scroll upwards Enter to exit the menu Switch the instrument off for a minute and on again in order to activate the changes Se Installation Protocol Jetstream Series 8 INSTAL
16. witch on the right rear side ON The instrument goes into a self test and displays after satisfactory conclusion of the diagnostic procedure Jetstream Series Installation Open the thermostat door and place the column s into the clips inside the oven Model Jetstream IT Plus In order to install the inlet and outlet tubings to valves injectors detector etc remove the caps on the sidewall of the oven The tubing can now easily be fed through the openings When working in low temperature ranges it is recommended to cut a small hole or slit in the caps and feed the tubing through Model Jetstream Plus Close the door The tubings can be fed between the sealing of the door and the main unit You can now proceed to set the desired temperature profiles with the control unit your thermostat is now ready to use ya Ee a 4 3 Control unit The control unit consists of a 4 x 4 matrix keyboard and a display with 2 lines On the bottom side of the keyboard there 1s a little opening through which you can adjust the contrast of the display with a small screw driver nx AAx oas U u r Operation Jetstream Series 5 OPERATION 5 1 General Settings After you switched on the thermostat on the back panel you can read following message on the display JETSTREAM b1 17 Sser 130213 Whereas the 6 digits number indicates the serial number of your instru
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