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HAZCAT Chemical Identification System - CLU-IN

1. Front of GM Tube Detector Surface alpha alpha k5 beta beta 4 gamma E gamma Read the source directly Cover the source with a sheet of Flip the probe over facing the aluminum back hold the probe within one paper shielding any alpha particles of the probe towards the source effectively inch of the source detecting from reaching the detector surface shielding alpha and beta from the detector alpha betaand gamma QSG 2241 2 v1 1 doc AP2Ce Chemical Warfare Agent Detector __cexeraninrorvanion id National Telephone 954 760 9990 Manufacturer E mail eric damiens proengin com Contact Website http www proengin com NOTE Guides are to be used by trained personnel only DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides The AP2Ce is used to test for the presence of hazardous concentrations of nerve and mustard agents in liquid and vapor forms It 1s designed for use in explosive atmospheres Limitatio
2. Calibration NOTE Prior to performing calibration the instrument must be on and warmed up for approximately 30 minutes The pump must be ON the PID lamp must be ON and the FID must be ignited throughout the warm up period ra Press 2 to enter Setup 7 Press 1 to Calibrate Press 2 to enter span concentration Enter the concentration of the span gas being used 1 Both 2 PID 3 FID Use the A Y keys to select units of measurement ppm ppb and key in numbers using number keypad on unit Press ENTER to accept Press 3 to zero the unit 1 Both 2 PID 3 FID Press 1 to zero both the PID and the FID Connect Zero Gas to probe or use ambient air Press ENTER to start Wait for readings to stabilize and press ENTER to accept and follow the instructions on screen to save values Press 4 Span Press 2 PID apply the appropriate span gas 100 ppm Isobutylene to probe using a clean and labeled Tedlar bag and then press ENTER wait for reading to stabilize and press ENTER to accept Follow the instructions on screen to save values Repeat step 6 amp 7 choosing 3 FID and using 100ppm Methane span gas instead of Isobutylene Press EXIT 2 times to return to the MAIN MENU 10 Press 1 RUN You are now in the SURVEY MODE 11 Press and hold EXIT to stop run and return to the MAIN MENU
3. QSG Model 192 v1 1 doc Ludlum 192 Gamma MicroR Survey Meter QUICK START GUIDE Visually inspect the unit for serviceability and condition Do not use if unit s case shows signs of being broken cracked or damaged without prior approval from the factory Use of a damaged unit may result in inaccurate readings and may cause injury to the user and others Prior to Starting Install two D cell batteries in accordance with polarity marks on underside of battery box lid The battery box is located under the handle on the meter face and is opened by twisting the knob counterclockwise and lifting the compartment door Close and secure door prior to operation Toggle Audio AUD Switch to the ON position This provides an audiable alarm notification when unit detects levels of radiation exposure above the preset limits User may cancel the audio alarm function by placing the toggle switch to the OFF position if necessary Toggle Response F S Switch to either the F or S position The F position indicates fast response between trigger events and meter deflection on the instrument 4 seconds to full scale The S position indicates a slow response between trigger events and meter deflection 22 seconds to full scale S position is used only to get accurate hot spot measurements User should check with the appropriate agency s procedures and policies for switch setting if applicable Rotat
4. Turn Off 1 Press and hold the OFF key until unit turns off With FID versions you must also shut off the hydrogen valve so the tank does not deplete Removing hydrogen tank also reduces chances of hydrogen leaking from tank QSG TVA 1000B PID FID v1 1 doc
5. key to select or deselect sensor an next to the sensor indicates the sensor will be calibrated Hold down Mode key to save and when save is displayed attach calibration gas cylinder to unit using a regulator and calibration adaptor press the appropriate Y or N key to save the values and start the calibration process Follow instructions on screen Disconnect regulator from gas cylinder when calibration is complete QSG MultiRAE v1 1 doc 5 Single Sensor Calibration Note if no gas flow is detected during calibration press Y key to start calibration process If you are using a single gas cylinder at Single Sensor Calibration press Y key use Mode key to select desired sensor Attach calibration gas cylinder to unit using a regulator and calibration adaptor press the Y key and follow instructions on screen Disconnect regulator from gas cylinder when calibration is complete Modify Span Value allows you to change the concentration of the calibration gas Change LEL VOC Span Gas allows you to change the calibration gas from methane LEL and isobutylene VOC Turn Off Press the Mode key for 5 seconds to power down the instrument ALARM LEVEL AND RESPONSE RANGE LOW ALARM HIGH ALARM RESPONSE RANGE 19 5 0 30 volume 10 ppm 0 100 ppm 10 LEL 20 LEL 1 2 000 ppm QSG MultiRAE v1 1 doc RADeCO High Volume
6. Equipment Name Multi Gas Monitor AreaRAE POMSO SP RAE Systems Ine Manufacturer Telephone 877 723 2878 408 752 0723 Contact Fax 408 852 0724 Website www RAEsystems com 680 West Maude Avenue 1 Sunnyvale CA 94086 NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying EOG To detect CO H2S VOCs O2 and combustible gas LEL VOCs as a lump sum Concentration readings may not mean much if compounds are unknown PID Lamps 10 6 eV Installed and 11 7 eV Spare Product Safety Intrinsically safe Battery Rechargeable battery Fully charged in 12 hours Run Time 36 hours on full charge Calibration Gas Four gas calibration a 58 liter 500 psig cylinder containing CO 50 ppm H2S 25 ppm LEL methane 50 O2 19 and balance N2 VOC calibration a 58 liter 500 psig cylinder containing 100 ppm isobutylene and balance air Purchase from manufacturer or distributor QSG AreaRAE v1 1 Multi Gas Moni
7. Features p lt QUICK OPERATIONS GUIDE Using the connection cable connect the probe to the unit Do not force the plug into place Power on the SAM 935 by pressing the ON OFF Button behind the sliding door in the upper left corner of the instrument Allow the instrument to perform self test and stabilize the Nal detector This self test takes about 5 minutes to perform Do not interrupt the sequence by shutting the unit off or aborting the startup do not press OK F2 button The initial screen will display the date time pass or fail the self test along with the status of the battery Internal Nal Internal He3 System memory and Spectrum Memory The SAM possesses an internal Cs 137 source that usually allows it to calibrate itself during startup In some circumstances the SAM may prompt the user for a gross calibration using an external Cs 137 source Ifa gross calibration is required see below if not proceed to the Dose Rate section below Once prompted to begin calibration press the F3 Button ADJUST to perform the calibration Follow on screen instructions to place the Cs137 check source on detector and press F2 Button OK After the calibration spectrum is captured the unit will beep twice and prompt the operator to take a background spectrum The Screen will display wait time 1 min Remove the Cs137 check source and press the F2 Button BKG and allow the unit to acquire the background spectrum The screen
8. 501 Oak Street Sweetwater Texas 79556 National Telephone 800 622 0828 toll free 325 235 5494 office 325 235 4672 FAX Manufacturer E mail ludlum ludlums com Contact Website http www ludlums com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded A in a logbook Additional product information may be found in the B G N Switch N accompanying Equipment Operating Guides GM Detector Neutron Detector SPECIFICATIONS Limitations Cannot monitor for a and n radiation simultaneously detector change required y radiation can be monitored with either detector To calculate dose the instrument reading duration of exposure and target must be considered Instrument reading is NOT equivalent to dose Response Range 0 500 000 Counts Minute Alarm Level No alarm Audible click frequency relative to the rate of incoming pulses when AUD switch in ON position Product Safety Not intrinsically safe Battery Two D cell alkaline batteries Typical battery life is 600
9. Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Provides real time measurements ug m level of mercury vapor in the air Limitations 1 Can easily saturate the detector requiring a regeneration procedure to be performed 2 Can not achieve the detection limit recommended for residential occupancy 0 0003 mg m 3 Interferences from high humidity temperature variation household cleaners and smoke 4 Old oxidized mercury used for functional test may give inaccurate results Response 0 003 mg m 0 999 mg m Range Alarm Level If sensor completely saturated display shows 8 8 8 sensor regeneration is required to operate Product Safety Caution designed for vapor use only DO not allow probe or intake to contact liquids dust or foreign material Not intrinsically safe Battery To prevent a memory effect from occurring in the nickel cadmium battery resulting in a decreased usable battery capacity follow these steps 1 At least once a month wait until LO BAT appears before recharging 2 Charge the battery as soon as LO BAT appears 3 Complete battery recharging takes 14 hours 4 A fully charged battery can operate for a minimum of 6 hours Calibration Factory calibration required Perform mercury functional test to check calibration of the instrument Additional Functional test should be performed monthly Refer to the manual for the test procedure
10. Gamma and x ray 50 KeV to 6 MeV G nerve 15 ppb 30 seconds Dose H pio 0 1 mrem to 1 000 mrem H blister 300 ppb 15 seconds Dose rate 1 mrem hr to 100 rem hr L 200 ppb 15 seconds Response lt 5 seconds Detection time is 10sec at higher concentrations Alarm Level See above detection level section Product Safety Not intrinsically safe Instrument contains a 10 millicurie Nickel 63 radioactive source DO NOT SHIP THIS INSTRUMENT WITHOUT PROPER SHIPPING PAPERS AND A COPY OF THE MOST RECENT WIPE TEST Battery Six alkaline or rechargeable C batteries Under normal conditions the batteries will last up to 7 hours In cold weather the batteries may only last up to 1 hour Calibration Gas N A Instrument is self calibrating can be checked with a confidence test QSG APD2000 v1 1 doc APD 2000 QUICK START GUIDE Prior to Install 6 C batteries into the handle of the instrument Starting 2 Unscrew black protective cap from barrel of instrument and store it on battery cap retainer located on the bottom of the handle DO NOT touch the APD 2000 nozzle or the filtered nozzle standoff 2 Remove filtered nozzle standoff package from transit case Peel covering from package until one filter is exposed Press nozzle into exposed filter by using the filter cap holder DO NOT TOUCH FILTER Pare WITH YOUR PE E E E E ET A 5 Lay clear Lay clear plastic covering back in place over the foa
11. Manufacturer Ohio Lumex Company National Telephone 888 876 261 1 Manufacturer E mail mail ohiolumex com Contact Website http www ohiolumex com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Provides portable real time measurements of mercury vapor in ambient air natural and stack gases Attachments allow analysis of water and complex matrices Limitations 1 Temperature sensitive needs time to stabilize 2 Dusty environments and moisture high humidity effect accuracy by absorbing moisture 3 Fragile Strong vibrations and shocks in use and transit effect accuracy 4 Battery lifespan Response Range In Air 2 ng m In Water 0 5 ng L In Soil 0 5 mg kg Alarm Level Alarm warning in Sm mode indicates mercury readings above present high limit Product Safety Not Intrinsically Safe Battery Rechargeable Ni Ca Battery Complete battery rech
12. and press the ENTER key Select DELETE LOGGED DATA and press the ENTER key Press the NEXT key to view more data You have the option to DELETE TAG DATA or DELETE ALL DATA Use the A V to select appropriate option and press the ENTER key and following instructions on the screen Press the EXIT key to return to the MAIN MENU If deploying repeatedly at the same locations at the same site follow steps 2 3 and 7 and deploy appropriately labeled instruments Note Record the data on the screen in the logbook including concentration TWA and Run Time This data is not again readily available Shut Down To Power Off the DR 4000 press and hold the On Off key for 2 seconds follow instructions on the screen QSG DataRAM v1 1 doc MIE DataRAM 4 Model DR 4000 HH TETIT i Bi al tal Plastic filter holder i N IA AAN N POH i HEE f w Al me HE daim le DR TCH Plastic Plug m aeee TT r eS eaoat eta ETE tata ET ERETTE PaPa aT ST ll a a O T i i e Exhaust Figure 2 DataRAM Figure 1 QSG DataRAM v1 1 doc Drager Chip Measuring System CMS National Telephone 800 615 5503 Manufacturer E mail rodinfo draeger net Contact Website http www draeger com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides wer
13. Air Sampler GENERAL INFORMATION Equipment Name RADeCO High Volume Air Sampler Air Volume Totalizer H 810 RADeCO LLC National Telephone 860 823 1220 Manufacturer E mail techsupport radeco com Contact Website http www radecollc com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS The Model H 810 sampler is a grab sampler with an air volume totalizer will automatically shut off the unit when a specified volume of air has been sampled This microprocessor based unit is designed to eliminate the use of rotameters and mechanical time meters The air volume totalizer portion of the sampler is composed of an enclosed air turbine that rotates at speeds proportional to the air flow velocity of the sampled air The flow rate total volume and elapsed time are displayed on the liquid crystal display LCD screen Limitations Accuracy is limited to 5 percent Re
14. If the sample is showing greater then normal background levels consult a radiological expert regarding further tests and or refer to organization s radiation procedures If the sample is showing greater then 300 cpm counts per minute probable gamma source EVACUATE Evaporation An important safety screening observation test do not skip Test Quickly evaporating liquids can be dangerous because of potential fire and inhalation hazards Interferences Results depend on wind temperature and humidity Liquids evaporate more rapidly on dry warm days This test should be performed in an area out of the wind and away from direct sunlight 1 Add the unknown liquid to a watch glass to form a pool the size of a dime 2 Observations a Evaporates quickly no residue Volatile substance indicated A fire and or inhalation hazard 1s present b Evaporates quickly leaves a residue Mixture indicated I Liquid residue Liquid mixed with oil solvent or water indicated II Waxy residue Organic solid dissolved in an organic liquid indicated III Fine crystals or powders Inorganic salt in liquid indicated If testing the liquid does not reveal its identity continue testing this substance as a solid unknown Refer to HazCat Chemical Identification User s Manual to continue with testing QSG HAZCAT v1 1 doc HAZCAT Chemical Identification System Oxidizers Acid The oxidizer acid test is designed to screen out strong oxidizers and wa
15. LCD should indicate BATT OK if not recharge battery Press Flow and Battery Check to place the pump in Hold Connect the flow meter BIOS Calibrator to the intake of the sampling medium press Flow and Battery Check and set the flow rate by turning the flow adjust screw Low flow rate calibration Connect the 1 4 inch Tygon tube low flow holder and sorbent tube with the arrow pointing towards rubber sleeve Start the pump using the on off switch and press the Start Hold button press the Flow and Battery Check Adjust the flow by turning the flow adjust screw until build in rotameter reads 1 5 L min Connect the flow meter to the exposed end of the sorbent tube Connect the flow meter BIOS Calibrator to the intake of the sampling medium press Flow and Battery Check and set the flow rate by turning the flow adjust screw Additional Built in pressure regulator allows user to take up to 4 simultaneous tubes at different Operational flow rates using optional adjustable flow holder Intrinsically safe Information QSG SKC v1 1 doc SKC UNIVERSAL SAMPLER PUMP QUICK START GUIDE up i Charge the batteries by connecting the charger plug to the sampler charging jack Start Flow On Off Re tas Set the flow rate High flow application Set the high flow rate by turning the regulator screw clockwise until it stops Adjust the flow by turning the flow adjust screw until build in rotameter reads 1 5 L min Start the pump using t
16. Response Switch is in the F position Expose the detector to a radiation check source a B Cs137 Proportional audible clicking should be heard with the AUD Switch in the ON position At this range setting meter deflection may not be apparent Press the High Voltage HV Button The meter should read approximately 900 1000 volts Rotate the Range Switch to the lower scales X10 or X1 until a meter reading is indicated Vary the distance between the check source and the detector while watching the deflection speed of the meter Now toggle Response Switch to the S position while varying the distance to the check source and note that the meter deflection is slower in this position Return the F S Switch to the F position Press the Reset RES Button in the vicinity of the check source and ensure the meter goes to zero Neutron Detector y and n radiation l aia Rotate the Range Switch from OFF to X1000 Ensure Radiation Selector Switch is in the N position the Audio Switch is in the ON position and the Response Switch is in the F position Press the High Voltage Button The meter should read approximately 1500 volts Expose detector to a neutron check source n Note audible clicking and adjust Range Switch until deflection registers on the meter QSG Ludlum15 v1 1 doc 4 Toggle Radiation Selector Switch to B G position Expose detector to a gamma check source Cs137 Note audible clicking and adjust Range Swit
17. SPM Tape Gas Monitor GENERAL INFORMATION SPM Chemical Tape Monitor MDA Scientific Zellweger Analytics Honeywell Analytics National Telephone 847 634 2840 Manufacturer Website http www honeywellanalytics com Contact NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations Itis recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Sampling and recording of concentrations of various airborne chemicals see manufacturer s data for analyte listing Monitoring is possible for 15 or 30 days depending on tape used 1 Requires use of chemical specific tape which have limited shelf life and ChemKeys 3 Requires 120 volt power and weather protection for extended use 4 Gas to be monitored must be known so appropriate tape and key can be installed 5 Some tapes require refrigeration or freezer storage and are light sensitive 6 Heavy bulky and shock sensitive Response Range Varies by chemical monito
18. Tray Locking Knob to UNLATCHED position and remove the sample Store sample in proper storage container until the sample can be properly shipped and or disposed of 5 Decontaminate the tray with a DI moistened KimWipe throw wipe in a marked Radioactive Waste container Close the Sample Tray rotate the Tray Locking Knob to LATCHED and press the COUNT Button The unit should register no activity above background levels Ifthe Sample Tray is still contaminated repeat this process until background activity is achieved Turn Off Push the power switch to the OFF position QSG Model 3030 v1 1 doc MultiRAE Plus GENERAL INFORMATION Equipment Name Model Manufacturer National Manufacturer Contact Gas Inlet and Filter Liquid Crystal Display LCD N Programming Keys Light LED Alarm amp Charge Status Limitations Response Range MultiRAE Plus PGM 50 RAE Systems Inc Telephone 877 723 2878 E mail tech raesystems com Website http www raesystems com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by a field personnel for utilization by EPA and their 3 contractors and are helpful in quick start up and ib citi aul operations Various limitations have been identified through the experience of the development group RS 232 Port for PC a Ze Different makes models and updates to this equipm
19. Water Attachment Water Analysis Calibration Maximum EA aaa After injecting the blank wait 50 90 seconds then press End in integration window Data acquired will be entered in the table automatically 3 Double click the description field for entry number 2 Select Standard the cursor will be present after Std_ at this point type in the standard concentration in parts per billion ppb or parts per trillion ppt The concentration is from the standard that was made in the Start Up section do a three point calibration curve Use 1 ml of standard solution which is 1000uUg of actual mercury Enter 1000 after Std_ 1000 Enter 1 ml in the V ml column Then Press the START button on the integration window D a a a a a ee ee a Immediately introduce the standard in Impinger 1 Click the End button in the Integration window when the signal returns to the baseline after about 90 120 seconds Repeat steps 3 amp 4 with 2 0 and 3 0 ml standard sizes to establish multipoint calibration You can do as many duplicates as required to increase accuracy and precision SE Click the Table button on the Program toolbar and click the Select button Click Row number then hold down the Shift and press the down arrow or Ctrl and mouse to highlight the Blank and all the Standards rows Note Only Blank and Standard rows should be selected for calibration curve On the Calculation toolbar click on the Cal Graph button The Grap
20. and Operational acceptable range of readings Information QSG Jerome v1 1 doc Jerome Mercury Vapor Analyzer MVA QUICK START GUIDE Start up Turn unit on by pressing ON button and waiting minute for warm up Display will flash 000 when ready This procedure must be completed at the beginning of sampling end of sampling and if the sensor is saturated Press SAMPLE to take the reading Note the saturation bars displayed If 8 8 8 is present proceed with the sensor regeneration procedure If regeneration is required wait 10 minutes to zero the unit Start sensor regeneration by pressing the REGEN button HHH will flash on the screen while sensor regeneration is in progress When finished screen will flash 000 to indicate it is ready for sampling Attach inlet probe if point source monitoring is desired The instrument has two modes Sample Mode Push SAMPLE button and take 12 second reading in mg m Survey Mode Push and hold SAMPLE button and take one 12 second reading followed by repeated readings every 3 seconds decreased sample volume effects accuracy by 20 NEVER ZERO THE INSTRUMENT UNTIL THE ABOVE TURN ON PROCEDURE IS COMPLETED NEVER ZERO THE INSTRUMENT BETWEEN SAMPLES Ideally wait for 30 minutes after the Turn On procedure is completed In an emergency situation you may zero the instrument immediately following the Turn On procedure
21. are helpful in quick start up and pe operations Various limitations have been smsow Identified through the experience of the reve development group Different makes models nooeecron and updates to this equipment may change the eo limit ations It is recommended that calib ration maintenance and use be recorded in a logbook Additional product inform ation may be found in the accompanying Equipment Operating Guide ELECTRIC AND PNEUMATIC CABLES FROM SAMPLE PROBE CONNECT HERE HYDROGEN GAS TANK WITH INTEGRAL GAUGE aN af A g kea F lt A S Pi a p ae s PAL i 5 ae Environmental Instruments a a BB k tas KEYPAD AND DISPLAY SHOULDER STRAP Se ee eae MWN O O Q Q aa mman peze INTERFACE OUT CHRG HOST SPECIFICATIONS The TVA 1000 Toxic Vapor Analyzer shown above is an organic inorganic vapor monitor for the gas survey industry This analyzer uses either a flame ionization detector FID a photo ionization detector PID or both The vapor concentration may be read immediately on either of two displays one mounted directly on the hand held sample probe and the other on the instrument sidepack itself Vapor concentration can be displayed on both displays in either parts per million ppm parts per billion ppb or percent concentration Limitations The FID requires gt 16 oxygen to maintain the h
22. developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and ai Operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment wensrameann may change the limitations It is recommended that m on lis quvtetvetmak prema calibration maintenance and use be recorded in a sigma standard deviations above Continuously displays identified isotopes and updated each second MCA performs background category isotope specific dose rate and analysis on present or stored alarms and neutron count prepares a multipage report for printing or email Monitor Mode Real Time Surveillance Detail MCA SAM 935 m 15Jan 03 SAM 955 logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Limitations To provide field surveillance and measurement of multiple radioactive nuclides by identifying signature y radiation energies by spectrometry and matching them to a database of nuclide energies in the unit s memory thereby identifying the isotopes present Cannot identify a or B emitting isotopes but will identify y emitting daughter products The SAM may not work at temperatures below 40 F Quick changes in temperature can adversely affect SAM readings The neutron detector must be purchased to detect special
23. experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guide S4PE Surface Sampler and Associated Sampling Tips and Nozzles SPECIFICATIONS The S4PE is used for sampling liquids or solids to allow the AP2C to analyze for the presence of hazardous concentrations of nerve and mustard agents in liquid and vapor forms Limitations Only detects HD sulfurated blister agents and GA GB and VX phosphated nerve agents May give false response in an enclosed space such as a maintenance shop or engine test bay downwind from or in dense smoke and fumes Some of the vapors that may give a false response are wintergreen peppermints menthol cigarettes cough lozenges and smoke The AP2Ce will not detect nitrogen mustard Lewisite or irritants The AP2Ce has not been tested against industrial or household chemicals found in the civilian environment The instrument will not work properly above 10 000 feet in elevation or in Oxygen levels below 19 The AP2Ce will operate between 10 C and 55 C The AP2Ce requires the use of proprietary batteries and proprietary hydrogen cells The batteries and hydrogen cells will have to be shipped by air as dangerous goods Detection Limits Based on AP2C Vapors Aerosols and Dro
24. gasses see sec 4 10 in manual for more info Insert sample tubing into sample inlet fitting fig 1 15 24 do not over tighten Connect any auxiliary devices Installation of Chemcassette Tape Open tape load lever fig 1 18 if unit is on the green system status LED will flash slowly Remove center retaining screw and remove old Chemcassette fig 1 4 if present Install new Chemcassette make sure chemical tape is not expired with raised lettering facing up Pull 12 of tape off new cassette and place end in take up reel cover fig 1 27 Thread tape through detector head capstan assembly and over the guide posts fig 1 7 17 25 26 and install the take up reel cover Rotate take up reel to remove slack and re install retaining screw in center of Chemcassette tape Close the tape load lever if unit is on monitoring will begin automatically and green LED fig 1 9 will be lit Running Unit Turn on main power fig 1 8 and check display fig 1 19 to verify Gas Type Alarm Levels and Chemcassette Type Leak test unit by plugging end of sample line A FAULT 17 message will be displayed indicating that there are no leaks between the sampling point and SPM Press ALARM RESET key to reset pump Unit will go into sampling mode automatically following leak test as indicated by green LED The unit may be turned off at any time Remove Chemcassette and dou
25. hours Battery condition can be checked on the meter Calibration Calibration performed annually by manufacturer Periodical bump test using a check source provided by the manufacturer is recommended Do not use if calibration is out of date unknown or not available Shipping Special shipping requirements may be necessary if check source is attached to instrument See Instructions dangerous goods shipping manual for further instructions Call manufacturer for complete instructions and requirements for shipping unit back to factory Refer to the appropriate DOT requirements for shipping and handling of dangerous materials when shipping QSG Ludlum15 v1 1 doc Ludlum Model 15 Neutron Counter QUICK START GUIDE Prior to Starting Visually inspect unit and accessories Check module wires probe s and other accessories Do not attempt to substitute probes from like units Probes are calibrated to the unit Changing probes may result in incorrect readings Make sure the end cap 1s on the probe If missing check the mylar screen for damage Do not use if probe and or unit is damaged Install two D cell batteries in accordance with polarity marks on underside of battery box lid The battery box is located under the handle on the meter face and is opened by twisting the knob counterclockwise Close lid and secure Connect the appropriate probe to the module using the connection cable Position the B G N toggle to the appropriate
26. in this mode is identical to Standard Non LEAP analysis Tests can be started or stopped either by pulling the trigger or by tapping the Start Stop button on the iPAQ screen The results screen for a test will show results for all elements analyzed with the LEAP mode ie Inno Analysis af 4 56 q 9 53 Reading 2 19 Aug 2003 Soil Mode Detected ppm 25 ppu Ba 852 319 ppm 277 ppl Cr 110 Mn 614 Fe se1y Not Detected ppm 5 el Innoy Results Soil Mode Factory Test in progress 25 seconds g27 163 t 2236 r 9349 r 413 ppu Light Element Analysis Mode End Condition Maximum Time File Edit Yiew Options Help Back vext Start RRS File Edit iew E Test in progress screen LEAP Only Live Updates on Results Screen Showing LEAP results 5S 7 Innov X User Manual Version 2 1 If Sequential testing is selected Fl Innov Analysis n 4 57 the words Sequential Current Test Standard will appear above the currently selected End Soil Mode Factory Test in progress 20 seconds Condition When a test is started Fe 9144 402 ppm the instrument will appear to fe e fs Bi Gaye operate in the same manner as a Rb BG 13 ppu Standard test H if the test 3 D ae ee andard test However if the tes ar ose 0 See sta sen ends according to the specified Ag 506 66 ppm d di l di Ti 5043 ppm end condition excluding Ba lt 2743 ppm Manual the
27. is reported on the y axis on the right of the graph The proper value must be 15000 arb units or higher Sterilize and clean the sample boats by inserting them into the oven for 30 seconds and then let them cool r Press on the Baseline Check button on the Control toolbar Wait 10 seconds and then click the button again to establish the baseline N Maximum Press cursor on the Table window brings up Complex analysis table Enter the test site information in the top blank window Press on the Description field and double click left mouse button The windows with Blank and Standard selection will pop up Select Blank and press on Tab key Press Start in the Integration window then insert an EMPTY boat in the oven Maximum peso Wait approximately 30 seconds then press End and remove the boat Data will be entered in the table automatically QSG Lumex Soil Attachment v1 1 doc Lumex Mercury Vapor Analyzer MVA Soil Attachment Soil Analysis Calibration Double click the description field for entry number 2 Select Standard and the cursor will be present after Std__ at this point type in the standard concentration in parts per billion ppb or ug kg with the standard that is labeled NIST 2709 1 4 ppm and do a three point calibration curve Enter 1400 after Std 1400 Enter 10 mg in the M column and press the tab key Then Press the START button on the integration window Place
28. keying EXIT Confirm the run termination by keying ENTER The DataRAM 4 performs a purging operation for about 1 minute after terminating a run VIEWING DATA ON SCREEN To access stored data select the VIEW TRANSFER DATA line on the MAIN MENU and press the ENTER key Select VIEW LOGGED DATA and press the ENTER key Press the NEXT key to view more data After reviewing the appropriate data key EXIT key twice to return to the MAIN MENU TRANSFERING DATA TO A PC Attach the RS 232 cord to the rear of the DataRAM DR 4000 and the other end to the communications port COMPORT on your computer DataRam 4 software should also be running From the software window click the Data Text tab and then click the Get new data icon located in the top left hand corner right below the Main tab To download data to a PC select the VIEW TRANSFER DATA line on the MAIN MENU and press the ENTER key Select TRANSFER TEXT FILE and press the ENTER Software should communicate with DataRam and download logged data Following the downloading of data you can use the various options on the accompanying software to create tables graphs etc to present the data After completing the successful download of data press the EXIT key to return to the MAIN MENU DELETING LOGGED DATA To delete logged data select the VIEW TRANSFER DATA line on the MAIN MENU
29. manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Suitable for a broad range of applications in air monitoring including industrial hygiene studies and environmental testing Limitations Time consuming sampling procedure Automatic fault shutdown due to excessive restricted flow or low batteries voltage may cause that collected on sampling media air volume is less than require for analytical method Temperature of operation 20 C 45 C 4 F 1 13 F Battery 6 0 V plug in Ni Cad rechargeable batteries Fully charged batteries allow pump operation for approximately 8 hours It is important to charge the batteries before sampling using the SKC approved charger Calibration High flow rate calibration Connect the 1 4 inch Tygon tubing with the sampling medium to the pump intake Start the pump using the on off switch and press the Start Hold button press the Flow and Battery Check Adjust the flow using the flow adjust screw until the build in rotameter reads 2 L min The
30. nuclear material When in manual mode and user deletes data using the F3 key no warning is given prior to deletion The SAM will give an inaccurate reading while experiencing high level of stimulation Response Range 0 01 uR hr 99 0 R hr Alarm Level Adjustable alarm levels for both dose and dose rate Beep and illuminated alarm light upon exceeding alarm threshold Adjustable spectrum capture trigger criteria for isotopes Product Safety Intrinsically safe Battery Calibration Additional Operating Information Internal trickle charged battery with a battery life of approximately 8 hours The battery should be charged once a month May be run off of direct power using the supplied adapter Fine calibration performed annually by manufacturer It is the responsibility of the user to ensure the calibration service documentation is present or available Do not use unit if calibration documentation is missing unknown or out of date Selecting specific isotopes from the library to monitor 1 Press UTIL button select Area Monitor Set up select triggers 2 Scroll to unused select F2 isotope 3 Scroll to isotope you wish to monitor and press Enter Press F1 to return to Dose Rate Screen QSG SAM935 with Update v1 1 doc SAM 935 Gamma Spectrometer and Radiation Survey Meter Turn On Gross Calibration Dose Rate Detail Reviewing and Printing Alarms Turn Off Advanced
31. spatula add 4 of a pea size amount to the watch glass Heat the explosive test tool tip until it glows red Roll tip into unknown observe reactions Place explosive tool tip sample is on tip into torch flame observe reaction Observations flashes detonates or ignites violently positive Stop testing and follow agency protocol burns with or without flame negative Stop go to HazCat Chemical Identification User s Manual to continue testing burns with sparks negative Stop go to HazCat Chemical Identification User s Manual to continue testing smokes negative Stop go to HazCat Chemical Identification User s Manual to continue testing no reaction negative Continue to HazCat Chemical Identification User s Manual to continue testing QSG HAZCAT v1 1 doc Jerome Mercury Vapor Analyzer MVA Manufacturer Telephone 800 528 7411 Contact E mail support azic com Website http www azic com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook
32. the gamma spectrum building This will allow the operator to verify the existence of distinguishing peaks during alarms When the alarm is triggered press the F3 Button CAPTURE to manually capture a spectrum of the incoming gamma energies The unit will automatically store all alarm conditions so this procedure 1s not required to collect and store this alarm data In any operating mode pressing the Right Left Arrow will allow cycle through all stored and captured alarms If the SAM is connected to the printer via the serial port during this review of the stored alarms pressing the F3 Button PRN SEL will print the stored data for analysis Pressing the F4 Button MCA will allow you to match stored spectra against the isotope library signature peaks User may print using the supplied printer and cable to print the results Ensure unit in Dose Rate or Sigma Mode press the ON OFF Button Unit will power down and all data will be saved For more thorough discussion of the advanced features of this instrument such as the Manual Multi Channel Analysis MCA please see the EOG Additional functions and operations can also be found in the user s manual QSG SAM935 with Update v1 1 doc SKC Universal Sampler Pump Manufacturer Telephone 800 752 8472 Contact E mail skctech skcinc com Website http www skcinc com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical
33. will display a wait time of 1 minute Once complete the unit will enter and display the Surveillance Mode Unit is now ready for operation In the Dose Rate Mode a continuously monitored dose rate will be displayed a cumulative dose is shown and the unit will analyze for possible isotopic contributions to the overall dose rate When any preset triggers are exceeded the unit will automatically save and report the alarm condition When the unit reports an alarm condition the suspect isotope 1 e Cs137 Tc99m will be listed on the screen with its contribution to the total dose rate If the isotope cannot be matched to the library spectrum Unidentified will be displayed with its contribution to dose rate In Dose Rate Mode press the F1 Button Sigma to see the bar graphs of each enabled isotope in the library The bar graphs show detector response above background in number of sigma standard deviations above background for the listed isotopic signature peak gamma energies An isotope must be in the trigger list to appear during a search The components of the trigger lists are available for examination in the Utilities menu When in Sigma Mode and the preset triggers are exceeded the isotope bar will begin flashing and the word ALARM will be shown with the sigma value This data and the spectra will be stored in memory Note that alarms are stored until manually deleted by the user In Sigma Mode press the F1 Button DETAIL to watch
34. y emitting daughter products The SAM may not work at temperatures below 40 F Quick changes in temperature can adversely affect SAM readings It is important to calibrate the instrument using quick calibration The neutron detector must be purchased to detect special nuclear material When in manual mode and user deletes data using the F3 key no warning is given prior to deletion The SAM will give an inaccurate reading while experiencing high level of stimulation 0 01 uR hr 99 0 R hr Adjustable alarm levels for both dose and dose rate Beep and illuminated alarm light upon exceeding alarm threshold Adjustable spectrum capture trigger criteria for isotopes Intrinsically safe Internal trickle charged battery with a battery life of approximately 8 hours The battery should be charged once a month May be run off of direct power using the supplied adapter Fine calibration performed annually by manufacturer Gross calibration required and background spectrum capture required prior to every use and periodically during use It is the responsibility of the user to ensure the calibration service documentation is present or available Do not use unit if calibration documentation is missing unknown or out of date Selecting specific isotopes from the library to monitor 1 Press UTIL button select Area Monitor Set up select triggers 2 Scroll to unused select F2 isotope 3 Scroll to isotope you wish to monitor and pres
35. 2 v1 1 doc Ludlum 192 Gamma MicroR Survey Meter Zero 1 Zero of the unit should be done at the factory Never attempt to zero the scale unless authorized by the factory to do so Changing the zero settings may alter the unit s readings Turn Off 1 Rotate the Range Switch to the OFF position and remove the batteries Make sure the unit if contaminated has been cleaned before returning to its storage container or shelf l Calibration Calibration is performed annually by the manufacturer Prior to use the user should verify the calibration and service sheets are present and or readily available The user should not use the unit if the calibration is out of date not available or is unknown QSG Model 192 v1 1 doc Ludlum Model 3030 A B GENERAL INFORMATION Equipment Name Model 3030 Alpha Beta Sample Counter 3030 Manufacturer Ludlum Measurements Inc 501 Oak Street Sweetwater Texas 79556 National Telephone 800 622 0828 toll free 325 235 5494 office 325 235 4672 FAX Manufacturer E mail ludlum ludlums com Contact Website http www ludlums com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experienc
36. 5 minutes for temperature gt 0 C lt 10 C About 20 minutes for temperatures lt 0 C When the AP2C is operational green READY light flashing insert and hold the nose of the S4PE in the sampling pipe of the AP2C keep the S4PE perpendicular to the AP2C 7 Apply continuous pressure about 15 to 20 sec To the push button of the S4PE to control the heating of the TEST scraper The red light of the S4PE comes on The lights G V HD V of the display unit should come on From detection stop pressure to the push button of the S4PE to avoid the AP2C saturation e a oe Field Calibration AP2Ce must be checked with a confidence test before each use Turn Off Environment must be clean with no alarms Ifthe unit is alarming wait for it to clear Uncouple the sampling pipe from the front of the AP2C 3 Turn the hydrogen cartridge to the left and line up the white mark opposite the OFF index green READY light and display window lights go out Decontaminate if necessary Extract the hydrogen cartridge Stow the cartridge in the case 5 Extract the battery slide unit from the body of the AP2C Remove the battery block from the slide unit and place it in its housing in the case Latch the empty battery slide unit in the body of the AP2C EPA National Equipment List 03 04 A ERTG Quick Start Guide Version 1 0 February 7 2008 APD 2000 National Telephone 888 473 6747 Man
37. AP2C with sampling pipe and Equip S4PE with a TEST SCRAPER BLUE When the AP2C is operational green READY light flashing insert and hold the nose of the S4PE in the sampling pipe of the AP2C keep the S4PE perpendicular to the AP2C Apply continuous pressure about 15 to 20 sec To the push button of the S4PE to control the heating of the TEST scraper The red light of the S4PE comes on The lights G V HD V of the display unit should come on From detection stop pressure to the push button of the S4PE to avoid the AP2C saturation N Not applicable Calibration Field Calibration Not Required this attachment used to perform confidence test for the AP2C P each use Turn Off 1 The nose of the AP2C nozzle or sampling pipe are uncoupled by pulling them directly apart During storage the gas sampling nozzle is in place on the nose of the AP2C To eject a scraper from the S4PE push the nose of the S4PE towards the scraper QSG S4PE v1 1 doc SAM 935 Gamma Spectrometer and Radiation Survey Meter GENERAL INFORMATION Equipment Name Isotopic Surveillance amp Measurement System y Spectrometer SAM 935 Original Software and Hardware Firmware Version 02 11 01 Berkeley Nucleonics Corporation 2955 Kerner Blvd Suite D San Rafael CA 94901 National Manufacturer Contact Telephone 800 234 7858 415 453 9955 415 453 9956 fax E mail bernadette murphy berkeleynucleonics com W
38. Chapter 5 Soil Analysis The Innov X analyzer can be used to analyze in situ directly on the ground bagged or prepared soil samples A guide to Soil analysis using field portable X ray fluorescence is found in the appendix This document summarizes EPA Method 6200 which is the standard protocol for field screening It also provides information on prepared sample testing 5 0 CHECK STANDARDS It is recommended that a check standard is measured after each standardization and periodically throughout the day Innov X provides several NIST certified standards for verification The certified values for these samples are provided in the appendix At least one standard should be measured for a minimum of 1 minute Elemental concentrations for elements of interest plus or minus the error on the reading should be within 20 of the standard value The Field screening guide in the appendix describes in more detail recommended quality assurance considerations The standards provided with the XRF analyzer are contained in XRF sample cups with a Mylar window through which the soil can be viewed on one side and a solid cap on the other side Samples should be measured in the sample cup through the Mylar window The best way to measure a prepared sample is using the test stand If this is not available the sample may be placed on the ground and the analyzer may be pointed downwards in full contact with the soil cup Do not hold the soil cup in your hand while
39. F3 Button CAPTURE to manually capture a spectrum of the incoming gamma energies The unit will automatically store all alarm conditions so this procedure is not required to collect and store this alarm data Reviewing and Printing Alarms Turn Off Advanced In any operating mode pressing the Right Left Arrow will allow cycle through all stored and captured alarms If the SAM is connected to the printer via the serial port during this review of the stored alarms pressing the F3 Button PRN SEL will print the stored data for analysis Pressing the F4 Button MCA will allow you to match stored spectra against the isotope library signature peaks User may print using the supplied printer and cable to print the results p lt Ensure unit in Surveillance or Monitor Mode press the ON OFF Button Unit will power down and all data will be saved For more thorough discussion of the advanced features of this instrument such as the Manual Multi Channel Analysis MCA please see the EOG Additional functions and operations can also be found in the user s manual Features QSG SAM935 v1 1 doc National Manufacturer Contact Telephone 800 234 7858 415 453 9955 415 453 9956 fax E mail bernadette murphy berkeleynucleonics com Website http www berkeleynucleonics com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were
40. Level Product Not intrinsically safe Safety Battery Two alkaline D Batteries or Ni Cd rechargeable batteries June 18 2009 US EPA Quick Start Guide QUICK OPERATIONS GUIDE Prior to l Check calibration date Starting Start up l Turn the unit on by turning the range selector knob to the lowest scale 0 1 TEST If it does not replace the batteries before proceeding Move the AUD switch to on and verify the detector noise arson E S e Pactaraianes Press the RES reset button and confirm that the meter pointer returns to the zero position ae ra Record background readings before proceeding to the survey area If a source of known intensity is available an instrument performance or confidence check may be performed Expose the instrument to the known source and observe the reading Move the F S switch to verify the reading in both fast and slow response modes Compare the readings with the known source intensity a reading of or 20 of the known source intensity is acceptable zero Press the RES reset button and confirm that the meter pointer returns to the zero position Calibration m Not applicable yearly manufacturer calibration Turn Off a Turn the range selector knob to the off position Pa The batteries should never be stored in the instrument for more than 30 days Press the BAT button The display pointer should move to the area of the display marked BAT Front of G
41. M Tube Detector Surface y a alpha P a alpha alpha g oS ee d i i l beta beta SS re lt r beta C es a gamma l gamma l Sa ee a 1 gamma Sa eel l l y Read the source directly Cover the source witha sheet of Flip the probe over facing the aluminum back hold the probe within one paper shielding any alpha particles of the probe towards the source effectively inch of the source detecting from reaching the detector surface shielding alpha and beta from the detector alpha beta and gamma June 18 2009 US EPA Quick Start Guide TecnTiPs The latest from Photovac Volume 3 Number 1 st MicroFID Flame Ionization Detector Operational Reference Guide INTRODUCTION This TechTIP is a reference guide for day to day operation of the MicroFID Flame Ionization Detector For more detailed information please refer to the MicroFID User s Manual The MicroFID measures the concentration of airborne Volatile Organic Compounds VOCs displays and then records these concentrations It does not distinguish between individual compounds The reading represents the total concentration of all VOCs present in the sample MicroFID will display concentration in PPM TUTOR KEY To assist you in learning the key functions MicroFID has a built in tutorial session that displays a two line description of the function o
42. Mustard See specific tube for details Alarm Level This test kit does not have any alarms If positive results EVACUATE IMMEDIATELY Product Safety Be wary of shards of glass from broken tips Calibration No calibration is necessary Additional All five tubes of one set I or V are tested simultaneously Operational Flush the pump with fresh air after each use to clear out any remaining vapors Information Be sure to compress the pump the number of times specified in the tube directions QSG CDS Kit v1 1 doc QUICK START GUIDE Prior to Perform leak test on bellow pump Starting 2 Reset pump counter to zero Start up Scrape the ceramic edge of the Simultest Set Opener at the tip of the tubes multiple times to score the Assembly glass 2 Push opener completely over rubber block with ceramic cutter up and apply pressure down until all tube tips break off Insert the tube set into the adapter flow arrow pointing in Then break the tips on the other side of the tubes the bellow pump Use the special adapter to connect the hose to the manifold containing the tubes Snap fit the hose to 5 Grip the pump with one hand thumb on top fingers along the bottom Compress the pump until it will no longer collapse The counter will advance Release pressure on the pump Compress the pump 50 times according to instructions Pumping action should take approximately 2 5 minutes per set of five tubes 7 Color Ch
43. Zero Depress the Zero button on the top of the instrument If the instrument displays a zero no additional steps are required If the unit displays an H turn the Zero Adjust screw just below the On button counter clockwise while depressing the Zero button until the instrument displays a zero If the unit displays an L turn the Zero Adjust screw clockwise while depressing the Zero button until the instrument displays a zero The Zero Adjust screw may be turned using the trimmer tool supplied with the unit A small standard head screw driver may also work Instrument is ready for sampling if functional test is not required Sampling is conducted simply by depressing the Sample button and waiting approximately 12 seconds for a result to be displayed Calibration Functional Test This test does not calibrate the instrument Calibration should be conducted yearly at the Arizona Instruments facility This functional test checks the factory calibration It 1s not required to perform air monitoring but is advised if the unit will be used extensively or is subjected to high levels of mercury vapor The temperature range for the test 1s 18 22 C 64 4 71 6 F Perform the functional test only after the heat regeneration Turn On procedure is completed To begin plug the tubing adapter end of the septum assembly into the instrument s intake and tighten the intake tube nut The seal should be
44. adionuclides in air that if breathed for a work year would result in an intake corresponding to a dose limit Press the STOP key and the CLEAR key 4 Set desired total air volume to sample and press the START key The sampler will run until the desired total air volume had been sampled ra Once the total air volume is achieved collect the paper filter sample and prepare it for analysis p e Calibration Install the sample holder assembly containing the sample medium paper filter used for sampling into front of the sampler and connect the sample holder inlet to an air flow calibrator Depress amp hold ENTER and SET keys simultaneously turn the power switch ON Note The LCD screen will read CALIBRATE FLOW press 1 for yes 2 Screen Prompt UNIT OF MEASURE 1 for cubic feet or 0 for liters Screen Prompt ADJUST FLOW HIGH POINT Example 3 4 5 cfm 3 LOW POINT 4 MIDPOINT 5 HIGH POINT Adjust enter the high flow rate ENTER for 15 seconds LCD screen will read ADJUST FLOW MIDPOINT Adjust enter the midpoint flow rate on keypad and press ENTER Keep flow constant for 15 seconds LCD screen will read ADJUST FLOW LOW POINT Adjust enter the low flow rate on keypad and press ENTER Keep flow constant for 15 seconds LCD screen will read VERIFY LINEARITY Adjust the flow to various points within the cal
45. ak off Insert the tube set into the adapter flow arrow pointing in Then break the tips on the other side of the tubes Use the special adapter to connect the hose to the manifold containing the tubes Snap fit the hose to the bellow pump Grip the pump with one hand thumb on top and remaining fingers along the bottom Compress the pump until it will no longer collapse The counter will advance Release pressure on the pump Compress the pump 50 times according to instructions Pumping action should take approximately 2 5 minutes per set of five tubes a Ft Color change in tube indicates presence of agent Use laminated instruction card to decipher results Reset the counter on the pump to zero by pressing reset button Turn Off No power required QSG CDS_V v1 1 doc MIE DataRAM 4 Model DR 4000 National Telephone 866 282 0430 Manufacturer E mail www thermo com Contact NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be
46. ange in tube indicates the presence of agent Use laminated instruction card to decipher results 8 Repeat for second set of tubes It does not matter which set is used first Reset the counter on the pump to zero by pressing reset button Turn Off No power required Hydrocyanic Acid Hydrocyanic acid 1 ppm Organic Arsenic Compounds amp Arsine 3 mg m organic arsenic 0 1 ppm Arsine Organic Based Nitrogen Compounds 1 mg m Drager Tube Sensitivity Phosphoric Acid Esters 0 025 ppm Cyanogen Chloride 0 25 ppm QSG CDS Kit v1 1 doc Drager Civil Defense Simultest 1 GENERAL INFORMATION Manufacturer Drager Safety Inc National Telephone 800 615 5503 Manufacturer E mail rodinfo draeger net Contact Website http www draeger com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Uses The CDS Kit is composed five specially designed and
47. arging takes 5 hours 3 5 hours of operation Should remain attached to charger with unit off until ready for use Do not store unit with discharged battery for more than 3 days to avoid permanent damage Calibration Performs auto calibration every time it is turned on Factory calibration required if relative standard deviation greater than 25 Calibration standard Soil NIST 2709 1 4 ppm Water Aldrich Cat No 40 401 2 100ml of 1002 ug ml of Hg in 8 10 wt HNO3 Additional Complete Test Run prior to use Make sure dust filter is present before operating Operational Information QSG Lumex v1 1 doc Lumex Mercury Vapor Analyzer MVA QUICK START SHEET Attach hose by inserting and turning clockwise Turn on unit by pressing the Power button and wait 15 minute for warm up display shows Lumex Title Screen Start up Press ENT until LCD reads Main Menu Press Lamp Ignition the disappears let warm 5 minutes Scroll down to Test and press ENT After warm up message will appear Enter the Test Cell toggle test cell switch on instrument s side between on and off several times and leave in ON position Press ENT R less than 25 indicates unit ready for use Press ESC message remove Test Cell will appear toggle test switch to off Do NOT leave the test switch on during normal sample measurement Press ENT to get back t
48. ated on the right of the screen QUICK START GUIDE 5 When CHIP OK is displayed slide the switch to POSITION 3 to start measurement The analyzer displays MEASURING and bars begin to fill in the space between gt and lt 7 Once measurement is complete the concentration will be displayed on the screen For the next measurement slide the switch to POSITION 0 eject the chip and reload again Zero Not applicable Calibration 1 No calibration is required Turn Off Slide the switch to POSITION 0 the chip will be ejected QSG DraegerCMS v1 1 doc HAZCAT Chemical Identification System GENERAL INFORMATION Equipment Name HAZCAT Chemical Identification System KT 1009 HAZTECH Systems Inc National Telephone 800 543 5487 Manufacturer E mail sales hazcat com Contact Website http www hazcat com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals ete eee These guides were developed by field personnel for utilization MAIN INVENTORY OF ITEMS ACCESSORIES Kuck ebony Zane Alo aid PERS on Game Gee Se by EPA and their contractors and are helpful in quick start up Ter Test Te Te ter Te I x Tex Waa AE amas e and operations Various limitations have been identified through Chlorid Qhromiul Cobalt Fluorid Iron lod Lead M esium Mercur p anal s ia e ee
49. ation 5 When exposed to predominantly low energy gamma radiation the instrument will over respond Response Range 0 5 000 microrems per hour microR hr Product Safety Not intrinsically safe Battery Two alkaline D Cell Batteries or Ni Cad rechargeable batteries Batteries should not be stored in detector when not in use Calibration Annual Manufacturer Calibration check calibration date on a tag or sticker Prior to use the user should verify the calibration and service sheets are present and or readily available The user should not use the unit if the calibration is out of date not available or is unknown QSG Model 19 v1 1 doc Ludlum Model 19 Gamma Detector QUICK START SHEET Prior to l Visually inspect unit and accessories Do not use if unit appears damaged Check calibration date Insert two D cell batteries into the unit Rotate the dial to the 5000 position and press the battery button and note the location of the needle It should be between the BAT OK Starting arrow Push the AUD audio switch to the ON position Push the F S switch to the F position F indicates fast response 4 seconds S indicates slow response 22 seconds Push and check the L button The internal meter light should come on Start up ra Turn the unit on by turning the range selector knob to the lowest scale 25 Press the button marked BAT The needle should move to the area of the d
50. available The user should not use the unit if the calibration is out of date not available or is unknown QSG Model 3030 v1 1 doc Ludlum Model 3030 A B QUICK START GUIDE Prior to Visually inspect unit wires and accessories Make sure all accessories are present and serviceable Starting before attempting to use If the unit appears to be damaged do not attempt to use Damaged unit may not provide accurate results Ensure the unit is plugged into a power source or that the batteries are sufficiently charged Plug unit into electrical outlet Set the COUNT TIME to 1 MINUTE on the Count Time Selector Knob Ensure the VOLUME 1s turned up to an audible level Install Ludlum software package on PC Connect cables to PC Check the instrument s battery level If the instruments operating parameters have not been set the red QC LED will illuminate and an alae quality control QC check must be performed Turn On 1 Push the power switch to the ON position Press and release the QC button Insert alpha source and press the count button When count is complete remove alpha source from the tray assembly replace with beta source close and lock tray and press the count button When count is complete remove the beta source from the tray assembly close and secure the tray and press count If the unit is functioning properly the QC LED will go out Unit is now ready If the QC LED remains on repeat the pr
51. ble bag in a plastic bag to preserve sample Remove ChemKey and store in instrument case QSG SPM vl 1 doc Sn euron gt b eS E Single Point Monitor SPM Tape Gas Monitor Line power cord Power port 14 pin circular connector Chemcassette Guide post Vent Tape path Main power switch Green system status LED Alarm test key Alarm reset key Red system status LED Figure 1 13 14 15 16 V4 18 19 20 a 22 23 24 Red Relay disable LED Relay disable key Sample inlet port Alarm lamp Detector head Tape load lever Digital display Cover screw Retaining ring Collar fixing screw Door thumbscrew Exhaust port 25 26 27 28 29 30 31 32 33 Note Capstan assembly Guide post Take up reel Vent Cover Collar Body Chemkey slot Fuse fuse holder Features may vary depending on instrument options QSG SPM v1 1 doc TV A 1000B Toxic Vapor Analyzer PID FID GENERAL INFORMATION TVA 1000 Toxic Vapor Analyzer 1000B Thermo Fisher Scientific Inc National Telephone 888 643 4968 Manufacturer E mail lori gorski thermofisher com Contact Website http www thermofisher com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or _ technical HYDROGEN manuals These guides were developed by field I Connector OUTPUT GAUGE personnel for utilization by EPA and their contractors and
52. ble button on the Program toolbar Click the description field and type in the sample ID and enter the sample weight in milligrams in the M field Soil Sample Analysis Table em l Click the Graph button on the Table toolbar in the Table Complex Analysis Screen Tare a room temperature boat on a balance Then put some of the sample into the boat and record the weight in the M field of Table column in milligrams BEI Elar atr eatime Area Maximum _ Press the Start button in the Integration window and insert the boat into the oven Wait for the signal to return to the baseline or 60 to 90 seconds o x __ Then press the End button in the Integration window Click the Select button to enable you to highlight an entire row and highlight the row that contains you sample data Click the Calculation button on the Table toolbar The Mercury concentration in parts per billion or ug kg will be reported in the C field Table L H a After all samples are analyzed click Report in the Table toolbar when finished to see a tabulated report of the samples This report data can be exported into Microsoft Excel by pressing the Export to Excel button located on the File toolbar Before dismantling soil analysis setup allow enough time for oven to cool QSG Lumex Soil Attachment v1 1 doc Lumex Mercury Vapor Analyzer MVA GENERAL INFORMATION Equipment Name Lumex Mercury Analyzer Model Model RA915
53. book NIOSH Merck Hawley s etc QSG HAZCAT v1 1 doc HAZCAT Chemical Identification System QUICK START GUIDE Field Screening The following field screening tests can be performed on each sample in order to identify the to determine if major hazards of the material unknown is a Each test must be done in a precise order DO NOT deviate from the steps unless the manual solid or a liquid directs you too Note The following field screening tests are BASIC SCREENING TESTS ONLY For more complete and or comprehensive testing refer to the HAZCAT Chemical Identification System User s Manual and follow the steps laid out in the manual itself Radiological Note This test is for point source detection only Screening Test Check batteries replace if necessary Click the power switch to audio Set the sensitivity to x1 establish the natural background radiation count by observing the counts per minute Place the monitor near the closed container If the sample has a higher then background radiation count consult an expert and or refer to your organization s radiation procedures Place a small amount of the unknown substance on a watch glass The substance can not touch the RadCat Monitor Hold the monitor 4 to 1 2 inch away from the substance and observe the count If the count is off scale switch to x10 x100 as needed Observations If there is no change from the natural background sample is negative for radiation
54. calibrated detector tubes Each tube detects a different chemical agent The set allows for a very rapid determination of agents Limitations Limited to 5 specific agents Limited by sensitivity of detection tubes No response from tubes does not mean there are no harmful agents present Tube Sensitivity Agent Tube Sensitivity Hydrocyanic Acid Hydrocyanic Acid 1 ppm Phosgene Phosgene 0 2 ppm Lewisite Org Arsenic 3 mg m amp Arsine 0 1 ppm arsine N Mustard Org Basic N Comp 1 mg m S Mustard Thioether 1 mg m Alarm Level This test kit does not have any alarms If positive results EVACUATE IMMEDIATELY Product Safety Be wary of shards of glass from broken tips Calibration No calibration is necessary Additional All five tubes of the set are tested simultaneously Operational Flush the pump with fresh air after each use to clear out any remaining vapors Information Be sure to compress the pump the number of times specified in the tube directions QSG CDS _I vl 1 doc Drager Civil Defense Simultest 1 QUICK START SHEET Prior to Perform leak test on bellow pump Starting Start up 1 Scrape the ceramic edge of the Simultest Set Opener at the tip of the tubes multiple times to score the Assembly glass 2 Push opener completely over rubber block with ceramic cutter up and apply pressure down until all tube tips break off Insert the tube set into the adapter flow arrow pointing in Then break the tips on
55. ch until deflection registers on the meter Press the High Voltage Button The meter should read approximately 900 volts Do not attempt to zero unit Zero should only be conducted at the factory using appropriate procedures Turn Off l Rotate the Range Switch to the OFF position and remove batteries Batteries should not be stored in unit when not in use Disconnect probe and cables Return unit to its proper storage container l Calibration Calibration performed annually by the manufacturer Prior to use the user should verify the calibration and service sheets are present and or readily available The user should not use the unit if the calibration is out of date not available or is unknown QSG Ludlum15 v1 1 doc Lumex Mercury Vapor Analyzer MVA Soil Attachment Soil l There is a CD with the attachments and the standards that has the software to run the Lumex Analysis copy it and install the software or before field work go to Start Up http www ohiolumex com fware index shtml and download the control software for the Matrix Lumex Once the file is downloaded unzip the file 18 files will unzip open the setup exe file and install the software The program will be opened later N Remove the main unit from its hard and soft cases Then remove the LCD screen unit and attach the two 15 pin cables to the Lumex and the 9 pin cable to the computer that has the software Turn the power switch on
56. consideration must also be given to duration of dose in addition to instrument readings Instrument is unidirectional The surface of the pancake probe is the only detecting surface 2 Although the instrument will detect a B and y the meter will not differentiate between the three types of ionizing radiation Simple field techniques can help differentiate see reverse side 3 Instrument does not detect neutron microwave radio frequency laser infrared or ultraviolet radiation 4 Instrument may be sensitive or inoperable in radio microwave electrostatic or magnetic fields Response Range Auto ranging from 0 0 microR hr 9999 R hr 0 000 microSv hr 9999 Sv hr 0 cpm 999k cpm or 0 cps 100k cps Alarm Level Programmable visual and audible ALERT and ALARM points for both RATEMETER and SCALER modes Product Safety Not intrinsically safe Battery Two alkaline D Cell batteries or Ni Cad rechargeable batteries Battery life is 200 hours Unit will display low battery warning when battery is below approximately 10 Calibration Annual manufacturer calibration check calibration date on a tag or sticker QSG 2241 2 v1 1 doc Ludlum 2241 2 A B G QUICK START GUIDE Prior to Starting Visually inspect unit check source CS 137 located on side of unit connection cords probes and batteries Inspect the probes and make sure the protective cover s are present If the alpha probe cover is missing visually ch
57. d Go to Organic Analysis located in the HazCat Chemical Identification Manual Water level did not change The pH should be neutral QSG HAZCAT v1 1 doc HAZCAT Chemical Identification System Water Solubility If itis not the unknown has partially dissolved into the water indicating a polar functional Test Continued group in which case you must go to Organic Analysis to continue testing Reacts violently to arrive at this point means you did the Oxidizer test incorrectly Re do the water reactivity portion of the oxidizer test Any other reaction do the pH test The pH test is a screening test for corrosivity A corrosive material is defined by DOT as a liquid or solid that causes visible destruction to or irreversible alterations in human tissue at the site of contact or in the case of leakage from its packaging a liquid that causes severe corrosion to steel or aluminum pH is the more common way of expressing corrosivity with ph of gt 12 5 or lt 2 being of particular concern Interferences Because pH strips can change color during storage it is a good idea to set up a blank for this test Add 1 2 inch of water solubility test to a test tube and dip a pH strip in the water solubility test as a standard Refer to the blank while testing the unknown solution The colors that appear on the blank should be considered neutral results in the pH 5 10 range should be adjusted accordingly Readings for strong acids 0 2 and bas
58. d personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Designed to provide a rapid identification of a chemical agent using specially designed and calibrated detector tube sets The CDS kit includes both the CDS 1 and CDS V kits which are designed to detect up to five different chemical agents simultaneously in only five minutes With this kit a total of eight different chemical agents can be detected Primary users of the kit would include First Responders the Fire Service Emergency Responders Response Teams such as HAZMAT and Federal Agencies Limitations Limited to agents that the detector tubes are specific to Limited by sensitivity of detection tubes A negative response with the tube does not mean there are no other harmful agents present Tube Sensitivity Each detector tube has a sensitivity specific to one chemical The tubes range from a sensitivity of 0 025 ppm for nerve agents to 1 mg m for S
59. de appears press Y button Press N button to scroll through the options Both On Both Off and Light Only Press Y button to select option Press MODE button until the default screen appears Switching First make sure that the AreaRAE Unit is off and unplugged Then open the case using QSG AreaRAE v1 1 Multi Gas Monitor Area RAE Sensors Bi allen wrench and remove the four hex screws 2 on top and 2 on bottom Be Bi not to pull the electrical cords from the connections when opening the case 2 Next remove the 3 screws from the silver metallic plate and remove the plate gently to avoid pulling the tubing from the inlet and outlet Once the cover is off and the sensors are exposed remove the unnecessary sensor and replace with the desired sensor Make sure that the black line on the sensor label is lined up with the white marker on the sensor Replace the plate and screws then the case and the hex screws Once turned on the AreaRAE will recognize the sensors installed and configured However the sensors will still need calibration Turn Off Press and hold MODE key until the AreaRAE is OFF Shutdown Computer 20 LEL QSG AreaRAE v1 1 Drager Civil Defense Simultest CDS Kit GENERAL INFORMATION Civil Defense Simultest CDS Kit Drager Safety Inc National Telephone 800 615 5503 Manufacturer E mail rodinfo draeger net Contact Website http www draeger com NOTE Guides are to be used by traine
60. det Ten Gere Te Cts ui the experience of the development group Different makes Ainda send Kc Aon Kan fren Arend arom D dih models and updates to this equipment may change the Test 1 ec 1 Test 2 ise3 les 4 lese5 Tee tex E oy Sarena j i oe ee es limitations It is recommended that calibration maintenance and ium Cyanidd Cyanidd Flour S oxi 5 Oyo s G Lie ea Recek rec Opra ee use be recorded in a logbook Additional product information HOS OS er Rete a A ED EA Gd CA OH GS Ws may be found in the accompanying Equipment Operating EnS L O 37 Be glass rary 3 Flame Test wires Rides Sli Cal pH Tex Supe SPECIFICATIONS The Chemical Identification System can be used to identify hazardous characteristics of unknown materials By following the HAZCAT CHARTS an unknown material can be segregated by Hazard Class and possibly identified Limitations This system is used for qualitative testing only Mixtures and wastes are often quite varied in their composition and it s likely that the HAZCAT charts will not provide adequate results Although by following the charts field screening can identify major hazards properties of the materials Kits vary in their contents reference manual based on the date of manufacture publication Specialized training or expertise is required to fully utilize the kit s capabilities Accuracy Chemical Chemical Family Identification Mode If th
61. ding to the survey area Optional l If a source of known intensity is available an instrument performance or confidence check may Performance be performed Expose the instrument to the known source and observe the reading Check Move the F S switch to verify the reading in both fast and slow response modes Compare the readings with the known source intensity a reading of or 20 of the known source intensity is acceptable zero Press the RES reset button and confirm that the meter pointer returns to the zero position Calibration Yearly manufacturer calibration only Turn Off a Turn the range selector knob to the off position Pa The batteries should never be stored in the instrument for more than 30 days Front of GM Tube Detector Surface ra N ii alpha alpha beta bota L beta gamma gamma gamma m i ee Read the source directly Cover the source with a sheet of Flip the probe over facing the aluminum back hold the probe within one paper shielding any alpha particles of the probe towards the source effectively inch of the source detecting from reaching the detector surface shielding alpha and beta from the detector alpha beta and gamma QSG Model 12 v1 1 doc Ludlum Model 19 Gamma Detector GENERAL INFORMATION Equipment Name Ludlum Gamma Detector Ludlum Measurements Inc 501 Oak Street Sweetwater Texas 79556 National Telephone 800 622 0828
62. due to background sources Expose the detector identified by dimples in the case to a radiation check source Cs137 Audible beeps should be heard with the AUD Switch in the ON position These beeps should be accompanied by a flashing ALARM light and upscale meter deflection Vary the distance between the check source and the detector while watching the deflection speed of the meter Now toggle Response Switch to the S position while varying the distance to the check source and note that the meter deflection is slower in this position Return the F S Switch to the F position Ensure that once the meter shows deflection beyond the preset alarm threshold the ALARM light illuminates and the tone alarm is constant Pressing the RESET Button will silence the alarm and return the unit s scale to zero and re set If the detection unit is still in close proximity of the source and the user has not changed the dial s settings the unit will continue to alarm Rotate the dial to the next higher detection level and re check Continue checking and moving the dial until the no longer continues to alarm Note the dial setting and scale value and the point where the alarm activates Always begin on the lowest setting X1 and work towards X1000 7 Pressing the RESET Button when the ALARM threshold has not been achieved returns the meter to zero and starts the 8 second background sequence This will not effect the readings QSG Model 19
63. e The scale should return to zero Rotate the dial to ratemeter and press reset Unit is now functional and ready to record readings Prior to entry into the suspected radiation area collect and record background readings If a source of known intensity is available an instrument performance or confidence check may be performed Expose the instrument to the known source and observe the readings using the ratemeter position and the scaler position Note and record the results Move the F S switch to verify the reading in both fast and slow response modes Compare the readings with the known source intensity a reading of or 20 of the known source intensity is acceptable Press the RES reset button and confirm that the meter returns to the zero position In the scale mode press and release the black button on the handle Yearly manufacturer calibration Prior to use the user should verify the calibration and service Optional Performance Check Zero Calibration sheets are present and or readily available The user should not use the unit if the calibration is out of date not available or is unknown Turn Off l Turn the range selector knob to the off position Disconnect the probe and connection cable Replace the protective cover on the probe and store properly N Never store the batteries in the unit when not in use QSG 2241 2 v1 1 doc Ludlum Model 2241 2 A B G Detector
64. e developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guide SPECIFICATIONS Quantitatively measure hazardous gases and vapors Limitations Limited shelf life for all chips Chips are subject to feed jamming Smaller subset of chips is available for CMS See manufacturer s technical specifications in each case of chips cross interferences quantitation and etc Limited to the chemicals that the chips are specific to One chemical is measured at a time The chemical has to be known Interference from other compounds may affect accuracy Response Range Various depending on individual chemicals Product Safety Intrinsically safe Battery Four alkaline AA batteries are required for operation One set of batteries allows the analyzer to run for 450 minutes and perform more than 100 measurements Only use Varta LR64006 Energizer alkaline LR6 E91 or Panasonic AA LR6 AM3 AA MN 1500 alkaline foil PMBC Calibration No calibration is required Bene wane mA COe Coen QSG DraegerCMS v1 1 doc Additional 1 One chip co
65. e instrument can be used with other Model 43 and Model 44 series detectors for measurement of other radiation intensities Limitations 1 Instrument provides no isotopic information as to the source of the radiation In order to calculate dose consideration must also be given to duration of exposure in addition to instrument readings Instrument is unidirectional The surface of the pancake probe is the only detecting surface instrument reading is not equivalent to dose 2 Although the instrument will detect a B and y the meter will not differentiate between the three types of ionizing radiation Simple field techniques can help differentiate See reverse 3 Instrument does not detect neutron microwave RF laser infrared or ultraviolet radiation 4 Instrument may be sensitive or inoperable in RF microwave electrostatic or magnetic fields Alarm Level Product Safety Battery Calibration QSG Model 12 v1 1 doc Ludlum Model 12 Ratemeter QUICK START SHEET Prior to Starting Turn the range selector knob to BAT The needle should move to the area of the display marked BAT TEST If the needle is out of this range replace the batteries Start up Turn the unit on by turning the range selector knob to the lowest scale 0 1 Move the AUD switch to on and verify the detector noise a Press the RES reset button and confirm that the meter pointer returns to the zero position ol Record background readings before procee
66. e material appears to be fairly pure then it is possible for you to determine its identity by appropriately using the chart and your test results Field Screening Mode If the material is a mixture of compounds it is likely that identifying its hazard class by field screening will provide you with more useful and safe results General Safety PRIOR TO CONDUCTING SCREENING TESTS OBSERVE CONTAINERS FOR SIGNS OF LEAKAGE BULGING DEGASSING OR IDENTIFICATION Perform Peroxide tests on any leaked product around lids or bungs if positive DO NOT OPEN Some of the HazCat reagents are flammable corrosive and or need to be kept from an open flame Follow the directions on the bottle for each individual reagent and take the necessary precautions Product Safety The kit utilizes reagent grade chemicals including acids bases oxidizers and other hazardous materials Wear proper PPE follow directions and refer to MSDS s Manual The manual describes the specific tests to be conducted including positive and negative results Make sure you are using the appropriate manual for the respective kit Additional Many tests require judgments to be made before proceeding to the next step Operational If you are unable to make a clear judgment try multiple paths and choose the best endpoints Once you Information have arrived at an endpoint in your analysis compare the properties of the material to a complete set of properties listed in a chemical reference
67. e of the development group Different makes models and updates to this equipment may change the limit ations It is recommended that calibration maintenance and use be recorded in a logbook Additional product or hone information may be found in the accompanying Power i _ GAE Equipment Operating Guide SPECIFICATIONS To perform simultaneous a and radiation measurement on air filter soil and wipe samples Advanced sample tracking and analysis methods when used in conjunction with integrated computer software see instrument manual for more information Knob Limitations The instrument can accept a maximum sample size of 2 inches in diameter by 0 4 inch thick The instrument does not detect gamma radiation A PC interface is necessary in order to access the advanced functions of the instrument Response Range 0 999999 Counts per Minute CPM or Disintegrations per Minute DPM for both a and B Alarm Level Adjustable alarm levels for both a and B counts Constant tone and illuminated alarm light for both a and B Audible beep frequency relative to the rate of incoming pulses above background when VOLUME is turned up Not intrinsically safe AC is primary power Internal trickle charged battery with an approximate life of 8 hours Calibration Calibration performed annually by manufacturer Prior to use the user should verify the calibration and service sheets are present and or readily
68. e the Range Switch from the OFF position to the BAT battery check position The meter should deflect to the BAT TEST portion of scale Batteries are good 1f the needle falls anywhere within the arrowed portion of the scale If not check to make sure the batteries were proper installed and or replace batteries with new batteries Recheck battery status and verify condition Detector Response Checks Make sure you are not in a radiation area or have any radiation sources nearby Rotate the Range Switch from BAT to X1000 Verify the Audio Switch is in the ON position and the Response Switch is in the F position as applicable Unit will temporarily alarm as it acquires a background setting Wait for the instrument to establish background for the purpose of alarm The instrument will beep and the ALARM lamp will flash every half second during the 8 10 second background period Once a background level has been obtained the audible alarm and the flashing light will cease Should the alarm continue verify that there are no radiological sources present and or move to another location and re check Should the alarm continue a third time verify with a secondary radiological unit to confirm deny presence of radiological source If no radiological source is noted the unit should be deadlined and returned for service Do not use if alarm will not stop 3 Rotate the Range Switch from X1000 to X10 Any deflection is
69. easurement is complete the results screen will open displaying the final results of the measurement 5 3 SOIL RESULTS SCREEN 5 3 1 Results View Menu The standard Soil Mode results screen displays the concentration in ppm and error in measurement for detected elements followed by the list of non detected elements with the calculated limit of detection for each element for that test If the display does not show soil chemistry results change the display by selecting View Results Soil Mode Detected ppm 10382 39180 2032 6730 tif 1492 File Edit iew 5S 2 ij Innov X Analysis a2 5 13 Soil Mode Test in progress 29 seconds Mri 2g 6 ppu a Fe 255624 t 654 ppm an 453 r 51 ppm AS 255 47 pp Ph iioa r 48 ppm Eb 123 i l3 ppm Sr 247 l ppm ZE 220 10 ppm Ti lt 4920 ppm Ba lt 2624 ppm End Condition Maximum Time m 5 13 Soil Mode Test in progress 52 seconds 1173 110 he tis as ait aan tS S607 ppu 2004 ppm 554 ppn Ll 3 ppm 90 ppm 31 ppm End Condition Maximum Time S509 lt B23 1124 z AAN File Edit iew Innov X User Manual Version 2 1 The standard soil chemistry display can be modified by using the View Menu As with all Innov X analytical modes it is possible to view spectra and Test Information 5 3 2 Spectrum Screen This screen displays a plot of the x ray fluorescence spectrum for an BF i411 x individual test plo
70. ebsite http www berkeleynucleonics com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their oe eects mail contractors and are helpful in quick start up and Ms SS sen MS Tae we gle ces Operations Various limitations have been identified through the experience of the development group i Different makes models and updates to this equipment T an e may change the limitations It is recommended that ane i ii ordai nonk a A calibration maintenance and use be recorded in a DS DEM poupenn miyam punto undian logbook Additional product information may be found in the accompanying Equipment Operating Guides CIAU z saseg Hie 3 2 z a ajz E e gt gt z Sis e an sess neutron count prepares a multipage report for printing or email SPECIFICATIONS Limitations Response Range Alarm Level Product Safety Battery Calibration Additional Operating Information To provide field surveillance and measurement of multiple radioactive nuclides by identifying signature y radiation energies by spectrometry and matching them to a database of nuclide energies in the unit s memory thereby identifying the isotopes present Cannot identify a or B emitting isotopes but will identify
71. eck the mylar screen for damage If damaged do not use Check connection cord for damage Replace if crushed or damaged Check calibration date If unit s calibration is out of date not present or unknown do not use unit Insert batteries into unit Using the connection cable attach the appropriate probe to the unit Select the detection switch on the unit to the appropriate probe designation Alpha or Beta Gamma Do not turn unit on unless a probe is attached and selected Select the probe by switching the DET switch to either Det 1 or Det 2 depending on probe used Turn the unit on by turning the range selector knob from the off position to the ratemeter position Upon start up the unit will display the unit s information and attachments The unit will note the battery condition and operating capabilities With the switch in the ratemeter position and once the start up is complete the unit will begin counting Push and release the reset switch to return the unit to zero and begin counting again Move the AUD switch to on and verify the detector noise Place the F S switch in the F position for fast counting Place in the S position for slow counting Start up N Check the detection capabilities by holding the probe near the provided check source Move the dial from ratemeter to scale to verify both methods are operating Zero the scale meter by pressing the black button on the handl
72. ectrum The screen will display a wait time of 1 minute Once complete the unit will enter and display the Surveillance Mode Unit is now ready for operation Surveillance In the Surveillance Mode a continuously monitored dose rate will be displayed a cumulative dose shown and the unit will analyze for possible isotopic contributions to the overall dose rate When any preset triggers are exceeded the unit automatically saves and reports alarm condition When the unit reports an alarm condition the suspect isotope 1 e Cs137 Tc99m will be listed on the screen with its contribution to the total dose rate If the isotope cannot be matched to the library spectrum Unidentified will be displayed with its contribution to dose rate Monitoring In Surveillance Mode press the F1 Button MONITOR to see the bar graphs of each enabled isotope in the library The bar graphs show detector response above background in number of sigma standard deviations above background for the listed isotopic peak gamma energies When in Monitoring Mode and the preset triggers are exceeded the isotope bar will begin flashing and the word ALARM will be shown with the sigma value This data and the spectra will be stored in memory Detail In Monitoring Mode press the F1 Button DETAIL to watch the gamma spectrum building This will allow the operator to verify the existence of distinguishing peaks during alarms When the alarm is triggered press the
73. ence lvl Innov X User Manual Version 2 1 Action Level System ends test when result for target analyte Innov X Analysis a 2 8 03 including chosen precision level is above or below pre set action level Test End Condition D Manual O Maximum time O Rel Std Dev W Action Level To choose to end a test based on an Action Level select Options Set Test End Condition and select Action Level Select a target analyte Maximum time 6 secant specify an action level in ppm and a confidence level This Target Analyte confidence level refers to the number of sigma required for the precision This should typically be set to 2 Tap OK to save your selections Rel Std Dey 10 Action level 400 Confidence yl Relative Standard Deviation RSD When RSD is selected as a test AeIE T TEAT 8 04 end criteria the system will end a test when the relative standard i deviation on a target analyte reaches a pre set level This standard deviation is specified as a percentage of the reading For example if the measured value for an analyte was 1000 ppm and the RSD was set to 10 the reading would stop when the error reached 100 ppm or Maximum time 50 seconds 10 of 1000 Test End Condition D Manual D Maximum time Rel Std Dev KO Action Level Target Analvte Rel Std Dey 10 To choose to end a test based on a Relative Standard Deviation select Options Set Test End Condition and select Rel Std Dev Act
74. ent ren a 4 Lee may change the limitations It is recommended that ge calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides Sensor Wrist Strap The MultiRAE uses both standard gas detection sensors for detection of O CO H S VOC and combustible gas LEL The MultiRAE also has an integrated Photo Ionization Detector PID for broad range toxic gas detection Gas concentrations exceeding the upper limit of detection of the instrument refer to table manual pages 1 3 will not be properly detected Any up scale reading followed by a declining or erratic reading may indicate a gas concentration beyond the upper scale limit which may be hazardous Properly operates in ambient conditions of 4 to 113 F and 0 95 relative humidity non condensing Instrument not tested in explosive gas air atmosphere having an oxygen concentration greater than 21 The internal and external filters should be inspected and replaced as necessary Some sensors are cross sensitive to many chemicals See attachment 3 RAE TN 114 Can be found on the Air Sampling CD Not compound specific PID calibrated to isobutylene Other compounds have different response factors If the ionization potential of a compound is higher than the lamp energy the compound will not be detected PID lamp requires periodic cleaning depending on operating conditions Detection
75. es 12 14 will not be affected Expect accuracy of 2 units near the neutral portion of the pH scale Liquid Add inch of the unknown to a test tube containing 2 inch of water solubility test Solid Add a pea size amount of the unknown to 2 inch of water solubility test or use the water solubility test solution if it is available Dip the pH test strip into the unknown solution Allow a few seconds for the colors to develop then compare with the colors on the box of pH test strips Note if the unknown is an oxidizer the colors on the test strip will fade quickly as they are bleached by the oxidizer Observations pH of 2 or less the unknown is an acid corrosive according to the US EPA Go to Acids Chart pH near 11 1f the unknown is organic nitrogen is indicated pH of 12 may indicate cyanide arsenic strychnine or amines Follow up with more comprehensive testing pH of 12 5 or higher the unknown is a basic corrosive according to the US EPA pH of 13 or higher if inorganic indicates sodium potassium calcium lithium or cesium hydroxide To identify the cation go to Metal Analysis Test One If organic may indicate guanine guanidine or piperidine QSG HAZCAT v1 1 doc HAZCAT Chemical Identification System Explosives Test Provides an approximation of the flash point If it is a liquid Using a pipette add the unknown to a watch glass to fom a pool the size of a dime If it is a solid Using a
76. ethyl sulfate are possible The reaction is slow at first but becomes progressively more vigorous Destroys the strip concentrated sulfuric acid indicated Boils sulfuric acid indicated Water Solubility Test The Water Solubility Test 1s the most important test specifically for organic liquids Liquid Add 4 inch of water solubility test distilled water to a test tube and mark the water level with an indelible water proof marker Then add 4 inch of the unknown and shake the test tube gently If the unknown seems to be acting oddly e g forming a skin shake a little harder Carefully feel the test tube for any temperature change Solid Add a pea size amount of the unknown to a test tube containing 2 inch of water solubility test Allow time for an unknown to dissolve or otherwise react Carefully feel the test tube for any temperature change Observations Unknown floats any liquid that floats is organic Unknown dissolves indicates water a soluble inorganic or organic compound in water or a polar functional group Unknown sinks re do the test as follows add 2 inch of the unknown to a new test tube and mark the level with an indelible marker Add 2 inch of water solubility test to the unknown If the unknown level is below the line it has partially dissolved Water level changed indicates that the unknown is either a polar compound with approximately four carbons in the skeleton or a mixture of a polar and nonpolar compoun
77. f each key gt Press the TUTOR key to begin a tutorial session gt Press the EXIT key after any other key to end the session Note While in the tutorial session key presses have no effect on the MicroFID s operation CALIBRATION Note The hydrogen cylinder must be filled prior to operation Before beginning calibration ensure you have a reliable source of zero air and calibration gas gt Select the CAL key gt Select the desired Cal Memory The MicroFID has 10 Cal Memories and can be calibrated with 10 different span gases or response factors if desired Only one Cal Memory can be used at atime Each Cal Memory stores a different Response Factor zero sensitivity and alarm level gt Key in desired Response Factor and hit Enter Note If the Response Factor is not listed in the User s Manual or if you are measuring complex VOC mixtures a value of 1 00 gt CALIBRATION Continued Select Low Range or High Range and hit Enter Use Low Range if you are sampling concentrations between 0 5 and 2000 ppm methane equivalents Use High Range if you are sampling concentrations between 10 and 50 000 ppm methane equivalents Connect the supply of zero air If you are using room air press Enter If you are using a gas zero air connect the gas bag adapter to the inlet Open the gas bag and press Enter Zero calibration will take 60 90 seconds MicroFID prompts for the span gas concentration Enter the known span gas concentra
78. found in the accompanying Equipment Operating Guides SPECIFICATIONS The MIE DataRAM 4 measures the concentration of airborne particulate matter aerolized liquid or solid as well as mean particle size air temperature and humidity providing direct and continuous readout as well as electronic recording of the information Limitations High humidity may cause elevated readings Annual factory cleaning and calibration required Routinely change dust filters Not designed to sample highly corrosive aerosols or solvent fumes The DataRAM4 must be protected from all forms of precipitation and may fail under extreme temps Never operate without one of its internal filters in place Due to the relatively low flow rate the unit may not be applicable for fence line monitoring of cleanups involving low concentrations of contaminants in soil Response Range It covers a wide measurement range from 0 001 mg m 0 1 g m to 400 mg m a 4 million fold span corresponding to very clean air up to extremely high particle levels Alarm Level The alarm function can be enabled disabled and the alarm level trigger threshold can be selected by the user through the DataRAM 4 keyboard While the alarm is on it can be disabled momentarily by pressing any key on the DataRAM 4 Product Safety Not intrinsically safe Battery Internal battery rechargeable sealed lead acid gel cell type 7 2 Ah 6V 20 hour run time between charges typical Requi
79. g to measure very subtle effects and want to be sure of your zero press Esc down arrow to On stream then press Ent Water Analysis 1 See Attachment A for how to use the Lumex to analyze water samples Soil Analysis See Attachment B for how to use the Lumex to analyze soil or tissue samples Turn Off 1 Press POWER to turn off unit Wash the probe thoroughly with tap water AX OSG Lumex v1 1 doc Lumex Mercury Vapor Analyzer MVA Water Attachment Water Analysis Start Up There is a CD with the attatchments and the standards that has the software to run the Lumex copy it and install the software or before field work go to http www ohiolumex com fware index shtml and download the control software for the Lumex Once the file is downloaded unzip the file 18 files will unzip open the setup exe file and install the software The program will be opened later Remove the main unit from its hard and soft cases Then remove the LCD screen unit and attach the two 15 pin cables to the Lumex and the 9 pin cable to the computer that has the software Turn the power switch on the Lumex and ignite the lamp See No 4 on Air Analysis Startup but ignore the portion Set the optical bridge on the back of the instrument to Position II Preparation of SnCl2 Solution In a 100 mL flask add 95 mL water and then add 5 mL concentrated sulfuric acid this is the solution that you will put the stannous chl
80. h will appear Click the Apply button The graph can be saved as a bitmap if you press the Save button Click Exit and click the Yes button to save the calibration coefficients After that click on the Calculation button at the Table toolbar and the calculated concentration values will appear in C ng L column The concentration reported in the column is in ppb s or ug L units Water Sample Analysis or sample analysis click on Pause in Graph Window and then Click in New File button The New file will open Click on Run When liquid in impinger 1 gets near the neck open the clamp at the bottom and drain liquid into waste container Add approximately 10 mL of the fresh SnCl solution Click on the Table window or click on the Table button on the Program toolbar Click the Description field enter the sample ID then the volume in milliliters in the V ml field 4 Press the Start button in the Integration window and introduce the sample into Impinger 1 Wait for the signal returns to the baseline or 60 90 sec Then press the End button in the Integration window Table En 2 Click the Select button to enable you to highlight an entire row highlight the row that contains the data from the sample that was just analyzed and click on the Calculation button on the Table toolbar The mercury concentration in ppb will be reported in the C field N Table EBH 2 After all samples are analyzed click Report in the Table t
81. he on off switch Perform calibration for the high flow rate Low flow application Start the pump using on off switch Press the Flow and Battery Check key Adjust the flow by turning the flow adjust screw until build in rotameter reads 1 5 L min The LCD screen should indicate Battery OK than press the Flow and Battery Check Turn the regulator valve screw counterclockwise four and half turns Perform calibration for the low flow rate Programming To enter Delayed Start Mode From Hold press Set up and enter the number of minutes delay by pressing Digit Select and Digit Set The Digit Select key advances the flashing digit and the Digit Set increases the value of flashing digit To enter Sample Period Mode Press Mode than Digit Select and Digit Set to enter sampling time period To enter Pump Period Mode Press Mode and use the Digit Select key and the Digit Set key to enter the actual time of running the pump While the LCD displays Hold start the sampling by pressing Start Hold If the pump is programmed to the delayed start mode LCD will show time remained until sampling starts Before shut down the pump note the total running time connect the flow meter BIOS Dry Cell Calibrator and check the final flow Turn off the pump by sliding the switch to Off position Calculate the average flow and total air volume collected on sampling media Tubing Flowmeter Low Flow Calibration QSG SKC v1 1 doc Single Point Monitor
82. hloride batteries A battery will last for 24 hours at 20 C and 11 hours at 0 C The batteries can be stored up to 3 years Detector Gas Hydrogen gas cylinder provides 12 hours of operation A yellow warning light illuminates prior to depletion QSG AP2Ce v1 1 doc AP2Ce Chemical Warfare Agent Detector QUICK START SHEET Prior to Starting Start up Extract the battery slide unit from the body of the AP2C Insert a battery block in the slide unit and push until it latches Insert a hydrogen cartridge in the handle of the device lining up on of the two marks on the cartridge in front of the OFF index placed on the body of the AP2C Push the storage device into handle until it latches Turn the tip of the hydrogen cartridge until the white mark is opposite the ON index Display lights should all flash on upon insertion of cylinder A blinking yellow WAIT light indicates initialization of the instrument During initialization the unit is automatically pre heated the hydrogen circuit is purged and the flame is ignited When first starting up allow the following warm up times 2 minutes maximum for temperature gt 10 C About 5 minutes for temperature gt 0 C lt 10 C About 20 minutes for temperatures lt 0 C The green READY lights up when the unit is ready for use When first starting up allow the following warm up times 2 minutes maximum for temperature gt 10 C About
83. ibration range and press ENTER to accept calibration or CLEAR to reject it BAD CALIBRATION inaccurate flow data or the turbine speed sensor requires service Screen Prompt DEFAULT RUN MODE mode of operation 0 for TOTAL VOLUME or 1 for TOTAL TIME Screen Prompt ENTER TARGET Select Liters or cubic feet TOTAL VOLUME MODE or minutes and seconds TIME MODE Note Normal operation both volume and time displayed Screen Prompt WARM UP DELAY IN SECONDS Enter the time desired for the sampler to become operational before the actual sampling period begins typically 2 seconds Screen Prompt KEYPAD SECURITY Select either 0 for OFF or 1 for ON all keys on the keypad are disabled except the UNITS START and STOP keys Off 1 Press START STOP keys QSG RADECO v1 1 doc S4PE GENERAL INFORMATION Equipment Name Persistent Substance Sampling and Evaporation System SAPE Proengin Inc amp Arrow Tech Inc National Telephone 954 760 9990 Manufacturer E mail eric damiens proengin com Contact Website http www proengin com NOTE Guides are to be used by trained personnel only DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the
84. ing y gamma radiation during area surveys Limitations 1 Instrument detects gamma and x ray radiation 2 Instrument does not detect neutron microwave radio frequency laser infrared or ultraviolet radiation 3 The instrument may be sensitive or become inoperable in radio microwave electrostatic or magnetic fields Will not detect a or B radiation through case shielding 4 When exposed to predominantly low energy gamma radiation the instrument will over respond 5 The instrument will respond to x ray machines and pulsed radiation sources but not linearly 6 To calculate dose the instrument reading type of radiation duration of exposure and target must be considered Response Range 0 5000 uR hr Alarm Level Alarm level automatically set to 3 x background Constant tone and illuminated alarm light Audible beep frequency relative to the rate of incoming pulses when AUD switch is ON Product Safety Not intrinsically safe Battery Unit uses two D cell alkaline batteries Under normal use battery life is approximately 600 hours Battery condition may be checked using the unit s meter Note Do not store batteries in the unit when not in use Calibration Calibration and services are performed annually by manufacturer Copies of the certification and service performed should be maintained with the unit Periodical bump test using a check source of known activity provided by the manufacturer is recommended before each use
85. ion level 400 Select a target analyte and the desired Relative Standard Deviation de Tap OK to save your selections 5 5 LEAP Mode Light Element Analysis Program This is a factory installed optional module Instruments can be upgraded to LEAP capabilities Please contact the Innov X Systems Sales department for information and pricing The LEAP module provides the lowest possible detection limits for elements lighter than iron The standard LEAP package includes the elements Ti Ba and Cr Elements as low as Phosphorus can be detected with the Advanced LEAP package which includes a thin window detector The standard x ray beam conditions used by Innov X environmental analyzers are designed to provide good excitation for a wide range of detected elements However it is not possible to select one beam condition which provides the absolute best excitation conditions for all elements of interest Elements such as Chromium produce lower energy x rays then other elements analyzed These lower energy x rays are not as effectively excited by the standard conditions LEAP works by changing the X ray tube beam conditions to settings which are optimized for the detection of elements lighter than iron Instruments are factory calibrated with the LEAP beam conditions for all applicable elements 5S 6 Innov X User Manual Version 2 1 5 5 1 LEAP Settings To activate LEAP select Options LEAP Settings from the Soil analysis screen This brings up
86. is tapped on the iPAQ screen Results will be calculated if the testing time has exceeded the Minimum Test time which is set up in Options Set Testing Times In order to preserve battery life the software will stop if the testing time exceeds 300 seconds since there is little to no advantage to continuing a test beyond 300 seconds To use Manual Test End Condition simply choose Options Set Test End Condition and select Manual Press OK to return to the analysis screen Maximum Time If Maximum Time is selected the test will continue until the preset time is reached This is useful if you wish to do a set of measurements with the same testing time To choose to end test based on a maximum time select Options Set Test End Condition and select Maximum Time Enter the desired testing time in the appropriate box Tap OK to save your selections 5S 5 a Innov Analysis a 5 10 Soil Mode Ready to Test End Condition Set Testing Times Set Test End Condition Element Rates File Edit iew Options Help E 2 Innov X Analysis a 8 03 Test End Condition E Manual O Maximum time Rel Std Dev C Action Level Maximum time E seconds Target Analyte Pb Rel Std Dey 10 Action level 400 Confidence ll a 3 03 a Innoy Analysis Test End Condition E Manual E Maximum time K Rel Std Dev Action Level Maximum time seconds Target Analyte Pb Rel Std Dey 10 Action level 400 Confid
87. isplay marked BAT TEST If the needle is out of this range replace the batteries Press the button marked L to verify that the meter display illuminates Move the AUD switch to on and verify the detector noise Set the meter response switch F S as desired Press the RES reset button and confirm that the meter pointer returns to the zero position Record background readings before proceeding to the survey area Turn the range switch to the highest level 5 000 and then 500 250 50 25 until a response on the meter is detected Read red scale when the switch is pointed to a red range and read black scale when the switch is pointed to a black range The measurement is as follows Ba At 25 red the measurement range is 0 25 uR hour At 50 black the measurement range is 0 50 uR hour At 250 red the measurement range is 0 250 uR hour At 500 black the measurement range is 0 500 wR hour At 5 000 black the measurement range is 0 5 000 uR hour Optional Performance Check If the gamma source is of a known intensity a confidence check or instrument performance may be performed Expose the instrument to the known source and observe the reading Move the F S switch to verify the reading in both fast and slow response modes Compare the readings with the known source intensity a reading of or 20 of the known source intensity is acceptable Press the RES reset button and confirm that the meter poin
88. lecting spectra Since there is some detector dead time associated with a measurement the live time of a test will be slightly shorter than the preset Real time 5 4 2 Soil Mode Test End Condition Four options exist for the test end criteria in soil mode Depending on your application you may choose to end the test manually at a preset testing time or when the uncertainty in the measurement is within a 5S 4 Innov X User Manual Version 2 1 specified relative standard deviation of the reading Additionally you can set up an action level for a single element As soon as the measuring statistics are good enough to ensure that that the reading is above below or at the action level the test will end automatically This allows for very rapid tests for elements that are well above or below an action level In all modes pressing Stop or pulling the trigger will end the test If the minimum testing time has elapsed results will be calculated Otherwise the test will be aborted without calculating results Changes to the test end condition are made by selecting Options Set Test End Condition The currently selected end condition will be displayed at the bottom of the screen above the Start button on the Ready To Test screen Manual This option allows you to look at the results which are being continually updated on the screen and determine when the results look satisfactory The test will continue until the trigger is pulled or Stop
89. m filter cap holder to protect filter caps covering back in place over the foam filter cap holder to protect filter caps rn Press and hold POWER button until APD 2000 appears on the display Turn On Wait for APD 2000 to complete SELF TEST and STNDBY approximately 3 minutes 3 When display shows READY CW press MODE key 2 times or until READY TEST appears on the display Press H end of confidence sample to nozzle for no longer than 1 second Make sure to press las TEER oe to open plunger at end of confidence samples a verify that horn sounds and Verify that hom sounds and display shows ALARM TEST and SIMH OOOO O shows ALARM TEST and SIM H When display returns to READY TEST repeat steps 4 and 5 using G end of confidence samples T Press MODE key 2 times or until READY CW appears on the display The APD 2000 is now ready to operate Calibration Not applicable Instrument is self calibrating Turn Off l Make sure environment is clean and APD2000 is not alarming If unit is alarming indicated by ALARM on the display wait for it to clear Press and hold POWER to turn off POWER DOWN Remove filter cap from barrel and replace back into foam filter cap holder DO NOT TOUCH CAP WITH YOUR HANDS 4 Replace black protective cap back onto barrel tip Replace black protective cap back onto barrel tip Remove and store batteries QSG APD2000 v1 1 doc Multi Gas Monitor Area RAE GENERAL INFORMATION
90. measuring 5 1 SAMPLE PRESENTATION In situ testing In situ testing is performed by pointing the analyzer at the ground Any grass or large rocks should be cleared away and the analyzer should be held such that the front of the probe head is held flush to the ground Since dirt can accumulate on the analyzer window it is recommended that the window is wiped clean after each analysis The window should also be checked to ensure it is not ripped or punctured Instructions for replacing the window are found in the appendix Bagged or prepared sample testing It is strongly recommended that all prepared samples be analyzed in the testing stand Samples should be placed on top of the testing stand completely covering the window Never hold prepared or bagged samples while testing as this could expose the operator to the x ray beam Avoid measuring very thin samples as this can affect results Prepare samples cups to contain at least 0 5 inches of packed samples When analyzing bagged samples make sure that sufficient sample exists in the bag to completely cover the window with a sample thickness of a minimum of 0 5 inches 5 2 TESTING IN SOIL MODE After the instrument has been standardized testing can begin Simply pull the trigger or press Start on the iPAQ screen to begin the test The red warning light on the top of the instrument will blink indicating X rays are being emitted The screen will display the words Test in progress a
91. nd D Hydrogen cylinders require Safety special shipping as dangerous goods UN 1049 The TVA 1000B operates on a rechargeable nickel cadmium battery When the battery is fully charged it will last a minimum of eight hours of continuous use at 20 C Extreme temperatures hot or cold and use of the backlight will shorten the run time The battery does not need to be removed from the instrument to be charged A fully discharged battery will take approximately 16 hours to recharge completely Battery Calibration Annual Manufacturer Calibration check calibration date on a tag or sticker Capable of multipoint and multiple response factors curves calibrations Instrument alerts user if calibration is bad QSG TVA 1000B PID FID v1 1 doc QUICK START GUIDE Prior to Charge battery Connect sample probe Fill install hydrogen tank Starting Open the red hydrogen valve located on the side of the unit by turning the handle to the ON position Let unit sit for approximately 5 minutes so hydrogen can stabilize in unit Start up Press ON button until unit beeps and MAIN MENU appears on screen Press CONTROL 3 Press 3 to ignite FID unit should pause and two audible pops may be head indicating flame is lit If ignition fails wait 5 minutes and then press 3 to ignite FID Press 1 to initiate run Press and hold EXIT to stop run and return to the MAIN MENU
92. nd span gas Maintenance Four gas calibration CO 50 ppm H S 25 ppm LEL methane 50 O 19 and balance N VOC calibration isobutylene 100 ppm Critical Any rapid up scale reading followed by a declining or erratic reading may indicate a gas Operational concentration beyond upper scale limit which may be hazardous Information QSG MultiRAE v1 1 doc MultiRAE Plus QUICK START GUIDE Prior to 1 Check batteries by unplugging the MultiRAE unit from the charger and noting battery level on Starting the display Make sure that the instrument is calibrated Start up 1 Press and hold Mode key until monitor beeps once monitor will go through a 90 second warm up sequence Watch display screen for messages such as sensor installed and their warranty expiration Alarm limits Last calibration date User Alarm Datalog modes After 90 sec warm up the MultiRAE goes into monitoring mode taking real time readings 4 When monitoring the unit alternately displays the instantaneous gas concentrations and the sensor names In a non hazardous environment the sensor readings should be similar to the following TOX1 and TOX2 0 VOC 0 LEL 0 and OXY 20 9 Alarm Limits are set for High Low STEL and TWA When an alarm condition occurs the monitor will provide audible and visual alarms to alert users of unsafe conditions Instruments response time for different gas varies from 15 second to 150 seco
93. nd the time elapsed The word Testing will blink on and off in the low right hand corner of the screen 5S 1 Innov X User Manual Version 2 1 After a minimum time has elapsed intermediate results will be displayed on the screen Until this minimum time has elapsed the words WAITING FOR DATA will appear instead This minimum time can be set by the user by selecting Options Set Testing Times which is described in Section 5 4 Soil Mode Options Each line of the results display shows the name of an element its calculated concentration and the error on the measurement This error is the sigma error on the counting statistics of the measurement The error will decrease with increased testing time m 5 12 Hg Innov X Analysis Soil Mode Test in progress 7 seconds WAITING FOR DATA End Condition Maximum Time E File Edit iew Options Help Too many elements are measured in soil mode to display them at one time However is possible to use the scroll bar located to the right of the chemistry display to view other elements The complete display shows detected elements first listed in order of emission line energy from lowest to highest Following the detected elements are the elements which are below the detection limit of the instrument These elements are shown as less than a calculated LOD This LOD is defined as three times the error on the counting statistics of the measurement When the m
94. nds Allow sufficient time before recording the reading Calibration 1 Hold down Mode and N keys simultaneously for 5 sec to get in Programming Mode If Multi RAE asks a question reply Y or N To accept or Escape use MODE key Repeatedly pushing the Mode key will eventually return user to main display When display shows Calibrate Monitor press Y key 3 Fresh Air Zero Calibration Zero Air can be from a cylinder clean ambient air or ambient air purified through a charcoal filter This procedure should always be performed prior to any sensor calibration When display shows Fresh Air Calibration press Y key When successful the display should show a reading of 20 9 for oxygen sensor and 0 0 or a very small number for all other sensors 4 Multiple Sensor Calibration If you are using a multiple gas cylinder at Multiple Sensor Calibration press Y key If all sensors in display window are to be calibrated attach calibration gas cylinder to unit using a regulator and calibration adaptor press the Y key to start calibration process and follow instructions on screen Disconnect regulator from gas cylinder when calibration is complete If only certain sensors in the display are to be calibrated press the N key and use the Mode key to select the sensors and press the Y or N
95. ns Only detects HD sulfurated blister agents and GA GB and VX phosphated nerve agents May give false response in an enclosed space such as a maintenance shop or engine test bay downwind from or in dense smoke and fumes Some of the vapors that may give a false response are wintergreen peppermints menthol cigarettes cough lozenges and smoke The AP2Ce will not detect nitrogen mustard Lewisite or irritants The AP2Ce has not been tested against industrial or household chemicals found in the civilian environment The instrument will not work properly above 10 000 feet in elevation or in Oxygen levels below 19 The AP2Ce will operate between 10 C and 55 C The AP2Ce requires the use of proprietary batteries and proprietary hydrogen cells The batteries and hydrogen cells will have to be shipped by air as dangerous goods Detection Limits Vapors Aerosols and Droplets All G agents nerve 1 5 ppb 3 seconds HD blister 60 ppb 5 seconds VX nerve 3 ug cm 6 seconds Alarm Level Buzzer can be attached which will alarm at first visual signal first red indicator light Product Safety Model AP2Ce is not intrinsically safe Instrument contains a hydrogen storage device DO NOT SHIP THIS INSTRUMENT WITHOUT PROPER SHIPPING PAPERS UN 1049 Hydrogen compressed Battery The AP2Ce uses a 7 3V lithium battery pack that slides into a battery drawer The battery pack contains two LSH20 liquid cathode lithium thionyl c
96. nsists of 10 measurements capillaries filled with a substance specific reagent Operational system Information 2 A printed bar code on the chip contains information about gas type measuring range and time required for completing the analysis 3 When ordering new chips request chips with a 2 year shelf life 4 The analyzer is able to perform 10 tests on one chip for the same chemical 5 The internal data recorder stores up to fifty measurements with the time date contaminant concentration and sequential order of the measurement Prior to Select the appropriate chip for the gas or vapor to be analyzed Each chip detects only one Starting chemical The measuring range and expiration date should be checked On the chip if the orange pin for a measurement channel is depressed that channel has been used Slide the blue switch to POSITION 1 The instrument will perform a self test If only one battery symbol is displayed batteries must be changed before further measurements Turn On When LOAD CHIP message appears insert the chip with arrow pointing toward the analyzer and barcode up into the bottom port by pressing chip in upward direction lifting the blue gate Slide chip evenly and completely into the chip inlet Gas to be measured and concentration range will be shown on the screen Following the prompt slide the switch to POSITION 2 to check the chip The number of available measurement channels is indic
97. o Main Menu ready to sample For air monitoring turn Rotary switch to Position III on the back of the width of the LUMEX Turn Power switch on front end Red toggle switch LCD display will show Lumex Title Screen LUMEX Ver 3 0 L 2000 Sample Measurement Attach sampling hose by inserting and turning the connection clockwise Make sure it is snug Also attach the muffler on the outlet port on the same panel as sampling hose Press Ent button on top LCD display will show Main Menu the means the lamp is off D Press Lamp Ignition push button dark red that is just below amp to the left from the Power switch The will disappear Let the lamp warm up for five minutes before collecting data N Press down arrow key to On stream Press Ent button Baseline Test occurs for 20 seconds Readings then start with update every second in the upper right corner of LCD screen 7 Press Ent again Readings continue every second but with various summary functions Three 10 second averages are displayed after 1 2 and 3 After 30 seconds a 30 second Below Sc the associated Relative Standard Deviation will be displayed after R Three different choices are available at this point Calculate another 30 second average by pressing Ent again can be done many times Turn off machine press Esc and then turn the red Power switch to Off Calculate a new baseline especially if you are tryin
98. ocess and check operating parameters The unit CPM or DPM LED will remain green Click on Normal QC in tab marked QC Settings click on Reload Last Values Start up Performance Check Using Enter Standard Alpha Efficiency Standard Beta Efficiency from sources click Update Computer Enter values for Allowable QC Efficiency click Update interface Enter Alpha Source Size Update Enter Upper amp Lower Background Limits Update Disconnect PC from instrument Press QC Check insert alpha calibration sources and press Count repeat for beta The instrument is now ready for use Select the count time and statistical accuracy based on field monitoring with a Model 12 Rotate the sample tray knob open and insert sample Adjust volume Press Count results in CPM or DPM Sample a Insert the sample into the Sample Tray close the tray and LATCH the Tray Locking Knob Counting Press the COUNT Button and wait the required count time If the red aAL LED illuminates the sample has exceeded the alarm threshold for a radiation and if the red BAL LED illuminates the p radiation alarm threshold has been exceeded If the red OL LED illuminates the sample is too radioactive and has overloaded the detector Dilute the sample or reduce the sample volume Record the counts shown in the a ALPHA and B BETA display windows 4 Rotate the
99. of chemical warfare agents are un reliable even if calibrated Oxygen 0 30 Combustible gas 0 100 LEL VOCs 0 2000 ppm Carbon Monoxide 0 500 ppm Hydrogen Sulfide 0 100 ppm Sulfur Dioxide 0 20 ppm Nitric Oxide 0 250 ppm Nitrogen Dioxide 0 20 ppm Chlorine 0 10 ppm Hydrogen Cyanide 0 100 ppm Ammonia 0 50 ppm Phosphine 0 5 ppm QSG MultiRAE v1 1 doc Alarm Level 90 dB buzzer and flashing red LED to indicate that preset limits were exceeded HIGH 3 beeps LOW 2 beeps STEL and TWA 1 beep and flash per second Alarm latching with manual override or automatic reset Additional diagnostic alarm and display message for low battery and pump stall Product Safety UL Classified as Intrinsically Safe for use in Class 1 Division 1 Group A B C amp D Hazardous Locations Battery Rechargeable nickel cadmium NICAD or Li ion battery pack or 4 AA alkaline battery adapter The factory supplied rechargeable NICAD battery is designed to last for 10 hours of normal operation no backlight no alarms under best conditions Li ion batteries are expected to last up to 20 hours As the battery becomes older and or under cold ambient temperatures battery capacity will be reduced significantly NICAD are especially prone to build up a memory if not discharged deeply Fresh alkaline batteries will provide approximately 12 14 hours of operation under ideal conditions Calibration and Two point field calibration for zero a
100. oil Mode Ready to Test Set Testing Times Set Test End Condition Element Rates End Condition E A screen appears prompting you to enter a Minimum and Maximum EF m 5 09 Testing times Instruments equipped with the optional LEAP package E will be able to set Light Element Testing times in this screen as well vi a Minimum testing time Maximum testing time 120 The minimun testing time is the required time that must elapse before results can be calculated Live Update results will not be displayed on the screen until the minimum has elapsed likewise a test must complete the minimum time before any test end condition can be used If a test is stopped before the minimun testing time has elapsed the test will be aborted and no results will be calculated Maximum testing time is relevant only if Maximum Testing Time is selected from Set Test End Condition This will automatically end the test at a preset testing time Typically the maximum testing time will be in excess of 30 seconds and may be 1 or 2 minutes depending on detection limits and desired precision It should be noted that all testing times in this section refer to Real Time the time the measurement takes when timed on a normal clock The time stored with each analytical result accessible by selecting View Test Information from the Results screen refers to the test s Live Time This is the amount of time that the analyzer hardware was col
101. ompounds are acid reactive Many acid reactive compounds are not water reactive Establishing that something is indeed water reactive is important Warning Water reactive materials are dangerous Consult applicable regulations prior to transport or storage Liquid Add the unknown to the watch glass to form a pool the size of a dime Solid Add 4 of a pea size amount of the unknown to the watch glass Wet an oxidizer test strip with 2 or 3 drops of water solubility test distilled water Touch the wetted oxidizer test strip to the unknown on the watch glass If the unknown does not react add several drops of water solubility test directly to the unknown on the watch glass If the unknown reacts to the water observe the reaction If the unknown does not react to the water the unknown is acid reactive only Go to the water solubility test instructions noted below Solid Observations Explodes alkali metal with an oxidized coating indicated A stong white crust may be noted over the water reactive metal Bursts into flame alkali metal or hydride indicated Strong effervescence do ignition of off gas test refer to user s manual on how to perform this test Boils water alkali hydroxides or oxides indicated Becomes hot inconclusive Do a pH test Becomes cold nitrates or thiosulfate indicated Liquid Observations Hesitates reacts with copious fumes thionyl chloride boron trichloride phosphorous trichloride and dim
102. oolbar when finished to see a tabulated report of the samples This report data can be exported into Microsoft Excel by pressing the Export to Excel button located on the File toolbar QSG Lumex Water Attachment v1 1 doc Ludlum Model 12 Ratemeter GENERAL INFORMATION Ludlum Ratemeter Meter Model 12 Count Ratemeter Equipped with Model 44 9 Geiger Meuller Pancake Probe Ludlum Measurements Inc 501 Oak Street Sweetwater Texas 79556 National Telephone 800 622 0828 Manufacturer E mail ludlum ludlums com Contact Website http www ludlums com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It 1s recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS The Ludlum Model 12 Count Ratemeter monitors radiation with proportional scintillation or Geiger Mueller G M detectors The instrument shown above left is equipped with a Model 44 9 G M pancake probe that will detect alpha beta and gamma radiation Th
103. opped before the minimum testing time has elapsed the test will be aborted and no results will be calculated 5S 8 Innov X User Manual Version 1 3 Ludlum Model 14C Telephone 800 622 0828 E mail ludlum ludlums com SPECIFICATIONS The Ludlum Model 14C Geiger Counter monitors radiation with either a thin wall Geiger Meuller G M tube detector or a pancake G M detector The instrument can be used with certain Model 44 series detectors for measurement of alpha beta or gamma radiation The meter scale used either CPM or mR hr will depend on what detector is used with the instrument Limitations 1 Instrument provides no isotopic information as to the source of the radiation In order to calculate dose consideration must also be given to duration of exposure in addition to instrument readings Instrument is unidirectional The window of the pancake or tube probe is the only detecting surface 2 Although the instrument will detect a B and y The meter will not differentiate between the three types of ionizing radiation Simple field techniques can help differentiate see reverse side 3 Instrument does not detect neutron microwave radio frequency laser infrared or ultraviolet radiation 4 Instrument may be sensitive or inoperable in radio microwave electrostatic and magnetic fields Response 0 2 000 mR hr Used to describe gamma radiation Range 0 8 000 cpm Used to describe alpha and beta radiation Alarm None
104. or to reach the TAG line Run adjust to desire which is usually 01 Key cursor to reach the AUTO START line for most field applications these should be noted but not modified AUTO START normally set to DISABLED Now return to the MAIN MENU screen by keying the EXIT and then the NEXT key SELECTING SET UP PARAMETERS From the EDIT MENU key the cursor and select the SETUP PARAMETERS key and press the ENTER key Make changes per your requirement and press the NEXT key At the second Setup Screen the relative humidity RH CORRECT should remain DISABL when relative humidity is less than 50 If relative humidity is greater than 50 or operated during a wet weather period the RH CORRECT should be in the ENABLE mode The TEMPERATURE UNITS C and the FLOW RATE 2 00 LPM remain as the default Key NEXT twice to get screen to set the time and date make any necessary changes Key NEXT again for the next set up screen to display In this screen site specific Alarm and Action Levels can be set or modified Refer to Instructional Manual for explanation of all unfamiliar fields To exit SETUP PARAMETERS press Exit key and to return to QSG DataRAM v1 1 doc MIE DataRAM 4 Model DR 4000 MAIN MEN peste eNe yO START RUN From the MAIN MENU Initiate sampling by selecting START RUN and pressing the ENTER key At the end of sampling period terminate the run by
105. oride in Mix thoroughly Remove 20 mL of the prepared solution from volumetric flask then add 10 g of stannous chloride to volumetric flask Mix the solution until the crystalline solid dissolves Add back the prepared solvent solution that was removed during the previous step up to 100 mL Ensure all the stannous chloride is dissolved prior to pouring into the Lumex or container Preparation of Mercury Calibration Standard 1ppb Using the 1000 ug mL Mercury Standard Solution add luL of standard to 1 0L of distilled water in a 1 0 L volumetric flask This will produce a solution with a concentration of lppb 1ug L Img mL 10uL 0 000010 mg L Open the RP 91 box that contains the pump and the impingers Glass tubes Attach the impingers to the slip groove in the swivel stand Place the flow meter onto the swivel stand also Place the single path cell into the auxiliary compartment of the Lumex Place the glass cap into impinger 2 and connect the stem near the top of impinger 1 to the glass cap with tubing Pinch the two pieces of tubing at the bottom of the impingers amp 2 with the two clamps provided in the case A diagram is in the manual for the water attachment The manual can be found attached to this quick start on the CD or from the Lumex website Pour approximately 10 ml of the SnCl solution made in step 4 into Impinger 1 Connect the power supply to the pump and to an outlet then start the pump Adjust the flow to 1 Liter pe
106. perating software will be displayed at full screen If it is not displayed open the shortcut on the desktop ProRAERemote V1 41 data is being received from all AreaRAEs deploy AreaRAEs to appropriate locations for monitoring The panel view F2 displays the four units with room for a total of 32 units Set up F3 can change various setting more information is in the Manufacturer s Manual Log View F4 will display the data logged information from the AreaRAE s The data can be shown in detail and graph form RAELink2 Repeater Operation When the Host and AreaRAE are too far from each other to communicate the use of the RAELink2 Repeater may be necessary The repeater can be found in the truck To operate attach the antenna to the unit and turn on by holding down the ON button located on the Repeater until the light turns a solid green Place in a line of sight between the RAELink Host and the AreaRAE to establish a communication bridge Turning Hold down the MODE and N buttons together until Enter Password 0000 appears 4 To begin receiving data from the AreaRAEs press F9 The computer will scan for the signals from the AreaRAEs and begin downloading information once connected Once on off the on the screen Hold down the MODE button until Calibrate Monitor appears on the screen Press N button until Change Monitor Setup appears on the screen then press Alarms Y button Press N until Change Light and Buzzer Mo
107. plets All G agents nerve 1 5 ppb 3 seconds HD blister 60 ppb 5 seconds VX nerve 5 seconds Alarm Level Buzzer can be attached to the AP2C which will alarm at first visual signal first red indicator light Product Safety Model AP2C is NOT intrinsically safe Instrument contains a hydrogen storage device DO NOT SHIP THIS INSTRUMENT WITHOUT PROPER SHIPPING PAPERS UN 1049 Hydrogen compressed Battery The S4PE uses a 3 5V lithium battery supplied with unit It can provide sufficient charge 1 000 samples and can be stored up to 3 years Calibration Gas Field Calibration Not Required this attachment is used to perform confidence test for the AP2C before each use QSG S4PE v1 1 doc S4PE QUICK START SHEET Take an LSH20 type battery from the transport case and install it in the handle Prior to Starting N Screw up the cap on the handle of the S4PE Start up Bar Take a scraper bar from its pack Release ONE SINGLE SCRAPER from the bar holding the protective band Place the nose of the S4PE facing the scraper to be installed as illustrated in the top left schematic under the General Information section Force the nose end of the S4PE into the opening of the scraper Take the scraper out of its pack For detecting persistent products replace the sampling nozzle by the sampling pipe combined with the use of the S4PE N Confidence Test To test the operation of the AP2C Equip
108. probe used Connect the desired detector to the meter Connect the Neutron Detector for response from y and n radiation Connect the G M Geiger Meuller Detector for response from a B and y radiation Rotate dial to BAT position and check battery status Needle should move onto the bat test bar Rotate the dial to the X1000 position and press the HV red button and note where on the meter the needle falls It should be approximately to the 1 position Toggle Response F S Switch to the F position F indicates fast response between trigger events and meter deflection on the instrument 4 seconds to full scale S indicates a slow response between trigger events and meter deflection 22 seconds to full scale S position is used only to get accurate hot spot measurements Toggle the AUD to the ON position for audible alarm signal Toggle Radiation Selector B G N Switch to desired radiation detector specific response G M Detector will only give response when switch is in B G position Neutron Detector will give y response in B G position and n response in N position 7 With the proper detetion probe attached and away from any known radiological source obtain and record a background reading G M Detector a B and y radiation Detector Response Checks Rotate the Range Switch from OFF to X1000 Ensure the Radiation Selector Switch is in the B G position the Audio Switch is in the ON position and the
109. quires 110 V AC with backup battery used for sample data retrieval in the event of a power loss Response Range Not Applicable Alarm Level Not Applicable Product Safety A 2000 Watt Inverter Model RAD2KINV is commonly used and is not for use in explosive or combustible atmospheres Can not come into contact with foam liquid including water or other foreign substances could result in severe electrical shock 9 VDC used for Back up Calibration Unit requires re calibration with Model C 828 Calibration unit each time a different filter media is used Additional Handle the instrument with care Model H 810 sampler with air volume totalizer will Operational automatically shut off the unit when a specified volume of air has been sampled The flow rate Information total volume and elapsed time are displayed on the liquid crystal display LCD screen QSG RADECO vl 1 doc RADeCO High Volume Air Sampler QUICK START SHEET Prior to Plug the instrument into a power source Calibrate the meter as discussed under Calibration Starting 2 Install the sample holder with the filter media between outer retaining and mesh filter support grid and then turn the power switch on Start up Press START key Adjust the flow rate as desired by turning the screw on the side of the sampler default 1 6 CFM The site specific flow rate will be used to calculate the derived air concentration DAC for the site DAC concentration of r
110. r minute Wait 5 10 minutes to purge the system before starting calibration apm go amin Open the Lumex operating software on the computer On the main menu select the Liquid and click on it Two screens will appear the Liquid Sample analysis screen and the Table screen Press Run on the graph toolbar of the analysis screen The integration window will pop up You will see two lines running on the screen a Blue line and Red line The Red line is the analytical signal line with the y axis on the left of the graph The Blue line is a Photo multiplier current signal which is reported on the y axis on the right of the graph The proper value must be 15000 arb units or higher Press on the Baseline Check button on the Control toolbar Wait 10 seconds and then click the button again to establish the baseline Water Analysis Calibration Eee Click on the Table window brings up Liquid analysis table Enter the test site information in the top blank line Press on the Description field on line 1 and double click left mouse button The windows with Blank and Standard selection will pop up Select Blank and press on Tab key enter 1 in V ml column and press Tab Key Press Start in the Integration window then inject 1 milliliter of Blank deionized water in the first impinger using a pipette nl z 2E Pea ai W 2 2 D SA ae 2 i 3 D IE QSG Lumex Water Attachment v1 1 doc Lumex Mercury Vapor Analyzer MVA
111. r panel power switch is in the upward INT BATT position Remove the sampling inlet protective cap by pulling up on the knurled metal outer piece and lifting it off Place the sampling inlet protective cap on the inlet storage post located on the bottom left corner of the rear panel of the instrument Install inlet tubing omni directional sampling inlet and PM 10 or 2 5 separators if needed Make sure internal HEPA filter is installed Press and hold ON OFF key until product information appears on screen the MAIN MENU screen will follow shortly ZERO INITIALIZE OPERATION From the MAIN MENU select ZERO INITIALIZE by moving the A V cursor to that line Press the ENTER key The pump starts up and ZEROING INITIALIZING will be completed in 299 seconds Return to the MAIN MENU screen by pressing the EXIT key otherwise see manual for trouble shooting it this process does not work SELECTING LOGGING PARAMETERS Key NEXT from the MAIN MENU and the EDIT MENU is displayed The flashing cursor appears on the LOGGING PARAMETERS line Key ENTER and press the or key to toggle between DISABLED and ENABLED select desired data logging function Key the cursor and select the LOG PERIOD adjust to desire 1 minute would be 00 01 00 Use the lt or cursor to move between significant digits and the or key to increase or decrease the values Key the curs
112. red set by ChemKey used Alarm Level Varies by chemical monitored set by ChemKey used Product Safety This instrument is not intrinsically safe Limitations Battery Fresh fully charged internal battery should provide 8 hours of operation but frequent alarms will shorten operating times The message BATT LOW appears when there is 60 to 90 minutes of run time is left on the batteries 120 volt power will need to be supplied to unit through the charger for longer term operation Batteries not easily field replaceable When not in use should remain on charge at all times Calibration Not required in field determined by ChemKey used ae 1 Unit will not operate without ChemKey installed Additional aca 2 Make sure Chemcassette tape is not past expiration date 3 Do not use in direct sunlight temps above 104EF or below 32EF 4 Some humidity necessary for proper operation Information QSG SPM v1 1 doc Single Point Monitor SPM Tape Gas Monitor QUICK OPERATIONS GUIDE Start Up Fully charge battery or connect external power and make sure that the correct ChemKey is installed before turning unit on Activate ChemKey by inserting ChemKey into ChemKey slot and turning 1 4 turn clockwise Installation of Sample amp Exhaust Tubing Note Use 1 8 ID 1 4 OD FEP Teflon tubing at sample inlet to avoid possible sample interference and incorrect readings Sample inlet tubing length may be limited for some target
113. res approximately 12 hours to recharge AC line universal voltage charger power supply 100 250 V 50 60 HZ Note To enable operation with either its internal battery or with the charger power supply the 3 position power selector switch must be placed in its upward INT BATT position Calibration Before initiating a measurement run it is advisable to perform the automatic zeroing and internal check out sequences to ensure optimal operation See Start Up for the procedure The DR 4000 is factory calibrated in accordance with National Institute of Standards and Testing NIST QSG DataRAM v1 1 doc Additional Information MIE DataRAM 4 Model DR 4000 gravimetric standard protocols for particulate levels in air The zeroing of the instrument will be the determination of whether factory cleaning servicing is necessary A reading of BACKGROUND HIGH following the zeroing of the instrument is indicative that the internal optics need cleaning This can be performed using the special tool that consists of a cut off cotton swab inserted into a plastic sleeve and held by a right angle Allen wrench using denatured alcohol Do not operate with pump cap covering inlet Do not operate without internal filter in place May be equipped with separator to monitor for PM 10 or 2 5 size particles only Unit may also be set up using the computer utility and a serial cable Start Up QUICK OPERATIONS GUIDE Make sure that the rea
114. results screen will Mn lt 1 ppm not open Instead the timer will O ates Seaman reset to 0 and the description of the current test will change from Standard to LEAP The live File Edit Yiew Options Help E update screen will begin to show Test in progress screen analysis for all LEAP elements Sequential First Test Standard Analysis 5 5 2 Testing Times To set the minimum and maximum test lengths for LEAP analysis select Options Set Testing Times The testing time screen includes an extra section labeled Light Element Test that is not found on non LEAP systems These are the minimum and maximum test lengths for any LEAP tests Bi Innov Analysis a 4 55 Soil Mode Factory Test in progress 18 seconds Ba r 159 ppm Cr r 25 ppm Mn 355 ppm Fe r 32l ppm i Sequential Current Test LEAP End Condition Maximum Time File Edit Yiew Options Help Test in progress screen Sequential Second Test LEAP Analysis ha Innoy Analysis Standard Test Minimum testing tine Maximum testing time Light Element Test Minimum testing time Maximum testing time As with standard tests the minimum testing time is the required time that must elapse before results can be calculated Live Update results will not be displayed on the screen until the minimum has elapsed likewise a test must complete the minimum time before any test end condition can be used If a test is st
115. s SPECIFICATIONS The CDS Kit is composed five specially designed and calibrated detector tubes Each tube detects a different chemical agent The set allows for a very rapid determination of agents Limitations Limited to 5 specific agents Limited by sensitivity of detection tubes No response from tubes does not mean there are no harmful agents present Tube Sensitivity Agent Tube Sensitivity Nerve Agents Phosphoric Acid Esters 0 025 ppm Phosgene Phosgene 0 2 ppm Cyanogen Chloride Cyanogen Chloride 0 25 ppm Chlorine Chlorine 0 2 ppm S Mustard Thioether 1 mg m Alarm Level This test kit does not have any alarms If positive results EVACUATE IMMEDIATELY Product Safety Be wary of shards of glass from broken tips Battery System does not require any batteries Calibration No calibration is necessary Additional All five tubes of the set are tested simultaneously Operational Flush the pump with fresh air after each use to clear out any remaining vapors Information Be sure to compress the pump the number of times specified in the tube directions QSG CDS_V v1 1 doc Drager Civil Defense Simultest V QUICK START GUIDE Prior to Perform leak test on bellow pump Starting Start up 1 Scrape the ceramic edge of the Simultest Set Opener at the tip of the tubes multiple times to score the Assembly glass 2 Push opener completely over rubber block with ceramic cutter up and apply pressure down until all tube tips bre
116. s Enter Press F1 to return to Dose Rate Screen QSG SAM935 v1 1 doc SAM 935 Gamma Spectrometer and Radiation Survey Meter PC QUICIRKOPERATIONS GUIDE OPERATIONS GUIDE Turn On Using the connection cable connect the probe to the unit Do not force the plug into place Power on the SAM 935 by pressing the ON OFF Button behind the sliding door in the upper left corner of the instrument Allow the instrument to perform self test and stabilize the Nal detector This self test takes about 5 minutes to perform Do not interrupt the sequence by shutting the unit off or aborting the startup do not press OK F2 button The initial screen will display the date time pass or fail the self test along with the status of the battery Internal Nal Internal He3 System memory Spectrum Memory A countdown wl be displayed on the screen and the instrument will automatically prompt the operator to begin a gross calibration once this detector stabilization process is complete Gross ee prompted to begin calibration press the F3 Button ADJUST to perform the calibration Calibration ieee on screen prompt to place the Cs137 source on the detector and press F2 Button OK After the calibration spectrum is captured the unit will beep twice and prompt the operator to take a background spectrum The Screen will display wait time 1 min Remove the Cs137 check source and press the F2 Button BKG and allow the unit to acquire the background sp
117. s complete 6 Press NEXT vo start a run orto wmn ott June 18 2009 US EPA Quick Start Guide Ludlum 2241 2 A B G GENERAL INFORMATION Ludlum Digital Survey Meter Model 2241 2 Digital Survey Meter Ludlum Measurements Inc 501 Oak Street Sweetwater Texas 79556 National Telephone 800 622 0828 toll free 325 235 5494 office 325 235 4672 FAX Manufacturer E mail ludlum ludlums com Contact Website http www ludlums com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS The Ludlum Model 2241 2 survey meter monitors radiation with either Zinc Sulphide scintillation Model 43 90 or a pancake detector Model 44 9 The ZnS scintillation only measures alpha radiation The pancake probe measures alpha beta and gamma radiation Limitations 1 Instrument provides no isotopic information as to the source of the radiation In order to calculate dose
118. ter reactive tests compounds before placing them into a test tube The Acid Test is done simultaneously with the Oxidizer Test to enhance the results Remove the swab and test substance from their respective packaging Add one to two drops of Acid Test to the Oxidizer Test Paper Touch the Oxidizer Test Paper to the sample Observations Paper turns black immediately then turns white positive Refer to HazCat Chemical Identification User s Manual to continue testing Paper turns blue black purple or black positive Refer to HazCat Chemical Identification User s Manual to continue testing Melts paper to black strings negative Refer to HazCat Chemical Identification User s Manual to continue testing Slight discolorization or very slow reaction negative Move on to the water solubility reactivity test No color change negative Move on to the water solubility reactivity rest Add several drops of Acid Test_directly to unknown substance note the reaction Observations Burns or smokes positive Confirm with water reactivity test Fumes vigorously positive Confirm with water reactivity test Effervesces with odors positive Confirm with water reactivity test Effervesces positive Confirm with water reactivity test No reaction negative Continue to water reactivity test QSG HAZCAT v1 1 doc Water Solubility Reactivity HAZCAT Chemical Identification System Water Reactivity Test All water reactive c
119. ter returns to the zero position Yearly manufacturer calibration Prior to use the user should verify the calibration and service sheets are present and or readily available The user should not use the unit if the calibration is out of date not available or is unknown Turn Off l Turn the range selector knob to the off position Remove batteries from the unit Batteries should never be stored in the instrument when not in use Zero Calibration QSG Model 19 v1 1 doc Ludlum 192 Gamma MicroR Survey Meter GENERAL INFORMATION Ludlum Measurements Inc 501 Oak Street Sweetwater Texas 79556 National Telephone 800 622 0828 toll free 325 235 5494 office 325 235 4672 FAX Manufacturer E mail ludlum ludlums com Contact Website http www ludlums com NOTE Guides are to be used by trained personnel only Detector and DO NOT replace the manufacturer s operations or 3 technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It 1s recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS To detect low level ioniz
120. the Lumex and ignite the lamp See No 4 on Air Analysis Startup Set the optical bridge on the back of the instrument to Position I D W gt e j li 2E 5 elms E aa 5 a o a J IE Attach the Pyrolysis oven to the external analytical cell port on the side of the instrument long side Warning the oven connection is fragile Make sure the output line off the glass pvc T is connected to the pump and inline with the zero mercury filter and flow meter 5 Attach the flow meter to the stand and check all tubing for kinks or holes Replace tubing if necessary Discoloration or blackened tubing does not affect the results Connect the power supply cables to the Pyro oven and the pump and plug them in and turn on the oven s power to allow it to heat Caution Oven will get extremely hot Allow oven on attachment and Lumex lamp to warm up for 30 minutes Turn on the pump and adjust the flow to be between 2 3 Liters minute Soil Analysis Calibration a Open the Lumex operating software on the computer On the main menu select Complex and click on it Two screens will appear Complex Sample analysis and Table screen Press Run on the graph toolbar of the analysis screen The integration window will pop up You will see two lines running on the screen a Blue and Red line The Red line is the analytical signal line with the y axis on the left of the graph The Blue line 1s a Photo multiplier current signal which
121. the menu shown below on the right f 1 18 DF Innoy Analysis f 1 00 Hg Innov X Analysis Soil Mode Ready to Test LEAP Settings Standard Test Only O Light Element Analysis Only T Seguential Testing Standard followed by Light Element LEAP Settings Set Testing Times Set Test End Condition Element Rates End Condition File Edit iew Options Help Standard Test Only The analyzer will provide analysis for the standard suite of elements Light Element Analysis Only The analyzer will provide analysis for elements in the LEAP suite Typically Ti Ba and Cr Sequential Testing When sequential testing is selected all tests will start with an analysis of elements in the standard suite If that test ends due to reaching the selected end condition of Maximum Test Time Action Level or RSD then the analyzer will immediately begin a second test analyzing the LEAP suite of elements At the conclusion of this test the Results screen will open with two new entries The first summarizes the standard test results while the second summarizes the LEAP results For safety reasons the second test will not begin if the test ends due to user intervention pulling the trigger or hitting Stop In this case the Results screen will open with only one reading If Light Element Analysis Only is activated the words Light Element Analysis Mode will appear above the currently selected End Condition Instrument operation
122. the other side of the tubes Use the special adapter to connect the hose to the manifold containing the tubes Snap fit the hose to the bellow pump Grip the pump with one hand thumb on top and remaining fingers along the bottom Compress the pump until it will no longer collapse The counter will advance Release pressure on the pump Compress the pump 50 times according to instructions Pumping action should take approximately 2 5 minutes per set of five tubes Color change in tube indicates presence of agent Use laminated instruction card to decipher results Reset the counter on the pump to zero by pressing reset button Turn Off No power required QSG CDS _I vl1 1 doc Drager Civil Defense Simultest V National Telephone 800 615 5503 Manufacturer E mail rodinfo draeger net Contact Website http www draeger com NOTE Guides are to be used by trained personnel only and DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guide
123. the sample boat on the balance and hit the tare button Use a balance that weighs to 1 mg or 0 001 g with a draft ring or doors Weigh out approximately 10 mg of the NIST standard into the tared sample boat Take the sample boat loaded with standard to the Lumex Press the Start button on the Integration window Immediately place the sample boat inside the oven When the signal returns to the baseline or about 45 seconds Press the End Button in the Integration Window Repeat steps 6 through 8 with 20 and 60 mg standard sizes to establish multipoint calibration You can do as many duplicates as required to increase accuracy and precision Program He Click the Table button on the Program toolbar and click the Select button Click on Row number 1 then hold down the Shift button and press the down arrow to highlight the Blank and all the Standards rows Note Only Blank and Standard rows must be selected for calibration p lt e e e e e OD e o SE Calculation On the Calculation toolbar click on the Cal Graph button The Graph will appear Click the Apply button The graph can be saved as a bitmap if you press the Save button Click Exit and click the Yes button to save the calibration coefficients After that click on the Calculation button at the Table toolbar and the calculated concentration values will appear in C ng g column The concentration reported in the column is in ppb s or ug kg units Program H Click the ta
124. tight Attach a zero air filter to the opposite end of the septum assembly Record the temperature from the thermometer in the mercury thermos N Draw the 1 cc sample from the mercury thermos with a preset syringe QSG Jerome v1 1 doc Jerome Mercury Vapor Analyzer MVA Calibration Insert the syringe into the septum of the septum assembly already attached to the analyzer Functional Test Press the sample button wait 2 seconds when the display flashes inject the mercury vapor into the septum assembly by depressing the syringe p NNNNNR RP Re ej BRWNrR OW OND S 0 Record the result displayed on the instrument p lt Repeat steps 6 10 three more times 12 The last three readings should be within 5 percent of each other The last three readings should also be within a concentration range based upon the temperature noted in step 6 The ranges are as follows for the thermos temperature C Range 091 to 123 100 to 135 108 to 146 118 to 159 129 to 174 138 to 187 151 to 204 164 to 222 177 to 240 If the average of the final three readings is within the above range the instrument is functioning properly 14 Refer to the Operational Manual if the functional test results are not within the specified range Turn Off l Press the Off button QSG Jerome v1 1 doc Ludlum Model 15 Neutron Counter GENERAL INFORMATION Ludlum Measurements Inc
125. tion and then connect the span gas Press Enter and MicroFID sets its span After 60 90 seconds calibration is complete Press the Alarm key and enter the alarm level for the selected Cal Memory For further information contact your area representative or Photovac ott Photovac Inc 176 Second Avenue Waltham MA 02451 Phone 781 290 0777 Fax 781 290 4884 www photovac com DataRAM PDR Manufacturer Telephone 888 643 4968 Contact 866 282 0430 E mail lori gorski thermofisher com Passive instrument no air pump is installed May not detect when particulate concentration is very low 0 001 mg m 400 mg m June 18 2009 US EPA Quick Start Guide QUICK OPERATIONS GUIDE Turn On Press ON key The screen will display start zero enter go to run next Press NEXT key to start a run without zeroing instrument should be zeroed before each use Press ENTER The instrument is in real time monitoring mode Concentrations must be manually recorded or recorded via data logging An is displayed beside the concentration indicating data logging In a clean environment place the instrument inside a Z pouch Close the zipper 2 Connect a rubber hand pump to the inlet with filter of Z pouch and start to pump in air into the Z pouch When Z pouch begins to bulge slightly press ON key When Zpouch begins to bulge slightly press ON key OOo When CALIBRATION OK is displayed zeroing i
126. toll free 325 235 5494 office 325 235 4672 FAX Manufacturer E mail ludlum ludlums com Contact Website http www ludlums com ee 0 nr z T 4 NOTE Guides are to be used by trained personnel only and Ou a T 15 E DO NOT replace the manufacturer s operations or technical og Ery of manuals These guides were developed by field personnel ERG S pe for utilization by EPA and their contractors and are helpful of NGA in quick start up and operations Various limitations have J 202 1070 e been identified through the experience of the development s p p group Different makes models and updates to this equipment may change the limitations It is recommended that calibration maintenance and use be recorded in a logbook Additional product information may be found in the accompanying Equipment Operating Guide SPECIFICATIONS A rapid real time quantitative measurement of low level gamma radiation Limitations 1 Instrument will not detect alpha or beta radiation and provides no isotopic information as to the source of the radiation To calculate dose consideration must also be given to duration of dose in addition to instrument readings instrument reading is not equivalent to dose 2 Instrument does not detect neutron microwave RF laser infrared or ultraviolet radiation 3 Instrument may be sensitive or inoperable in RF microwave electrostatic or magnetic fields 4 The instrument detects gamma and x ray radi
127. tor Area RAE QUICK OPERATIONS GUIDE Operation amp Guidelines for the Calibration and Operation of the individual AreaRAE units can be Calibration 1 found in the Quick Start Guide for the MultiRAE Units should be Fresh Air Calibrated before deployment Place pre filter on inlet port turn units on when units are ready hold down the MODE and N buttons together until Enter Password 0000 appears on the screen Hold down the MODE button until Calibrate Monitor appears on the screen Press the Y twice After the calibration is done press the MODE button until the normal screen appears ER Truck Attach the Antenna to the RAELink2 Host found in the truck then attach the RS 232 and Repeater 1 cable to the serial port on the ER Computer or any computer with the ProRAE Remote Computer Software loaded on it If your computer doesn t have a Serial Port use the USB Operation converter located in the Host carrying case Hold down the ON button located on the and Data Host unit until the light is solid green Logging Turn on the AreaRAE s and make sure that each unit s antenna is connected and that the LED light for Radio broadcasting is lit Then take the AreaRAE Kit 1 of 2 and plug the extension cord located inside case into a power supply to the exterior adapter Open and turn on the computer Remove the antenna from the case and place on top of vehicle or highest point available Once the computer starts up the o
128. tting the intensity on the y axis versus the energy of the fluorescence x rays on the x axis Counts secs Reading 35 Tapping on the spectra will show the energy scale and counts rate at the selected point Mh 00 5 0 10 0 15 0 20 0 25 0 30 0 35 0 Energy kev Bak Ca x File Edit iew It is possible to zoom in on certain areas of the graph by selecting one corner and drawing out the region Reading 26 Tapping the symbol in the upper right hand corner beneath the X will restore the graph to full scale Energy ke Energy ke Back Next Stare EBA Beck Nowe Stare DT 5 3 3 Test Info Screen The test information screen shows any test information that was entered prior to the start of the test Changes to that test information can be made by selecting Edit Test Information 5 4 SOIL MODE OPTIONS The length of tests in Soil Mode is user settable Users may select a minimum testing time and as well as choose from a variety of test end conditions The options related to test time are contained in two menus Options Set Testing Times and Options Set Test End Condition Set Testing Times contains minimum and maximum testing time information while Set Test End Condition allows the user to select test end conditions 5S 3 Innov X User Manual Version 2 1 5 4 1 Set Testing Times To set the minimum and maximum test lengths select Options Set AF Innov x Analysis e 5 10 Testing Times i 8 S
129. ufacturer E mail support danbury smithsdetection com Contact Website http www smithsdetection com NOTE Guides are to be used by trained personnel only DO NOT replace the manufacturer s operations or technical manuals These guides were developed by field personnel for utilization by EPA and their contractors and are helpful in quick start up and operations Various limitations have been identified through the experience of the development group Different makes models and updates to this equipment may change the limitations It 1s recommended that calibration maintenance and use be recorded in a_ logbook Additional product information may be found in the accompanying Equipment Operating Guides SPECIFICATIONS Automatically detects and identifies chemical warfare agents nerve GA GB GD VX and blister HD HN Lewisite L or irritants pepper spray and mace present in the atmosphere Limitations Detector may become saturated when exposed to high concentrations of chemical agents or interferences Poor detection of irritants Susceptible to interferences false positive readings with perfume wintergreen oil some deodorants cleaning compounds smoke and fumes Unit temporarily disengages monitoring during Auto Cal and Clear functions Requires periodic leak testing of radioactive source Extensive decontamination is necessary Operating temperatures of 22 F to 126 F Response Range VX 4 ppb 30 seconds
130. ydrogen flame If there is not sufficient amount of oxygen the flame will go out Neither detector is compound specific PID is calibrated to isobutylene The FID is calibrated to methane Other compounds have different response factors for each detector Low oxygen can also effect the characteristics of the flame causing false elevated readings If the ionization potential of a compound is higher than the lamp energy the compound may not be detected PID has a smaller dynamic range and is not the best choice for measuring high concentrations of vapors PID is susceptible to interference from water vapor more so than the FID As the unit ages the PID lamp energy may decrease so compounds with ionization energy near the lamp energy may not be detected PID lamp requires periodic cleaning depending on operating conditions Detection of chemical warfare agent vapors is unreliable even if instrument is calibrated Must follow proper shipping instructions due to the hydrogen tank The hydrogen storage tank needs to be shipped as dangerous goods Air Cargo Only 1049 Hydrogen Compressed Response PID Instrument 0 5 2 000 ppm isobutylene accurate to 500 ppm isobutylene Min 100 ppb benzene Range FID Instrument 1 0 50 000 ppm methane accurate to 10 000 ppm methane Min 300 ppb hexane QSG TVA 1000B PID FID v1 1 doc Alarm Set by user High Low STEL Level Product FM Intrinsically safe for Class 1 Division 1 Groups A B C a

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